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61441562-Preparation-of-tris-thiourea-copper-І-sulphate

61441562-Preparation-of-tris-thiourea-copper-І-sulphate

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منشور بواسطةAsih Tri Marini

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Published by: Asih Tri Marini on Apr 25, 2013
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11/18/2013

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COM
Preparation of tris(thiourea)copper(І)sulphate
[Cu(H
2
NCSNH
2
)
3
]SO
4
Equation:-
H
2
N-C-NH
2
S
CuSO
4
. H
2
O
[Cu(H
2
NCSNH
2
)
3
]SO
4
+
5
Chemicals:-
1- thio urea
H
2
N-C-NH
2
S

2- copper sulphate
CuSO
4
. H
2
O 5

Procedure:-
1- 2.5 gm thiourea dissolved in least amount of
H
2
O
2- 2.5 gm copper sulphate dissolved in least
amount of H
2
O
- !dd "2# to "1#
$- %&'( )*+,'(- ./01 23 5 45/,6 78&9 :;<=>
5- !dd 1 gm thiourea to solution
?- @A<0B5/C 8- DE05F @-/G= <H- 7*I05 J0K <L5- DC/01
M- 7F8N O PQR O /0+S
ةمقلا تايدتنم WWW.elqemma.COM
1
1
tris(thiorea!"o##er($!sl#hat
e
O"tahe%ral
&iama'(eti"
ةمقلا تايدتنم WWW.elqemma.COM
T<BK Uield V
H
2
N-C-NH
2
S
CuSO
4
. H
2
O
[Cu(H
2
NCSNH
2
)
3
]SO
4
+
5
1 mol 1 mol
249.5 gm 297.5 gm
2.5 gm X
we take
X (2.5 X 297.5) ! 249.5 2.9" gm
# $%el& ('(a)t%)al ! t*eo(et%)al) X 1++
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)

COM ‫منتديات القمة‬ 2 .5 gm we take 2. 5 H2O [Cu(H2NCSNH2)3]SO4 1 mol 297.5 =2.5) / 249.WWW.98 gm % yield = (Practical / theoretical) X 100 WWW.COM ‫منتديات القمة‬ %yield ‫حساب‬ S H2N-C-NH2 + CuSO4.5 gm X = (2.5 X 297.5 gm X 1 mol 249.elqemma.elqemma.

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