AT-510

Ver.03
#595-0189

2.
2-3.
2-3-1.
<>

(1)
(5)
(2)

(3)

(6)

(4)

(7)

1) (IDP-100/DPU-414)
.

2)
.

3)
.

4)
(, pH ) .
5)
, .

6)
ON/OFF .
7)
.

<>

(12)
(8)
(9)

(13)
(14)
(15)

(10)
(11)
8) S-BUS
.

9)
.

10)
.
.
.

11)
.

12)
.

13)
, .

14) RS-232C
RS232C , ( SOFT-CAP ).
15)
.

<>

(17)
(18)
(16)
(19)

16)
.

17)
(5A) , .
18)
.

19)
.

2-3-2. ()
:

:
APB key

Up key

Down key

Purge key

Print key

Calibration key

pH

Stirrer key

ON/OFF ,
2 ,

Method key

Titration key

Control key

Result key

Sample key

Function key

,
0.

5.

10.

1.

6.

11.

2.

7. 12. pH

3.

8. 13.

4.

9.

14.
4

0.

3.

6.

1. &

4. LCD

7.

2.

5.

8. pH

0-9

. , -

2-3-3.
<>
[Function] [Setup] , [], [] [] .

<>
[], [] . <*****> ***** , .
[], [] [] .

<>
[*****] , . , A , a
1 .
:
1) [Disp.] . [Disp.] ,
.
2) , [] .
: [C] , [7ABC] . [2] , [2RST] .
2-3-3

Blk

Space

Space

STU

STUS

s(t(u(s

VWX

VWXV

v(w(x(v

YZ

YZY

y(z(y

JKL

JKLJ

j(k(l(j

MNO

MNOM

m(n(o(m

PQR

PQRP

p(q(r(p

ABC

ABCA

a(b(c(a

DEF

DEFD

d(e(f(d

GHI

GHI(G

g(h(i(g

( ( ) ((( (

( ) % (

+(/(((+

+/+

()

+/

2-3-4.
,

<>

.
.

!
Set, .

2-4. (Setup1)
[Setup] .

, Date & Time [(] .

!
, ,,, , , [(] .
Date Style .

!
Minute [] , .
, .

2-5. (Setup 2)
. .

[Setup] .

, Regist Operator [] .

[], [] . 2-2-3 .

10

3.
3-1.
pH .
pH .

I.

II.

pH (pH7/pH4) .
*,

III.

0.1mol/L-HCl.
* , 7-5.

IV.

.
*, .
.

V.

.
* PC .
, .

VI.

[Start] .

VII.

!
. .

11

3-2. (pH )
, pH , . pH .
[Calib.] .

Detector No. Calib. Method .

, .

Detector No.

, ( 1 / 3 ).

No.1

: .
pH .

No.3

: .
. .

Calib. Method

pH , (Auto/Manual) (/).

: pH .
3 .

: pH . . 3 .

!
STD-510 pH .
, pH , .1
TET-510 .1 .3.
, 4-1-3. .

12

3-2-1. pH , Auto
, Function pH , PC pH
, . 3-2-1 :
3-2-1

Temp. of

STD

T-111 , .
, T-111 , .

Calib. Table

Calib. Buffer

(Standard/User) (/)

: () pH7, pH4, pH9 PC .

: Function pH .

, . Calib. Table .

: pH7/pH4/pH9, pH7/pH4, pH7/pH9, pH4/pH9

: 2/1/3, 2/1, 2/3, 1/3

, [Calibration] [] .

, .
, [] .

!
, .
, .

13

, . , .
, 9. .
Function Periodic .

14

3-2-2. pH , Manual
. 3-2-2 .
3-2-2

Calib. Points

(2/3).
2: 2-point

3: 3-point

STD Buffer1

pH (0.00 ~ 14.00).

(STD Buffer2)

pH (0.00 ~ 14.00).

(STD Buffer3)

pH (0.00 ~ 14.00).

, [Calibration] [] .

, .
, [] .

!
, .
, .

15

, .

!
. OK.
.

16

3-3.
, , (ppm) .

AT-510

C-172

1
1

T-111

0.1mol/L

500mL

0.1mol/L-

500mL

500mL

200mL

2 3

(5mL)

<>
1 ) , ( G ) .
2 ) T - 111 ( T ) .
3 ) , .
4 ) .

17

< >
1 ) 0.1mol / L .
2 ) [APB] 1. Manual Operation .
3 ) 7- 5 , to Bottle , 10 .

!
to Bottle.
to Nozzle, [APB] to Bottle.
3 ) [] . . .
4 ) , .
5 ) , [] .
6 ) , [Reset] .
7 ) .

!
.
, .

18

<>
a )
1 ) [ Method] .
2 ) [0], [1], [] 01(Auto) .
b )
1 ) [ Titration] .
2 ) [], [] , .

Method Name

(Auto Titration)

Method Type

(Titration)

Titration Mode

(Auto Titr.)

Form

EP Stop

APB No.

Unit No.

Detector No.

Unit

pH

Max. Volume

20.000

Wait Time

Direction

Auto

c)
1) [Control] .
2) [], [] , .

End Point No.

End Sense

Auto

End Point Area

Off

Separation

Off

Over

0.0mL

Titr. Vol.

Gain

Data Samp. Pot.

4.0mV

Data Samp. Vol.

0.5mL

Control Speed

Medium

19

d)
1) [Result]
2) Calculation [ ] .
3) [], [] , .

Calculation Type

Sample

Conc.1

Set

Formula

(EP1-BL1)TFC1K1/SIZE

TF Unit File
.

Unit

ppm

EP No.

Conc.2

Off

Conc.3

Off

Conc.4

Off

Conc.5

Off

Temp. Comp.

Off

4) Constant [ ] .
5) [], [] , .

C1

14.00

K1

11000

ppm.

e)
1) [Result] .
2) Report [ ] . .

Report Format

Short

Titration Curve

Yes

Data List

Off

20

f)
1) [ APB ] .
2) Unit File [ ] . .

APB Unit File

Skip

APB Unit No.

Reagent Name

0.1M-HCl

Factor

1.000

TF .

Concentration

10.1

Molecular Weight

136.5

Equiv. Number

Unit Type

20mL

Alarm

Off

Permit. Err.

0.02mL

g)
1 ) [ Function] .
2 ) Common blank .
3 ) Blank 1 1 [ 0.0 ] . , 0.0 mL .
< >
a)

1 ) 5mL .
2 ) 0.1mol/L .
3 ) 0.1mol/L 5mL, 200mL .
4 ) , 100mL .
5 ) , .
6)

, .

21

b)

1) [Function] .
2) Sample File.
3) Sample FileNo.
4) [Sample] .
5) [], [] , .

Sample No.

01-01

Sample ID

(none)

Sample Unit

gmL

Sample Size

5.000mL

Molecular Weight

40.0

Equiv. Number

Operator

<

>

<>
1) [Start] .
2) , .

<>
1) , , .
2) .
3) .

22

4.
, .
, , .

4-1.
50 . .
, , (No.00-06), (No.10-47)
(No.50-54). .

4-2-2 .

Method 00 Blank Titr.

Titration

Control

Result

Method 01 Auto Titration

Titration

Control

Result

Method 02 Auto Intermit

Titration

Control

Result

Method 03 Intermit

Titration

Control

Result

Method 04 KF Titration

Titration

Control

Result

Method 05 COD Titration

Titration

Control

Result

Method 06 Petroleum

Titration

Control

Result

Method 10 User

Titration

Control

Result

.
.
.

User
Mehtod

Method 47 User

Titration

Method 50 Combine

Titration

.
.
.
Method 54 Combine

Standard
Method

Control

Result

Combined
Method
Titration

23

4-1-1.
(Titration mode) .
(00-06) .
. 4-1-1-1.
4-1-1-2 4-1-2 .
4-1-1-1

00

01

02

03

04

, , , ,

(Blank Titr.)

, , , ,

(Auto Titr. )

, , , ,

(Auto Intermit)

, , , ,

(Intermit)

Karl-Fischer

(K.F.Titration)
05

COD

(COD Titration)
06

10-47

, , , ,

(Petroleum)

No.00-06 .

*1
50-54
*2

5 (Method 00-47)
.

!
*1: 10-47 00-47 ( 07-09).
, , , .
00-06 , , ,
.
*2: 50-54 , ( 07-09) .
, , ,
.
, 7-14. .

24

 4-1-1-2

(Blank Titration)

, ,

Auto Titration.

, .

(Auto Intermit)

. .
.

(Intermit)

0
. .

Karl Fischer

KF KF-510 .

(KF Titration)
COD
(COD Titration)

.
JIS K0102

(COD) (). COD-510

JIS K2501 ASTM D-664 .

(Petroleum Titr.)

() (dE/dmL) ,
, ,

. (dE;

1st (2nd) , .

25

4-1-2.
.

4-1-2

(Full)

5 .

(EP Stop)

(Level Stop)

(Level & EP)

5 , ,
, .
, ,
, 2 .
2 2 , ,
, .
2 , ,

(Intersect)

, , .

, , .

(Stat)

(Learn)

26

<: Full>
, , , 5 .
mV

EP5
EP4
EP3
EP2
EP1

Max volume
mL

<: EP Stop>
5 , , ,

mV
mV

EP2

Max. Volume

EP1

mL

mL

.
, .
, .
, .

<: Level Stop>

, , , 2 .
mV

Second End Level

First End Level

mL

, ,

M , P , .
, .

27

<: Level & EP>

.
mV

EP2
Second End Level

EP1

First End Level

mL

<: Intersect>
. .
, .
, .

1mL

10mm

1pH

10mm

100mV

10mm

10%

10mm

0.1Abs

10mm

10A

10mm

10mm

CMT 0.01S/cm

:
pH

mm
90

tangent 2

tangent 1

30

3
0

angle

13

mL

130 mm

28

<: Stat>
,

, ,

, .

Time
EP2

EP1

mL

<: Learn>
.

, .

, .
, .

mV
EP2
Max. Volume
EP1

mL

29

4-1-3. ,
, , ,

Blank(00)

0.3ml

Auto(01)

01

C-172 ()
: STD, TET

Auto(01)

Control Speed Slow

A.Int(02)

AgNO3-I/Br/Cl/CN

Auto(01)

S/ SCN
Pb(ClO)2-SO4

C-172 ()

1/100N

: STD, TET

1/100N

C-372 ()

Control Speed Slow

For non-aqueous:

A.Int(02)

M-371 (Silver electrode)

H-171 (Glass electrode)
: STD

Na2S2O3-I2

Auto(01)

1/100N

C-272 ()

KMnO4-Fe

Control Speed Slow

I2-As2O3

A.Int(02)

: STD

C-172 ()

R-115

When noisy, use:

A.Int(02)

H-171 (Glass electrode)

R-172

R-115 (Reference electrode)

: STD

Petroleum(06)

EDTA-Zn

EDTA-Ca

Auto(01)

Add Zn2+ Cu-EDTA ()

Add Ca2+-Ag.EDTA ()
: STD

EDTA-Ca,Mg

EDTA-Zn

A.Int(02)

Ca2+,Mg2+

EBT

Zn2+

XO

2+

MX

Ni

EDTA-Ni

: PTA

KBrO3-Olefin,

A.Int(02)

Back titration,

Na2S2O3-Petroleum

Auto(01)

resin

NaNO2-Sulfonamide
acid aromatic
primary amine

A.Int(02)

M-511 ()
Use M-512 for low current
flucturation.

: POT

M-511 ()
Use M-512 for low current

Intermit(03)

flucturation.
: POT

30

4-2-1.
[Method] .

, [], [] .
, [], [] Yes/No. (, : , )

4-2-2. (Function 0)
[Function]

, [], [] Method file [] .

31

, [], [] .
[], [] Copy [] .

, [], [].
[] .

!
, .

. 4-2-2.
4-2-2

Copy

Load

, PC .
, 7-12-3 /.

Save

PC .
, 7-12-3 /.

32

4-3-2.
[Titration] .

, Method Name, [] .
Method Type, [], [] [] .
4-3-2.
4-3-2

Method Name

Method Type

(Titration/Dose+Titr./Dose).
Titration

: .

Dose

: .

Dose+Titr.

: .

00-06 . 10-47.

!
.
<Titration>: 4-3-4. .
<Dose>: 4-3-3. .
<Dose+Titr.>: 4-3-3 4-4-4.

33

4-3-3.
4-3-2 <Dose> <Dose+Titr.>

. , 4-3-3-1. [], [] , [] .
4-3-3-1

Volume Stop

, , .

, 4-3-3-2 4-3-3-3.

Level Stop

, .

, 4-3-3-2 4-3-3-3.

Diff. Stop

, , .

, 4-3-3-2 4-3-3-3.

mV

mV

mV

(Dose)Level
(Dose)Diff
(Dose)Volume
mL

mL

mL

!
(00-06) .
(4-2-2. ).

34

 4-3-3-2

APB No.

Unit No.

(No. 1-20).

(Volume)

(0 - 9999mL).

Volume Stop , .

(Max Volume)

(0 - 9999mL).

, .
Level Stop Diff. Stop .

Detector No.

APB-510-01B

0-1000mL

APB-510-20B

0-9999mL

APB-510-05B

0-5000mL

APB-510-50B

0-9999mL

APB-510-10B

0-9999mL

(1/2/3).

Unit

, :

STD-510

PTA-510

%TAbs

POT-510

(CMT Range)

pHmV

mV

AmV

CMT-510

S/cm

TET-510

pHmV

(100/1000/10000S).
CMT-510 3 .

(CMT Temp. Co.)

, (0 - 9999).

CMT-510 3 .

35

 4-3-3-3

Dose Level

(0 - 99999).

Level Stop .
.

Differential

(0 - 9999).
Diff.Stop .
.

Cut-off Time

Unit Volume

(0 9999 ).
0 ().
(0 9999mL).
0 , .

Dispense Speed

(0 9999sec/mL).

, :

Wait Time

APB-510-01B

20 9999s/mL

APB-510-20B

1 9999s/mL

APB-510-05B

9999s/mL

APB-510-50B

1 3000s/mL

APB-510-10B

2 9999s/mL

. (0 9999 ).
, .

36

4-3-4.
4-3-2. Method type, Titration() Dose+Titr.(+).

. . [], [] . 4-3-4-1 4-3-4-2.

4-3-4-1

Titration Mode

Form

. .
. , 4-1-1-1 4-1-2.

APB No.

Unit No.

Detector No.

(No.1-10).
1.
(No.1-20).
(, , , ) , 4 -7 .
(1/2/3).

Unit

. :

STD-510

PTA-510

%TAbs

POT-510

pHmV

mV

uAmV

CMT-510

uS/cm

TET-510

pHmV

37

 4-3-4-2

(CMT Range)

(100/1000/10000S).
CMT-510 3 .

(CMT Temp. Co.)

, (0 - 9999).

CMT-510 3 .

Max Volume

Wait Time

Direction

(0 - 9999). , .
:

APB-510-01B

0-1000mL

APB-510-20B

0-9999mL

APB-510-05B

0-5000mL

APB-510-50B

0-9999mL

APB-510-10B

0-9999mL

(0 - 9999sec), .
, .
(Positive /Negative /Auto ).
Auto

: A B , .

Positive

: A.

Negative : B..

mV
A
B

mL

38

 4-3-4-3

(EP Stop Mode)

Both

: , (A,B).

Positive

: , (A).

Negative

: , (B).

mV

Negative
B

Positive
A
mL

!
<Dose+Titr> +,
.

39

4-3-5.
, 4-3-5-1, 4-3-5-2, 4-3-5-3.
4-3-5-1

Method Name

, 14

Method Type

Titration/Dose/Dose+Titr.

Titration

//+

!
00-06 +.
, .

4-3-5-2

Volume Stop/Level Stop/Diff. Stop

Volume Stop

APB No.

110

Unit No.

120

Volume

09999(mL)

Max Volume

09999(mL)

20.0000

Detector No.

1-3

pH/mV/%T/Abs/A/S

mV

100S /1000S /10000S

100S

CMT Temp.Co.

09999

2.0

Level

09999

20.0

Differential

09999

20.0

Cutoff Time

09999(sec)

Unit Volume

09999(mL)

0.05

09999sec/mL

09999sec

Dose Mode

Unit
CMT Range

Dispense Speed
Wait Time

!
, .

40

 4-3-5-3

Form

EP Stop/Level Stop/

EP Stop

Level & EP/Full/Learn/Intersect

APB No.

110

Unit No.

120

Detector No.

13

pH/mV/%T/Abs/A/S

mV

100S /1000S /10000S

100S

09999

2.0

09999(mL)

20.000

Unit
CMT Range
CMT Temp. Co.
Max Volume

(Method 002.0000)
Wait Time

09999(sec)

Direction

Auto/Negative/Positive

Auto

EP Stop Mode

Both/Positive/Negative

Both

!
, .

41

4-4.
4-4-1.
, , . .
.

Control Key
End Point No.

(EP Stop)

(Level Stop)

(Level & EP)

End Sense

1st End Level

2nd End Level
Over Titr. Vol.

E Sense
E/mL Sense
1st End Level
2nd End Level

End Point Area

Separation
Auto Simulation
Over Titr. Vol.

(Intersect
End Sense
End Point Area

(Full
End Sense
End Point Area

Related EP determination
Gain
Data Samp.Pot
Data Samp. Vol

(Auto Titr.)
Control Speed

Related to Data List

(Blank/Auto Int.) (Intermit)
Stability(mV/sec)
Delay Time
Limit Time

Cut-Off Time
Unit Volume
Dispense

(Stat)
Rel.Change Lev.
1st D Speed
Lag Time
Stat Level
Offset Pot.
Limit Time

(Petroleum)
Integral Time
Start Lim. Time
Limit Time
1st Dose Vol.
2nd Dose Vol.
StabilityE/min
E(1st2nd) Pot

Related to Dose control

42

4-4-2.
[Control] .

. [], [] [], [] .
.
.

EP Stop titration

4-4-2-1 and 4-4-2-2

Level Stop titration

4-4-2-3

Level & EP titration

4-4-2-4

Intersect titration

4-4-2-5

Learn titration

4-4-2-6

Full titration

4-4-2-7

43

<Titration form : EP Stop >

4-4-2-1

End Point No.

End Sense

. (1-5). .
Auto

: .
, , ,
, (Fix).

Fix

: , (E, E/mL).
, (Fix)

E Sense

(0 - 999999).
(E2) (E1) .
.

(E/mL Sense)

(0 - 999999)
(E2/mL) (E/mL) .
.
mV

mV
E2

E2/mL

E1

E1/mL
mL

mL

.
End Point Area

. (Set /Off )
.
.

(Lower Volume)

. (0 9999mL)

(Upper Volume)

. (0 9999mL)

(Lower Level)

. (0 999999)

(Upper Level)

. (0 99999)
mV

Upper Level
Lower Level

Lower Volume

E1
mL
Upper Volume

44

 4-4-2-2

Separation
(Level)

. (Set /Off )
(0 999999).

(Level Stop)

. (Set /Off )

(End Level)

. (0 999999)
EP2 , ,
.
mV

mV

EP2

EP2

Level

EP1

EP1

mL

End Level

mL

: EP1 .
: , .
Auto Simulation

(Set /Off ).
End Sense Fix . ,
.

Over Titr. Vol.

(0 9999mL).
, .
.

45

<Titration form : Level Stop >

4-4-2-3

End Point No.

(1/2).

1st End Level

(0 999999).

(2nd End Level)

(0 999999).
.
:
Auto

: . EP1 EP2 ,
, EP2, EP1 0mL.

Negative : . EP1 EP2 ,

EP1=0mL.
Positive

: . EP1 EP2 ,
EP1=EP2=0mL. .

mV

EP1

1st End Level

EP1=0mL

2nd End Level

EP2

mL

Over Titr.Vol.

EP2

mL

. (0 999999)
, .
.

!
,
.

46

<Titration form : Level & EP >

4-4-2-4

End Point No.

(1/2).
.
.

E Sense

(0 - 999999).
(E2) (E1) .
.

E/mL Sense

(0 - 999999)
(E2/mL) (E/mL) .
.
mV

mV
E2

E2/mL

E1

E1/mL
mL

mL

1st End Level

(0 999999).

(2nd End Level)

(0 999999).
.
:
Auto

: . EP1 EP2 ,
, EP2, EP1 0mL.

Negative : . EP1 EP2 ,

EP1=0mL.
Positive

: . EP1 EP2 ,
EP1=EP2=0mL. .

mV

EP1

1st End Level

2nd End Level

EP2

mL

EP1=0mL
EP2

mL

!
), .
47

<Titration form : Intersect >

4-4-2-5

End Point No.

(1/2).
.

End Sense

(Auto /Fix ).
Auto

: .
, , ,
, (Fix).

Fix

: , (E, E/mL).
, (Fix)

Deg Sense

.
, , .
pH
9

mm

Deg Sense

90

EP2

tangent 2

Normalization

tangent 1

EP1

Deg Sense

30
13

mL

130 mm

<Titration form : Learn >

4-4-2-6

End Point No.

. (1-5)

48

<Titration form : Full >

4-4-2-7

End Sense

(Auto /Fix ).
Auto

: .
, , ,
, (Fix)..

Fix

: , (E, E/mL).
, (Fix).

(E Sense)

(0 - 999999).
(E2) (E1) .
.

(E/mL Sense)

(0 - 999999)
(E2/mL) (E/mL) .
.
mV

mV

E2

E2/mL

E1
E1/mL

mL

End Point Area

mL

. (Set /Off )
.
.

(Lower Volume)

. (0 9999mL)

(Upper Volume)

. (0 9999mL)

(Lower Level)

. (0 999999)

(Upper Level)

. (0 99999)
mV

Upper Level
Lower Level
Lower Volume

E1
mL
Upper Volume

!
, , .
.

49

4-4-3.
[Control] .

[], [] . , 4-4-3.
4-4-3

Gain

(1 10) .
1.
, .

Data Samp.Pot.

(0.1 10000mV).
, (1 2mV).
, .

Data Samp.Vol.

(0 9999mL).
, (0.1 0.2mL).
, .
mV

Data Samp. Vol.

Data Samp. Level
mL

!
, Data Samp. Pot Data Samp. Vol .
Data Samp. Pot Data Samp. Vol ( 256 ),
.

50

4-4-4.
[Control] .

: Auto Titr .

[], [] , , .

00

Blank titration

4-4-4-2

01

Auto titration

4-4-4-1

02

Auto intermittent titration

4-4-4-2

03

Intermittent titration

4-4-4-3 4-4-4-4

.
06

Petroleum nuetralization

4-4-4-5

51

<Titration control mode (Method) (): Auto Titration >

4-4-4-1

Control Speed

(Fast , Medium , slow , Set )

Fast : -
Medium : , -, -.
Slow
Set

(Set Speed)

: . 0.01mol/L
: .

. (0 999)
.
, ,
.
: Fast =4.0, Medium =2.0, Slow = 0.5

<Titration control mode (Method) (): Blank Titr. Auto Intermit. >
4-4-4-2

Stability (mV/sec)

Delay Time

(0 10000mV/sec).
(1sec) , .
(0 9999sec).

0-30 (sec).

Limit Time

(0 9999sec).

Stability

, .

52

<Titration control mode (Method) (): Intermit >

4-4-4-3

Cut off

Time

(0 9999sec).
.
0 .

(Unit Volume)

(0.01 50mL).
Cut-off Time 0 , .

Dispense Speed

(1 9999sec/mL).

(Stat), :
4-4-4-4

Rel.Change Lev.

Set up relative potential to switch dose speed (0 999999).

Dispense speed can be changed by this parameter.
mV
Rel.Change Lev.
Stat Level

Offset Level

mL

1st D. Speed
Lag Time

Set up dose speed (1 9999sec/mL) until it reaches switching relative potential.

Set up interval (0 9999sec) for data sampling.
In Stat titration, data (titration volume, potential, time) is stored at every selected time.

Stat Level
Offset Potential

Set up potential (0 999999) for stat control.

Set up offset level (0 999999).
Even when deviation exists between control potential and detection potential, if it is within
offset level, it stops dosing.
Offset level is the potential relative to control potential.

Limit Time

Set up limit time (0 9999sec) for titration.

Titration ends when the limit time elapses.

53

<Titration control mode (Method) (): Petroleum >

4-4-4-5

Integral Time

Set up time (0 999999sec) to read potential for stability sense.

Potential reading time is for petroleum neutralization number.
When 60 sec is selected, stability is sensed by potential fluctuation every 60 seconds.
JIS K-2501 and ASTM D664 specifies the time setting for 60 sec.

Start Limit

Set up limit time (0 999999sec) for stability sense at start of titration.

Potential is read for this time length in the beginning of titration.
0 sec means no limit time.

Limit Time

Set up time (0 999999sec) to limit stability sense.

When the time elapses, it starts data sampling and dispensing.

1st Dose Vol.

Enter the first dose volume (0.05 0.02mL).

When potential change after dosed is smaller than dose switching potential(E(1st2nd)),
it dispenses preset amount of solution.

2nd Dose Vol.

Enter the second dose volume (0.05 0.02mL).

When potential change after dosed is larger than dose switching potential(E(1st (2nd)), it
dispenses preset amount of solution.
Typically set smaller amount for second dose than the first.

Stability(E/min)

Set up stability sense value (0(999999).

JIS K-2501 and ASTM D664 specifies 5.0 (mV/min) for setting.
Titrant is dosed when potential change in a minute is within 5.0mV. Even if potential
reading time is less than 60 sec, set up value converted to 60 seconds.

E1st2nd

Set up potential (0 ( ( (999999) to change dose volume.

When potential change becomes larger by reaction and potential difference after dosed
becomes greater than preset value, the volume for one time changes from the first volume
to second.
mV

2nd Dose Vol.

1st Dose Vol.

E(1st2nd

mL

54

4-4-5.
<Method 00 () 02 ()>

EP

Full

Level

Lev.&EP

Intersect

Learn

1-5

1-2

End Sense

Auto/Fix

Auto

Auto

Auto

E Sense

0-999999

50

50

50

E/mL Sense

0-999999

100

100

100

Deg Sense

0-180

30

End Point Area

Off/Set

Off

Off

Lower Volume

0-999999

Upper Volume

0-999999

Lower Level

0999999

Upper Level

0999999

Off/Set

Off

0999999

End Pont No.

Separation

Level

Level Stop

Off/Set

Off

End Level

0999999

1st End Level

0999999

2nd End Level

0999999

No/Yes

No

No

No

0-999999

1-10

0-999999

0.5

0.5

0.5

0.5

0.5

Auto Simulation
Over Titr.Vol.
Gain
*

Stability(mV/)

Delay Time

0-9999

Limit Time

0-9999

30

30

30

30

30

Data Samp. Pot.

0-2400

4.0

4.0

4.0

4.0

4.0

Data Samp. Vol. (M00)

0-999.99

0.1

0.1

0.1

0.1

0.1

(M03)

0-999.99

0.5

0.5

0.5

0.5

0.5

* . .

55

Method 01

EP

Full

Level

Lev.&EP

Intersect

Learn

1-5

1-2

End Sense

Auto/Fix

Auto

Auto

Auto

E Sense

0-999999

50

50

50

E/mL Sense

0-999999

100

100

100

Deg Sense

0-180

30

End Point Area

Off/Set

Off

Off

Lower Volume

0-999999

Upper Volume

0-999999

Lower Level

0999999

Upper Level

0999999

Off/Set

Off

0999999

End Pont No.

Separation

Level

Level Stop

Off/Set

Off

End Level

0999999

1st End Level

0999999

2nd End Level

0999999

No/Yes

No

No

No

0-999999

1-10

Fast/Medium

Medium

Medium

Medium

Medium

Medium

0-10

2.0

2.0

2.0

2.0

2.0

Auto Simulation
Over Titr. Vol.
Gain
*

Control Speed

/Slow/Set
*

Set Speed

Data Samp. Pot.

0999999

4.0

4.0

4.0

4.0

4.0

Data Samp. Vol.

0-999.99

0.5

0.5

0.5

0.5

0.5

* . .

56

<Method 03 () - 1: >

EP

Full

Level

Lev.&EP

Intersect

1-5

1-2

End Sense

Auto/Fix

Auto

Auto

Auto

E Sense

0-999999

50

50

50

E/mL Sense

0-999999

100

100

100

Deg Sense

0-360

30

End Point Area

Off/Set

Off

Off

Lower Volume

0-999999

Upper Volume

0-999999

Lower Level

0999999

Upper Level

0999999

Off/Set

Off

0999999

End Pont No.

Separation

Level

Level Stop

Off/Set

Off

End Level

0999999

1st End Level

0999999

2nd End Level

0999999

No/Yes

No

No

No

0-999999

1-10

Cut-off Time

0-99999

Unit Volume

0-999999

0.05

0.05

0.05

0.05

0.05

Dispense Speed

1-999

100

100

100

100

100

Data Samp. Pot.

0999999

4.0

4.0

4.0

4.0

4.0

Data Samp. Vol.

0-999.99

0.5

0.5

0.5

0.5

0.5

Auto Simulation
Over Titr. Vol.
Gain

* . .

57

<Method 03 () 2 : >

Stat

Gain

1-10

Cut-off Time

0-9999

Unit Volume

0-999999

0.05

1-100

100

0-999999

1st D. Speed

1-999

50

Lag Time

0-9999

30

Stat Level

0999999

Limit Time

0-9999

0999999

Dispense Speed
Rel. Change Lev.

Offset Potential

58

Method 06

EP

Full

Level

Lev.&EP

Intersect

1-5

1-2

End Sense

Auto/Fix

Auto

Auto

Auto

E Sense

0-999999

50

50

50

E/mL Sense

0-999999

100

100

100

Deg Sense

0-180

30

End Point Area

Off/Set

Off

Off

Lower Volume

0-999999

Upper Volume

0-999999

Lower Level

0999999

Upper Level

0999999

Off/Set

Off

0999999

End Pont No.

Separation

Level

Level Stop

Set/Off

Off

End Level

0999999

1st End Level

0999999

2nd End Level

0999999

No/Yes

No

No

No

0-999999

1-10

Integral Time

0-9999

60

60

60

60

Start Limit

0-9999

Limit Time

0-9999

1st Dose Vol.

0.05-0.2

0.1

0.1

0.1

0.1

0.1

2nd Dose Vol.

0.05-0.2

0.05

0.05

0.05

0.05

0.05

Stability(dE/min)

0-999999

5.0

5.0

5.0

5.0

5.0

dE(1st2nd)

0999999

30

30

30

30

30

Data Samp. Pot.

0999999

4.0

4.0

4.0

4.0

4.0

Data Samp. Vol.

0-999.99

0.5

0.5

0.5

0.5

0.5

Auto Simulation
Over Titr.Vol.
Gain

* .

59

4-5.
4-5-1. [Result]
[Result] .

, [], [] [] . .
4-5-1

Calculation

.
.

Constant

, .

Report

Graphic

60

4-5-2. (Result 0)
[Result] , Calculation.

, [], [] .
4-5-2-1, 4-5-2-2 4-5-2-3.
4-5-2-1

Calculation Type

(Sample /Factor /Blank ).

.

Conc-1
(Formula)

1 (Off /Set ).
. conc-1 1 Set .
[ ] ( ) +, , , , , 50 .

SIZE

EP1 EP5

SMW

C1 C5

SEQN

K1 K5

MW

CO1

EQN

TF

DRI

(Karl Fischer)

TN

PK1

BL1
BL10

CO5

PK5

(Unit)
(EP No.)

TMW

N1 N5

TEQN

DMW

DF

DEQN

DN

.
.

61

 4-5-2-2

(Level or EP)

(EP /Level ).
Level & EP .
EP

: . .
.

Level

: . .
.

(Blank Replace)

(0-20) .
blank .

Conc-2Conc-5
Temp. Comp.

Conc-1 -1 .
(Auto /Manual /Off ).
Manual: manual temperature compensation
Auto: automatic compensation by optional temperature sensor (#430-5350)
Off: not perform temperature compensation

(Titrant Temp.)

Set temperature (0-100C) of titration solution

This appears when Temp. Comp is Manual.

(Correct Temp.)

Set compensated temperature (0-100C).

(A Parameter)

Set conversion coefficient A (0999999).

(B Parameter)

Set conversion coefficient B (0999999).

Temperature compensation formula is as follows:
V=V0(1+AT10-3+BT2(10-6)
V(mL)

: titration volume after compensation

V0(mL)

: titration volume

: compensated temperature ( temperature of solution

A,B

: conversion coefficient

62

 4-5-2-3

Sample

(EPnBLn)TFCnKn/SIZE

(EPnEPn-1)TFCnKn/SIZE

(BLnEPn)TFCnKn/SIZE

((EPnBLn)TFCn +DDF Cn+1 Kn)/SIZE

((EPnEPn-1)TFCn+DDF Cn+1Kn/SIZE

Hydroxyl value

((EPnBLn)TFCnKn +SIZEKn+1)/((EPn

BLn) TFCn Kn+2+SIZEKn+3)+R

Dissociation

PKn

constant of acid

KapH-log [B]
[HB ]
BH
B+H

From this Eq., [B]=[HB+], that is, half neutralized pH shows pKa.
More precisely,
approximately [B]=[HB+] at half equivalent point, however, due to
little error at pKa3-11, the pH at half equivalent point is regarded as
pKa.
Factor

Factor

(SIZERKn)/((EPnBLn)Cn)

(SIZERKn)/(( BLnEPn)Cn)

<>
Sample File

APB
100Files

Manual Operating

Manual Dose

Unit File
APB Unit No.
Reagent Name[
Factor
[
Concentration[
Equiv.Nimber [

Sample No.
[01-01]
Sample ID
[9809878]
Sample Unit
[ g ]
Sample Size
[2.4567]g
Molecular Weight [ 40.00]
Equiv.Number
[ 2.00]
Operator < KEM JIRO
>

20Files
[ 1]
]
1.0162]
0.1]
1.0]

Method54
Method50
Method47
Method10
Method 06
Method 00

Titration

Control

Result
Calculation
Conc.1
Formula=(EP1-BL1)TFSMWTEQN/SEQNTNK1/SIZE

Constant
K1=[

Report

0.1]

Graphic

Combine
5Files
User
38Files
Maker
File

63

4-5-3. (Result 1)
[Result] , Constant.

. [], [] .
, 4-5-3.
4-5-3

C1C5

(00 - 999999mg/mL).
, NaOH 1mol/L-HCl :
HCl+NaOHNaCl+H2O, 1:1.
NaOH 40.00, 40.00mg NaOH 1mL of 1mol/L-HCl .
C1=40.00mg/mL.

K1K5

(0 - 999999). , % ppm .
, NaOH 1mol/L-HCl , %, :
NaOH (%)=EP1-BL1)TFC1K1/S
EP1:10 (mL)BL1=0.02 (mL)TF=1.006C1=40.00(mg/mL)
S: 5.0000 (g), %, K1=0.1. ppm, K1=1000

MW,TMW,DMW

. TMW, DMW.

EQN,TEQN,DEQN

. TEQN, DEQN.

N1N5,TN,DN

. TN, DN.

R
DRI
D
BL1BL10

.
(Karl Fischer KF )

TF

DF

. .

!
[Sample], [APB] .

64

4-5-4. (Result 2)
.

[Result] , Report [] .

. [], [] [], [] . , 4-5-4.

4-5-4

Report

(Off/GLP/Short/Variable).
Off

GLP : GLP .
Short : .
Variable
Titration Curve

Data List

: .

.
Yes

: . .

No

: .

(Off/Short/Detail).
Off

: .

Short

: , , .

Detail

: .

65

<: GLP >

AT-510

Model

<Constant>

Serial No.NZA09802

K1

0.1

Version No.1.00

40.00

C1

N1

_______________

*** R e s u l t ***

Sample No.01-01

Date : 1999/08/01 00:02

Sample ID :19990801

ID

Method No. : 1

<Auto Titr.>

Method Name:
Auto Titration
Titr.Reagent Name:

: 1.0000

MW

: 1.0000

EQN

Titr.Time

:00:04:30

Size

: 5.1647g

MW

: 1.0000

EQN

: 1.0000

Conc-1

<Titration>

APB No.

: 1

End Point-1
: 8.1176mL

Potential :
:EP Stop

33.895%

Volume

Form

1.0000

__________________

Method Type : Titration

0.1

<Titr.Constant>
Factor

5.26pH

3.00

:
Direction

Sample

[pH]

13.00

0.000

: Auto

<Control>
End Point No.: 1
End Sense

: Auto
:

Control Speed:
<Medium>

10.000
[mL]

<Calculation>
Calc. Type

: Sample

Name :<Kyoto Taro

>

___________________

:
Temp. Comp

: Off

66

<>

Data List
No. Volume
[mL]

Potential S

[mV]

0.00000 - 40.00 0

0.43000 -192.20 0

0.46000 -196.30 0

0.79500 -200.30 0

after a little passing the point, however, the end sense status for

1.14500 -204.40 0

max inflection pint is expressed by status 3, 6 or 7.

1.47500 -208.40 0

1.82000 -212.90 0

2.20000 -217.10 0

2.58000 -221.30 0

10

2.96000 -225.10 0

11

3.46000 -100.00 0

12

3.57000

13

3.64000 228.80 0

14

3.80000 224.90 0

18

5.38000 212.90 0

19

5.76000 208.60 0

20

6.11500 204.40 2

21

6.47000 200.20 0

23

6.83000 195.90 0

24

7.16000 191.50 0

No. dE

-
2

13 1.66E 2 4.91E 2 3

Data Count :

: The max inflection point satisfying the end sense (dE) and
(dE/dmL) prints measurement results.

: The inflection point is not determined to be an endpoint due to

its direction.

: The inflection point is not determined to be an endpoint due to

the end sense (dE) smaller than preset dE.

1.30 3

dE/dmL

: An inflection point is determined to be the max inflection point

: The inflection point is not determined to be an endpoint due to

the end sense (dE/dmL) is smaller than preset dE/dmL.

St

24

!
.
, .

67

4-5-5. (Result 3)
[Result] Graphic.

. [], [] .
, 4-5-5.
4-5-5

Graphic Type

(Titration Curve /Titr.Curve+Diff .)

Titration Curve

: .

Titr.Curve +Diff.
Graphic Range

: .

(Auto /Fix ):
Auto

: .

Fix

: .

(Volume Upper)

(0 9999mL). Fix .

(Volume Lower)

(0 9999mL). Fix .

(Level Upper)

(0 999999). Fix .

(Level Lower)

(0 999999) Fix .

(Time Upper)

(09999 ).
Fix . Stat .

(Time Lower)

(0 9999 ).
Fix . Stat .

68

4-6.
4-6-1.
, ID, , , .
, .

4-6-2. (Sample)
[Function] Sample FileNo.
Sample FileYes , 6-1-4 .
[Sample] .

. [], [] [], [] , 4-6-2.

4-6-2

Sample No.

. [-] (00 00 99 99),

, .
.

Sample ID
Molecular Weight

.
(0 - 999999).
SMW .

Equiv. Number

(0 - 999999).
SEQN .

Sample Unit

(g/mg/mL).

Sample Size

(0.0000- - 999999).

Operator

.
Setup Regist Operator
.

!
Function Sample File on , .
69

4-7. (APB 2)
(, , , ) , .
20 . , .
[APB] , Unit File.

. , 4-7.
4-7

APB Unit File

APB (Skip /Save /Load ).

APB Unit No.

(1 - 20).

Reagent Name

Factor

(0 999999).
, . TF () DF(
) .

Concentration

(0 999999).
TN () DN () .

Molecular Weight

(0 999999).
TMW, DMW .

Equiv. Number

(0999999).
TEQN, DEQN .

Unit Type

(1mL/5mL/10mL/20mL/50mL)
.

Alarm
(Volume)
(Lower Volume)
(Next Replace)
Permit. Err.

(Off /Set ).
, .
.
.
(0 9999).

!
, .
70

5. (Function 1)
5-1.
, . , 5-1.
5-1

(Mean , SD , RSD ).

Statistics

, , ,
.

Re-Calculation

, .

Data Simulation

, .

Load

PC .

Read/store of data in PC card / PC .

Save

PC .

Read/store of data in PC card / PC .

!
100 , 100 ,
.
[Function] .

[], [] Data File [] .

71

. [], [] [] .
, [Disp.] , (*) ,
, [Disp.] , (*) .

72

5-2.
[Function] Data FileStatistics.

, [], [] , [], [] [], , 5-2.

5-2

Method No.
Method Name

(00-06, 10-47, 50-54) .

.

Sample No.

Calc. Type

(Blank /Sample /Factor ) .

Data Print

!
, .
Set, 00-47 .
50-54 , .
, Statistics [] .

73

. 1 , [], [] , [Print] .
Exit [] .

<>
Mean (), SD () RSD (). RSD CV ().
Mean, SD and RSD :
n : X1, X2, ....Xn;

Mean ( X )

( X 1 + X 2 + L + Xn)
n
n

SD

RSD

( Xi X )

i =1

n 1
SD
100(%)
X

!
(0), RSD (0) .

74

5-3.
[Function] Data File. [], [] , [], []
Re-calculation, [] .

. , 5-3.
5-3

Sample size

[Sample] Size.
Exit [] . .

Calculation formula

[Result] Calculation.
[Esc] . ..

Constant

[Result] Constant.
[Esc] . .

Print format

[Result] Report.
[Esc] . ..
[Print] . (#) .

Reprint
<>
Model

: AT-510

Method Name:

Serial No. : NZA09802

[Re-Calculation]

3.00

Juice

[pH]

13.00

0.000

Titr.Time

:00:00:55

Size

5.0000mL

Sample No. : 01-01 (#)

MW

: 1.0000

Date : 1999/08/05 00:24

EQN

: 1.0000

Sample ID : 99080501

Conc-1

0.8227

End Point-1
Method No. : 10
<Auto Titr.>

Volume
Potential :

: 2.2234mL
8.3pH

5.000
Name <Kyoto

>

75

5-4.
, .
[Function] Data File [], [] , .
Data Simulation [], [] [] .

. , [], [] [] .
, 5-4.
5-4

Auto Simulation

Manual End Point

Manual Intersect

Pin-Point EP

, .
, .
.
, .
.
, .
.
,

!
, (, ) .
.

76

5-4-1.
[Function] Data file, [], [] , .
Data Simulation, [], [] [] .
Auto Simulation.

. [] .

, . [Print] , Report.

(#)

77

5-4-2.
[Function] Data file, [], [] , .
Data Simulation, [], [] [] .
Manual End Point.

. , [] .

, . [Print] , Report.

(#)

78

5-4-3.
[Function] Data file, [], [] , .
Data Simulation, [], [] [] .
Manual Intersect.

.
( 2 ) [] .

. [], [] [] .
, [] .
.
EP1 1.
, .

79

, . [Print] , Report.

(#)

!
, .

80

5-4-4.
[Function] Data file, [], [] , .
Data Simulation, [], [] [] .
Pin-Point EP [] .

[] .

. [], [] . .
[] , , [] .
[] . .

. . [Print] , Report.

(#)

6.
81

7.
7-1.
7-1-1. (Function 6)
.
[Function] . Set Check [], [] [] .

. 7-1-1 .
7-1-1

Check Mode

(Daily/Periodic) /.

Detector No.

(1/2/3) .

Standard Name
(Enter each for daily and

.
2-3-3 .

periodic)
Standard Value

(-999999999999).

(Enter each for daily and

periodic)
Permit. Err.

(0999999).

(Enter each for daily and

periodic)

!
Check Mode Daily .
, 9-5 .

82

7-1-2. (Function 7)
.
[Function] . Periodic [], [] [] .

, 7-1-2 .
7-1-2

Periodic

(check/Calib.) /.
Calib.: .
Check: .

Detector No.
Alarm
(Enter each for daily and

(1/2/3).
Set Off , /.
Set: /.

periodic)

Off: . .

Next Date

/.
Periodic , ----/--/-- .

Interval

/ (0 999 ).

Record

PC (Skip /Load /Save ) , /.

Skip: .
Load: PC , .
Save: PC .

Show List
(Enter each for daily and

[] , /.
10 .

periodic)

83

!
/.
, 9-5. .
Show List [] .

. [] . [Print] .

!
/ PC .
, PC .

84

7-1-3. (Function 5)
[Function] Check Titration.

. , (00-06, 10-47), [] .

!
Sample File Off .
, 9-5. .

. (, , ) [Sample] Size.
[Start] .

!
Sample File On Check Titr. , Sample file
.
(Method 50-54).

85

7-2. (Function 8)
.
[Function] Buret Check.

. . 7-2.
7-2

APB No.

(No. 1-10).

Unit File

(No.1-20) .

Unit Type

.
APB .

Permit. Err.

.
APB ..

Temperature

(0 -100C).

!
(#430-5350) , ,
. 1C.
, 0.1C .
[Burette Check] [] .
, [Start] .
.
, [] .

!
, [Disp.] .
, [] .
, 0.0002g .

86

, , .

, . , [APB] Unit File

. [Esc] .

!
25C 1013.25hPa
20C .
.
.
KEM . , .

87

7-3. pH (Function 12)

, JIS , pH7/pH4/pH9 .
pH , pH pH pH Calib. TablepH , .
..

1) [Function] , pH Calib. TablepH .

2) . [Set Buffer 1] [] .

3) . (Buffer1) 1 pH . , (Buffer 2) 2 (Buffer 3) 3

pH .

!
, pH (Buffer 1) 1, (Buffer 2)
2 (Buffer 3) 3.
(Buffer 2) 2 .
: pH4Buffer1( 1)pH7Buffer2( 1)pH9Buffer3( 1)
(3-2-1. Calib. Method Auto ) , Calib. Table
User , .

88

7-4. (Function 4)
EP Stop Full , , .
, [Function] .

. Re-Titr. [], [] [] .

. [Titration] Max Volume [] . [Start] .

!
, Full .
: , EP Stop Full
, , .

89

7-5.
7-5-1. (APB 0)
[APB] .

. Manual Operation, [], [] [1] [] .

:
Reset : .
Top : .
Replace
Up

: .

: .

Down

: .

Stop : .
Purge : .
--------: .
. Burette No. [] , [] , [] ,
[] . , 7-5-1.
7-5-1

Burette No.
Burette Speed

(No. 1 - 10).
. (Fast /Medium /Slow )
Fast : .
Medium

: .

Slow : .
Purge Times

(0/1-99). 0 .

Purge Mode

(To bottle /To Nozzle )

To Bottle

: .
.

To Nozzle :
. , .

!
[ ][ ] [ ] .
, [ ] [ ] .
90

7-5-2. (APB 1)
[APB] .

. Manual Dose [], [] [1] [] .

. 7-5-2. [Start] .
7-5-2

Burette No.

(No.1-- 10).

Dispense Volume

(0 -- 999999mL).

Dispense Speed

(0 -- 9999sec/mL).
, .

!
, .
Dispense Speed.

91

7-6. (Setup 7)
[Setup] .

. Beep [], [] [] .

. , [], [] [] .
Beep Type (Type 1/2/3/4), [] . .

92

7-7. (Setup 4)
[Setup] .

. LCD Contrast. [], [] [] .

. [], [] [] .

93

7-8. (Setup 6)
[Setup] .

. Lock. [], [] [] .

. New Password. [], [] [] ,

Confirm.
[Change Password] [] .

!
, [Titration] , [Control] , [Result] ,
[Function] [Setup] .
, Lock, Password.
, New Password [Clr.] Confirm.

[Change Password]

[] .

94

7-9. (Stirrer)
[Stirrer] , On/Off .
, [Stirrer] 2 .

. . 0 .
4. , 6 8 .
, 7 9 .

!
, .
4 6 .

95

7-10. pH (Setup 8)
(, ), pH , ,
.

[Setup] .

. pH PolaritypH [], [] [] .

. pH PolaritypH Reverse [], [] [] .

.

!
, Standard.
Reverse,
.

96

7-11. (Function 13)

.
[Function] . Card Utility [], [] [] .

. Card Information [], [] [] .

Method File

: 958 .

Data File

: 109 .

Sample File

: 196 .

Check File

: 958
(1 10 )

Calib. File

: 645
(1 10 )

APB Unit File : 28

(1 20 )
.

97

7-12. / PC
(#434-0039) , , .
1MB SRAM (static random-access memory) .

7-12-1. PC Format (Function 13)

7-12-2. / (Function 1)

7-12-3. / (Function 0)

7-12-4. / (Sample)

7-12-5. /(APB 2)

7-12-6. / (Function 7)

7-12-7. / (Function 7)

7-12-8. / (Function 3)

98

7-13. / (Function 10)

APB Unit FileCommom Blank
.
.

[Function] Auto Statistics.

. Yes [], [] [(] .

/,
.
()

99

7-14. ()
, 00-06 10-47 . 50-54.
1) [Method] .
2) , .
3) [Method] 50-54.
4) [Titration] .

, , .

5) [Sample] .
6) .

[Start] .

!
(, )
() , .
.
, .
, (Function : Re-Titration ) .
, COD KF .

100

8.
8-1.
, .

(1)
. , . .

(2)
, .
, .
, .
, .

(3)
, , .

(4)
. , .

(5)
, , . , . ,
.

(6)
[APB] . Manual Operating, ,.
, 9-2 .
(7)
. , 9-2 .

101

(8)
.

, .

(9)
, .
, .
, .

(10)
. ( 3-2. ).
(11)
, Zeolite sold under 5A .

102

8-2.
8-2-1.
. .
5 , , .

8-2-2.
, , , 0.1N ,
, , , ,
, , , ,,
KEM , .
, , , ,
, pH7 , , .

103

8-2-3.
, .
Tube end
Washer A

Washer B

Tube

Joint

O-ring

8-2-4.
, 7-5.
, Replace .

1) .
2) .
3) .
4) .
5) [Reset] .

104

8-2-5.
<>
1) .
2) [] [] , .
3) [] , .
4) .

Burette cover

Holder

Loosen

5) , [] .
6) , [] , , .
<>
1) , .
2) , .

3) .

105

<>
1) .
2) .
3) . .
4) , .

<>

Piston screw

1) , .
2) .
3) [] , .
4) .

Fasten

[], [] , , , .
5) .

!
, .
.

106

8-2-6.
<>
1) .
2) [] [] , .
3) [] , .
4) .

Burette holder

Loosen
5) , [] .
6) , [] , ,
<>
1) , .
2) , .

107

<>
1) , ..
2) .
3) [] , .
4) .

Burette holder

Loosen
[], [] , , , .
5) .

!
, .

<>
1) .
2) .
3) [] [] .
4) 1 3.

108

8-2-7.
, , , :

<>
1) .
2) . ()
3) , .
4) .
5) .

!
.
, .

<>
1) , . .
2) , .
3) .
4) 2 3.
5) .

!
, .
, .
.

109

8-2-8.
1) .
2) .
3) .
4) .

Degas
tube

Titration
nozzle

Joint

!
.
, .

110