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The main content contained in PT. Pupuk Iskandar Muda wastewater are urea and ammonium. Urea and ammonium in this study were processed using conventional oxidation !"#"$ and Advanced #xidation Processes com%ination of !"#"&'e"()fenton$. 'rom the preliminary treatment results of using !"#" *+++ ppm o%tained p! * as the optimum p! with the highest decreasing of urea concentration from "*,,-./* ppm to 0".-"0/ ppm. The parameters used in this study were variation of the !"#" concentration 0+++- /+++*+++- ,+++ and 1+++ ppm$ and 'e"( concentration *++ ppm at various initial concentrations !"#". The result of this study indicated that the highest decreasing of urea concentration was o%tained %y using fenton reagent ! "#" 1+++ ppm and 'e"( *++ ppm$ with the initial urea concentration "*,,-./* ppm to + ppm urea. The decomposition reactions of urea to ammonium were represented %y the first order reaction kinetics and the reaction rate constant k.$ were +-+.2. The decomposition reaction of ammonium to nitrite also were represented %y the first order reaction kinetics and it3s reaction rate constant k"$ were +-+"". The results of this study indicate that fenton reagent can %e applied to the degradation of urea in the treatment of industrial wastewater urea. 4eywords5 Advanced Oxidation Processes (AOP), Hydrogen Peroxide, Fenton, Fertilizer Industry Wastewater