5 Apr 13 Ms-003400-01 Son a 2 @ cameron ae Page of 25 PROCEDURE FOR MATERIAL PROCESSING AND QUALIFICATION (WROUGHT AND CAST MATERIALS) ‘API 6A, PSL 1-4 HANGERS (CRA MATERIALS ONLY), BODIES, BONNETS, END AND OUTLET CONNECTIONS, AND STEMS 1.0 GENERAL: This document specifies the processing end qualification requirements for API 6A, product specification level (PSL) 1, 2, 3, and 4 materials for bodies, bonnets, and end and outlet connections stems, and CRA (Le, 410 SS, 716, etc.) hangers. It must be used in conjunction with another Cameron maternal specification that gives the requirements for a specific material. When referenced in another material specication, this specification must be also be complied wth 2.0 MANUFACTURING PRACTICE: 2.1 Wrought Material All material shall be of pressure vessel quality and shall have @ wrought structure throughout. ‘Atully wrought structure is defined as one that is free from pipe and harmful segregation (the presence of which would indicate insufficient iscard from the starting ingot). 2. is free from burst, flakes, cracks, seams, laps, or other injurious defects detrimental to the end use of the part, 3. is free from any open discontinuities (porosity, shrinkage, pipe, etc.) when macroetched or viewed under a light microscope at 250 4. has a homogenous microstructure in any given area, Note: Some banding may be present in heavy sections. This is normal and will not be cause for rejection unless it can be shown to be detrimental to the end use of the part. 5. shows no evidence of macrosegregation (ingotism) that may be detrimental to the end use of the part. 6. in the case of carbon, low alloy, and martensitic stainless steels - has isotropic ductility properties within any given area. Note that this does not require that ductlity properties be Uniform throughout the entire cross section. These materials must be capable of meeting the following test unless otherwise agreed upon with Cameron Metallurgy. Original Date: 16 May 86PROPERTY OF @camERON ==" ees Trane W. Proveast ORE FETEOT 5 Apr 13 ws-003400-01 or 28 5 Aprts Page 2 of 25 If Equivalent Round is 10° or below then: In any given area, the elongation and reduction in area values of two tensile specimens. taken adjacent to and 90° to each other shall satisfy the following: Elongation (larger value)/Elongation/ (smaller value) < 4.20 Reduetion in Area (larger value/Reduction in Area (smaller value) < 1.20, If Equivalent Round is greater than 10° then’ In any given area, the elongation and reduction in area values of two tensile specimens taken adjacent to and 90° to each other shail satisfy the following: Elongation (larger value)/Elongationy (smaller value) < 1.40 Reduction in Area (larger value)/Reduction in Area (smaller value) < 1.40 24.4 Hot Work Practice Material shall be forged ("Yorged” here refers to any mechanical process that shapes metal at an elevated temperature utlizing one or more dies, €.a. openiciosed die forging, ring roling, extrusion, roling, etc.) according to a witten procedure specified by the forging supplier. The minimum acceptable total hot work ratio from ingot to billet shall be 3 to 1 (except as noted). The total hot work ratio for hot work practices Is defined as the product of the hot work ratio for each hot working operation, i (hot work ratio of operation #1) X (hot work ratio of operation #2) X (..). The forging reduction shall be the product of al forging sequences using the original ingot cross section as the starting point and the final cross section of the billet prior fo any closed die work Note: The minimum acceptable hot work ratio is 3 to 1. Hot work shall be sufficient to guarantee a fully wrought structure as defined above, but in no case less than 3 to 1. Just because a forging has a hot work ratio exceeding the 3 to 1 minimum does not necessarily mean that the forging is acceptable. It must have a fully wrought structure as defined in 2.1 ‘As an alternate to this 3 to 1 ratio requirement, the material supplier may propose other options for Cameron's consideration If the proposal is acceptable to Cameron Metallurgy, the material supplier shall perform tests to confirm that a wrought structure throughout is present. Test results shall be submitted to Cameron Metallurgy for approval. Evaluation of these test resutts, may be used to accept processing of components forged with similar processes provided that the total hot work of the similar components is greater than the component process previously evaluated, Note: Unless prohibited by the specific material specification, bar stock may be open dle forged, rolled, or extruded ‘Original Date: 16 May 85PROPERTY OF sae W Rae oe ia 5 Apr13 MS-003400-01 vier 8 Tehran oe 28 @camMERON ait eee 2.4.2 Microcleanliness of Stee! Alloys Forging supplier shall guarantee that production forgings are capable of meeting the following requirements if tested by Cameron: ‘A. Rate the specimen per ASTM E45, Standard Test Method for Determining the Inclusion Level Rating, Method A. Type A ThiniHeavy 20/15 Type B ThiniHeayy 2.0/1.5 Type ThiniHeavy 20/15 TypeD ThiniHeayy 20/15 2.2 Casting Practices 2.241 All castings shall be of pressure vessel quality. The materials manufacturer shall document foundry practices which establish limits for sand control, core making, rigging and metting to insure repeatability in producing castings which meet the requirements of this specification 2.2.2 Microcleaniiness of Steel Castings Casting supplier shall guarantee that steel castings are capable of meeting the following requirements if tested by Cameron: Rate the specimen per ASTM E45, Standard Test Method for Determining the Inclusion Level Rating, Method A Type A ThiniHeavy 2.01.6 Type B ThinHeavy 2.0/1.5 Type C ThinHeavy 2.0/1.5 Type D ThinHeayy 2.0/1.5 2.3 Heat Treatment Sections 23.1 through 23.6 apply to conventional batch type heat treating, Section 23.7 applies to continuous fumace heat treating, Original Date: 16 May 86 ne pts, ce ee saan anon ae yun th a ha wh eH ah a5 Apr 13 Ms-003400-01 Son a 2 @ cameron ae Page 40125 2.3.4 Heat Treatment Equipment All heat treatment equipment used for production material and the Qualification Test Coupon (GTC) shall be qualified Qualification shall be done in accordance with one of the following ‘A. AMS-H-6875A, Section 3 (and AMS 2750D in accordance with appropriate furnace class) British Standard M54: 1982, Section § APIGA, Latest Edition ‘A written procedure that has been submitted to and approved by Cameron Metallurgy. vom Furnace Loading The material shall be loaded into the heat treatment equipment such that the presence of one part does not adversely affect the heat treatment response of any other part in the same heat treatment load, Heat Treatment Instrumentation 2.3.8.1 Only automatic controlling and recording instruments shall be used, Controlling ‘thermocouples shall be located in the working zone of a furnace. 2.3.3.2 Heat treatment controlling and recording instrumentation shell possess an accuracy of +1% of their full scale range and shall be calibrated at least once every three months. 2.3.3.3 Instrumentation used to calibrate the production instruments shall possess an accuracy of + 0.25% of full scale range. Approved Heat Treatment Time at Temperature Monitoring Methods There ate many methods of monitoring time at temperature which will assure that the requirements of the Cameron material specification are satisfied, The following methods are the recognized and approved methods (for batch furnaces only). Any heat treatment certification which requires actual time or charts shall reference the method utllized, The heat treater shall specify and use an approved monitoring method, The cross-section of a part is defined as the diameter of the largest sphere that can be whally inscribed ‘anywhere within thet part. Note: for PSL. 4 body, bonnet, end and outlet connections, and hanger materials, only method C is acceptable, Method A - Furnace Temperature Monitoring This method shall use a thermocouple which monitors the furnace atmosphere temperature, Holding time shall start after the furnace atmospheric thermocouple reaches the set point temperature, Holding times shall be as indicated below (see Note) + For parts up to and including 10" (25.4 cm) in cross section, hold for a minimum of 12 houriper inch of heaviest cross section for normalizing, austenitizing, or annealing operations; and a minimum of 3/4 hour/inch of heaviest cross section for tempering and aging operations. If double tempering is specified, the first temper oyole shall be for a minimum of 3/4 hourlinch of heaviest cross section. The second temper for 2 minimum of 1/2 hourfinch of heaviest cross section Original Date: 16 May 86PROPERTY OF sae W Rae oe ia 5 Apr13 MS-003400-01 vier 8 Tehran oe 28 @camMERON ait eee = For parts over 10" (25.4 cm) in cross section, hold for @ minimum 1/2 hourfinch of heaviest cross section for normalizing, austeritizing, or annealing operation; and minimum of 1 hourfinch of heaviest cross section for tempering and aging operations. It double tempering is speoified, the first temper shall be for @ minimum of one hourfinch of heaviest cross section. The second temper for a minimum of 4/2 hourfinch of heaviest cross section + As an altemative for barstock up to and including 10 inches (25.4 om) in diameter, holding times at temperatute may be selected by the material supplier that are appropriate for his speciic heat treat feciliies, the alloy being heat treated, and the ‘cross section of the part; and are consistent with the required mechanical properties. Holding times, however, must be at least 15 minutes/inch of heaviest cross section for each operation. If this option is selected, material must be qualified utilizing a full cross section prolongation that remains attached to a production part throughout heat treatment. All required mechanical test specimens shall be taken with their longitudinal axes at mid-radius or deeper and with the gage lengths of tensile ‘specimens and the root of the Charpy V-notch for impact specimens at least 1/4T (where T= heaviest cross section) from the end of the prolongation. Note: It should be noted that some vendors will report on their material test reports (MTR’s) something that is referred to as the ‘time at temperature” This is considered! to be the time at which the entire cross-section of a partis at the specified heat treating cycle temperature (i.e, normalizing, austenitizing, solution annealing, tempering, etc), ‘The “time at temperature” doesn't start until the entite cross-section of the part has reached equilibrium (or, is at the same temperature). The actual furnace times may be considerably longer to allow the parts to be heated up to the specified temperature of the heat treat oyole. The time used shall be sufficient to allow for the complete transformation of the matenal depending upon the specific alloy and heat treat cycle selected. It should also be noted that the time at temperature" given on an MTR for certain materials may be less than the heat up and holding times calculated using the requirements above. However, as long as the MTR reports a proper ‘ime at temperature’ statement and the material meets the mechanical property requirements of ‘the material specification, the material is considered to be acceptable, Any questions in regards to this note should be directed to Cameron Metallurgy. Method 8 - Contact Surface Thermocouple This method shall use a thermocouple in surface contact with the product or a heat sink. The equivalent round (ER) of the heat sink shall be determined per Figure 1. The ER of the heat sink shall be greater then or equal to the largest ER of any part in the heat treatment load, The heat sink shall be made of the same class of material when the components are made of an alloy of the following classes: carbon steel, alloy steel, stainless steel, titanium base alloys, nickel-copper alloys, and nickel base alloys. For components which do not meet one of the preceding classes, the heat sink shall be made ‘rom the same allay as the component. Once the thermocouple reaches temperature, the part(s) or heat sink shall be held at temperature for the time required by each cycle stated in the Cameron material specification Method G - Heat Sink Thermocouple This method shall use a thermocouple located such that the temperature sensing tip of the thermocouple is imbedded within the part or heat sink and is no closer than one inch {0 any extemal or intemal surface. The equivalent round (ER) of the heat sink shall be the greater of Original Date: 18 May 88 ay apna rah yest ian i ah tn papperPROPERTY OF Tenor W. Proveast RE FENEOT 5 Apr 13, Ms-003400-01 CE camenon ream By 4. The ER as determined using Figure 1 2 The ER as celermined using the thickest cross.secion ofthe largest 2.35 2.36 Original Date: 16 May 86 Srna ete i, tn entra yo ht on wh snd nyt osha oe part. ‘As an alternative, the largest part in the heat treat load may be used as a heat sink. This option requires that thermocouple location be specified by Cameron Product Engineering, The heat sink shall be made of the same class of material when the components are made of an alloy of the following classes: carbon steel, alloy steel, stainless steel, titanium base alloys, nickel-copper alloys, and nickel base alloys. For components which do not meet one of the preceding classes, the neat sink shall be made from the same alloy as the component. The time at temperature required by the Cameron material specification shall be initiated once the thermocouple comes to temperature Other methods of monitoring temperature during heat treatment may be used provided they are first subrritted to and epproved by Cameron Metallurgy. Double Tempering Operations When @ QTC is processed with a double temper operation, the product shall receive 2 double temper operation and shall be processed in accordance with time and temperature tolerances specified in section 3.3.4 2 for each oycle Optional Retempering Carbon, low alloy, and martensitic stainless steel parts and QTCs that exceed the maximum hardness in the applicable material specification after tempering must be relempered until the correct hardness is obtained. Retempering shall be done in accordance with one of the following paragraphs (as applicable). 2.3.6.1 QTC Too Hard - Single Temper Specified ‘When working to a material specification requiring a single temper and the hardness of the QTC is toa high after tempering, the QTC must be retempered The QTC may be retempered by itself provided that the QTC tempering time at temperature does not exceed that of the parts) thet it qualifies, Alternatively, the QTC and the part(s) it qualifies may both be retempered. Retempering shall consist of one or more additionel temper cycles performed in accordance with the times and temperatures specified for the temper oyole in the material specification. For PSL 2, 3, and 4, the times and temperatures for the retemper cycles for the QTC and part(s) must comply with section 3.3.4 if the QTC and part(s) are retempered separately 2.3.6.2 QTC Too Hard - Double Temper Specified When working to 2 material specification requiring 2 double temper and the hardness of the QTC is too high after tempering, the QTC must be retempered The QTC may be retempered by itself provided that the QTC tempering time at temperature does not exceed that of the part(s) that it qualifies. Alternatively, the QTC and the part(s) it qualifies may both be retempered. Retempering shall consist of double tempering again in accordance with the applicable material specification. For PSL 2, 3, and 4, the times and temperatures for the double retemper cycles for the QTC and part(s) must comply with section 3.34 if the TC and part(s) are retempered separately.5 Apr 13 Ms-003400-01 Son a 2 @ cameron ae Page 7 of 25 2.3.6.3 Part{s) Too Hard - Single Temper Specified When working to a material specification requiring a single temper and the hardness of the part(s) is too high after tempering and the hardness of the QTC 's acceptable, then just the part(s) need be retempered, Retempering shall consist of ane or more additional temper cycles performed in accordance with the times and temperatures specified for the temper cycle in the applicable material specification. For PSL 2, 3, and 4, the times and temperatures for the reternper cycle(s) of the part(s) must comply with section 3.3.4, 2.8.6.4 Part(s) Too Hard - Double Temper Specified ‘When working to a material spectfication requiring @ double temper and the hardness of the part(s) is too high and the hardness of the QTC is acceptable, then just the part(s) need be retempered. Retempering shall consist of double tempering again in accordance with the applicable material specification, For PSL 2, 3, and 4, the times and temperatures for the double retemper oycle(8) of the part(s) must comply with section 3.3.4 Continuous Furnace Heat Treatment For PSL 1-3 applications, continuous fumace heat treatment shall be an acceptable alternative to conventional batch type heat. Continuous furnaces typically contain several cifferent temperature zones through which the bar travels. The zane temperatures in the austenitizing furnace are chosen so as to heat the part to @ completely austenitic state in a relatively short time. The part is then spray quenched before entering the tempering furnace. Zone temperatures in the tempering furnace are chosen to produce the desired tempering effect, again in a relatively short time. The time spent in the austenitizing and tempering furnaces depends primarily upon the length of the fumace and the travel speed. The travel speed varies according to the size of the part. The time in each furnace shall be sufficient to produce the desired mechanical properties and a microstructure equivalent to that obtained by @ conventional batch type quench and temper heat treatment For continuous furnace heat treatment, the following parsmeters shall apply A, The minimum part temperature upon exiting the final zone of the austenitizing fumace shall meet the minimum austenttizing temperature listed in the applicable material specification 8, The minimum time in the austenitizing furnace shall be 10 minutes, C. The minimum part temperature upon exiting the final zone af the tempering furnace shall meet the minimum tempering temperature listed in the applicable maternal specification 1D. The minimum time in the tempering furnace shall be 10 minutes. E. The maximum temperature of the quench water prior to quenching shall be 10°F (38°C). F. The QTC shall be from the same heat treat batch as the material it represents. For continuous furnaces, 2 heat treat batch is defined as a group of bars having the same diameter and from the same heat run through the furnace sequentially at the ‘same zone temperatures, travel speed, and other parameters, A minimum of one QTC shall be provided for each heat of material. In addition, a minimum of one QTC Original Date: 16 May 86 ry aro ngtloa sl eroheouee anne sac inaten,Fagvastoncecs co ntnenon i a us crane eh hed oy tbe rhas vs00e400.01 ae KS RR a 2 @ cameron ae Page 8 of 25 shall be provided for each group of 150 parts from the same heat. Mechanical property tests shall be conducted on the QTC in accordance with section 3.4 of this specification except thet all specifications shell be taken at the 1/4T location. In addition to the hardness testing required on the QTC, each part shall be Individually hardness checked with Brinell hardness measurements taken on the surface at each fend of the bar. The hardness measurements shall meet the requirements of the applicable material specification, 2.4. Weld Repair of Material 2.4.4 PSL 4 Materials: Except for weld overlays, welding is not permitted on any PSL 4 material 2.4.2 Weld repairs of PSL 3 castings are not permitted without written approval from Cameron Product Engineering. Weld repairs of wrought material are prohibited, 2.4.3 PSL 3 materials (when approved) and PSL's 1 and 2 castings may be weld repaired provided. (2) The procedures and welders used are qualified in accordance with ASME Sect. IX (see API 6A). (0) The filer metal chemistry, hardness and stress relieving temperature meet the requirements of NACE MR-O175, () The PQR is supported with hardness measurements of the Weld, Base Metal and Heat Affected Zones (see API 6A) 2.8 NDE Requirements (Weld Repairs) 2.5.1 NDE requirements for forged material (when approved) shall be performed as required by the Cameron Bill of Materials and the requirements of API 6A, 2.8.2 NDE requirements for PSL 3 castings (when approved) and PSL 1 and 2 castings. NDE shall be performed as required by the Cameron Bills of Material and the requirements of API 64, In addition, the following requirements are mandatory and must be complied with, (2) A weld map is required for each casting which details the surface area, configuration and depth of each weld repair. (©) A unique number or symbol is required and shall be assigned to each casting which has been weld repaired. (©) A hardness measurement on the weld deposit of one of the weld repairs is required and shall be made after the final stress relieving operation. Note: The information and test results from the above requirements are to be properly documented and reported on the Materials Test report Original Date: 16 May 86 gt aense aaFROFERTVOF sae W Rae oe Tes 5 Apr 13. MS-003400-01 vier 8 Tehran oe 28 @camMERON =u ee 2.6 Chemical Composition 27 28 29 The chemical composition of the material shall be determined using the latest edition of an appropriate ASTM, ISO, DIN, or French A Standard or other nationally of internationally recognized standard approved by Cameron Metallurgy and shall meet the requirements of the specific material specification. Elements (other than elements used for grain refinementideoxidation) not specified in the MS shall not be intentionally added. Material composition shall be determined on a heat basis (or a remeit ingot basis for remeit grade materais) Any other element not specified and over 0.25% shall be reported. Total amount of residual elements shall not exceed 1.00%, NDE Capabilities Materials must meet the Quality and NDE requirements as specified by the Cameron Bils of Material Visual Examination and Other Tests The supplier shall guarantee the material is homogenous and free of all anomalies or deleterious phases which are detrimental to the mechanical ot machining properties of the material or may adversely impact its corrosion resistance, ‘Scale Removal During the production of any material where excessive surface scale (such as in heavily forged parts) Is produced through oxidizetion or any other process during either the forging or heat treatment operations, it must be removed prior to delivery to Cameron. ‘The scale can be removed through any recognized method (for example air-blast, shot blasting, F grinding), however it must in no way cause the material to deviate from the requirements. outlined in the Bill of material or and other reference document 3.0 QUALIFICATION TESTING: at General ‘The properties exhibited by the Qualification Test Coupon (QTC) shall represent the properties of the thermal response of the material comprising the production parts it qualifies. Depending upon the hardenabilty of @ given material, the QTC results may not always correspond with the properties of the actual components at all locations throughout their cross- section A single QTC may be used to represent the impact and/or tensile properties of the part(s) produced from the same heat provided it satisfies the requirements of this specification. For batch heat treatinent only: When the QTC Is a trepanned core or prolongation removed from @ production part or @ sacrificial production part, the QTC may only qualify production parts having the same or smaller ER. The QTC shall only qualify material and parts produced from the same heat. For material heat treatment in a continuous furnace, the GTC shall consist of @ sacrificial production part or a prolongation removed from a production part. The sacrificial production part fr prolongation QTC shall only qualify production parts having identical size and shape, The QTC shail only qualify material and parts produced from the same heat and heat treat lot Original Date 16 May 86 porns tom CAMERON, ince descent rah yee aPROPERTY OF @ cAMERON Taner W. Provoast TRE FEE 5 Apr 13, Ms.003400.01 KS. Johnson mE 28 5 Apr 13 Page 10 of 25 3.2 Equivalent Round (ER) The size of a QTC for a part shall be determined using the following equivalent round (ER) methods. ER Methods Figure 1 illustrates the basic models for determining the ER, The ER of a part shell be determined using the actual dimensions of the part in the "as heat treated" condition. Figure 2 shows examples of how prolongations are determined con several product configurations to meet the ER requirements, ‘The ER of a studded type part shall be determined by using T equal to the thickness of the thickest flange that can be bolted to that part, ER determination of studded, non-studded or flange parts shall be in accordance with Figure 1 methods for complex shaped parts. ‘When a prolongation is used, it shall remain integrally attached during all heat treatment operations except post weld heat treatment, stress relief, and any re-tempering or re- aging that may be required. For tubular components, bar stock, mill shapes and other raw material with a uniform cross section, the prolongation shall have the same cross section as that raw material, For a production part with @ complex shape or varying cross section, the projongation need not be an extension of the largest cross section of the part However, the extension shall meet or exceed the minimum equivalent round (ER) required for a separate QTC. ‘Maximum ER QTC Size Requirement The ER of the QTC, as determined using Figure 1, shall be equal or greater than maximum ER of the part which it qualifies, except as follows: 3.2.3.1 For PSL 1 and2 3.23.14 Forgings Size not required to exceed 2-1/2 inches (63 mm) ER. 3.2.3.1.2 Castings Size not required to exceed size shown in ASTM A703 (latest revision), 2.2.3.2 For PSL3and4 Size not required to exceed 5 inches (125 mm) ER, 3.3 QTC Processing 3.34 Original Date: 16 May 86 ‘Melting Practices In no case shall the QTC be processed using a melting practice(s) cleaner than that of the material it qualifies (e.g. a QTC made from a remelt grade or vacuum degassed material may not qualify material from the same primary melt which has not experienced the identical metting practice). For PSL 1, 2, and 3, remelt grade material remaved from a single remelt ingot may be used to qualify other remelt gracle material which is from the same primaty melt; no additional alloying shall be performed on these individual remelt5 Apr13 MS-003400-01 @ cameRON fle ae 3.3.2. Hot Working Practices (Wrought Materials Only) Hot working ratios on the QTC shall be equal to or less than those used in processing the part(s) the QTC qualifies. The total hot work ratio for the QTC shall not exceed the total hot work ratio of the part(s) the QTC qualifies, 3.8.3 Casting Practices (Cast Materials Only) ‘The QTC shall be made using the same foundry practices that were used on the part(s) it qualifies, 3.3.4 QTC Heat Treating 3.3.4.1 Equipment Qualification All heat treatment operations shall be performed utilizing equipment qualified in ‘accordance with 2.3.4 3.3.4.2 Methods The QTC shall experience heat treatment per Section 2.3 and the Cameron material specification, The QTC shall be heat treated in @ production furnace that is routinely used to produce production parts having an equivalent round equal or n 5.0 FORGING VENDOR PROCEDURES: Forging vendors shall have written procedures controlling the following areas. These procedures must be made avaliable to Cameron for review during an onsite audit 5.1 _Billet/ingot Supplier Qualification BAA Original Date: 16 May 86 The forging vendor shall have a procedure in place for qualiying billevingot supplies that is based upon both a quality assurance and a technical evaluation An acceptable quality program, such as an ISO accreditation is not sufficient by itself to satisfy this requirement. ‘There must be documented evidence that @ billeVingot supplier has the technical know-how and the Necessary procedures and equipment in place to consistently produce acceptable product. Technical epproval of a bilel/ingot supplier may be done Using one or more ofthe flowing methods An onsite technical audit Receipt inspection that includes NDE, chemistry check, macroetch, etc. on a ‘sample basis. A fist article cut up evaluation ‘Successful experience over a period of time. Documentation must include teste/inspections that were performed on either the starting material or finished forgings.5 Apr13 MS-003400-01 @ cameRON fle ae 6.1.2 The forging vendor is responsible for insuring that a billetvingot supplier has an acceptable quality program, and has procedures addressing the following ‘Chemistry control (including chemistry balance or aim) Metting practice Pouring practice and type of ingot mold Hot work practice (method of forging, amount of reduction, forging temperature, etc.) Cooling rate and method after forging Cropping the billet Inspection and acceptance criteria (cleanliness requirements, limitations on porosity or inclusions, grain size, secondary phases, microstructure, macrostructure, etc. 28 applicable) Hydrogen control. in carbon, low alloy, and martensitic stainless steels (410, FENM, etc.) hydrogen must be controlled to 2ppm maximum 5.2. Receiving inspection and material clearance of billevingot 5.3. Chemistry verification 8.4 Hot work requirements (how is the minimum reduction of area during forging determined in order to produce a fully wrought structure for a given forging) 5.8 Forging sequence, temperature 8.6 Cooling after forging 5.7 Heat treating (if applicable) 5.8 Hardness testing 5.9. Nondestructive testing (if applicable) 5.10 Mechanical testing 6.11 Macrostructure and microstructure control (as applicable) 5.12 Quality control including inspection and acceptance criteria 6.0 CERTIFICATION REQUIREMENTS: The actual certification requirements are dependent on the API 6A product Specification Level (PSL). Whenever “if applicable” appears below, verify that the operatioritest is required by the material specification - fits, then certification is required, Note: For duplex and super duplex stainless steel materials, the results for the ASTM G48, corrosion testing, ferrite content determination, and metallographic examination shall also be reported in the certification requirements for all PSL levels, Original Date: 18 May 8 cumay tla let dart cee scan, Fabbri nernation er ry purpose cer an a fo wi i iireded may et ba made athe writenPROPERTY OF ‘cRAwner: W. Provoast ae Peer as ws.ov2ea00n Sn = 28 @ CAMERON ae Page 10025 6.1 PSL 1 and 2 Certification * Certification of Compliance - Certification shall include certification to the requirements of the material specification and the heat treat requirements. The MS and revision shall be included on certifications. * P.O. Number © Material Description - Certification shall inclucie description of the material (configuration, size) and quantity. + Material Heat number ‘+ Material Chemistry - Certfications shail include actual chemistry per heat or re-mett ingot + QTC Description - Certifications shall include the configuration and size of the QTC * QTC Hardness - Certifications shall include the actual hardness of the QTC after final heat- treating and prior to cutting the tensile and impact specimens * QTC Tensile Test Results (If applicable) - Certfications shall include uttimate tensile, yield, elongation and reduction in area. It is required that the tensile specimen size be included only if the specimens were other than standard 0.500" Dia, with 2" gage length. * QTC Impact Test Results (if applicable) - When impact testing is required, certification shall include impact test results for each specimen and include the orientation (if ather than longitudinal) and test temperature. It is required that the impact specimen size be included only if the specimens were other than standard 10mm X 10mm, + NDE Records (PSL 1) - NDE personnel qualification records + NDE Records (PSL 2) ~ NDE personnel qualification records, = Surface NDE records + Weld volumetric NDE records (If applicable) = Repair weld NDE records (If applicable) ‘+ Hardness Test Record of Parts (if applicable) Original Date: 18 May 88PROPERTY OF @ cAMERON Taner W. Provoast TRE FEE 5 Apr 13, Ms.003400.01 KS. Johnson mE 28 5 Apr 13 Page 19 of 25 6.2 PSL Certification Certification of Compliance - Certification shall include certifcation to the requirements of the material specification and the heat treat requirements. The MS and revision shall be included on certifications. Material Description - Certifications shall include description of the material including configuration, size and quantity. Material Heat Number Material Chemistry - Certification shall include actual chemistry per heat or remett ingot, ‘Actual Hot Work Ratio Material Heat Treatment - Certifications shall include actual temperatures and times at temperature for each heat treat cycle, quench media type and temperature monitoring method, Heat Treat Lot Identification - Certification to include heat-treat load identification. If serialization marking of material is employed instead of heat treat load, certifications shall indicate the serial numbers included in each heat treat load QTC Description - Certitications shall include the configuration and size of the QTC. QTC Heat treatment - Certifications shall include actual temperatures and times at temperature for the QTC heat treat cycle, quench mecia type, and temperature-monitoring method, QTC Hardness - Certifications shall include the actual hardness of the QTC efter final heat treating and prior to cutting the tensile and impact specimens. QTC Tensile Test Results - Certifications shell include ultimate tensile, yield, elongation and reduction in area. It is required that the tensile specimen size be included only of the specimens were other than standard 0.600" dia. with 2" gage length, QTC Impact Results - Certifications shall include impact test results for each specimen and include the orientation (if other than longitudinal) and test resulls. It is required that the impact specimen size be included only if the specimens were other than standard 10mm X 10mm. Original Date: 16 May 865 Apr 13 Ms-003400-01 Sn = 28 @ CAMERON ae Page 2025 6.2 PSL 3 Certification (cont) ‘+ NDE Records ~ NDE personne! qualification records. = Surface NDE records = Weld volumetric NDE records (If applicable) - Repair weld NDE records (If applicable) + Volumetric NDE records (except valve-bore sealing mechanisms) ‘+ Hardness Test Record of Parts (if applicable) 6.3 PSL 4 Certification © Certification of Compliance - Certifications shall include certification to the requirements of the material specification and the heat treat requirements, The MS and revision shall be included on the certifications. * P.O. Number * Part Number and Revision * Material Description - Certification shall include description of the material including configuration, size and quantity. + Material Heat Number + Material Melting Practice + Material Chemistry - Certifications shall include actual chemistry per heat or re-melt ingot + Actual Hot Work Ratio + Material Heat Treatment - Certifications shall include actual temperatures and limes at temperature for each heat treat cycle, quench media type and temperature monitoring method, + Heat Treat Charts - Actual heat treat charts shall be provided which are identified with heat treat load and cycle, * Heat Treatment Lot Identification - Certifications to inclucle heat-treat load identification, If serialization marking of material is employed instead of heat treat load, certifications shall indicate the serial numbers included in each heat treat load © QTC Description - Certifications shall include the configuration and size of the QTC, * QTC Heat Treatment - Certifications shall include actual temperatures and times at temperature for the QTC heat treat cycle, quench media type, temperature-monitoring method, © QTC Hardness - Certification shall include the actual hardness of the QTC after final heal- treating and prior to cutting the tensile and impact specimens. Original Date: 16 May 86