SATL Results From Crystal City Water Testing

February 25, 2016
Pilar Arias
KSAT-12
1408 N. St.Mary's
San Antonio, TX 78215
SATL Report No.:
1602357
RE: Crystal City Water
Dear Pilar Arias

SATL received 1 Sample(s) on 02/23/2016 for analyses identified on the chain of custody.
performed using methods indicated on the laboratory report.
The analyses were
Any deviations observed at sample receiving are
notated on the Sample Receipt Checklist and/or Chain of Custody documents attached as part of this analytical
report.
There were no problems in the sample analyses unless otherwise noted.
Sample data and associated QC are
presented in the attached laboratory report. QC sample data were within laboratory acceptance limits except where
noted on the report.
Sincerely,
For San Antonio Testing Laboratory, Inc.
Richard Hawk,
General Manager
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be
reproduced in its entirety.
1610 S. Laredo Street, San Antonio, Texas 78207-7029
(210) 229-9920
Fax (210) 229-9921
www.satestinglab.com
Page 1 of 25
LABORATORY REPORT
NELAC Cert. No.:
Project: Crystal City Water
KSAT-12
1408 N. St.Mary's
San Antonio TX, 78215
T104704360-16-12
Reported:
02/25/16 09:48
Received:
Project Number: [none]

Project Manager: Pilar Arias
02/23/16 14:02
Additional Notes:
Report No. 1602357
SAMPLE SUMMARY
Total Samples received in this work order:
The following samples were requested for analysis as per the CoC. Any re-runs or re-analyses requested are identified as such.
Sample ID
Laboratory ID
Matrix
Sampling Method
Date Sampled
Date Received
Crystal City Water
1602357-01
Liquid
Grab
02/17/16 22:00
02/23/16 14:02
Notes
All quality control samples and checks are within acceptance limits unless otherwise indicated.
Test results pertain only to those items tested.
All samples were in good condition when received by the laboratory unless otherwise noted.

(210) 229-9920
Fax (210) 229-9921

Page22of
of 22
Page
25
LABORATORY REPORT
NELAC Cert. No.:
KSAT-12
1408 N. St.Mary's
T104704360-16-12
Reported:
02/25/16 09:48
Received:

02/23/16 14:02
Additional Notes:
Report No. 1602357
Sample ID #: Crystal City Water
Sampling Method: Grab
Sample Matrix: Liquid

Analyte
Lab Sample ID #: 1602357-01
Date/Time Collected: 02/17/16 22:00

Result
Units
PQL
Prep Method
Batch
Analyzed
Method
Analyst
Notes
Total Metals By ICP-OES

Aluminum *
Antimony *
Arsenic *
Barium *
Beryllium *
Boron *
Cadmium *
Calcium *
Chromium *
Cobalt *
Copper *
Iron *
Lead *
Magnesium *
Manganese *
Molybdenum *
Nickel *
Potassium
Selenium *
Silver *
Sodium *
Strontium *
Thallium *
Tin *
Titanium *
Vanadium *
Zinc *
Mercury *
0.940
<0.010
<0.010
0.541
0.008
0.562
<0.005
57.5
<0.010
0.012
0.815
171
0.098
12.8
6.98
0.010
<0.010
3.95
<0.010
<0.010
68.1
0.620
<0.010
0.049
0.030
<0.010
0.842
<0.0002
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
0.050
0.010
0.010
0.010
0.004
0.010
0.005
1.00
0.010
0.010
0.010
0.050
0.010
0.050
0.010
0.010
0.010
1.00
0.010
0.010
1.00
0.010
0.010
0.010
0.010
0.010
0.010
0.0002

EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 245.1
B609085
B609085
B609085
B609085
B609085
B609085
B609085
B609085
B609085
B609085
B609085
B609085
B609085
B609085
B609085
B609085
B609085
B609085
B609085
B609085
B609085
B609085
B609085
B609085
B609085
B609085
B609085
B609081
(210) 229-9920
02/24/16 14:05
02/24/16 14:05
02/24/16 14:05
02/24/16 14:05
02/24/16 14:05
02/24/16 14:05
02/24/16 14:05
02/24/16 14:05
02/24/16 14:05
02/24/16 14:05
02/24/16 14:05
02/24/16 14:05
02/24/16 14:05
02/24/16 14:05
02/24/16 14:05
02/24/16 14:05
02/24/16 14:05
02/24/16 14:05
02/24/16 14:05
02/24/16 14:05
02/24/16 14:05
02/24/16 14:05
02/24/16 14:05
02/24/16 14:05
02/24/16 14:05
02/24/16 14:05
02/24/16 14:05
02/24/16 14:12
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 200.7
EPA 245.1
XE
XE
XE
XE
XE
XE
XE
XE
XE
XE
XE
XE
XE
XE
XE
XE
XE
XE
XE
XE
XE
XE
XE
XE
XE
XE
XE
FH
Fax (210) 229-9921

Page33of
of 22
Page
25
LABORATORY REPORT
NELAC Cert. No.:
KSAT-12
1408 N. St.Mary's
T104704360-16-12
Reported:
02/25/16 09:48
Received:

02/23/16 14:02
Additional Notes:
Report No. 1602357

Analyte

Result
Units
PQL
Prep Method
Batch
Analyzed
Method
Analyst
Notes
Volatile Organic Compounds by GC/MS

Acetone *
Allyl Chloride (3-Chloropropylene) *
Benzene *
Bromobenzene *
Bromochloromethane *
Tetrachloroethene *
Bromodichloromethane *
Bromoform *
Bromomethane *
Trichloroethene *
Butylbenzene *
sec-Butylbenzene *
tert-Butylbenzene *
Carbon disulfide *
Carbon Tetrachloride *
Chlorobenzene *
Chloroethane *
2-Chloroethyl Vinyl Ether *
Chloroform *
Chloromethane *
2-Chlorotoluene *
4-Chlorotoluene *
Dibromochloromethane *
1,2-Dibromo-3-chloropropane *
1,2-Dibromoethane *
Dibromomethane *
1,2-Dichlorobenzene *
trans-1,4-Dichloro-2-butene *
cis-1,4-Dichloro-2-butene
Dichlorodifluoromethane *
1,1-Dichloroethane *
1,2-Dichloroethane *
1,1-Dichloroethene *
cis-1,2-Dichloroethylene *
trans-1,2-Dichloroethylene *
1,2-Dichloropropane *
<0.010
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
0.010
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005

5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
(210) 229-9920
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
Fax (210) 229-9921

Page44of
of 22
Page
25
LABORATORY REPORT
NELAC Cert. No.:
KSAT-12
1408 N. St.Mary's
T104704360-16-12
Reported:
02/25/16 09:48
Received:

02/23/16 14:02
Additional Notes:
Report No. 1602357

Analyte

Result
Units
PQL
Prep Method
Batch
Analyzed
Method
Analyst
Notes
Volatile Organic Compounds by GC/MS

1,1-Dichloropropylene *
cis-1,3-Dichloropropylene *
trans-1,3-Dichloropropylene *
Ethylbenzene *
Ethyl Methacrylate *
Hexachlorobutadiene *
Isopropylbenzene (Cumene) *
Isopropyl alcohol
4-Isopropyltoluene *
Methacrylonitrile *
Methyl Butyl Ketone (2-Hexanone) *
Methyl Ethyl Ketone (2-Butanone) *
Acetonitrile *
Methyl Iodide *
Methyl Methacrylate *
Methyl-tert-Butyl Ether *
Methylene Chloride *
Naphthalene *
Propylbenzene *
Styrene *
1,1,1,2-Tetrachloroethane *
1,1,2,2-Tetrachloroethane *
Toluene *
1,2,3-Trichlorobenzene *
1,2,4-Trichlorobenzene *
1,1,1-Trichloroethane *
1,1,2-Trichloroethane *
Trichlorofluoromethane *
1,2,3-Trichloropropane *
1,2,4-Trimethylbenzene *
1,3,5-Trimethylbenzene *
Vinyl acetate *
Vinyl chloride *
m,p-Xylenes *
o-Xylene *
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
0.005
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
5030B
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
B609087
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
02/24/16 12:31
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
EPA 8260C
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
REB
Surrogate: Toluene-d8
102 %
87.4-109
5030B
B609087
02/24/16 12:31
EPA 8260C
REB
Surrogate: 4-Bromofluorobenzene
100 %
65.7-120
5030B
B609087
02/24/16 12:31
EPA 8260C
REB
Surrogate: Dibromofluoromethane
106 %
81.2-126
5030B
B609087
02/24/16 12:31
EPA 8260C
REB

(210) 229-9920
Fax (210) 229-9921

Page55of
of 22
Page
25
LABORATORY REPORT
NELAC Cert. No.:
KSAT-12
1408 N. St.Mary's
T104704360-16-12
Reported:
02/25/16 09:48
Received:

02/23/16 14:02
Additional Notes:
Report No. 1602357
Total Metals By ICP-OES - Quality Control

Analyte
Result
Reporting
Limit
Units
Spike
Level
Source
Result
%REC
%REC
Limits
RPD
RPD
Limit
Batch B609081 - EPA 245.1

Prepared: 02/24/16 09:10 Analyzed: 02/24/16 14:12
Blank (B609081-BLK1)
Mercury
<0.0002
0.0002
mg/L
LCS (B609081-BS1)
Mercury
0.00961
0.0002
mg/L
LCS Dup (B609081-BSD1)

Mercury
0.0103
Duplicate (B609081-DUP1)
Mercury
0.0002
mg/L
96
85-115
Matrix Spike (B609081-MS1)
0.0002
mg/L
0.0002
103
85-115
25
<0.0002
25
Source: 1602335-01
0.00985
0.0100
Source: 1602335-01
<0.0002
Mercury
0.0100
mg/L
0.0100
<0.0002
99
75-125
Batch B609085 - EPA 200.7

Aluminum
<0.050
0.050
mg/L
Antimony
<0.010
0.010
mg/L
Arsenic
<0.010
0.010
mg/L
Barium
<0.010
0.010
mg/L
Beryllium
<0.004
0.004
mg/L
Boron
<0.010
0.010
mg/L
Cadmium
<0.005
0.005
mg/L
Calcium
<1.00
1.00
mg/L
Chromium
<0.010
0.010
mg/L
Cobalt
<0.010
0.010
mg/L
Copper
<0.010
0.010
mg/L
Iron
<0.050
0.050
mg/L
Lead
<0.010
0.010
mg/L
Magnesium
<0.050
0.050
mg/L
Manganese
<0.010
0.010
mg/L
Molybdenum
<0.010
0.010
mg/L
Nickel
<0.010
0.010
mg/L
Potassium
<1.00
1.00
mg/L
Selenium
<0.010
0.010
mg/L
Silver
<0.010
0.010
mg/L
Sodium
<1.00
1.00
mg/L
Strontium
<0.010
0.010
mg/L

(210) 229-9920
Fax (210) 229-9921

Page66of
of 22
Page
25
LABORATORY REPORT
NELAC Cert. No.:
KSAT-12
1408 N. St.Mary's
T104704360-16-12
Reported:
02/25/16 09:48
Received:

02/23/16 14:02
Additional Notes:
Report No. 1602357

Analyte
Result
Reporting
Limit
Units
Spike
Level
Source
Result
%REC
%REC
Limits
RPD
RPD
Limit
Batch B609085 - EPA 200.7

Thallium
<0.010
0.010
mg/L
Tin
<0.010
0.010
mg/L
Titanium
<0.010
0.010
mg/L
Vanadium
<0.010
0.010
mg/L
Zinc
<0.010
0.010
mg/L
LCS (B609085-BS1)
Aluminum
1.99
0.050
mg/L
2.00
99
85-115
Antimony
1.98
0.010
mg/L
2.00
99
85-115
Arsenic
1.99
0.010
mg/L
2.00
99
85-115
Barium
2.02
0.010
mg/L
2.00
101
85-115
Beryllium
1.98
0.004
mg/L
2.00
99
85-115
Boron
1.99
0.010
mg/L
2.00
100
85-115
Cadmium
1.98
0.005
mg/L
2.00
99
85-115
Calcium
1.99
1.00
mg/L
2.00
100
85-115
Chromium
1.98
0.010
mg/L
2.00
99
85-115
Cobalt
1.98
0.010
mg/L
2.00
99
85-115
Copper
1.98
0.010
mg/L
2.00
99
85-115
Iron
1.98
0.050
mg/L
2.00
99
85-115
Lead
1.98
0.010
mg/L
2.00
99
85-115
Magnesium
1.98
0.050
mg/L
2.00
99
85-115
Manganese
1.99
0.010
mg/L
2.00
100
85-115
Molybdenum
1.99
0.010
mg/L
2.00
100
85-115
Nickel
1.99
0.010
mg/L
2.00
100
85-115
Potassium
19.8
1.00
mg/L
20.0
99
85-115
Selenium
2.00
0.010
mg/L
2.00
100
85-115
Silver
1.11
0.010
mg/L
1.00
111
85-115
Sodium
2.03
1.00
mg/L
2.00
101
85-115
Strontium
1.98
0.010
mg/L
2.00
99
85-115
Thallium
2.00
0.010
mg/L
2.00
100
85-115
Tin
1.98
0.010
mg/L
2.00
99
85-115
Titanium
1.99
0.010
mg/L
2.00
100
85-115
Vanadium
1.98
0.010
mg/L
2.00
99
85-115
Zinc
1.98
0.010
mg/L
2.00
99
85-115

Aluminum
1.99
0.050
mg/L
2.00
99
85-115
0.05
20
Antimony
1.99
0.010
mg/L
2.00
100
85-115
0.4
20

(210) 229-9920
Fax (210) 229-9921

Page77of
of 22
Page
25
LABORATORY REPORT
NELAC Cert. No.:
KSAT-12
1408 N. St.Mary's
T104704360-16-12
Reported:
02/25/16 09:48
Received:

02/23/16 14:02
Additional Notes:
Report No. 1602357

Analyte
Result
Reporting
Limit
Units
Spike
Level
Source
Result
%REC
%REC
Limits
RPD
RPD
Limit
Batch B609085 - EPA 200.7


Arsenic
1.99
0.010
mg/L
2.00
100
85-115
0.3
20
Barium
2.03
0.010
mg/L
2.00
101
85-115
0.7
20
Beryllium
1.98
0.004
mg/L
2.00
99
85-115
0.3
20
Boron
2.00
0.010
mg/L
2.00
100
85-115
0.2
20
Cadmium
1.98
0.005
mg/L
2.00
99
85-115
0.1
20
Calcium
1.99
1.00
mg/L
2.00
100
85-115
0.05
20
Chromium
1.99
0.010
mg/L
2.00
100
85-115
0.4
20
Cobalt
1.99
0.010
mg/L
2.00
99
85-115
0.2
20
Copper
1.98
0.010
mg/L
2.00
99
85-115
0.1
20
Iron
1.99
0.050
mg/L
2.00
99
85-115
0.4
20
Lead
1.98
0.010
mg/L
2.00
99
85-115
20
Magnesium
1.98
0.050
mg/L
2.00
99
85-115
0.1
20
Manganese
1.99
0.010
mg/L
2.00
100
85-115
0.1
20
Molybdenum
2.00
0.010
mg/L
2.00
100
85-115
0.3
20
Nickel
1.99
0.010
mg/L
2.00
100
85-115
20
Potassium
19.8
1.00
mg/L
20.0
99
85-115
0.4
20
Selenium
2.00
0.010
mg/L
2.00
100
85-115
0.05
20
Silver
1.10
0.010
mg/L
1.00
110
85-115
0.5
20
Sodium
1.99
1.00
mg/L
2.00
100
85-115
20
Strontium
1.98
0.010
mg/L
2.00
99
85-115
0.2
20
Thallium
2.00
0.010
mg/L
2.00
100
85-115
0.05
20
Tin
1.98
0.010
mg/L
2.00
99
85-115
0.2
20
Titanium
2.00
0.010
mg/L
2.00
100
85-115
0.5
20
Vanadium
1.98
0.010
mg/L
2.00
99
85-115
0.2
20
Zinc
1.98
0.010
mg/L
2.00
99
85-115
0.2
20
Source: 1602335-01
Aluminum
0.195
0.050
mg/L
0.179
20
Antimony
0.0231
0.010
mg/L
0.0256
10
20
Arsenic
0.0150
0.010
mg/L
0.0149
0.7
20
Barium
0.0399
0.010
mg/L
0.0378
20
Beryllium
<0.004
0.004
mg/L
<0.004
Boron
3.58
0.010
mg/L
3.53
Cadmium
<0.005
0.005
mg/L
<0.005
Calcium
26.9
1.00
mg/L
26.6
20
Chromium
0.00430
0.010
mg/L
0.00390
10
20
Cobalt
<0.010
0.010
mg/L
<0.010
Copper
0.0728
0.010
mg/L
0.0714

(210) 229-9920
20
2
20
20
20
2
20
Fax (210) 229-9921

Page88of
of 22
Page
25
LABORATORY REPORT
NELAC Cert. No.:
KSAT-12
1408 N. St.Mary's
T104704360-16-12
Reported:
02/25/16 09:48
Received:

02/23/16 14:02
Additional Notes:
Report No. 1602357

Analyte
Result
Reporting
Limit
Units
Spike
Level
Source
Result
%REC
%REC
Limits
RPD
RPD
Limit
Batch B609085 - EPA 200.7

Source: 1602335-01
Iron
0.218
0.050
mg/L
0.204
20
Lead
0.00250
0.010
mg/L
0.00250
20
Magnesium
3.76
0.050
mg/L
3.71
20
Manganese
0.0321
0.010
mg/L
0.0315
20
Molybdenum
2.08
0.010
mg/L
2.06
20
Nickel
0.00630
0.010
mg/L
0.00600
20
Potassium
9.52
1.00
mg/L
9.43
20
Selenium
<0.010
0.010
mg/L
<0.010
Silver
0.00600
0.010
mg/L
0.00590
20
Sodium
16.6
1.00
mg/L
16.4
20
Strontium
0.108
0.010
mg/L
0.106
20
Thallium
<0.010
0.010
mg/L
<0.010
20
Tin
<0.010
0.010
mg/L
<0.010
20
20
Titanium
0.0105
0.010
mg/L
0.00940
11
20
Vanadium
0.00420
0.010
mg/L
0.00390
20
Zinc
0.531
0.010
mg/L
0.526
0.9
20
Source: 1602335-01
Aluminum
2.35
0.050
mg/L
2.00
0.179
108
75-125
Antimony
2.21
0.010
mg/L
2.00
0.0256
109
75-125
Arsenic
2.20
0.010
mg/L
2.00
0.0149
109
75-125
Barium
2.25
0.010
mg/L
2.00
0.0378
111
75-125
Beryllium
2.13
0.004
mg/L
2.00
<0.004
107
75-125
Boron
5.55
0.010
mg/L
2.00
3.53
101
75-125
Cadmium
2.16
0.005
mg/L
2.00
<0.005
108
75-125
Calcium
27.6
1.00
mg/L
2.00
26.6
49
75-125
Chromium
2.13
0.010
mg/L
2.00
0.00390
106
75-125
Cobalt
2.14
0.010
mg/L
2.00
<0.010
107
75-125
Copper
2.17
0.010
mg/L
2.00
0.0714
105
75-125
Iron
2.33
0.050
mg/L
2.00
0.204
106
75-125
Lead
2.15
0.010
mg/L
2.00
0.00250
107
75-125
Magnesium
5.61
0.050
mg/L
2.00
3.71
95
75-125
Manganese
2.14
0.010
mg/L
2.00
0.0315
105
75-125
Molybdenum
4.17
0.010
mg/L
2.00
2.06
106
75-125
Nickel
2.18
0.010
mg/L
2.00
0.00600
109
75-125
Potassium
30.7
1.00
mg/L
20.0
9.43
106
75-125
Selenium
2.24
0.010
mg/L
2.00
<0.010
112
75-125

(210) 229-9920
Fax (210) 229-9921

Page99of
of 22
Page
25
LABORATORY REPORT
NELAC Cert. No.:
KSAT-12
1408 N. St.Mary's
T104704360-16-12
Reported:
02/25/16 09:48
Received:

02/23/16 14:02
Additional Notes:
Report No. 1602357

Analyte
Result
Reporting
Limit
Units
Spike
Level
Source
Result
%REC
%REC
Limits
RPD
RPD
Limit
Batch B609085 - EPA 200.7

Source: 1602335-01
Silver
1.21
0.010
mg/L
1.00
0.00590
120
75-125
Sodium
17.9
1.00
mg/L
2.00
16.4
77
75-125
Strontium
2.19
0.010
mg/L
2.00
0.106
104
75-125
Thallium
2.22
0.010
mg/L
2.00
<0.010
111
75-125
Tin
2.14
0.010
mg/L
2.00
<0.010
107
75-125
Titanium
2.15
0.010
mg/L
2.00
0.00940
107
75-125
Vanadium
2.10
0.010
mg/L
2.00
0.00390
105
75-125
Zinc
2.67
0.010
mg/L
2.00
0.526
107
75-125
Units
Spike
Level
%REC
%REC
Limits
Volatile Organic Compounds by GC/MS - Quality Control

Analyte
Result
Reporting
Limit
Source
Result
RPD
RPD
Limit
Batch B609087 - 5030B

Acetone
<0.010
0.010
mg/L
Allyl Chloride (3-Chloropropylene)
<0.005
0.005
mg/L
Benzene
<0.005
0.005
mg/L
Bromobenzene
<0.005
0.005
mg/L
Bromochloromethane
<0.005
0.005
mg/L
Tetrachloroethene
<0.005
0.005
mg/L
Bromodichloromethane
<0.005
0.005
mg/L
Bromoform
<0.005
0.005
mg/L
Bromomethane
<0.005
0.005
mg/L
Trichloroethene
<0.005
0.005
mg/L
Butylbenzene
<0.005
0.005
mg/L
sec-Butylbenzene
<0.005
0.005
mg/L
tert-Butylbenzene
<0.005
0.005
mg/L
Carbon disulfide
<0.005
0.005
mg/L
Carbon Tetrachloride
<0.005
0.005
mg/L
Chlorobenzene
<0.005
0.005
mg/L
Chloroethane
<0.005
0.005
mg/L
2-Chloroethyl Vinyl Ether
<0.005
0.005
mg/L
Chloroform
<0.005
0.005
mg/L
Chloromethane
<0.005
0.005
mg/L

(210) 229-9920
Fax (210) 229-9921

Page
of 25
22
Page
1010of
LABORATORY REPORT
NELAC Cert. No.:
KSAT-12
1408 N. St.Mary's
T104704360-16-12
Reported:
02/25/16 09:48
Received:

02/23/16 14:02
Additional Notes:
Report No. 1602357

Analyte
Result
Reporting
Limit
Units
Spike
Level
Source
Result
%REC
%REC
Limits
RPD
RPD
Limit
Batch B609087 - 5030B

2-Chlorotoluene
<0.005
0.005
mg/L
4-Chlorotoluene
<0.005
0.005
mg/L
Dibromochloromethane
<0.005
0.005
mg/L
1,2-Dibromo-3-chloropropane
<0.005
0.005
mg/L
1,2-Dibromoethane
<0.005
0.005
mg/L
Dibromomethane
<0.005
0.005
mg/L
1,2-Dichlorobenzene
<0.005
0.005
mg/L
1,3-Dichlorobenzene
<0.005
0.005
mg/L
1,4-Dichlorobenzene
<0.005
0.005
mg/L
trans-1,4-Dichloro-2-butene
<0.005
0.005
mg/L
<0.005
0.005
mg/L
Dichlorodifluoromethane
<0.005
0.005
mg/L
1,1-Dichloroethane
<0.005
0.005
mg/L
1,2-Dichloroethane
<0.005
0.005
mg/L
1,1-Dichloroethene
<0.005
0.005
mg/L
cis-1,2-Dichloroethylene
<0.005
0.005
mg/L
trans-1,2-Dichloroethylene
<0.005
0.005
mg/L
1,2-Dichloropropane
<0.005
0.005
mg/L
1,3-Dichloropropane
<0.005
0.005
mg/L
2,2-Dichloropropane
<0.005
0.005
mg/L
1,1-Dichloropropylene
<0.005
0.005
mg/L
cis-1,3-Dichloropropylene
<0.005
0.005
mg/L
trans-1,3-Dichloropropylene
<0.005
0.005
mg/L
Ethylbenzene
<0.005
0.005
mg/L
Ethyl Methacrylate
<0.005
0.005
mg/L
Hexachlorobutadiene
<0.005
0.005
mg/L
Isopropylbenzene (Cumene)
<0.005
0.005
mg/L
Isopropyl alcohol
<0.005
0.005
mg/L
4-Isopropyltoluene
<0.005
0.005
mg/L
Methacrylonitrile
<0.005
0.005
mg/L
Methyl Butyl Ketone (2-Hexanone)
<0.005
0.005
mg/L
Acetonitrile
<0.005
0.005
mg/L
Methyl Ethyl Ketone (2-Butanone)
<0.005
0.005
mg/L
Methyl Iodide
<0.005
0.005
mg/L
Methyl Methacrylate
<0.005
0.005
mg/L
Methyl-tert-Butyl Ether
<0.005
0.005
mg/L
Methylene Chloride
<0.005
0.005
mg/L

(210) 229-9920
Fax (210) 229-9921

Page
of 25
22
Page
1111of
LABORATORY REPORT
NELAC Cert. No.:
KSAT-12
1408 N. St.Mary's
T104704360-16-12
Reported:
02/25/16 09:48
Received:

02/23/16 14:02
Additional Notes:
Report No. 1602357

Analyte
Result
Reporting
Limit
Units
Spike
Level
Source
Result
%REC
%REC
Limits
RPD
RPD
Limit
Batch B609087 - 5030B

Naphthalene
<0.005
0.005
mg/L
Propylbenzene
<0.005
0.005
mg/L
Styrene
<0.005
0.005
mg/L
1,1,1,2-Tetrachloroethane
<0.005
0.005
mg/L
<0.005
0.005
mg/L
Toluene
<0.005
0.005
mg/L
1,2,3-Trichlorobenzene
<0.005
0.005
mg/L
<0.005
0.005
mg/L
1,1,1-Trichloroethane
<0.005
0.005
mg/L
<0.005
0.005
mg/L
Trichlorofluoromethane
<0.005
0.005
mg/L
1,2,3-Trichloropropane
<0.005
0.005
mg/L
1,2,4-Trimethylbenzene
<0.005
0.005
mg/L
<0.005
0.005
mg/L
Vinyl acetate
<0.005
0.005
mg/L
Vinyl chloride
<0.005
0.005
mg/L
m,p-Xylenes
<0.005
0.005
mg/L
o-Xylene
<0.005
0.005
mg/L
0.0510
mg/L
0.0500
102
87.4-109
0.0511
mg/L
0.0500
102
65.7-120
0.0540
mg/L
0.0500
108
81.2-126
LCS (B609087-BS1)
Acetone
0.0514
0.010
mg/L
0.0500
103
46.3-139
0.0538
0.005
mg/L
0.0500
108
33.1-164
Benzene
0.0521
0.005
mg/L
0.0500
104
72.2-133
Bromobenzene
0.0482
0.005
mg/L
0.0500
96
58.6-143
Bromochloromethane
0.0512
0.005
mg/L
0.0500
102
74.2-123
Tetrachloroethene
0.0560
0.005
mg/L
0.0500
112
64.6-154
0.0517
0.005
mg/L
0.0500
103
73.2-124
Bromoform
0.0483
0.005
mg/L
0.0500
97
56.3-126
Bromomethane
0.0536
0.005
mg/L
0.0500
107
13.2-193
Trichloroethene
0.0507
0.005
mg/L
0.0500
101
71.1-136
Butylbenzene
0.0501
0.005
mg/L
0.0500
100
42.8-155
sec-Butylbenzene
0.0505
0.005
mg/L
0.0500
101
56.8-143
tert-Butylbenzene
0.0491
0.005
mg/L
0.0500
98
61.6-138
Carbon disulfide
0.0515
0.005
mg/L
0.0500
103
53.9-166

(210) 229-9920
Fax (210) 229-9921

Page
of 25
22
Page
1212of
LABORATORY REPORT
NELAC Cert. No.:
KSAT-12
1408 N. St.Mary's
T104704360-16-12
Reported:
02/25/16 09:48
Received:

02/23/16 14:02
Additional Notes:
Report No. 1602357

Analyte
Result
Reporting
Limit
Units
Spike
Level
Source
Result
%REC
%REC
Limits
RPD
RPD
Limit
Batch B609087 - 5030B

LCS (B609087-BS1)
0.0512
0.005
mg/L
0.0500
102
63.7-121
Chlorobenzene
0.0500
0.005
mg/L
0.0500
100
70.7-138
Chloroethane
0.0536
0.005
mg/L
0.0500
107
30.6-174
0.0285
0.005
mg/L
0.0500
57
25.2-136
Chloroform
0.0525
0.005
mg/L
0.0500
105
73.2-125
Chloromethane
0.0516
0.005
mg/L
0.0500
103
51.7-193
2-Chlorotoluene
0.0493
0.005
mg/L
0.0500
99
60.9-136
4-Chlorotoluene
0.0494
0.005
mg/L
0.0500
99
60.9-136
0.0494
0.005
mg/L
0.0500
99
65.2-126
0.0462
0.005
mg/L
0.0500
92
58.8-118
1,2-Dibromoethane
0.0494
0.005
mg/L
0.0500
99
71.6-124
Dibromomethane
0.0513
0.005
mg/L
0.0500
103
76.7-124
1,2-Dichlorobenzene
0.0482
0.005
mg/L
0.0500
96
56.8-137
1,3-Dichlorobenzene
0.0490
0.005
mg/L
0.0500
98
49.9-145
1,4-Dichlorobenzene
0.0485
0.005
mg/L
0.0500
97
51.7-138
0.0489
0.005
mg/L
0.0500
98
43-137
0.0474
0.005
mg/L
0.0500
95
39.8-131
0.0451
0.005
mg/L
0.0500
90
27.9-250
1,1-Dichloroethane
0.0518
0.005
mg/L
0.0500
104
59.9-136
1,2-Dichloroethane
0.0521
0.005
mg/L
0.0500
104
67.5-129
1,1-Dichloroethene
0.0524
0.005
mg/L
0.0500
105
67.1-138
0.0523
0.005
mg/L
0.0500
105
63.1-136
0.0530
0.005
mg/L
0.0500
106
62.6-138
1,2-Dichloropropane
0.0525
0.005
mg/L
0.0500
105
75.2-125
1,3-Dichloropropane
0.0508
0.005
mg/L
0.0500
102
79.9-123
2,2-Dichloropropane
0.0512
0.005
mg/L
0.0500
102
56.4-153
0.0527
0.005
mg/L
0.0500
105
60.4-136
0.0515
0.005
mg/L
0.0500
103
75-126
0.0504
0.005
mg/L
0.0500
101
72.1-128
Ethylbenzene
0.0515
0.005
mg/L
0.0500
103
63.3-130
Ethyl Methacrylate
0.0502
0.005
mg/L
0.0500
100
72.1-127
Hexachlorobutadiene
0.0474
0.005
mg/L
0.0500
95
16-207
0.0511
0.005
mg/L
0.0500
102
64.8-130
4-Isopropyltoluene
0.0500
0.005
mg/L
0.0500
100
54.2-144
Methacrylonitrile
0.0540
0.005
mg/L
0.0500
108
55.4-136
0.0571
0.005
mg/L
0.0500
114
70.5-130
0.0588
0.005
mg/L
0.0500
118
56.5-136

(210) 229-9920
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Page
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Page
1313of
LABORATORY REPORT
NELAC Cert. No.:
KSAT-12
1408 N. St.Mary's
T104704360-16-12
Reported:
02/25/16 09:48
Received:

02/23/16 14:02
Additional Notes:
Report No. 1602357

Analyte
Result
Reporting
Limit
Units
Spike
Level
Source
Result
%REC
%REC
Limits
RPD
RPD
Limit
Batch B609087 - 5030B

LCS (B609087-BS1)
Acetonitrile
0.0539
0.005
mg/L
0.0500
108
44-149
Methyl Iodide
0.0442
0.005
mg/L
0.0500
88
48.6-136
Methyl Methacrylate
0.0521
0.005
mg/L
0.0500
104
66.2-121
0.0510
0.005
mg/L
0.0500
102
16.3-183
Methylene Chloride
0.0519
0.005
mg/L
0.0500
104
61.3-148
Naphthalene
0.0439
0.005
mg/L
0.0500
88
5.3-152
Propylbenzene
0.0508
0.005
mg/L
0.0500
102
60.2-139
Styrene
0.0508
0.005
mg/L
0.0500
102
62.3-146
0.0495
0.005
mg/L
0.0500
99
72.4-130
0.0498
0.005
mg/L
0.0500
100
63.3-115
Toluene
0.0512
0.005
mg/L
0.0500
102
66-130
0.0447
0.005
mg/L
0.0500
89
6.55-144
0.0456
0.005
mg/L
0.0500
91
21.8-155
0.0511
0.005
mg/L
0.0500
102
66.9-126
0.0504
0.005
mg/L
0.0500
101
76.5-123
0.0534
0.005
mg/L
0.0500
107
60.5-160
0.0502
0.005
mg/L
0.0500
100
58.7-122
0.0502
0.005
mg/L
0.0500
100
60.7-138
0.0494
0.005
mg/L
0.0500
99
60.9-139
Vinyl acetate
0.0495
0.005
mg/L
0.0500
99
29.6-143
Vinyl chloride
0.0532
0.005
mg/L
0.0500
106
45.8-190
m,p-Xylenes
0.103
0.005
mg/L
0.100
103
27.4-146
o-Xylene
0.0502
0.005
mg/L
0.0500
100
64.9-129
0.0509
mg/L
0.0500
102
87.4-109
0.0510
mg/L
0.0500
102
65.7-120
0.0526
mg/L
0.0500
105
81.2-126

Acetone
0.0518
0.010
mg/L
0.0500
104
46.3-139
0.9
25.6
0.0544
0.005
mg/L
0.0500
109
33.1-164
31.6
Benzene
0.0539
0.005
mg/L
0.0500
108
72.2-133
14.4
Bromobenzene
0.0496
0.005
mg/L
0.0500
99
58.6-143
23
Bromochloromethane
0.0528
0.005
mg/L
0.0500
106
74.2-123
25.3
Tetrachloroethene
0.0547
0.005
mg/L
0.0500
109
64.6-154
17.2
0.0520
0.005
mg/L
0.0500
104
73.2-124
0.7
20.4
Bromoform
0.0495
0.005
mg/L
0.0500
99
56.3-126
22
Bromomethane
0.0562
0.005
mg/L
0.0500
112
13.2-193
198

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Page
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Page
1414of
LABORATORY REPORT
NELAC Cert. No.:
KSAT-12
1408 N. St.Mary's
T104704360-16-12
Reported:
02/25/16 09:48
Received:

02/23/16 14:02
Additional Notes:
Report No. 1602357

Analyte
Result
Reporting
Limit
Units
Spike
Level
Source
Result
%REC
%REC
Limits
RPD
RPD
Limit
Batch B609087 - 5030B


Trichloroethene
0.0502
0.005
mg/L
0.0500
100
71.1-136
17.5
Butylbenzene
0.0512
0.005
mg/L
0.0500
102
42.8-155
27.4
sec-Butylbenzene
0.0513
0.005
mg/L
0.0500
103
56.8-143
25.2
tert-Butylbenzene
0.0503
0.005
mg/L
0.0500
101
61.6-138
25.3
Carbon disulfide
0.0532
0.005
mg/L
0.0500
106
53.9-166
27.6
0.0521
0.005
mg/L
0.0500
104
63.7-121
18.6
Chlorobenzene
0.0505
0.005
mg/L
0.0500
101
70.7-138
0.9
18.4
Chloroethane
0.0532
0.005
mg/L
0.0500
106
30.6-174
0.7
20
0.0302
0.005
mg/L
0.0500
60
25.2-136
34.8
Chloroform
0.0539
0.005
mg/L
0.0500
108
73.2-125
17.8
Chloromethane
0.0528
0.005
mg/L
0.0500
106
51.7-193
26.9
2-Chlorotoluene
0.0514
0.005
mg/L
0.0500
103
60.9-136
24.7
4-Chlorotoluene
0.0506
0.005
mg/L
0.0500
101
60.9-136
23.5
0.0498
0.005
mg/L
0.0500
100
65.2-126
0.7
19.8
0.0477
0.005
mg/L
0.0500
95
58.8-118
27.3
1,2-Dibromoethane
0.0498
0.005
mg/L
0.0500
100
71.6-124
0.9
20.3
Dibromomethane
0.0517
0.005
mg/L
0.0500
103
76.7-124
0.8
22.4
1,2-Dichlorobenzene
0.0502
0.005
mg/L
0.0500
100
56.8-137
20.7
1,3-Dichlorobenzene
0.0504
0.005
mg/L
0.0500
101
49.9-145
20.7
1,4-Dichlorobenzene
0.0500
0.005
mg/L
0.0500
100
51.7-138
19.4
0.0500
0.005
mg/L
0.0500
100
43-137
32.4
0.0485
0.005
mg/L
0.0500
97
39.8-131
38.3
0.0469
0.005
mg/L
0.0500
94
27.9-250
16.6
1,1-Dichloroethane
0.0535
0.005
mg/L
0.0500
107
59.9-136
20.7
1,2-Dichloroethane
0.0523
0.005
mg/L
0.0500
105
67.5-129
0.2
16.5
1,1-Dichloroethene
0.0538
0.005
mg/L
0.0500
108
67.1-138
17.6
0.0538
0.005
mg/L
0.0500
108
63.1-136
23.5
0.0548
0.005
mg/L
0.0500
110
62.6-138
19.7
1,2-Dichloropropane
0.0527
0.005
mg/L
0.0500
105
75.2-125
0.5
19
1,3-Dichloropropane
0.0514
0.005
mg/L
0.0500
103
79.9-123
22.8
2,2-Dichloropropane
0.0517
0.005
mg/L
0.0500
103
56.4-153
40
0.0542
0.005
mg/L
0.0500
108
60.4-136
24.1
0.0514
0.005
mg/L
0.0500
103
75-126
0.1
22.3
0.0510
0.005
mg/L
0.0500
102
72.1-128
23.2
Ethylbenzene
0.0520
0.005
mg/L
0.0500
104
63.3-130
0.9
16.1
Ethyl Methacrylate
0.0506
0.005
mg/L
0.0500
101
72.1-127
0.9
24.9
Hexachlorobutadiene
0.0492
0.005
mg/L
0.0500
98
16-207
28.4

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Page
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22
Page
1515of
LABORATORY REPORT
NELAC Cert. No.:
KSAT-12
1408 N. St.Mary's
T104704360-16-12
Reported:
02/25/16 09:48
Received:

02/23/16 14:02
Additional Notes:
Report No. 1602357

Analyte
Result
Reporting
Limit
Units
Spike
Level
Source
Result
%REC
%REC
Limits
RPD
RPD
Limit
Batch B609087 - 5030B


0.0516
0.005
mg/L
0.0500
103
64.8-130
25.1
4-Isopropyltoluene
0.0513
0.005
mg/L
0.0500
103
54.2-144
25.8
Methacrylonitrile
0.0550
0.005
mg/L
0.0500
110
55.4-136
23.7
0.0563
0.005
mg/L
0.0500
113
70.5-130
23.7
0.0597
0.005
mg/L
0.0500
119
56.5-136
30.7
Acetonitrile
0.0552
0.005
mg/L
0.0500
110
44-149
30.1
Methyl Iodide
0.0471
0.005
mg/L
0.0500
94
48.6-136
28.5
Methyl Methacrylate
0.0526
0.005
mg/L
0.0500
105
66.2-121
28.8
0.0526
0.005
mg/L
0.0500
105
16.3-183
25.8
Methylene Chloride
0.0524
0.005
mg/L
0.0500
105
61.3-148
21.5
Naphthalene
0.0458
0.005
mg/L
0.0500
92
5.3-152
30
Propylbenzene
0.0521
0.005
mg/L
0.0500
104
60.2-139
25.2
Styrene
0.0515
0.005
mg/L
0.0500
103
62.3-146
23.4
0.0498
0.005
mg/L
0.0500
100
72.4-130
0.6
21.6
0.0511
0.005
mg/L
0.0500
102
63.3-115
20.5
Toluene
0.0515
0.005
mg/L
0.0500
103
66-130
0.6
15.6
0.0465
0.005
mg/L
0.0500
93
6.55-144
29.7
0.0467
0.005
mg/L
0.0500
93
21.8-155
27.2
0.0522
0.005
mg/L
0.0500
104
66.9-126
20.4
0.0506
0.005
mg/L
0.0500
101
76.5-123
0.3
18.7
0.0545
0.005
mg/L
0.0500
109
60.5-160
16.1
0.0507
0.005
mg/L
0.0500
101
58.7-122
24.7
0.0512
0.005
mg/L
0.0500
102
60.7-138
24.1
0.0511
0.005
mg/L
0.0500
102
60.9-139
25.6
Vinyl acetate
0.0523
0.005
mg/L
0.0500
105
29.6-143
27.1
Vinyl chloride
0.0541
0.005
mg/L
0.0500
108
45.8-190
32.4
m,p-Xylenes
0.103
0.005
mg/L
0.100
103
27.4-146
0.2
24.5
o-Xylene
0.0510
0.005
mg/L
0.0500
102
64.9-129
24.5
0.0502
mg/L
0.0500
100
87.4-109
0.0508
mg/L
0.0500
102
65.7-120
0.0532
mg/L
0.0500
106
81.2-126
Source: 1602357-01
Acetone
0.0526
0.010
mg/L
0.0500
<0.010
105
19.5-259
0.0530
0.005
mg/L
0.0500
<0.005
106
39.7-182
Benzene
0.0511
0.005
mg/L
0.0500
<0.005
102
77.2-127
Bromobenzene
0.0544
0.005
mg/L
0.0500
<0.005
109
55.6-147

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Page
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22
Page
1616of
LABORATORY REPORT
NELAC Cert. No.:
KSAT-12
1408 N. St.Mary's
T104704360-16-12
Reported:
02/25/16 09:48
Received:

02/23/16 14:02
Additional Notes:
Report No. 1602357

Analyte
Result
Reporting
Limit
Units
Spike
Level
Source
Result
%REC
%REC
Limits
RPD
RPD
Limit
Batch B609087 - 5030B

Source: 1602357-01
Bromochloromethane
0.0504
0.005
mg/L
0.0500
<0.005
101
68.4-140
Tetrachloroethene
0.0584
0.005
mg/L
0.0500
<0.005
117
19.3-228
0.0508
0.005
mg/L
0.0500
<0.005
102
68.2-127
Bromoform
0.0454
0.005
mg/L
0.0500
<0.005
91
56.5-116
Bromomethane
0.0586
0.005
mg/L
0.0500
<0.005
117
54.4-152
Trichloroethene
0.0496
0.005
mg/L
0.0500
<0.005
99
31.1-191
Butylbenzene
0.0651
0.005
mg/L
0.0500
<0.005
130
78.1-143
sec-Butylbenzene
0.0596
0.005
mg/L
0.0500
<0.005
119
58.9-157
tert-Butylbenzene
0.0548
0.005
mg/L
0.0500
<0.005
110
62.3-147
Carbon disulfide
0.0585
0.005
mg/L
0.0500
<0.005
117
62.9-179
0.0474
0.005
mg/L
0.0500
<0.005
95
50.8-136
Chlorobenzene
0.0511
0.005
mg/L
0.0500
<0.005
102
69.2-133
Chloroethane
0.0512
0.005
mg/L
0.0500
<0.005
102
54.3-149
0.0290
0.005
mg/L
0.0500
<0.005
58
31.1-160
Chloroform
0.0522
0.005
mg/L
0.0500
<0.005
104
70.5-129
Chloromethane
0.0519
0.005
mg/L
0.0500
<0.005
104
32.8-220
2-Chlorotoluene
0.0562
0.005
mg/L
0.0500
<0.005
112
78.1-131
4-Chlorotoluene
0.0576
0.005
mg/L
0.0500
<0.005
115
74.7-133
0.0486
0.005
mg/L
0.0500
<0.005
97
58.6-127
0.0458
0.005
mg/L
0.0500
<0.005
92
39.6-155
1,2-Dibromoethane
0.0458
0.005
mg/L
0.0500
<0.005
92
64.7-132
Dibromomethane
0.0492
0.005
mg/L
0.0500
<0.005
98
72-133
1,2-Dichlorobenzene
0.0540
0.005
mg/L
0.0500
<0.005
108
56.8-129
1,3-Dichlorobenzene
0.0576
0.005
mg/L
0.0500
<0.005
115
50.8-135
1,4-Dichlorobenzene
0.0576
0.005
mg/L
0.0500
<0.005
115
53.4-131
0.0495
0.005
mg/L
0.0500
<0.005
99
12.3-171
0.0404
0.005
mg/L
0.0500
<0.005
81
56.1-127
0.0525
0.005
mg/L
0.0500
<0.005
105
44.7-175
1,1-Dichloroethane
0.0499
0.005
mg/L
0.0500
<0.005
100
74.1-124
1,2-Dichloroethane
0.0494
0.005
mg/L
0.0500
<0.005
99
60.7-137
1,1-Dichloroethene
0.0507
0.005
mg/L
0.0500
<0.005
101
69.3-139
0.0525
0.005
mg/L
0.0500
<0.005
105
67.1-141
0.0546
0.005
mg/L
0.0500
<0.005
109
75.8-126
1,2-Dichloropropane
0.0503
0.005
mg/L
0.0500
<0.005
101
80.4-124
1,3-Dichloropropane
0.0488
0.005
mg/L
0.0500
<0.005
98
74.9-135
2,2-Dichloropropane
0.0460
0.005
mg/L
0.0500
<0.005
92
79-148
0.0528
0.005
mg/L
0.0500
<0.005
106
81.7-140

(210) 229-9920
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Page
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22
Page
1717of
LABORATORY REPORT
NELAC Cert. No.:
KSAT-12
1408 N. St.Mary's
T104704360-16-12
Reported:
02/25/16 09:48
Received:

02/23/16 14:02
Additional Notes:
Report No. 1602357

Analyte
Result
Reporting
Limit
Units
Spike
Level
Source
Result
%REC
%REC
Limits
RPD
RPD
Limit
Batch B609087 - 5030B

Source: 1602357-01
0.0497
0.005
mg/L
0.0500
<0.005
99
0.0499
0.005
mg/L
0.0500
<0.005
100
44.6-146
66-129
Ethylbenzene
0.0522
0.005
mg/L
0.0500
<0.005
104
67.1-121
Ethyl Methacrylate
0.0463
0.005
mg/L
0.0500
<0.005
93
80.8-141
Hexachlorobutadiene
0.0772
0.005
mg/L
0.0500
<0.005
154
11.1-246
0.0512
0.005
mg/L
0.0500
<0.005
102
67.7-134
4-Isopropyltoluene
0.0585
0.005
mg/L
0.0500
<0.005
117
59.4-151
Methacrylonitrile
0.0494
0.005
mg/L
0.0500
<0.005
99
52.7-155
0.0577
0.005
mg/L
0.0500
<0.005
115
51.9-155
0.0576
0.005
mg/L
0.0500
<0.005
115
41.9-177
Acetonitrile
0.0529
0.005
mg/L
0.0500
<0.005
106
54.7-167
Methyl Iodide
0.0326
0.005
mg/L
0.0500
<0.005
65
0-176
Methyl Methacrylate
0.0483
0.005
mg/L
0.0500
<0.005
97
72.7-155
0.0478
0.005
mg/L
0.0500
<0.005
96
73.7-111
Methylene Chloride
0.0513
0.005
mg/L
0.0500
<0.005
103
56.9-141
Naphthalene
0.0479
0.005
mg/L
0.0500
<0.005
96
51.9-173
Propylbenzene
0.0588
0.005
mg/L
0.0500
<0.005
118
62.2-152
Styrene
0.0518
0.005
mg/L
0.0500
<0.005
104
63.6-144
0.0489
0.005
mg/L
0.0500
<0.005
98
69.6-136
0.0472
0.005
mg/L
0.0500
<0.005
94
65.2-111
Toluene
0.0518
0.005
mg/L
0.0500
<0.005
104
64.3-132
0.0553
0.005
mg/L
0.0500
<0.005
111
52.8-166
0.0574
0.005
mg/L
0.0500
<0.005
115
46.9-175
0.0474
0.005
mg/L
0.0500
<0.005
95
61.5-135
0.0478
0.005
mg/L
0.0500
<0.005
96
76.7-122
48.8-162
0.0517
0.005
mg/L
0.0500
<0.005
103
0.0464
0.005
mg/L
0.0500
<0.005
93
64-123
0.0571
0.005
mg/L
0.0500
<0.005
114
84-132
0.0565
0.005
mg/L
0.0500
<0.005
113
73.8-138
Vinyl acetate
0.0407
0.005
mg/L
0.0500
<0.005
81
34.7-140
Vinyl chloride
0.0518
0.005
mg/L
0.0500
<0.005
104
53.7-167
m,p-Xylenes
0.105
0.005
mg/L
0.100
<0.005
105
85.3-124
o-Xylene
0.0496
0.005
mg/L
0.0500
<0.005
99
78.6-123
0.0510
mg/L
0.0500
102
87.4-109
0.0494
mg/L
0.0500
99
65.7-120
0.0537
mg/L
0.0500
107
81.2-126
Matrix Spike Dup (B609087-MSD1)
Source: 1602357-01

(210) 229-9920
Fax (210) 229-9921

Page
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Page
1818of
LABORATORY REPORT
NELAC Cert. No.:
KSAT-12
1408 N. St.Mary's
T104704360-16-12
Reported:
02/25/16 09:48
Received:

02/23/16 14:02
Additional Notes:
Report No. 1602357

Result
Reporting
Limit
Units
Spike
Level
%REC
%REC
Limits
RPD
RPD
Limit
Acetone
0.0553
0.010
mg/L
0.0500
0.0553
0.005
mg/L
0.0500
<0.010
111
19.5-259
10.3
<0.005
111
39.7-182
Benzene
0.0530
0.005
mg/L
43.6
0.0500
<0.005
106
77.2-127
Bromobenzene
0.0569
0.005
16.5
mg/L
0.0500
<0.005
114
55.6-147
Bromochloromethane
0.0512
38.2
0.005
mg/L
0.0500
<0.005
102
68.4-140
Tetrachloroethene
37.9
0.0632
0.005
mg/L
0.0500
<0.005
126
19.3-228
32.2
0.0517
0.005
mg/L
0.0500
<0.005
103
68.2-127
25.9
Bromoform
0.0468
0.005
mg/L
0.0500
<0.005
94
56.5-116
30.6
Bromomethane
0.0650
0.005
mg/L
0.0500
<0.005
130
54.4-152
10
73.5
Trichloroethene
0.0518
0.005
mg/L
0.0500
<0.005
104
31.1-191
24.3
Butylbenzene
0.0704
0.005
mg/L
0.0500
<0.005
141
78.1-143
37.6
sec-Butylbenzene
0.0637
0.005
mg/L
0.0500
<0.005
127
58.9-157
34.9
tert-Butylbenzene
0.0593
0.005
mg/L
0.0500
<0.005
119
62.3-147
34.9
Carbon disulfide
0.0617
0.005
mg/L
0.0500
<0.005
123
62.9-179
43.9
0.0502
0.005
mg/L
0.0500
<0.005
100
50.8-136
34.3
Chlorobenzene
0.0536
0.005
mg/L
0.0500
<0.005
107
69.2-133
24.2
Chloroethane
0.0532
0.005
mg/L
0.0500
<0.005
106
54.3-149
19.6
0.0255
0.005
mg/L
0.0500
<0.005
51
31.1-160
13
57.7
Chloroform
0.0543
0.005
mg/L
0.0500
<0.005
109
70.5-129
22.6
Chloromethane
0.0557
0.005
mg/L
0.0500
<0.005
111
32.8-220
25.4
2-Chlorotoluene
0.0600
0.005
mg/L
0.0500
<0.005
120
78.1-131
36.3
4-Chlorotoluene
0.0612
0.005
mg/L
0.0500
<0.005
122
74.7-133
37.9
0.0494
0.005
mg/L
0.0500
<0.005
99
58.6-127
26.4
0.0465
0.005
mg/L
0.0500
<0.005
93
39.6-155
38.7
1,2-Dibromoethane
0.0468
0.005
mg/L
0.0500
<0.005
94
64.7-132
26.5
Dibromomethane
0.0495
0.005
mg/L
0.0500
<0.005
99
72-133
0.6
34.1
1,2-Dichlorobenzene
0.0563
0.005
mg/L
0.0500
<0.005
113
56.8-129
25.2
1,3-Dichlorobenzene
0.0607
0.005
mg/L
0.0500
<0.005
121
50.8-135
25.3
1,4-Dichlorobenzene
0.0604
0.005
mg/L
0.0500
<0.005
121
53.4-131
22.9
0.0513
0.005
mg/L
0.0500
<0.005
103
12.3-171
50
0.0416
0.005
mg/L
0.0500
<0.005
83
56.1-127
50
0.0553
0.005
mg/L
0.0500
<0.005
111
44.7-175
95.4
1,1-Dichloroethane
0.0518
0.005
mg/L
0.0500
<0.005
104
74.1-124
22.7
1,2-Dichloroethane
0.0503
0.005
mg/L
0.0500
<0.005
101
60.7-137
20.6
1,1-Dichloroethene
0.0542
0.005
mg/L
0.0500
<0.005
108
69.3-139
19.7
0.0557
0.005
mg/L
0.0500
<0.005
111
67.1-141
29.8
0.0570
0.005
mg/L
0.0500
<0.005
114
75.8-126
21.4
1,2-Dichloropropane
0.0516
0.005
mg/L
0.0500
<0.005
103
80.4-124
24.7
1,3-Dichloropropane
0.0500
0.005
mg/L
0.0500
<0.005
100
74.9-135
40.3
Analyte
Source
Result
Batch B609087 - 5030B

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Fax (210) 229-9921

Page
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22
Page
1919of
LABORATORY REPORT
NELAC Cert. No.:
KSAT-12
1408 N. St.Mary's
T104704360-16-12
Reported:
02/25/16 09:48
Received:

02/23/16 14:02
Additional Notes:
Report No. 1602357

Analyte
Result
Reporting
Limit
Units
Spike
Level
Source
Result
%REC
%REC
Limits
RPD
RPD
Limit
Batch B609087 - 5030B

Source: 1602357-01
2,2-Dichloropropane
0.0496
0.005
mg/L
0.0500
<0.005
99
79-148
39.9
0.0554
0.005
mg/L
0.0500
<0.005
111
81.7-140
36.9
0.0510
0.005
mg/L
0.0500
<0.005
102
44.6-146
50
0.0509
0.005
mg/L
0.0500
<0.005
102
66-129
63.6
Ethylbenzene
0.0546
0.005
mg/L
0.0500
<0.005
109
67.1-121
18.5
Ethyl Methacrylate
0.0467
0.005
mg/L
0.0500
<0.005
93
80.8-141
0.9
47.1
Hexachlorobutadiene
0.0824
0.005
mg/L
0.0500
<0.005
165
11.1-246
47
0.0540
0.005
mg/L
0.0500
<0.005
108
67.7-134
36.7
4-Isopropyltoluene
0.0628
0.005
mg/L
0.0500
<0.005
126
59.4-151
35.9
Methacrylonitrile
0.0503
0.005
mg/L
0.0500
<0.005
101
52.7-155
27.2
0.0582
0.005
mg/L
0.0500
<0.005
116
51.9-155
0.9
30.8
0.0586
0.005
mg/L
0.0500
<0.005
117
41.9-177
21.3
Acetonitrile
0.0558
0.005
mg/L
0.0500
<0.005
112
54.7-167
43.7
Methyl Iodide
0.0343
0.005
mg/L
0.0500
<0.005
69
0-176
50
Methyl Methacrylate
0.0479
0.005
mg/L
0.0500
<0.005
96
72.7-155
0.9
21.4
0.0488
0.005
mg/L
0.0500
<0.005
98
73.7-111
28.1
Methylene Chloride
0.0531
0.005
mg/L
0.0500
<0.005
106
56.9-141
19.1
Naphthalene
0.0478
0.005
mg/L
0.0500
<0.005
96
51.9-173
0.2
36.9
Propylbenzene
0.0630
0.005
mg/L
0.0500
<0.005
126
62.2-152
30.7
Styrene
0.0541
0.005
mg/L
0.0500
<0.005
108
63.6-144
35.3
0.0502
0.005
mg/L
0.0500
<0.005
100
69.6-136
38.9
0.0480
0.005
mg/L
0.0500
<0.005
96
65.2-111
27.8
Toluene
0.0538
0.005
mg/L
0.0500
<0.005
108
64.3-132
10.1
0.0545
0.005
mg/L
0.0500
<0.005
109
52.8-166
37.2
0.0585
0.005
mg/L
0.0500
<0.005
117
46.9-175
38
0.0502
0.005
mg/L
0.0500
<0.005
100
61.5-135
24.6
0.0491
0.005
mg/L
0.0500
<0.005
98
76.7-122
21.5
0.0549
0.005
mg/L
0.0500
<0.005
110
48.8-162
17.5
0.0473
0.005
mg/L
0.0500
<0.005
95
64-123
47.2
0.0603
0.005
mg/L
0.0500
<0.005
121
84-132
14.2
0.0607
0.005
mg/L
0.0500
<0.005
121
73.8-138
25.1
Vinyl acetate
0.0397
0.005
mg/L
0.0500
<0.005
79
34.7-140
46.1
Vinyl chloride
0.0551
0.005
mg/L
0.0500
<0.005
110
53.7-167
12.6
m,p-Xylenes
0.109
0.005
mg/L
0.100
<0.005
109
85.3-124
21
o-Xylene
0.0525
0.005
mg/L
0.0500
<0.005
105
78.6-123
22.2
0.0508
mg/L
0.0500
102
87.4-109
0.0491
mg/L
0.0500
98
65.7-120

(210) 229-9920
Fax (210) 229-9921

Page
of 25
22
Page
2020of
LABORATORY REPORT
NELAC Cert. No.:
KSAT-12
1408 N. St.Mary's
T104704360-16-12
Reported:
02/25/16 09:48
Received:

02/23/16 14:02
Additional Notes:
Report No. 1602357

Analyte
Result
Reporting
Limit
Units
Spike
Level
Source
Result
%REC
%REC
Limits
RPD
RPD
Limit
Batch B609087 - 5030B

Source: 1602357-01
0.0532
mg/L
0.0500
106
81.2-126
DEFINITIONS
*
TNI / NELAC accredited analyte
PQL
MCL
mg/Kg
mg/L
PPM
L
M
RMCCL
Surr L
Surr H
Practical Quantitation Limit

Maximum Contaminant Level
Milligrams per Kilogram (Parts per Million)
Milligrams per Liter (Parts per Million)
Parts per Million
LCS recovery is outside QC acceptance limits, the results may have a slight bias.
MS recovery is outside QC limits, the results may have a slight bias due to possible matrix interferences.
Recommended Maximum Concentration of Contaminants Level
Surrogate recovery is outside QC limits due to matrix interferences.
Surrogate recovery is high due to contribution from hydrocarbon interferences.
R/hr
MicroRoentgens per hour (Measure of Radioactivity Level)
Test Methods followed by the laboratory are referenced in the following approved methodology, unless otherwise specified.
Standard Methods for the Examination of Water and Wastewater, 21st Edition 2005
Methods for Chemical Analysis of Water and Wastes, EPA 600/4-79-020, Rev. March 1983
EPA SW Test Methods for the Examination of Solid Waste, SW-846, 1996

(210) 229-9920
Fax (210) 229-9921

Page
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22
Page
2121of
LABORATORY REPORT
NELAC Cert. No.:
KSAT-12
1408 N. St.Mary's
T104704360-16-12
Reported:
02/25/16 09:48
Received:

02/23/16 14:02
Additional Notes:
Report No. 1602357
Aimee Landon For Marcela Gracia Hawk, President For
The results in this report apply to the samples analyzed in accordance with the chain of
custody document. This analytical report must be reproduced in its entirety.
Richard Hawk, General Manager

(210) 229-9920
Fax (210) 229-9921

Page
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22
Page
2222of
Page 23 of 25
Page 24 of 25
KSAT 12 Crystal City Water/Sediment Sample
1
2
Contaminant
Result
(ppm)*
EPA DW Limit
(ppm)1
Times Higher
Aluminum
0.94
0.2
4.7 X
Beryllium
0.008
0.004
2X
Iron
171
0.3
570 X
Manganese
6.98
0.05
139 X
Lead
0.098
0.015
6.5 X
Potential Health Effects from Long-term exposure above MCL2

Secondary Contaminant may cause cosmetic effects (such as skin or tooth
discoloration) or aesthetic effects (such as taste, odor, or color)
Intestinal Lesions
Infants & Children: Delays in physical or mental development;
Children could show deficits in attention span and learning abilities;
Adults: Kidney problems, high blood pressure.
PPM = Parts Per Million

Reference EPA National Primary & Secondary Drinking Water Regulations
Page 25 of 25
1610 S. Laredo Street, San Antonio, Texas 78207-7029 x (210) 229-9920 x Fax (210) 229-9921

SATL Results From Crystal City Water Testing

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SATL Results From Crystal City Water Testing

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February 25, 2016

RE: Crystal City Water

Dear Pilar Arias

The analyses were

Any deviations observed at sample receiving are

Sample data and associated QC are

1610 S. Laredo Street, San Antonio, Texas 78207-7029

Fax (210) 229-9921

Project: Crystal City Water

Project Number: [none]

Report No. 1602357

Total Samples received in this work order:

Crystal City Water

1610 S. Laredo Street, San Antonio, Texas 78207-7029

Fax (210) 229-9921

Project: Crystal City Water

Project Number: [none]

Report No. 1602357

Sample ID #: Crystal City Water

Sampling Method: Grab

Sample Matrix: Liquid

Lab Sample ID #: 1602357-01

Date/Time Collected: 02/17/16 22:00

Total Metals By ICP-OES

1610 S. Laredo Street, San Antonio, Texas 78207-7029

Fax (210) 229-9921

Project: Crystal City Water

Project Number: [none]

Report No. 1602357

Sample ID #: Crystal City Water

Sampling Method: Grab

Sample Matrix: Liquid

Lab Sample ID #: 1602357-01

Date/Time Collected: 02/17/16 22:00

Volatile Organic Compounds by GC/MS

1610 S. Laredo Street, San Antonio, Texas 78207-7029

Fax (210) 229-9921

Project: Crystal City Water

Project Number: [none]

Report No. 1602357

Sample ID #: Crystal City Water

Sampling Method: Grab

Sample Matrix: Liquid

Lab Sample ID #: 1602357-01

Date/Time Collected: 02/17/16 22:00

Volatile Organic Compounds by GC/MS

1610 S. Laredo Street, San Antonio, Texas 78207-7029

Fax (210) 229-9921

Project: Crystal City Water

Project Number: [none]

Report No. 1602357

Total Metals By ICP-OES - Quality Control

Batch B609081 - EPA 245.1

Prepared: 02/24/16 09:10 Analyzed: 02/24/16 14:12

LCS Dup (B609081-BSD1)

Matrix Spike (B609081-MS1)

Prepared: 02/24/16 09:10 Analyzed: 02/24/16 14:12

Prepared: 02/24/16 09:10 Analyzed: 02/24/16 14:12

Prepared: 02/24/16 09:10 Analyzed: 02/24/16 14:12

Batch B609085 - EPA 200.7

1610 S. Laredo Street, San Antonio, Texas 78207-7029

Fax (210) 229-9921

Project: Crystal City Water