H.

OBSERVATION RESULT
No

Procedure Of Experiment

1.
1 gram of
iodine
- Poured into
erlenmeyer 250
mL
- Added 1 mL of
acetone
- Added 1 mL of
aquades
- Shaked
- Added NaOH 2N
drop by drop until
produce yellow
Yellow
precipitation
- Added 25 mL of
aquades into
erlenmeyer
- Filtered by buchner
filter
- Observed

Observation Result

Hypothesis/Reaction

Before :
- Iodine : balck
crystals
- Acetone: colorless
solution
- Aquades : colorless
solution
- NaOH
2N
:
colorless solution
- Ethanol : colorless
solution
After :
- 1 gram of iodine +
1 mL of acetone +
1 mL of aquades
become
black
solution and there
is
black
precipitation.
- After
shaked:
become
yellow
solution and black
crystals
- After added 55
drops of NaOH 2
N: there is yellow
precipitation and
the
color
of

The reaction :
3 I2 (aq) + CH3COCH3 (aq)
3HI (aq) + I3CCOCH3 (aq)
CH3COCH3 (aq) + NaOH(aq)
CHI3 + CH3COONa
- The melting point

of iodoform based

on theory is 119 C

- 122 C.
Solubility of

Iodoform:
iodoform
insoluble in
-

Conclusion

water.
The odor of
iodoform is
medical smell.

Reaction between
iodine and acetone
produces iodoform
( CHI3 )
The odor of
iodoform like
medical smell.
Melting point of
iodoform is 120 C.
Iodoform insoluble
in water.
The rendemen is
97,62 %.

Filtrate

Residu
-

Iodofor

Residue

Washed with
aquades until the
precipitation free
from NaOH
Observed
Inserted into erlenmeyer
Closed with glass funnel
Poured ethanol drop by drop
using funnel
Filtered using buchner
funnel
observed

Filtrate
-

Closed the soluton

Cooled
Added 2,5 Ml
water
Stirred
Filtered with
buchner filter
Observed

solution is yellow.
After added 25 mL
of water: the color
of
solution
is
yellow.
Filtered by buchner
filter produce:
a. Residue
:
yellow powder
b. Filtrate
:
colorless
solution
After washed using
aquades:
the
residue still yellow
powder, but it
doesnt
contain
NaOH again. To
check if there is no
NaOH, we test it
using litmus paper.
The result of litmus
paper:
a. Blue
litmus
paper: still blue
color
b. Red litmus: still
red color
Residue + 6 mL of
ethanol : become
turbid,
because
there is yellow

Residue
-

Filtrate

Washed using
cool ethanol
Dried
Observed

Pondere
d the
mass of
iodoform
Mass of
iodofor
m

Determin
ed the
melting
point of
iodoform
Melting
point of
iodoform

-Poured
into
aquade
s

solubility
of
iodoform

precipitation.
After heated and
added 2,5 mL of
water: it produces
iodoform.
Iodoform is yellow
crystals.
Melting point of
iodoform is 120
C.
Iodoform crystals
is poured in 1 mL
of aquades: the
iodoform insoluble
in water, because
the
solution
become turbid.
Mass of iodoform
is 0,5 gram.