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INTRODUCTION
Location 3a
Location 3
Location 2a
Location 2
Location 1
Location 1a
a. b.
Location C
Location B
Location D
c. Location A
d. Location E
Table 1 shows the model parameters for the old and the 1 Location 1 08 Eight tuyeres as shown in Fig. 3a. All
tuyeres are equi-spaced.
new vessels. As can be seen from Table 1, the bottom
diameter of the new vessel has been increased. Lance 2 Location 1a 08 Eight tuyeres as shown in Fig. 3b. All
tuyeres are not equi-spaced.
height in the actual operation has been varied from 1500
to 2400 mm but for simulation purpose the average lance 3 Location 2 08 Eight tuyeres as shown in Fig. 3a. All
tuyeres are equi-spaced.
height of 1800 mm was considered. The lance height
considered in the model was 300 mm and was kept 4 Location 2a 08 Eight tuyeres as shown in Fig. 3b. All
constant for all the mixing experiments. tuyeres are not equi-spaced.
Bottom dia., mm 540 784 9 Location C 08 Eight tuyeres used: 6 tuyeres at one PCD
and two tuyeres very close to the centre
Top flow rate, Nm3/min 1.04 1.04 of the bottom as shown in Fig. 3d.
Bottom flow rate, lpm 15-40 15-40
10 Location D 08 Eight tuyeres used: 6 tuyeres at one PCD
Bottom hole size, mm 1.5 1.5 and two tuyeres very close to the centre
of the bottom as shown in Fig. 3d.
No. of bottom holes 6 8
Lance height, mm 300 300
Compressed Air
Tuyeres Locations KCI Tracer Top Lance
Meter
374
Rotameter
Bath
Depth
Bottom tuyere
METHODOLOGY arrangement Conductivity Probe
Conductivity ratio
the metal phase. The extent of mixing was determined by
conductivity measurements using potassium chloride of
strength 1.293 N as the tracer and a standard conductivity
meter was used for measuring the conductance of the
solution. The conductivity probe was dipped 80 mm into
the bath, about 200-mm away from the centre of the
model vessel at a location opposite to the tracer addition
point. This probe location was chosen after trying various time (sec)
other locations of conductivity probes. The probe location
point with the longest mixing time has been chosen to
represent the bulk uniform mixing time. A similar
arrangement has been used by many investigators3,4,6,7,8
for mixing time determinations. The accuracy of Probe 2
conductivity measurement decreases with increasing
concentration. Hence a very low-end concentration
(0.0014N KCl) was used6. A maximum of two experiments
was carried out in a water solution. Fresh water was used
after every two experiments. Air was introduced through
the top lance as well as from the bottom tuyeres at a Probe 1
predetermined rate. The flow rate of gas from the top Tracer
addition point
lance as well as from the bottom tuyeres was measured
with the help of rotameters and it was monitored
continuously during the experiments. When the steady
state was achieved, the tracer was added and conductivity
of the solution was recorded continuously by a Data
Acquisition System (DAS). A typical mixing plot is shown
in Fig. 5. The uniform mixing time was defined as the Fig. 6 : Comparison of conductivity ratio vs time for probe
time after which the tracer concentration falls in and locations 1 and 2
stays within ± 1.5 percent of the uniform concentration.
Each experiment was repeated at least once and sometimes
more than once or twice to ensure the reproducibility of For Location 1 at bottom flow rate 40 lpm
the results. Sufficient care was taken to ensure that the
variation in the mixing time for any identical set of
Conductivity ratio
1.2
dimensionless conductivity ratio
1.0
0.6
0.4
0.2
0.0
0 20 40 60 80 100 120 140 160 180
time (sec)
Miximg index
which the whole solution became homogeneous was very
close to the time taken by Probe 1. Thus it can be seen
that time taken by Probe 1 which was farthest away from
the tracer injection point was the highest. The time taken
by Probes 2 and 3 was either lower than or same as the
time taken by Probe 1 (for the solution to become
homogeneous). The conductivity probe that measures the
local concentration was used to compute the bulk mixing
of the whole bath. If probe locations 2 or 3 were used for
determination of mixing time of the bath, the correct
mixing time may not be obtained. Therefore, Probe Fig. 8 : Mixing time variation at locations 1, 2 and 3 in the
location 1 was used for all the mixing experimentation new vessel model
carried out in this study.
Mixing Study
Mixing Index
Mixing results have been plotted in terms of dimensionless
mixing index and percentage bottom flow rate. Mixing
index has been defined as:
tmix, top blowing = mixing time in case of top blowing only Fig. 9 : Mixing time variation at locations 1a, 2a and 3a in
the new vessel model
Lower is the mixing index, better is the mixing.
bulk of the liquid by rising bubbles is proportional to the
Percentage bottom flow rate (BFR) in abscissa has been
depth of the liquid inside the vessel. At location 1, the
defined as:
height of the liquid above the bottom tuyeres is lower
compared to other bottom tuyeres locations 2 and 3.
% BFR = (Bottom gas rate * 100) / Top gas rate
There is not much difference in the mixing time for the
bottom tuyeres locations 2 and 3 as shown in Fig. 8.
Mixing time for the top blowing only for six hole lance has
However, the bottom tuyeres location 2a was found to
been found to be 115 sec with the old vessel model. The
have a lower mixing time compared to the bottom tuyeres
same value of mixing time has been considered for
location 3a (Fig. 9).
computing mixing index for new vessel bottom also. This
has been done to compare the mixing results of both the The bottom tuyeres locations 1 & 1a, 2 & 2a and 3 & 3a
vessels. Actually mixing time with top blowing only using were compared for their mixing indexes in Fig.10 (a, b
SHL for new vessel model will be different. and c). It can be seen from Fig. 10 that the mixing index
decreased with the increase of bottom gas flow rate. The
Effect of bottom tuyeres locations on mixing: Ten mixing index with bottom tuyeres location 1a, as shown
different bottom tuyere locations as mentioned earlier in Fig. 10a, was found to be much lower compared to the
were studied for mixing in the new vessel which are being tuyeres location 1 which has 8 equi-spaced tuyeres. This
discussed here. The top gas flow rate, lance and bath was because the equi-spaced tuyeres at location 1 were
heights were kept constant for all the mixing experiments acting as a barrier to the liquid present inside and outside
as shown in Table 1. The effect of bottom gas flow rate of the bottom tuyeres which resulted in increase of mixing
was studied at each bottom tuyere location keeping other index. Large improvement in the mixing index was observed
parameters constant. Figs. 8 and 9 show the effect of with the bottom tuyeres location 1a where the tuyeres
tuyeres locations 1, 2, 3 and 1a, 2a, 3a respectively on were not equi-spaced compared to the location 1. Non-
mixing in the vessel. It was observed that the mixing time uniform positioning of tuyeres helps in breaking the
decreased with the increase of bottom gas flow rate for barrier caused by equi-spacing of tuyeres, which resulted
all the bottom tuyeres locations considered as shown in in improving the mixing with location 1a. Similarly, as
Figs. 3a and 3b. It can be seen from the figures (8 & 9) shown in Fig. 10b, bottom tuyeres location 2a (non-
that the tuyeres locations 1 and 1a which are farthest uniform positioning of tuyeres) has shown a large
away from the centre of the vessel have the highest mixing improvement in the mixing compared to location 2 where
index (poor mixing). This may be because of the lower the tuyeres were positioned equi-spaced. There was not
liquid height above the bottom tuyeres because of the much difference observed in the mixing index for bottom
curved bottom vessel. Sahai and Guthrie9 have shown tuyeres locations 3 and 3a as shown in Fig. 10c. This
that the network of energy input per unit volume to the may be because the tuyeres were close to the centre of
Mixing Index
Mixing index
% BFR
0.00 1.00 2.00 3.00 4.00 5.00
% BFR
Mixing index
% BFR
Location D
Location C
Mixing Index
12
Mixing index
(P)/[P] index
4
8 Bot. Tuyeres
6 Bot. Tuyeres
0
1620 1640 1660 1680 1700 1720 1740 1760
Fig. 14 : Comparison of mixing time for various bottom Fig. 15 : Comparison of phosphorus partition index with
tuyeres configurations used in LD1 using water model study respect to turndown temperature for 6 and 8 bottom tuyeres
% Frequency
12 40
(P)/[P] index
30
8
20
10
4
0
2.5 5 7.5 10 12.5 15 More
0
10 12 14 16 18 20 22 24 (P)/[P] index interval
% Fe in slag
(On average 10-12 points higher (P)/[P] achieved with 8 bottom
Fig. 16 : Comparison of phosphorus partition index with tuyeres compared to 6 bottom tuyeres)
respect to % Fe in the slag for 6 and 8 bottom tuyeres
30 6 Bot. Tuyeres
10.0 % Frequency 25 8 Bot. Tuyeres
20
8.0 15
10
6.0 8 Bot. Tuyeres 5
6 Bot. Tuyeres 0
4.0 10 12 14 16 18 20 22 24 More
1620 1640 1660 1680 1700 1720 1740 1760 % Fe in slag
Average turndown temperature,oC
(On average 1% lower Fe in slag achieved with 8 bottom
Fig. 17 : Variation of average phosphorus partition index tuyeres compared to 6 bottom tuyeres)
with average turndown temperature for 6 and 8 bottom
tuyeres Fig. 20 : Comparison of distribution of % Fe in slag for 6 and
8 bottom tuyeres
0.0
● Phosphorus partition was improved by about 10 to 12
points with the new bottom tuyere configuration
14.0 15.0 16.0 17.0 18.0 19.0 20.0
Avg. % Fe in slag
compared to earlier 6 bottom tuyere configurations.
Fig. 18 : Variation of average phosphorus partition index ● Fe in the slag was reduced by about 1 % with the eight
with % Fe in the slag for 6 and 8 bottom tuyeres bottom tuyere configurations compared to six bottom
tuyere configurations.
● A record vessel life of more than 2000 heats was
1 % lower compared to 6 bottom tuyeres. The campaign achieved in the first campaign of eight bottom tuyere
life of the vessel having dolomite lining was also increased. configurations itself.
A record vessel life of more than 2000 heats was achieved
with the first campaign of 8 bottom tuyeres in LD1.
ACKNOWLEDGEMENTS
CONCLUSIONS
The authors would like to acknowledge the help rendered
● Bottom tuyere configurations 2, 2a and B in the new by Mr Asit Roy, Facility Management personnel during
vessel were found to give lower mixing index compared experimentation of this work. The authors would also like
to other tuyere configurations studied. to thank the staff of LD1 vessel control room for their help
in implementing this work and Mr. Shantanu for supplying 5. Amit Chatterjee, C. Marique and P. Nilles, Ironmaking
data for analysis. and Steelmaking, 1984, Vol. 11, No. 3, p. 117.