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With this kind of Flexibility in an Analyzer, You Can Design Your Own IH/Safety Analyzer PID Analyzers, LLC
PID Analyzers, LLC copyright 2003-2013
102+
In
Schematic of PID
Photoionization Process
Where: R= a molecule with an IP <10.5 for the 10.6 or 11.9 for the 11.7 lamp h = a photon with an energy >= IP of the molecule R+ is the ion formed by the process that is collected in the ion chamberconcentration is proportional to the current produced
PID Analyzers, LLC copyright 2003-2013
R + h = R+ + e
Analyzers
102+ PID
Optional
ppb mode (1-50,000 ppb) 1-3 additional sensors can be added for cost of sensor at time of purchase or later Sensors: CG or TCD, EC (select from > 20) Optional 9.5 & 11.7 Snap on Heads
PID Analyzers, LLC copyright 2003-2013
IP (eV)
Response
Response
Response
Detector
Methanol Acetonitrile Toluene THF Acetic Anhydride Dichloromethane Pyridine Benzene 10.85 11.72 8.83 9.45 10.35 11.35 9.32 9.25
10.6
0 0 9.3 6.2 0.9 0.2 6.1 10.0
11.7
2.3 1.3 11.4 6.3 4 6.8 7 10.0
FID
0.6 1.6 7 4.5 2.5 0.6 5 6
PID Assembly
102
Snap-On Modules
It is possible to have multiple heads for the 102+ or other models- (electronics for head are $350 plus sensors) CG, TCD & IR use the same circuit but are setup differently (current)-can have separate heads for each Unbiased EC sensors can be interchanged by customer, recalibrated then run Readout unit will recognize type of PID or type of WB/sensor
Sensor Board
Electronic Schematic
ADC Keyboard Display Diagnostics AMP 1-4 DAC to 0-1V Sensors RS232
CPU
Display board-Provides a display of the signal, errors, and functions Processor board-A 32 bit processor is used to control the A/D, cal, other functions Amplifier board-Signal from the ion chamber is amplified and sent to the processor board Connector board-Power in from charger, RS232 out and PID output connections Interface board-Provided the input/output from the processor board Low Voltage board-Power supply for HV board, pump, electronics High Voltage board-for PID-Supplies the voltage for the lamp and the bias for the ion chamber
Cal Menu
RS232
The digital input/output is the telephone jack in the base of the 102 A bluetooth option is available to connect wirelessly to a PC that is < 200 away The RS232 is used to connect to the PC to download data or display a continuous graph of the concentration of up to 4 sensors simultaneously the software on the PC should be the Grapher software that is included with the 102
Grapher Software
Included with portable analyzer Need RS232 Cable & Software Can graph ,print & save data from Analyzer Connect RS232 cable to PC Turn logging on Analyzer & setup Open Grapher and connect Setup grapher: logging, channels, range and components Save data as csv file, save configuration
Log Menu
Safety/IH Monitoring Emergency Response Area Monitoring VOCs+ LEL +Toxics Leak Detection for VOCs in chemical/petrochemical plants Transportation- Loading/Unloading Chemicals Monitoring Pilot Plants Laboratory Monitoring Short term; medium term monitoring- using the sleep mode
102+ Features/Specifications
Detector 1 for VOCs: PID 10.2, PID 11.7 Detector 2-4: CG, TCD, IR, electrochemistry LEL, TCD, Electrochemical ( select from >20) NEMA 2 Enclosure 10.75 L x 3 W x 2.25D Weight 1.9 pounds Linear to 0.1 to 3,000 ppm (10.2); 1-3,000 ppm for (11.7) LEL- 0-100%; O2 0-30%; Toxics- ppb-ppm LCD digital display Fast response- <1 sec VOCs; 15 sec. LEL; 10-60 sec Toxics
PID Analyzers, LLC copyright 2003-2013
PID- ppb CH1 PID- ppm or EC1 CH2 CG or TCD or IR or EC1 (Wheatstone bridge or voltage) CH3 O2 or EC2 (current or voltage) CH4 EC3 (biased or unbiased)
PID Analyzers, LLC copyright 2003-2013
Electrochemical Reactions
Electrochemical sensors generate a signal from oxidation/reduction reaction that is proportional to concentration
Electrochemical Sensors
range of sensors (20) and growing Instant on for portables Long lifetime sensors (typically 2 yrs.; some available up to 5 yrs.) Fast response Easy to interchange sensors or heads Up to 3 EC sensors in Model 1004
PID Analyzers, LLC copyright 2003-2013
Types of Sensors-LEL
LEL Two heated catalytic elements are set in a block; one is sealed; the other is in contact with the sample. Each is in a leg of a Wheatstone Bridge circuit. If the sample contains hydrocarbons or combustible inorganic compounds, they will burn increasing the temperature of the sensors and changing the resistance. The change in resistance is proportional to the concentration.
PID Analyzers, LLC copyright 2003-2013
Wheatstone bridge circuitry is used for a variety of sensors such as: Combustible Gas, Thermal Conductivity, Semiconductor and IR sensors
PID Analyzers, LLC copyright 2003-2013
in portable instruments (Model 102 & 102+) for leak detection (measurement in % range to 100%); compliments PID that measures from 0.1 to 3000 ppm Other uses for TCD (Model 204)are for continuous monitoring of H2, in large power plant transformers
PID Analyzers, LLC copyright 2003-2013
TCD Sensitivities
Features of TCD
Useful for measurement of compounds with thermal conductivity different from air (1.0) Easy to calibrate Can be turned off to maximize battery lifetime Cal values stored in RAM The thermal conductivity sensor has a library of 15 compounds. This allows the user to calibrate with one gas and via the library function, correct for response and LEL value for any of the > 15 gases in the library
PID Analyzers, LLC copyright 2003-2013
Sensor Configurations
Sensor 1 Sensor 2 Sensor 3 Sensor 4 PID or EC1 LEL,TCD or EC1 EC2- O2 EC2- other
The uP recognizes the proper sensor configuration and sets up the appropriate library for the sensor in each configuration
PID Analyzers, LLC copyright 2003-2013
Typical Users
Health & Safety- Director of Safety, Director of environmental health & safety, Safety officer, safety technician, industrial hygienist Plant- Instrumentation technician, Maintenance supervisor, Plant engineer Environmental consultants- Project manager, project engineer, field manager HVAC- Engineer or Maintenance Manager
PID sensor for VOCs Ability to have 4 sensors in a single analyzer LEL sensor for high levels >20 electrochemical sensors to choose from Ability to build your own Analyzer Compact size PC software for downloading
PID Analyzers, LLC copyright 2003-2013
Summary (cont.)
PID Analyzers has a very wide range of portable analyzers that can be used to measure: VOCs, O2, LEL, H2S, HCl, ETO, NO, NO2, SO2, CO, CO2, H2, PH3, SiH4, B2H6, Formaldehyde, HCN, NH3, AsH3, H2O, T
The Technologies include: PID, CG, TCD, IR, Electrochemistry (4 types- 30 different sensors ), Capacitance, RTD
PID Analyzers, LLC copyright 2003-2013