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M
f
1 A
f
100 5
where A
c
is ash content of clean coal, A
f
is ash content of
feed, M
c
is mass of clean coal and M
f
is mass of feed.
5. Results and discussion
A four-factor and ve-coded level CCRD was used to
determine the responses (ash content and combustible
recovery of clean coal). The four variables of MGS were
drum speed, tilt angle, wash water and feed solids. The
number of tests at the center points was six, making the
total number of tests required for the four independent
variables (drum speed, tilt angle, wash water and feed sol-
ids): 2
4
+ (2 4) + 6 = 30 [8].
The drum speed (v), tilt angle (a), wash water (w) and
feed solid (s) were independent variables studied to predict
y responses (ash content and combustible recovery of clean
coal). The four independent variables and their levels for
the CCRD used in this study are shown in Table 2.
Using the relationships in Table 2, coded and actual lev-
els of the variables for each of the experiments in the design
matrix were calculated as given in Table 3.
Considering the eects of main factors and also the
interactions between two-factor, Eq. (2) takes the form:
y b
0
b
1
x
1
b
2
x
2
b
3
x
3
b
4
x
4
b
11
x
2
1
b
22
x
2
2
b
33
x
2
3
b
44
x
2
4
b
12
x
1
x
2
b
13
x
1
x
3
b
14
x
1
x
4
b
23
x
2
x
3
b
24
x
2
x
x
b
34
x
3
x
4
6
The coecients, i.e. the main eect (b
i
) and two-factor
interactions (b
ij
) were estimated from the experimental data
obtained by computer simulation programming applying
least squares method using MATLAB 7.1.
From the experimental design in Table 3, experimental
results obtained listed in Table 4 and Eq. (4), the second-
order response functions representing ash content (y
1
)
and combustible recovery (y
2
) of clean coal can be
expressed as a function of four operating parameters of
the MGS, namely drum speed (v), tilt angle (a), wash water
(w) and solid (s). The relationship between responses (ash
content and combustible recovery of clean coal) and oper-
ating parameters were obtained for coded unit as follows:
For ash content of clean coal model equation:
y
1
22:62 1:46x
1
1:04x
2
0:45x
3
0:10x
4
1:08x
2
1
0:25x
2
2
0:23x
2
3
0:12x
2
4
1:52x
1
x
2
0:65x
1
x
3
0:14x
1
x
4
0:51x
2
x
3
0:22x
2
x
4
0:17x
3
x
4
7
Fig. 1. MGS experimental setup.
N. Aslan / Fuel 86 (2007) 769776 771
For combustible recovery of clean coal model equation:
y
2
76:41 3:07x
1
2:48x
2
1:52x
3
0:23x
4
2:49x
2
1
0:09x
2
2
0:40x
2
3
0:83x
2
4
3:57x
1
x
2
1:99x
1
x
3
0:50x
1
x
4
0:55x
2
x
3
0:50x
2
x
4
0:67x
3
x
4
8
The response factors at any regime in the interval of our
experiment design can be calculated from Eqs. (7) and (8).
Experimental results and the predicted values obtained
using model equations (Eqs. (7) and (8)) are given in Table
4 and Figs. 2 and 3. As can be seen, the predicted values
match the experimental values reasonably well, with R
2
of 0.84 for ash content and R
2
of 0.93 for combustible
recovery of clean coal.
5.1. Eect of variables of MGS on ash content
The three-dimensional (3D) response surface plots dem-
onstrate the eect of dierent variables of MGS on ash
content of the clean coal and they are depicted in
Fig. 4(af). The gures show the 3D response surface plots
relationship between two variables of MGS and ash con-
tent of the clean coal at center level of other two variables.
Fig. 4a shows the eect of drum speed and tilt angle on ash
content of clean coal at center level of wash water and
Table 2
Four independent variables of MGS and their levels for CCRD
Variable Symbol Coded variable level
Lowest Low Center High Highest
b 1 0 +1 +b
Drum speed (v), rpm x
1
175 200 225 250 275
Tilt angle (a), x
2
1 3 5 7 9
Wash water (w), lpm x
3
1 3 5 7 9
Solid (s), % x
4
10 20 30 40 50
Table 3
Coded and actual levels of four variables of MGS
Run Coded level of variables Actual level of variables
x
1
x
2
x
3
x
4
v (rpm) a () w (lpm) s (%)
1 1 1 1 1 200 3 3 20
2 1 1 1 +1 200 3 3 40
3 1 1 +1 1 200 3 7 20
4 1 1 +1 +1 200 3 7 40
5 1 +1 1 1 200 7 3 20
6 1 +1 1 +1 200 7 3 40
7 1 +1 +1 1 200 7 7 20
8 1 +1 +1 +1 200 7 7 40
9 +1 1 1 1 250 3 3 20
10 +1 1 1 +1 250 3 3 40
11 +1 1 +1 1 250 3 7 20
12 +1 1 +1 +1 250 3 7 40
13 +1 +1 1 1 250 7 3 20
14 +1 +1 1 +1 250 7 3 40
15 +1 +1 +1 1 250 7 7 20
16 +1 +1 +1 +1 250 7 7 40
17 b 0 0 0 175 5 5 30
18 +b 0 0 0 275 5 5 30
19 0 b 0 0 225 1 5 30
20 0 +b 0 0 225 9 5 30
21 0 0 b 0 225 5 1 30
22 0 0 +b 0 225 5 9 30
23 0 0 0 b 225 5 5 10
24 0 0 0 +b 225 5 5 50
25 0 0 0 0 225 5 5 30
26 0 0 0 0 225 5 5 30
27 0 0 0 0 225 5 5 30
28 0 0 0 0 225 5 5 30
29 0 0 0 0 225 5 5 30
30 0 0 0 0 225 5 5 30
772 N. Aslan / Fuel 86 (2007) 769776
solid. Noting that drum speed and tilt angle has a minor
eect on ash content of clean coal. However, it is worth
noting that a lower ash content of clean coal is obtained
at the center level of drum speed. Fig. 4b shows the eect
of drum speed and wash water on ash content of clean coal
at center level of tilt angle and solid. As can be seen in
Fig. 4b, ash content depends more on the drum speed
rather than on wash water. It is also worth noting that
lower ash content is obtained at the center level of drum
speed. Fig. 4c shows the eect of drum speed and solid
on ash content of clean coal at center level of tilt angle
and wash water. The general form of three-dimensional
relationship is similar to the previous gure. Fig. 4d shows
the eect of tilt angle and wash water on ash content at
center level of drum speed and solid. A minimum ash
Table 4
Observed and predicted values of ash content and combustible recovery
Run Variables Ash content, % Combustible recovery, %
v (rpm) a () w (lpm) s (%) Observed Predicted Observed Predicted
1 200 3 3 20 25.90 25.06 83.05 83.40
2 200 3 3 40 25.30 24.87 85.72 85.20
3 200 3 7 20 27.75 26.02 85.61 84.90
4 200 3 7 40 26.83 25.16 87.30 84.02
5 200 7 3 20 23.89 24.69 79.04 81.32
6 200 7 3 40 23.92 25.36 82.90 85.12
7 200 7 7 20 24.11 23.61 80.10 80.62
8 200 7 7 40 23.54 23.61 80.77 81.74
9 250 3 3 20 18.57 17.53 68.30 67.14
10 250 3 3 40 17.89 17.91 67.35 66.94
11 250 3 7 20 23.07 21.10 78.71 76.60
12 250 3 7 40 22.49 20.81 76.18 73.72
13 250 7 3 20 22.03 23.22 75.93 79.34
14 250 7 3 40 23.70 24.46 80.60 81.14
15 250 7 7 20 25.29 24.75 86.25 86.60
16 250 7 7 40 24.97 25.32 85.97 85.72
17 175 5 5 30 29.48 29.87 93.04 92.51
18 275 5 5 30 23.70 24.05 78.80 80.23
19 225 1 5 30 21.05 19.56 72.63 71.81
20 225 9 5 30 24.61 23.70 81.23 81.73
21 225 5 1 30 19.13 20.78 70.95 74.97
22 225 5 9 30 23.78 22.60 81.79 81.05
23 225 5 5 10 23.80 22.90 79.40 79.27
24 225 5 5 50 22.03 23.28 79.28 80.19
25 225 5 5 30 22.62 22.62 76.41 76.41
26 225 5 5 30 22.62 22.62 76.41 76.41
27 225 5 5 30 22.62 22.62 76.41 76.41
28 225 5 5 30 22.62 22.62 76.41 76.41
29 225 5 5 30 22.62 22.62 76.41 76.41
30 225 5 5 30 22.62 22.62 76.41 76.41
R
2
= 0.84
15
20
25
30
35
15 20 25 30 35
Ash content, (%)
Observed
A
s
h
c
o
n
t
e
n
t
,
(
%
)
P
r
e
d
i
c
t
e
d
Fig. 2. Relation between experimental and predicted ash content of clean
coal using Eq. (7).
R
2
= 0.93
60
65
70
75
80
85
90
95
100
60 65 70 75 80 85 90 95 100
Combustible recovery (%)
Observed
C
o
m
b
u
s
t
i
b
l
e
r
e
c
o
v
e
r
y
(
%
)
P
r
e
d
i
c
t
e
d
Fig. 3. Relation between experimental and predicted combustible recov-
ery using Eq. (8).
N. Aslan / Fuel 86 (2007) 769776 773
content is obtained with minimum level wash water at the
maximum tilt angle level. Fig. 4e shows the eect of tilt
angle and solid on ash content of clean coal at center level
of drum speed and wash water. The general form of three-
dimensional relationship is similar to the previous gure.
Ash content depends more on the tilt angle rather than
on solid. It is worth noting that lower ash content is
obtained at the maximum wash water level. Fig. 4f shows
the eect of wash water and solid on ash content of clean
coal at center level of drum speed and tilt angle. Noting
that wash water has a signicant eect on ash content of
clean coal whilst solid has a trivial eect.
5.2. Eect of variables of MGS on combustible recovery
Fig. 5(af) show the 3D response surface plots relation-
ship between two variables of MGS and combustible
recovery of clean coal at center level of other two variables.
Fig. 5a shows the eect of drum speed and tilt angle on
combustible recovery of clean coal at center level of wash
water and solid. As can be seen, maximum combustible
recovery is obtained with minimum level drum speed but
maximum tilt angle level. It can be also seen that the center
level of drum speed is not a good condition for getting
higher combustible recovery. Fig. 5b shows the eect of
-2
-1
0
1
2
-2
-1
0
1
2
10
15
20
25
30
Drum speed (v), rpm
Tilt angle (a),
A
s
h
c
o
n
t
e
n
t
,
%
-2
-1
0
1
2
-2
-1
0
1
2
22
22
24
26
28
30
32
Drum speed (v), rpm
Wash water (w), lpm
A
s
h
c
o
n
t
e
n
t
,
%
-2
-1
0
1
2
-2
-1
0
1
2
16
18
20
22
24
26
Drumspeed (v), rpm
Solid (s), %
A
s
h
c
o
n
t
e
n
t
,
%
-2
-1
0
1
2
-2
-1
0
1
2
10
15
20
25
30
Tilt angle (a),
Wash water (w), lpm
A
s
h
c
o
n
t
e
n
t
,
%
-2
-1
0
1
2
-2
-1
0
1
2
20
25
30
35
20
25
30
Tilt angle (a),
Solid (s), %
A
s
h
c
o
n
t
e
n
t
,
%
-2
-1
0
1
2
-2
-1
0
1
2
15
16
17
18
19
20
21
Wash water (w), lpm
Solid (s), %
A
s
h
c
o
n
t
e
n
t
,
%
Fig. 4. Response surface plots showing the eect of two variables on ash content of clean coal. Other two variables are held at center level. (a) Drum speed
and tilt angle; (b) drum speed and wash water; (c) drum speed and solid; (d) tilt angle and wash water; (e) tilt angle and solid; (f) wash water and solid.
774 N. Aslan / Fuel 86 (2007) 769776
drum speed and wash water on combustible recovery of
clean coal at center level of tilt angle and solid. The general
form of three-dimensional relationship is similar to the pre-
vious gure, however the eect of drum speed is more pow-
erful than previous. Fig. 5c shows the eect of drum speed
and solid on combustible recovery of clean coal at center
level of tilt angle and wash water. As can be seen from
Fig. 5c, combustible recovery depends more on the drum
speed rather than on solid. Fig. 5d shows the eect of tilt
angle and wash water on combustible recovery of clean
coal at center level of drum speed and solid. Both variables
have same eect on combustible recovery of clean coal.
As the tilt angle is increased, combustible recovery is
increased, just as wash water. Fig. 5e shows the eect of tilt
angle and solid on combustible recovery of clean coal at
center level of drum speed and wash water. Noting that,
as the tilt angle is increased, combustible recovery is
increased steadily, noting also that center level of solid is
not good for getting a higher combustible recovery. Fig. 5f
shows the eect of wash water and solid on combustible
recovery of clean coal at center level of drum speed and tilt
angle. Noting that the general form of three-dimensional
-2
-1
0
1
2
-2
-1
0
1
2
60
70
80
90
100
Drum speed (v), rpm
Tilt angle (a),
C
o
m
b
u
s
t
i
b
l
e
r
e
c
o
v
e
r
y
,
%
-2
-1
0
1
2
-2
-1
0
1
2
50
60
70
80
90
100
Drum speed (v), rpm
Wash water (w), lpm
C
o
m
b
u
s
t
i
b
l
e
r
e
c
o
v
e
r
y
,
%
-2
-1
0
1
2
-2
-1
0
1
2
65
70
75
80
85
90
Drum speed (v), rpm
Solid (s), %
C
o
m
b
u
s
t
i
b
l
e
r
e
c
o
v
e
r
y
,
%
-2
-1
0
1
2
-2
-1
0
1
2
65
70
75
80
85
Tilt angle (a),
Wash water (w), lpm
C
o
m
b
u
s
t
i
b
l
e
r
e
c
o
v
e
r
y
,
%
-2
-1
0
1
2
-2
-1
0
1
2
50
60
70
80
90
Tilt angle (a),
Solid (s), %
C
o
m
b
u
s
t
i
b
l
e
r
e
c
o
v
e
r
y
,
%
-2
-1
0
1
2
-2
-1
0
1
2
60
62
64
66
68
70
72
Wash water (w), lpm
Solid (s), %
C
o
m
b
u
s
t
i
b
l
e
r
e
c
o
v
e
r
y
,
%
Fig. 5. Response surface plots showing the eect of two variables on combustible recovery of clean coal. Other two variables are held at center level. (a)
Drum speed and tilt angle; (b) drum speed and wash water; (c) drum speed and solid; (d) tilt angle and wash water; (e) tilt angle and solid; (f) wash water
and solid.
N. Aslan / Fuel 86 (2007) 769776 775
relationship is similar to the previous gure. Namely, as the
wash water is increased, combustible recovery is increased
progressively, noting also that center level of solid is not
good condition to be obtained a higher combustible recov-
ery but the extreme levels of solid are good for combustible
recovery.
6. Summary and conclusions
The application of response surface methodology (RSM)
and central composite rotatable design (CCRD) for model-
ing the inuence of some operating variables on the perfor-
mance of the Multi-Gravity Separator (MGS) treating coal
has been discussed.
The central composite rotatable design (CCRD) was
used to design an experimental program to provide data
to model the eects of drum speed, tilt angle, wash water
and feed solids on the performance of Multi-Gravity Sepa-
rator treating coal from Yenicubuk/Turkey lignite coal
containing approximately 36.1% ash. The ranges of values
of variables of MGS used in the design were; drum speed:
175275 rpm, tilt angle: 19, wash water: 19 lpm and feed
solids: 1050%. A total of 30 tests including center points
were conducted. The mathematical model equations were
derived for both ash content and combustible recovery by
using sets of experimental data and a mathematical soft-
ware package (MATLAB 7.1).
The predicted values match the experimental values rea-
sonably well, with R
2
of 0.84 for ash content and R
2
of 0.93
for combustible recovery of clean coal.
In order to gain a better understanding of the eect of
the variables of MGS on ash content and combustible
recovery of clean coal, the predicted models were presented
three-dimensional (3D) response surface graphs.
This study demonstrates that the central composite
rotatable design (CCRD) and response surface methodol-
ogy (RSM) can be successfully used for modeling the some
operating parameters of Multi-Gravity Separator for Yen-
icubuk/Turkey coal and that it is economical way of
obtaining the maximum amount of information in a short
period of time and with the fewest number of experiments.
References
[1] Aslan N, Canbazoglu M. Processing of thickener underow from
celestite concentrator by Multi-Gravity Separator. In: Kemal M,
Arslan V, Akar A, editors. Changing scopes in mineral process-
ing. A.A Balkema; 1996. p. 1036.
[2] O