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A Thermal and Moisture Transport Property Database for Common

Building and Insulating Materials



Final Report from ASHRAE Research Project 1018-RP



Principal Investigator : Mavinkal K Kumaran

Key Researchers: John C Lackey
Nicole Normandin
Fitsum Tariku
David van Reenen

04 July 2002
2


Table of Content Page No.
Executive Summary 4
Examples of Applications of Various Test Methods:
Hygrothermal Properties of Aerated Concrete and Gypsum Board 12
Hygrothermal Properties of OSB 1 29
Hygrothermal Properties of OSB 2 36
Hygrothermal Properties of OSB 3 43
Hygrothermal Properties of Plywood 1 50
Hygrothermal Properties of Plywood 2 57
Hygrothermal Properties of Plywood 3 64
Hygrothermal Properties of Fibreboard 71
Hygrothermal Properties of Eastern White Cedar 78
Hygrothermal Properties of Western Red Cedar 85
Hygrothermal Properties of Spruce 92
Hygrothermal Properties of Eastern White Pine 99
Hygrothermal Properties of Southern Yellow Pine 106
Hygrothermal Properties of Composite Wood Siding 113
Hygrothermal Properties of Clay Brick 120
Hygrothermal Properties of Mortar 127
Hygrothermal Properties of Stucco 134
Hygrothermal Properties of Fibre Cement Board 141
Hygrothermal Properties of Cement Board 148
Hygrothermal Properties of Lime Stone 154
Hygrothermal Properties of Low-density Glassfibre Batt Insulation 160
Hygrothermal Properties of Cellulose Insulation 164
Hygrothermal Properties of Expanded Polystyrene Insulation 169
Hygrothermal Properties of Extruded Polystyrene Insulation 173
Hygrothermal Properties of Spray Polyurethane Foam Insulation 176
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Hygrothermal Properties of Polyisocyanurate Insulation 179
Hygrothermal Properties of Low-density Polyurethane Foam Insulation 182
Hygrothermal Properties of #15 Felt 186
Hygrothermal Properties of 10 min Paper 189
Hygrothermal Properties of 30 min Paper 192
Hygrothermal Properties of 60 min Paper 195
Hygrothermal Properties of Spun Bonded Polyolefin Membrane 198
Hygrothermal Properties of Bonded Polyolefin Membrane (Crinkled ) 201
Hygrothermal Properties of Vinyl Wallpaper 204
Hygrothermal Properties of Primer and Latex paint 207
Hygrothermal Properties of EIFS Base Coat and Finish Coat 214

Appendix I: How Well Should One Know the Hygrothermal Properties of Building
Materials ? 217

Appendix II: Experimental and Analytical Investigations on the Drying Processes
Undergone by Aerated Concrete. 223

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EXECUTIVE SUMMARY


This report presents results from a set of hygrothermal tests that were systematically
carried out on many building materials that are currently used in North America. The materials
include several wood based products, several species of wood, masonry products, cladding
materials, sheathing membranes, insulation products, one limestone, a primer and a latex paint
and a vinyl wallpaper. The properties that were determined include thermal conductivity,
equilibrium moisture content, water vapour permeance or permeability, water absorption
coefficient, moisture diffusivity and air permeance or permeability. Test conditions and details on
test specimens are given for each test. Many sets of primary data as well as their uncertainties
are reported. Also, wherever possible results are statistically analyzed to estimate probable
uncertainties in the derived values of various hygrothermal properties.


Principal Investigator:
Kumar Kumaran
Principal Research Officer
Building Envelope and Structure Program
Institute for Research in Construction
National Research Council Canada
Ottawa, Ontario K1A 0R6
Canada

kumar.kumaran@nrc.ca
Phone: 613 993 9611


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1. INTRODUCTION
ASHRAE Research project 1018-RP, Thermal and Moisture Transport Property
Database for Common Building and Insulating Materials was implemented to generate a set of
reliable and representative data on the hygrothermal properties of 30 common building materials.
Hygrothermal properties govern the details of heat, air and moisture transport through building
materials. A comprehensive list of the properties can be found in the project report B-1115.3
dated 1 April 1999 that was issued to ASHRAE from the Institute for Research in Construction.
That report also contains the definitions of the properties.
The project has now generated information on several hygrothermal properties of 38
materials. The properties that are compiled in this report include:
Dry density
Heat capacity
Thermal conductivity
Equilibrium moisture content (Sorption, Desorption and Pressure Plate Measurements)
Water vapour permeance or permeability
Water absorption coefficient
Moisture diffusivity and
Air permeance or permeability

Well-developed experimental procedures or international standard test procedures exist
to determine the properties listed above. The principles of the experimental procedures that are
used to determine the hygrothermal properties of building materials in the present investigation
are given below. Heat capacity data that are reported here are taken from a document published
by the International Energy Agency Annex 24 [1]. Density data reported here are the averages of
the densities of many test specimens (conditioned to laboratory environment, approximately
21 C and 50 % RH) for each material, calculated from direct measurements on the weight and
on the geometric dimensions that are used to characterize each test specimen. Further details on
each experimental procedure and data analyses may be found in the project report referred to
above.


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Thermal Conductivity of Dry Materials
The heat conduction equation is directly used to determine the thermal conductivity of dry
materials. Equipment that can maintain a known unidirectional steady state heat flux (under
known constant boundary temperatures) across a flat slab of known thickness is used for the
measurements. The most commonly used equipment is the guarded hot plate apparatus or the
heat flow meter apparatus. ASTM Standards C 177, Standard Test Method for Steady-State Heat
flux Measurements and Thermal Transmission Properties by Means of the Guarded-Hot-Plate
Apparatus and C518, Standard Test Method for Steady-State Heat flux Measurements and
Thermal Transmission Properties by Means of the Heat Flow Meter Apparatus are widely used
for this purpose. The latter is used in the present investigation. Similar standards are available
from the International Standards Organization and the European Union. In the ASTM Standards,
the heat conduction equation is written for practical applications as:
! = Q"l/(A"#T) (1)
Where,
Q = Heat flow rate across an area A
l = Thickness of test specimen
#T = Hot surface temperature Cold surface temperature
The thermal conductivity calculated according to (1) is called apparent thermal
conductivity. It is a function of the average temperature of the test specimen.
Equilibrium Moisture Content from Sorption/Desorption Measurements
For sorption measurements, the test specimen is dried at an appropriate drying
temperature to constant mass. While maintaining a constant temperature, the dried specimen is
placed consecutively in a series of test environments, with relative humidity increasing in stages,
until equilibrium is reached in each environment. Equilibrium in each environment is confirmed by
periodically weighing the specimen until constant mass is reached. From the measured mass
changes, the equilibrium moisture content at each test condition can be calculated and the
adsorption isotherm drawn.
The starting point for the desorption measurements is from an equilibrium condition very
near 100% RH. While maintaining a constant temperature, the specimen is placed consecutively
in a series of test environments, with relative humidity decreasing in stages, until equilibrium is
reached in each environment. Equilibrium in each environment is confirmed by periodically
weighing the specimen until constant mass is reached. Finally, the specimen is dried at the
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appropriate temperature to constant mass. From the measured mass changes, the equilibrium
moisture content at each test condition can be calculated and the desorption isotherm drawn.
A new CEN standard 89 N 337 E is under development for the determination of
Hygroscopic Sorption Curve. ASTM C16 Committee also is developing a standard.
Equilibrium Moisture Content from Pressure Plate (Desorption) measurements:
The test specimens are saturated with water under vacuum. Those are then introduced in
a pressure plate apparatus that can maintain pressures up to 100 bar for several days. The plates
in perfect hygric contact with the specimens extract water out of the pore structure until an
equilibrium state is established. The equilibrium values for moisture contents in the specimens
and the corresponding pressures (measured as the excess over atmospheric pressure; the
negative of this value is referred to as the pore pressure while the absolute value is the suction)
are recorded. The equilibrium pressure, p
h,
can be converted to a relative humidity, $, using the
following equation:
h
p
!RT
M
ln % & $ (4)
Where,
M = the molar mass of water
R = the ideal gas constant
T = the thermodynamic temperature and
' = the density of water
A Nordtest Technical Report [6] briefly describes a procedure for pressure plate
measurements and reports the results from an interlaboratory comparison. No standard
procedure is yet developed for the determination of suction isotherm.
Water Vapour Permeability/Permeance
The vapour diffusion equation is directly used to determine the water vapour permeability
of building materials [2]. The measurements are usually done under isothermal conditions. A test
specimen of known area and thickness separates two environments that differ in relative humidity
(rh). Then the rate of vapour flow across the specimen, under steady-state conditions (known rhs
as constant boundary conditions), is gravimetrically determined. From these data the water
vapour permeability of the material is calculated as:
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(
p
= J
v
"l/(A"#p) (2)
Where,
J
v
= Water vapour flow rate across an area A
l = Thickness of the specimen
#p = Difference in water vapour pressure across the specimen surfaces
Often, especially for membranes and composite materials, one calculates the water
vapour permeance, (
l
, of a product at a given thickness from the above measurements as:
(
l
= J
v
/(A"#p) (3)
ASTM Standard E96, Test Methods for Water Vapour Transmission of Materials,
prescribes two specific cases of this procedure- a dry cup method that gives the permeance or
permeability at a mean rh of 25 % and a wet cup method that gives the permeance or
permeability at a mean rh of 75 %. A new CEN Standard 89 N 336 E is being developed in the
European Union based on ISO standard. More recently a number of technical papers that deal
with various technical aspects, limitations and analyses of the experimental data of these
procedures have appeared in the literature [3-5].
For many hygroscopic materials, such as wood and wood products, the water vapour
permeability/permeance is a strong function of the local relative humidity and increases with rh.
The ASTM Standard E 96 is being revised to address this behaviour of building materials more
quantitatively. For practical building applications, in addition to the traditional dry and wet cup
conditions, it is desirable to determine the permeance or permeability of hygroscopic materials at
a mean rh of 85 %. This can be done using the wet cup method of E96, but the rh in the humidity
chamber shall be maintained at 70 %.
Water Absorption Coefficient:
One major surface of each test specimen is placed in contact with liquid water. The
increase in mass as a result of moisture absorption is recorded as a function of time. Usually,
during the initial part of the absorption process a plot of the mass increase against the square
root of time is linear. The slope of the line divided by the area of the surface in contact with water
is the water absorption coefficient
1
.

1
When this method was applied to membranes, the membranes were put in perfect hygric contact with a
substrate such as OSB.
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A new CEN Standard 89 N 370 E on the determination of water absorption coefficient is
under development.
Moisture Diffusivity:
Moisture diffusivity, D
w
, defines the rate of movement of water, J
l
, within a material,
induced by a water concentration gradient according to the following equation:
J
l
= - '
0
D
w
grad u (5)
Where,
'
0
= density of the dry material
u = moisture content expressed as mass of water / dry mass of material
In the experimental procedure, liquid water in contact with one surface of a test specimen
is allowed to diffuse into the specimen. The distribution of moisture within the specimen is
determined as a function of time at various intervals until the moving moisture front advances to
half of the specimen. Gamma spectroscopy is used as the experimental technique. The data are
analyzed using the Boltzmann transformation [7,8 ] to derive the moisture diffusivity as a function
of moisture content.
There is no standard test procedure for the determination of moisture diffusivity. There
are many publications in the literature that describe the technical and experimental details [9-12].

Air Permeability/ Permeance:
Test specimens with known areas and thickness are positioned to separate two regions
that differ in air pressure and the airflow rate at a steady state and the pressure differential across
the specimen are recorded. From these data the air permeability, k
a
is calculated as:
k
a
= J
a
"l/(A"#p) (6)
Where,
J
a
= Air flow rate across an area A
l = Thickness of the specimen
#p = Difference in air pressure across the specimen surfaces
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Often, especially for membranes and composite materials, one calculates the air
permeance, K
a
, of a product at a given thickness from the above measurements as:
K
a
= J
a
/(A"#p) (7)
ASTM Standard C 522, Standard Test Method for Airflow Resistance of Acoustical
Materials prescribes a method based on this principle. Bomberg and Kumaran[13] have extended
the method for general application to building materials.
References
1. M K Kumaran, Final Report, Volume 3, Material Properties, International Energy Agency
Annex 24 Report, Published by K. U. Leuven Belgium, 1996.
2. Joy F. A. and Wilson, A. G., Standardization of the Dish Method for Measuring Water
Vapour Transmission, Proceedings of the International Symposium on Humidity and
Moisture, Washington, D. C., Vol. 4, Chapter 31, 1963, pp 259-270.
3. Hedenblad, G., Moisture Permeability of Some Porous Building Materials, Proceedings of
the 4th Symposium, Building Physics in the Nordic Countries, Espoo,Volume 2, 1996, 747-
754.
4. Hansen, K. K. and Lund, H. B., Cup Method for Determination of Water Vapour
Transmission Properties of Building Materials. Sources of Uncertainty in the Method,
Proceedings of the 2nd Symposium , Building Physics in the Nordic Countries, Trondheim,
1990, pp 291-298.
5. Lackey, J. C., Marchand, R. G., and Kumaran, M. K., A Logical Extension of the ASTM
Standard E96 to Determine the Dependence of Water Vapour Transmission on Relative
Humidity, Insulation Materials: Testing And Applications: Third Volume, ASTM STP 1320, R.
S. Graves and R. R. Zarr, Eds, American Society for Testing and Materials, West
Conshohocken, PA, 1997, pp 456-470. Also Kumaran, M. K., An Alternative Procedure for
the Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581,
1998.
6. Hansen, M. H., "Retention Curves Measured Using Pressure Plate and Pressure Membrane,"
Nordtest Technical Report 367, Danish Building Research Institute, 1998, p 63.
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7. Bruce, R. R. and Klute, A, "The Measurement of Soil Diffusivity," Soil Science Society of
America Proceedings. Vol. 20, pp. 251-257, 1956.
8. Kumaran, M.K., Mitalas, G.P., Kohonen, R., Ojanen, T, "Moisture transport coefficient of pine
from gamma ray absorption measurements," Collected Papers in Heat Transfer, 1989 :
Winter Annual Meeting of the ASME (San Francisco, CA, USA, 1989) pp. 179-183,
1989(ASME Heat Transfer Division vol. 123).
9. Marchand, R.G. and Kumaran, M. K., "Moisture diffusivity of cellulose insulation," Journal of
Thermal Insulation and Building Envelopes, Vol. 17, pp. 362-377, 1994.
10. Kumaran, M.K. and Bomberg, M.T., "A Gamma-spectrometer for determination of density
distribution and moisture distribution in building materials," Moisture and Humidity:
Measurement and Control in Science and Industry : Proceedings of International Symposium
(Washington, D.C., USA, 1985), pp. 485-90, 1985.
11. Filip Descamps., "Continuum and Discrete Modelling of Isothermal Water and Air Transfer in
Porous Media," Ph. D. Thesis, Katholieke Uniersity, Belgium, pp. 57-107, 1997.
12. Pel, L., "Moisture Transport in Porous Building Materials," Ph. D. Thesis, Eindhoven
University of Technology, the Netherlands, pp. 47-80, 1995.
13. Bomberg, M. T.and Kumaran, M.K., " A Test method to determine air flow resistance of
exterior membranes and sheathings," Journal of Thermal Insulation, Vol.9, pp. 224-
235,1986.

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2. Examples of Applications of Various Methods to determine
the Hygrothermal Properties of Aerated Concrete and Interior
Gypsum Board.




The test conditions reported in this section for different test methods are
generally followed throughout the project. Also, the procedures used in this
section for data reduction and analyses are followed for all materials in this
report.


A: Aerated Concrete

The test specimens used for various measurements reported
here are taken from one block of aerated concrete,
approximately 1 X 1 x 1.5 in size.

Density: (460 ) 15) kg m
-3


Heat Capacity (According to International Energy Agency Annex 24 Report
2
): 840 J K
-1
kg
-1


Thermal Conductivity:
Measurements are according to ASTM Standard C518; 30 cm X 30cm specimens are used in
these measurements. The temperatures of the plates are maintained within 0.02 C for these
measurements, for 12 h period to confirm steady state.
Table 2.1. Thermal Conductivity of Aerated Concrete.
Specimen Thickness
mm
Hot Surface Temperature
C
Cold Surface Temperature
C
Conductivity
W m
-1
K
-1

24.24 31.51 9.75 0.121
24.24 11.45 -2.44 0.119

Note: The heat flow meter apparatus is built to measure the heat transmission characteristics of
insulating materials and for those materials the measurement uncertainties are within 2 %;
aerated concrete is more conductive than traditional insulation and the large heat fluxes
measured may give measurement uncertainties as high as 5 %.

2
M K Kumaran, Final Report, Volume 3, Material Properties, International Energy Agency
Annex 24 Report, Published by K. U. Leuven Belgium, 1996
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Sorption Desorption Measurements
3
:
Either eight specimens, 40 mm X 40 mm X 20 mm each, or six specimens 40 mm X 40 mm X 6
mm each or three specimens, 40 mm X 40 mm X 6 mm each are used in these measurements;
the numbers in parentheses indicate the experimental uncertainties.
Sorption:
Table 2. Sorption data for Aerated Concrete.
RH, % Temperature, C Moisture Content, kg kg
-1

100, total saturation Lab at 22 (1) 1.72 (0.01), eight specimens
100, capillary saturation,
after 72 h immersion
Lab at 22 (1) 0.83 (0.02), six specimens
88.1 (1) 23.0 (0.1) 0.050 (0.002), three specimens
71.5 (1) 23.0 (0.1) 0.021 (0.001), three specimens
50.6 (1) 23.0 (0.1) 0.011 (0.001), three specimens

Desorption:
Table 3. Desorption data for Aerated Concrete.
RH, % Temperature, C Moisture Content, kg kg
-1

99.99 (0.01) Lab at 22 (1) 0.92 (0.13), eight specimens
99.98 (0.01) Lab at 22 (1) 0.81 (0.09), eight specimens
99.96 (0.01) Lab at 22 (1) 0.77 (0.07), eight specimens
99.93 (0.01) Lab at 22 (1) 0.75 (0.06), eight specimens
99.85 (0.01) Lab at 22 (1) 0.72 (0.05), eight specimens
99.78 (0.01) Lab at 22 (1) 0.70 (0.05), eight specimens
99.71(0.01) Lab at 22 (1) 0.68 (0.04), eight specimens
99.63 (0.01) Lab at 22 (1) 0.66 (0.04), eight specimens
99.47(0.01) Lab at 22 (1) 0.64 (0.04), eight specimens
98.90 (0.01) Lab at 22 (1) 0.55 (0.02), six specimens
97.81 (0.01) Lab at 22 (1) 0.34 (0.05), six specimens
88.1 (1) 23.0 (0.1) 0.063 (0.001), three specimens
71.5 (1) 23.0 (0.1) 0.022 (0.001), three specimens
50.6 (1) 23.0 (0.1) 0.011 (0.001), three specimens
Throughout this document, results from the pressure plate measurements are listed as desorption
data above 95 % RH.

3
In the hygroscopic range, the measurements are done using the proposed procedure for ASTM
Standard C1498, which in turn is based on CEN 89 N 337 E, Hygroscopic Sorption Curve; at
the higher range the pressure plate method is used. Details of the pressure plate method are
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Water Vapour Transmission (WVT) Rate measurements
4
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used.

Table 2.4. Dry Cup Measurements on Aerated Concrete Specimens: The numbers in
parentheses indicate the experimental uncertainties for RH and temperature and standard errors
for WVT rate, obtained from statistical analyses of the data at a steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

20.11 50.6 (1) 22.9 (0.1) 1.09E-06 (5.5E-09)
20.56 50.6 (1) 22.9 (0.1) 1.14E-06 (5.6E-09)
20.44 50.6 (1) 22.9 (0.1) 1.03E-06 (4.0E-09)
20.11 71.5 (1) 22.7 (0.1) 1.69E-06 (6.0E-09)
20.56 71.5 (1) 22.7 (0.1) 1.79E-06 (3.3E-09)
20.44 71.5 (1) 22.7 (0.1) 1.63E-06 (5.3E-09)
20.11 88.1 (1) 23.3 (0.1) 2.18E-06 (6.5E-09)
20.56 88.1 (1) 23.3 (0.1) 2.30E-06 (4.4E-09)
20.44 88.1 (1) 23.3 (0.1) 2.23E-06 (5.6E-09)



Table 2.5. Wet Cup Measurements on Aerated Concrete Specimens: The numbers in
parentheses indicate the experimental uncertainties for RH and temperature and standard errors
for WVT rate, obtained from statistical analyses of the data at a steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

20.29 71.7 (1) 22.7 (0.1) 1.30E-06 (1.7E-08)
20.34 71.7 (1) 22.7 (0.1) 1.40E-06 (1.4E-08)
20.11 71.7 (1) 22.7 (0.1) 1.49E-06 (1.5E-08)
20.29 87.8 (1) 23.2 (0.1) 1.13E-06 (1.5E-08)
20.34 87.8 (1) 23.2 (0.1) 9.60E-07 (1.0E.08)
20.11 87.8 (1) 23.2 (0.1) 9.69E-07 (1.0E.08)


The average thickness of still air in the cups in both series is 11 mm

given by: Hansen, M. H., "Retention Curves Measured Using Pressure Plate and Pressure
Membrane," Nordtest Technical Report 367, Danish Building Research Institute, 1998, p 63.
4
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M. K.,
A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water Vapour
Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
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Derived Water Vapour Permeability
5



Table 2.6. The dependence of water vapour permeability of Aerated Concrete on relative
humidity.

RH, % Permeability
kg m
-1
s
-1
Pa
-1

RH, % Permeability
kg m
-1
s
-1
Pa
-1

10
1.12E-11
60
2.76E-11
20
1.33E-11
70
3.34E-11
30
1.59E-11
80
4.07E-11
40
1.91E-11
90
5.00E-11
50
2.29E-11
100
6.21E-11



The relation between WVT rate and Chamber RH is shown in Figure 1.

Rank 1 Eqn 8002 [Exponential] y=a+bexp(-x/c)
r
2
=0.993 DF Adj r
2
=0.992 FitStdErr=1.17e-07 Fstat=965
a=-7.41e-07 b=7.54e-07 c=-61.21
0 20 40 60 80 100
CHAMBER RH, %
0
5e-07
1e-06
1.5e-06
2e-06
2.5e-06
3e-06
3.5e-06
W

V

T

R
a
t
e
,

k
g

m
-
2

s
-
1


Figure 2.1. All data are interpreted as dry cup measurements; RH inside the cup is zero and
chamber RH is the RH outside the cup.

5
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

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The numeric summary of the analyses is listed below. The commercial software package called
TabbleCurve2 is used for the curve fit. The terminology below is from the package.

The equation that represents the relation between x = chamber RH and y = WVT rate is
[Exponential] y= a + b exp(-x/c)

r
2
, Coefficient of Determination = 0.993
Fit Std Error = 1.7E-07
F-value = 965

Parameter. Value Std Error t-value 90% Confidence Limits
a -7.41e-07 2.1e-07 -3.5 -1.12e-06 -3.69e-07
b 7.54e-07 1.9e-07 4.0 4.23e-07 1.08e-06
c -61.2 7.5 -8.1 -74.5 -47.9


From the above statistics, the estimated uncertainty in the derived value of the permeability may
be up to 28 %.

Note that all water vapour transmission data are combined to give one curve in Figure 2.1, and
dry cup and wet cup measurements are not independently analyzed. This approach is the same
as that described and applied to the plywood data in the reference document: Kumaran, M. K.,
An Alternative Procedure for the Analysis of Data from the Cup Method Measurements for
Determination of Water Vapour Transmission Properties, Journal of Testing and Evaluation,
JTVEA, Vol. 26 , pp. 575-581, 1998.
This same approach is followed throughout this document.



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Water Absorption Coefficient
6
:

Five test specimens, 5 cm X 5 cm X 5 cm each, were used in these measurements. Water is
maintained at (22 1) C. The numbers in parentheses give the standard deviations.

Table 2.7. Water absorption data for Aerated Concrete.

Square Root of
time, s


Water Absorption
kg m
-2

7.75 0.93 (0.13)
13.42 1.24 (0.17)
17.32 1.41 (0.21)
24.49 1.73 (0.25)
30.00 1.96 (0.29)
38.73 2.29 (0.34)
45.83 2.55 (0.37)
54.77 2.87 (0.44)
64.81 3.20 (0.47)
73.48 3.48 (0.53)
81.24 3.71 (0.56)
91.65 4.05 (0.62)
101.00 4.31 (0.69)

Linear regression using all the data from the first linear part of the absorption process for the five
specimens gives:

Water Absorption Coefficient for the major surfaces = 0.036 0.002 kg m
-2
s
-
.


6
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
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Moisture Diffusivity:

Gamma ray method
7
is used to measure the distribution of moisture in three test
specimens, 5 cm X 23 cm X 2.4 cm each, during the moisture uptake through the edge. The
principle of the methodology is described by Kumaran et. al
8
. Marchand and Kumaran
9
have
reported the procedure used for the data reduction.

The running average method that is described by Marchand and Kumaran gives the
characteristic curve shown in Figure 2, for this aerated concrete. Several hundreds of data pairs
obtained on the three test specimens, in 36 sets of measurements over a period of seven days
are included in the analysis.

0
50
100
150
200
250
300
0 0.0001 0.0002 0.0003 0.0004 0.0005 0.0006
Running Avg. Boltzmann Variable, m s
-
R
u
n
n
i
n
g

A
v
g
.

M
o
i
s
t
u
r
e

C
o
n
t
e
n
t
,

k
g

m
-
3


Figure 2.2. The characteristic curve for aerated concrete resulted from moisture uptake
and distribution measurements.

7
Kumaran, M.K. and Bomberg, M.T., "A Gamma-spectrometer for determination of density
distribution and moisture distribution in building materials," Moisture and Humidity: Measurement
and Control in Science and Industry : Proceedings of International Symposium (Washington,
D.C., USA, 1985), pp. 485-90, 1985.
8
Kumaran, M.K., Mitalas, G.P., Kohonen, R., Ojanen, T, "Moisture transport coefficient of pine
from gamma ray absorption measurements," Collected Papers in Heat Transfer, 1989 : Winter
Annual Meeting of the ASME (San Francisco, CA, USA, 1989) pp. 179-183, 1989(ASME Heat
Transfer Division vol. 123).
9
Marchand, R.G. and Kumaran, M. K., "Moisture diffusivity of cellulose insulation," Journal of
Thermal Insulation and Building Envelopes, Vol. 17, pp. 362-377, 1994.
B1115.13

19




The moisture diffusivity derived from the above characteristic curve is given in Table 8.

Table 2.8. The dependence of moisture diffusivity of Aerated Concrete on moisture content.

Moisture Content
kg kg
-1

Diffusivity
m
2
s
-1

Moisture Content
kg kg
-1

Diffusivity
m
2
s
-1

0.087 8.72E-09 0.326 3.44E-09
0.109 5.47E-09 0.348 3.64E-09
0.130 4.32E-09 0.370 3.91E-09
0.152 3.76E-09 0.391 4.29E-09
0.174 3.44E-09 0.413 4.81E-09
0.196 3.26E-09 0.435 5.56E-09
0.217 3.16E-09 0.457 6.71E-09
0.239 3.12E-09 0.478 8.71E-09
0.261 3.13E-09 0.500 1.3E-08
0.283 3.19E-09 0.522 2.89E-08
0.304 3.29E-09 0.543 5.15E-08

Note: The area enclosed by the characteristic curve in Figure 2 is ~ 0.033 kg m
-2
s
-
and
this value is very close to the water absorption coefficient = 0.036 kg m
-2
s
-
that was directly
determined. This should be the case and the correspondence between the two shows the internal
consistency of the two methods. However, the uncertainty in the derived moisture diffusivity is
estimated to be as high as 30 to 50 %.
The diffusivity derived from moisture distribution data during a water uptake process may
not quantitatively describe a drying process for all building materials. Earlier works at the Institute
for Research in Construction show that for a cement-based sheathing board
10
and for several
OSB test specimens under various boundary conditions
11
the drying process is reasonably well
described using the diffusivity that has been derived from a water uptake process.
For the present investigation, two series of drying experiments were conducted on this
same aerated concrete. Details of these investigations are given in Appendix II. Both series of
investigations reported there suggest that the diffusivity determined from a wetting process
describes the drying process with reasonable accuracy.

10
See Appendix I
11
Maref, W., Kumaran, M. K., Lacasse, M. A., Swinton, M. C. and van Reenen, D. Laboratory
Measurements and Benchmarking of an Advanced Hygrothermal Model. Accepted for
publication: 12
th
International Heat Transfer Conference, August 18-23, 2002, Grenoble (France).

B1115.13

20


Air Permeability:
Bomberg and Kumaran
12
have reported the principle of the method used in these
measurements. Appendix XIII of the Client Report to ASHRAE, B-1115.3 A Thermal and
Moisture Transport Property Database for Common Building and Insulating Materials 1018-RP
dated 1 April 1999 reports the details. Three circular test specimens (thickness 20.29 mm, 20.56
mm, 20.34 mm), each approximately 15 cm in diameter, are used in these measurements. The
measurements are conducted at a temperature = (22 1) C.
The summary of the statistical analyses of all data obtained from two series of
measurements on each specimen is shown in Figure 3 as three separate sets.
0
0.05
0.1
0.15
0.2
0.25
0 100 200 300 400 500 600 700 800
Pressure Difference (Pa)
F
l
o
w

,

l

m
-
2

s
-
1
Data Points Mean Permeance
Upper Confidence Interval Lower Confidence Interval

Figure 2.3. The dependence of airflow rate on pressure difference for aerated concrete.

For the range of pressure differences between 25 Pa and 700 Pa, the flow rate linearly
varies with the pressure difference. The air permeability is (4.9 2.6) E-09 kg m
-1
Pa
-1
s
-1
.

12
Bomberg, M. T. and Kumaran, M.K., " A Test method to determine air flow resistance of
exterior membranes and sheathings," Journal of Thermal Insulation, Vol.9, pp. 224-235,1986.
B1115.13

21



B: Interior Gypsum Board

The test specimens used for various measurements reported here are
taken from 4 X 8 sheets of a commercial product with a nominal thickness
of . A paper layer is adhered to the major surfaces and all test
specimens included this paper layer. Labels on the product say the
following: Manufactured to exceed standards Can/CSA-A82.27 and ASTM
C 36.


Thickness: (12.50 ) 0.03) mm

Density: (625 ) 7) kg m
-3


Heat Capacity (From International Energy Agency Annex 24 Report
13
): 870 J K
-1
kg
-1


Thermal Conductivity:
Measurements are according to ASTM Standard C518; 30.6 cm X 30.6 cm specimens are used
in these measurements. The temperatures of the plates are maintained within 0.05 C for these
measurements, for 12 h period to confirm steady state.
Table 2.9. Thermal conductivity of gypsum board.
Specimen Thickness
mm
Hot Surface Temperature
C
Cold Surface Temperature
C
Conductivity
W m
-1
K
-1

12.51 5.27 -4.94 0.16
12.51 29.24 18.89 0.16
12.51 5.42 -4.91 0.16
12.51 29.62 19.03 0.16

The heat flow meter apparatus is built to measure the heat transmission characteristics of
insulating materials and for those materials the measurement uncertainties are within 2 %;
gypsum board is very conductive and the large heat fluxes measured may give measurement
uncertainties as high as 5 %.

13
M K Kumaran, Final Report, Volume 3, Material Properties, International Energy Agency
Annex 24 Report, Published by K. U. Leuven Belgium, 1996
B1115.13

22


Sorption Desorption Measurements
14
:
Up to twelve specimens, 41 mm X 41 mm each, are used in these measurements; the numbers
in parentheses indicate the experimental uncertainties.

Table 2.10 Results from sorption/ desorption measurements.
a) Sorption:

RH, % Temperature, C Moisture Content, kg kg
-1

100, total saturation* Lab at 22 (1) 1.13 (0.02), six specimens
100, capillary saturation Lab at 22 (1) 0.689 (0.003), four specimens
94 (2) Lab at 22 (1) 0.042 (0.04), 12 specimens
90.8 (1) 23 (0.1) 0.018 (0.02), three specimens
70.5 (1) 23 (0.1) 0.0065 (0.0003), three specimens
50.5 (1) 23 (0.1) 0.0040 (0.0002), three specimens

* Total saturation under vacuum though destroys the rigidity, one careful measurement could be
performed on each specimen.

b) Desorption:

RH, % Temperature, C Moisture Content, kg kg
-1

88.3 (1) 23.3 (0.1) 0.0182 (0.0004), 12 specimens
84.8 (1) 23.0 (0.1) 0.0169 (0.0004), 12 specimens
71.5 (1) 23.0 (0.1) 0.0132 (0.0003), 12 specimens
50.4 (1) 23.0 (0.1) 0.0099 (0.0002), 12 specimens

Pressure plate measurements were not applicable for this material; full saturation destroys the
integrity of the test specimens.

14
Measurements are done using the proposed procedure for ASTM Standard C1498, which in
turn is based on CEN 89 N 337 E, Hygroscopic Sorption Curve.
B1115.13

23


Water Vapour Transmission (WVT) Rate measurements
15
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used.

Table 2.11. Dry Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature and standard errors for WVT rate, obtained from statistical
analyses of the data at a steady state.


Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

12.50 50.3 (1) 22.9(0.1) 2.99E-06 (1.3E-08)
12.48 50.3 (1) 22.9(0.1) 2.93E-06 (5.2E-09)
12.44 50.3 (1) 22.9(0.1) 2.94E-06 (9.0E-09)
12.50 70.3 (1) 23.0(0.1) 4.12E-06 (1.1E-08)
12.48 70.3 (1) 23.0(0.1) 4.18E-06 (1.3E-08)
12.44 70.3 (1) 23.0(0.1) 4.28E-06 (1.6E-08)
12.50 89.8 (1) 22.9(0.1) 5.65E-06 (2.0E-08)
12.48 89.8 (1) 22.9(0.1) 5.85E-06 (6.1E-09)
12.44 89.8 (1) 22.9(0.1) 5.77E-06 (1.1E-08)



Table 2.12. Wet Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature and standard errors for WVT rate, obtained from statistical
analyses of the data at a steady state.


Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

12.51 70.4 (1) 22.9(0.1) 2.44E-06 (1.2E-08)
12.50 70.4 (1) 22.9(0.1) 2.47E-06 (1.2E-08)
12.43 70.4 (1) 22.9(0.1) 2.53E-06 (1.5E-08)
12.51 90.0 (1) 22.9(0.1) 1.02E-06 (1.3E-08)
12.50 90.0 (1) 22.9(0.1) 1.03E-06 (1.2E.08)
12.43 90.0 (1) 22.9(0.1) 1.02E-06 (1.1E-08)


The average thickness of still air in the cups for both series is 15 mm.

15
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M. K.,
A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water Vapour
Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

24


Derived Water Vapour Permeability
16


Table 2.13. Dependence of water vapour permeability on relative humidity.


RH, % Permeability
kg m
-1
s
-1
Pa
-1

RH, % Permeability
kg m
-1
s
-1
Pa
-1

10
2.96E-11
60
4.49E-11
20
3.21E-11
70
4.91E-11
30
3.48E-11
80
5.38E-11
40
3.78E-11
90
5.91E-11
50
4.12E-11
100
6.52E-11



The relation between WVT rate and Chamber RH is shown below.


d:\tblcurve\ashrae gypsum.txt
Rank 1 Eqn 8002 [Exponential] y=a+bexp(-x/c)
r
2
=0.999 DF Adj r
2
=0.999 FitStdErr=8.22e-08 Fstat=8078
a=-7.78e-06 b=7.79e-06 c=-161.2
0 20 40 60 80 100
CHAMBER RH, %
0
1e-06
2e-06
3e-06
4e-06
5e-06
6e-06
7e-06
W

V

T

R
a
t
e
,

k
g

m
-
2

s
-
1


Figure 2.4. Dependence of WVT Rate on RH difference for gypsum board; all measurements are
interpreted as dry cup measurements.

16
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

25


The numeric summary of the analyses is listed below. The commercial software package called
TabbleCurve2 is used for the curve fit. The terminology below is from the package.

The equation that represents the relation between x = chamber RH and y = WVT rate is
[Exponential] y= a + b exp(-x/c)

r
2
, Coefficient of Determination = 0.999
Fit Std Error = 8.3E-08
F-value = 8077.8

Parameter. Value Std Error t-value 90% Confidence Limits
a -7.77e-06 1.0e-06 -7.6 -9.6e-06 -6.0e-06
b 7.79e-06 1.0e-06 7.7 6.00e-06 9.57e-06
c -161.2 15.5 -10.4 -188.6 -133.7


From the above statistics, the estimated uncertainty in the derived value of the permeability may
be up to 16 %.



B1115.13

26


Water Absorption Coefficient
17
:

Four test specimens, 51 mm X 51 mm each, were used in these measurements. Water is
maintained at (22 1) C. The numbers in parentheses give the standard deviations.

Table 2.14a. As water is absorbed across the major surface.

Square Root of
time, s


Water Absorption
kg m
-2

7.7 0.03 (0.01)
13.4 0.05 (0.01)
19.0 0.06 (0.02)
25.7 0.08 (0.01)
34.6 0.09 (0.01)
42.4 0.10 (0.01)
52.0 0.13 (0.01)
62.4 0.14 (0.01)
84.9 0.16 (0.02)
105.4 0.19 (0.01)
115.9 0.20 (0.02)
130.8 0.23 (0.02)
143.2 0.24(0.02)

Linear regression of the data from the first linear part of the absorption process gives:

Water Absorption Coefficient for the major surfaces = 0.0019 0.0001 kg m
-2
s
-
.

Table 2.14b. As water is absorbed along the edge of the board.


Square Root of
time, s


Water Absorption
kg m
-2

7.7 3.6 (0.2)
13.4 5.6 (0.1)
17.3 7.25 (0.1)
20.5 8.53 (0.1)
24.5 10.16 (0.07)
30.0 12.42 (0.1)
34.6 14.22 (0.07)
38.7 15.87 (0.03)
42.4 17.33 (0.06)
52.5 19.65 (0.01)
60.0 20.32 (0.05)

Linear regression of the data from the first linear part of the absorption process gives:

Water Absorption Coefficient for the edge = 0.399 0.003 kg m
-2
s
-
.


17
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
B1115.13

27


Moisture Diffusivity:

Gamma ray method
18
is used to measure the distribution of moisture in three test
specimens, 5 cm X 23 cm each, during the moisture uptake through the edge. The principle of the
methodology is described by Kumaran et. al
19
. Marchand and Kumaran
20
have reported the
procedure used for the data reduction.

The moisture diffusivity derived using all data on all three test specimens is listed below.

Table 2.15. Moisture diffusivity of gypsum board at various moisture contents.

Moisture Content
kg kg
-1

Diffusivity
m
2
s
-1

Moisture Content
kg kg
-1

Diffusivity
m
2
s
-1

0.032 2.09E-08 0.528 3.35E-07
0.064 3.81E-08 0.544 2.84E-07
0.096 5.36E-08 0.560 2.54E-07
0.128 6.98E-08 0.576 2.36E-07
0.160 8.82E-08 0.592 2.24E-07
0.192 1.1E-07 0.608 2.17E-07
0.224 1.34E-07 0.624 2.13E-07
0.256 1.6E-07 0.640 2.12E-07
0.288 1.87E-07 0.656 2.15E-07
0.320 2.13E-07 0.672 2.2E-07
0.352 2.44E-07 0.688 2.29E-07
0.384 2.91E-07 0.704 2.42E-07
0.400 3.3E-07 0.720 2.63E-07
0.416 3.91E-07 0.736 2.94E-07
0.432 5.07E-07 0.752 3.46E-07
0.448 8.22E-07 0.768 4.45E-07
0.464 4.13E-06 0.784 7.11E-07
0.480 1.47E-06 0.800 2.55E-06
0.496 8.46E-07


18
Kumaran, M.K. and Bomberg, M.T., "A Gamma-spectrometer for determination of density
distribution and moisture distribution in building materials," Moisture and Humidity: Measurement
and Control in Science and Industry : Proceedings of International Symposium (Washington,
D.C., USA, 1985), pp. 485-90, 1985.
19
Kumaran, M.K., Mitalas, G.P., Kohonen, R., Ojanen, T, "Moisture transport coefficient of pine
from gamma ray absorption measurements," Collected Papers in Heat Transfer, 1989 : Winter
Annual Meeting of the ASME (San Francisco, CA, USA, 1989) pp. 179-183, 1989(ASME Heat
Transfer Division vol. 123).
20
Marchand, R.G. and Kumaran, M. K., "Moisture diffusivity of cellulose insulation," Journal of
Thermal Insulation and Building Envelopes, Vol. 17, pp. 362-377, 1994.
B1115.13

28


Air Permeability:
Bomberg and Kumaran
21
have reported the principle of the method used in these
measurements. Appendix XIII of the Client Report to ASHRAE, B-1115.3 A Thermal and
Moisture Transport Property Database for Common Building and Insulating Materials 1018-RP
dated 1 April 1999 reports the details. Three circular test specimens, thickness = (12.50 ) 0.02)
mm, each approximately 15 cm in diameter, are used in these measurements. The
measurements are conducted at a temperature = (22 1) C.
The summary of the statistical analyses of all data obtained from two series of
measurements on each specimen is shown below.
Linear Regression of All Specimens
0
0.02
0.04
0.06
0.08
0.1
0.12
0.14
0 100 200 300 400 500
Pressure Difference, Pa
F
l
o
w
,

l

m
-
2

s
-
1
Data Points Mean Permeance
Upper Confidence Interval Lower Confidence Interval


Figure 2.5. Dependence of airflow rate on pressure difference for gypsum.

For the range of pressure differences between 25 Pa and 400 Pa, the flow rate linearly
varies with the pressure difference. The air permeability is (4.16 0.07) E-09 kg m
-1
Pa
-1
s
-1
.

21
Bomberg, M. T. and Kumaran, M.K., " A Test method to determine air flow resistance of
exterior membranes and sheathings," Journal of Thermal Insulation, Vol.9, pp. 224-235,1986.
B1115.13

29


1. HYGROTHERMAL PROPERTIES OF ORIENTED STRAND
BOARD -1



The test specimens used for various measurements reported
here are taken from one board of a commercial product, 4 X
8 with a nominal thickness of . The strands of this product
are manufactured from poplar and aspen.



Density: (650 ) 30) kg m
-3


Heat Capacity (From International Energy Agency Annex 24 Report
22
): 1880 J K
-1
kg
-1


Thermal Conductivity:
Measurements are according to ASTM Standard C518; 30.5 cm X 30.5 cm specimens are used
in these measurements. The temperatures of the plates are maintained within 0.04 C for these
measurements, for 12 h period to confirm steady state. Heat flow is perpendicular to the major
surfaces.
Table 3.1. Thermal Conductivity of OSB 1.
Specimen Thickness
mm
Hot Surface Temperature
C
Cold surface Temperature
C
Conductivity
W m
-1
K
-1

12.66 27.26 21.41 0.102
12.66 3.88 -3.20 0.0984
12.53 27.22 21.40 0.102
19.50 3.90 -3.17 0.0974

Note: The heat flow meter apparatus is built to measure the heat transmission characteristics of
insulating materials and for those materials the measurement uncertainties are within 2 %. This
same uncertainty is applicable to OSB.

22
M K Kumaran, Final Report, Volume 3, Material Properties, International Energy Agency
Annex 24 Report, Published by K. U. Leuven Belgium, 1996
B1115.13

30


Sorption Desorption Measurements
23
:
Up to nine specimens, 40 mm X 40 mm each at the full board thickness are used in these
measurements; the numbers in parentheses indicate the experimental uncertainties.

Sorption:
Table 3.2. Sorption data for OSB 1.
RH, % Temperature, C Moisture Content, kg kg
-1

100, total saturation Lab at 22 (1) 1.35 (0.05), six specimens
100, total saturation Lab at 22 (1) 1.24 (0.07), nine specimens
48.9 (1) 23 (0.2) 0.046 (0.001), three specimens
69.1 (1) 23 (0.2) 0.078 (0.001), three specimens
88.6 (1) 23 (0.2) 0.148 (0.005), three specimens

Desorption:

Table 3.3. Desorption data for OSB 1.
RH, % Temperature, C Moisture Content, kg kg
-1

99.8(0.1) Lab at 22 (1) 0.595 (0.002), six specimens
99.3 (0.1) Lab at 22 (1) 0.42 (0.02), six specimens
92.3 (1) 23.0 (0.2) 0.200 (0.003), two specimens
90.3 (1) 23.0 (0.2) 0.176 (0.006), three specimens
69.4 (1) 23.0 (0.2) 0.100 (0.002) two specimens
49.9 (1) 23.0 (0.2) 0.079 (0.001), two specimens

Note: Pressure plate measurements at 22 C on four similar products gave the following results
for equilibrium moisture contents at relative humidity very close to 100 %.
Table 3.3a. Desorption data for four similar OSB products.
RH, % Moisture Content, kg kg
-1

99.997 1.16 (0.11), 12 specimens
99.993 1.09 (0.12), 12 specimens
99.98 1.06 (0.11), 12 specimens
99.93 0.88 (0.12), 12 specimens

23
In the hygroscopic range, the measurements are done using the proposed procedure for ASTM
Standard C1498, which in turn is based on CEN 89 N 337 E, Hygroscopic Sorption Curve; at
the higher range the pressure plate method is used. Details of the pressure plate method are
given by: Hansen, M. H., "Retention Curves Measured Using Pressure Plate and Pressure
Membrane," Nordtest Technical Report 367, Danish Building Research Institute, 1998, p 63.
B1115.13

31


Water Vapour Transmission (WVT) Rate measurements
24
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used.

Table 3.4. Dry Cup Measurements on OSB 1 specimens: The numbers in parentheses indicate
the experimental uncertainties for RH and temperature; for WVT Rate the numbers indicate the
standard errors according to a linear regression of data on water vapour transmission rate at a
steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

12.19 49.3 (1) 23.1 (0.1) 3.50E-08 (3.4E-10)
12.21 49.3 (1) 23.1 (0.1) 4.77E-08 (3.8E-10)
12.21 49.3 (1) 23.1 (0.1) 5.23E-08 (3.2 E-10)
12.19 69.2 (1) 23.3 (0.1) 6.56E-08 (8.2E-10)
12.21 69.2 (1) 23.3 (0.1) 8.62E-08 (7.8E-10)
12.21 69.2 (1) 23.3 (0.1) 8.67E-08 (6.2 E-10)
12.19 91.2 (2) 22.9 (0.2) 1.01E-07 (3.4E-09)
12.21 91.2 (2) 22.9 (0.2) 3.02E-07 (4.6E-09)
12.21 91.2 (2) 22.9 (0.2) 2.71E-07 (3.6E-09)



Table 3.5. Wet Cup Measurements on OSB 1 specimens: The numbers in parentheses indicate
the experimental uncertainties for RH and temperature; for WVT Rate the numbers indicate the
standard errors according to a linear regression of data on water vapour transmission rate at a
steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

12.31 69.0 (1) 23.2 (0.1) 1.77E-07 (2.2E-09)
12.40 69.0 (1) 23.2 (0.1) 1.54E-07 (1.7E-09)
12.38 69.0 (1) 23.2 (0.1) 1.80E-07 (1.9E-09)
12.31 90.5 (2) 23.3 (0.2) 2.56E-07 (4.0E-09)
12.40 90.5 (2) 23.3 (0.2) 1.40E-07 (2.5E-09)
12.38 90.5 (2) 23.3 (0.2) 1.86E-07 (4.8E-09)


The average thickness of still air in the cups for both series is 15 mm

24
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M. K.,
A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water Vapour
Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

32


Derived Water Vapour Permeability
25



Table3.6. The dependence of water vapour permeability of OSB 1 on relative humidity.

RH, % Permeability
kg m
-1
s
-1
Pa
-1

RH, % Permeability
kg m
-1
s
-1
Pa
-1

10
4.39E-14
60
1.27E-12
20
1.61E-13
70
1.70E-12
30
3.44E-13
80
2.19E-12
40
5.91E-13
90
2.75E-12
50
9.00E-13
100
3.37E-12




From the TableCurve statistics, the estimated uncertainty in the derived value of the permeability
may be higher than 50 %. The scatter in the WVT data for this product is unusually high for a
building material.




25
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

33


Water Absorption Coefficient
26
:

Four test specimens, 5 cm X 5 cm each, were used in these measurements. Water is maintained
at (22 1) C. The absorption is across the major surface. The numbers in parentheses give the
standard deviations.

Table 3.7. Water absorption data for OSB 1.

Square Root of
time, s


Water Absorption
kg m
-2

7.75 0.09 (0.02)
13.42 0.07 (0.02)
17.32 0.08 (0.03)
24.49 0.09 (0.02)
30.00 0.10 (0.02)
38.73 0.10 (0.02)
48.99 0.11 (0.02)
64.81 0.14 (0.02)
93.27 0.18 (0.04)
112.78 0.21 (0.04)
131.22 0.24 (0.05)
145.33 0.27 (0.06)
168.82 0.30 (0.06)
290.55 0.49 (0.09)
314.17 0.55 (0.09)
337.19 0.59 (0.10)
412.43 0.73 (0.12)

Linear regression using all the data listed above

Water Absorption Coefficient for the major surface = 0.0016 0.00003 kg m
-2
s
-
.


26
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
B1115.13

34


Moisture Diffusivity:

Gamma ray method
27
is used to measure the distribution of moisture in three test
specimens, 6.5 cm X 25 cm each, during the moisture uptake in a direction parallel to the major
surfaces (that is across the edges). The principle of the methodology is described by Kumaran et.
al
28
. Marchand and Kumaran
29
have reported the procedure used for the data reduction.

The moisture diffusivity derived from the gamma ray measurements is given in Table 8.

Table 3.8. The dependence of moisture diffusivity of OSB 1 on moisture content; the moisture
transport is parallel to the major surfaces.

Moisture Content
kg kg
-1

Diffusivity
m
2
s
-1

Moisture Content
kg kg
-1

Diffusivity
m
2
s
-1

0.200 8.55E-11 0.369 5.37E-11
0.215 8.05E-11 0.385 5.23E-11
0.231 7.61E-11 0.400 5.12E-11
0.246 7.23E-11 0.415 5.01E-11
0.262 6.89E-11 0.431 4.93E-11
0.277 6.6E-11 0.446 4.86E-11
0.292 6.33E-11 0.462 4.81E-11
0.308 6.09E-11 0.477 4.78E-11
0.323 5.88E-11 0.492 4.77E-11
0.338 5.69E-11 0.508 4.79E-11
0.354 5.52E-11 0.523 4.85E-11


The uncertainty in the derived moisture diffusivity is estimated to be as high as 30 to 50 %.

27
Kumaran, M.K. and Bomberg, M.T., "A Gamma-spectrometer for determination of density
distribution and moisture distribution in building materials," Moisture and Humidity: Measurement
and Control in Science and Industry : Proceedings of International Symposium (Washington,
D.C., USA, 1985), pp. 485-90, 1985.
28
Kumaran, M.K., Mitalas, G.P., Kohonen, R., Ojanen, T, "Moisture transport coefficient of pine
from gamma ray absorption measurements," Collected Papers in Heat Transfer, 1989 : Winter
Annual Meeting of the ASME (San Francisco, CA, USA, 1989) pp. 179-183, 1989(ASME Heat
Transfer Division vol. 123).
29
Marchand, R.G. and Kumaran, M. K., "Moisture diffusivity of cellulose insulation," Journal of
Thermal Insulation and Building Envelopes, Vol. 17, pp. 362-377, 1994.
B1115.13

35


Air Permeability:
Bomberg and Kumaran
30
have reported the principle of the method used in these
measurements. Appendix XIII of the Client Report to ASHRAE, B-1115.3 A Thermal and
Moisture Transport Property Database for Common Building and Insulating Materials 1018-RP
dated 1 April 1999 reports the details. Three circular test specimens (thickness 12.29, 12.23 and
12.26 mm), each approximately 13 cm in diameter, are used in these measurements. The
measurements are conducted at a temperature = (22 1) C.
The summary of the statistical analyses of all data obtained from two series of
measurements on each specimen is shown in Figure 1 as three separate sets.

0
0.01
0.02
0.03
0.04
0.05
0.06
0.07
0.08
0.09
0 200 400 600 800 1000
Pressure Difference, Pa
F
l
o
w
,

l

m
-
2

s
-
1
Data Points Mean Permeance
Upper Confidence Interval Lower Confidence Interval

Figure 3.1. The dependence of airflow rate on pressure difference for OSB 1.

For the range of pressure differences between 25 Pa and 900 Pa, the flow rate linearly
varies with the pressure difference. The air permeability is (9.6 3.2) E-10 kg m
-1
Pa
-1
s
-1
.

30
Bomberg, M. T. and Kumaran, M.K., " A Test method to determine air flow resistance of
exterior membranes and sheathings," Journal of Thermal Insulation, Vol.9, pp. 224-235,1986.
B1115.13

36


4. HYGROTHERMAL PROPERTIES OF ORIENTED STRAND
BOARD -2



The test specimens used for various measurements reported
here are taken from one board of a commercial product, 4 X
8 with a nominal thickness of 3/8. The strands of this
product are manufactured from balsam poplar and trembling
aspen.



Density: (660 ) 30) kg m
-3


Heat Capacity (From International Energy Agency Annex 24 Report
31
): 1880 J K
-1
kg
-1


Thermal Conductivity:
Measurements are according to ASTM Standard C518; 30.5 cm X 30.5 cm specimens are used
in these measurements. The temperatures of the plates are maintained within 0.04 C for these
measurements, for 12 h period to confirm steady state. Heat flow is perpendicular to the major
surfaces.
Table 4.1. Thermal Conductivity of OSB 2.
Specimen Thickness
mm
Hot Surface Temperature
C
Cold surface Temperature
C
Conductivity
W m
-1
K
-1

10.25 27.04 21.40 0.0944
10.25 3.66 -3.16 0.0909
9.85 27.16 21.39 0.0812
9.85 3.70 -3.36 0.0778

Note: The heat flow meter apparatus is built to measure the heat transmission characteristics of
insulating materials and for those materials the measurement uncertainties are within 2 %. This
same uncertainty is applicable to OSB.

31
M K Kumaran, Final Report, Volume 3, Material Properties, International Energy Agency
Annex 24 Report, Published by K. U. Leuven Belgium, 1996
B1115.13

37


Sorption Desorption Measurements
32
:
Up to nine specimens, 40 mm X 40 mm each at the full board thickness are used in these
measurements; the numbers in parentheses indicate the experimental uncertainties.

Sorption:
Table 4.2. Sorption data for OSB 2.
RH, % Temperature, C Moisture Content, kg kg
-1

100, total saturation Lab at 22 (1) 1.21 (0.10), six specimens
100, total saturation Lab at 22 (1) 1.26 (0.08), nine specimens
48.9 (1) 23 (0.2) 0.046 (0.001), three specimens
69.1 (1) 23 (0.2) 0.076 (0.001), three specimens
88.6 (1) 23 (0.2) 0.147 (0.005), three specimens

Desorption:

Table 4.3. Desorption data for OSB 2.
RH, % Temperature, C Moisture Content, kg kg
-1

99.8(0.1) Lab at 22 (1) 0.606 (.009), six specimens
99.3 (0.1) Lab at 22 (1) 0.393 (0.005), six specimens
92.3 (1) 23.0 (0.2) 0.173 (0.003), two specimens
90.3 (1) 23.0 (0.2) 0.162 (0.005), three specimens
69.4 (1) 23.0 (0.2) 0.091 (0.001), two specimens
49.9 (1) 23.0 (0.2) 0.069 (0.001), two specimens



32
In the hygroscopic range, the measurements are done using the proposed procedure for ASTM
Standard C1498, which in turn is based on CEN 89 N 337 E, Hygroscopic Sorption Curve; at
the higher range the pressure plate method is used. Details of the pressure plate method are
given by: Hansen, M. H., "Retention Curves Measured Using Pressure Plate and Pressure
Membrane," Nordtest Technical Report 367, Danish Building Research Institute, 1998, p 63.
B1115.13

38


Water Vapour Transmission (WVT) Rate measurements
33
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used.

Table 4.4. Dry Cup Measurements on OSB 2 specimens: The numbers in parentheses indicate
the experimental uncertainties for RH and temperature; for WVT Rate the numbers indicate the
standard errors according to a linear regression of data on water vapour transmission rate at a
steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

9.86 49.3 (1) 23.1 (0.1) 2.70E-08 (1.8E-10)
9.98 49.3 (1) 23.1 (0.1) 4.64E-08 (4.1E-10)
9.98 49.3 (1) 23.1 (0.1) 1.88E-08 (1.9 E-10)
9.86 69.2 (1) 23.2 (0.1) 5.51E-08 (7.9E-10)
9.98 69.2 (1) 23.2 (0.1) 8.86E-08 (1.3E-09)
9.98 69.2 (1) 23.2 (0.1) 3.95E-08 (2.1 E-10)
9.86 92.8 (2) 22.7 (0.1) 2.80E-07 (4.3E-09)
9.98 92.8 (2) 22.7 (0.1) 2.77E-07 (2.6E-09)
9.98 92.8 (2) 22.7 (0.1) 1.93E-07 (2.8E-09)



Table 4.5. Wet Cup Measurements on OSB 2 specimens: The numbers in parentheses indicate
the experimental uncertainties for RH and temperature; for WVT Rate the numbers indicate the
standard errors according to a linear regression of data on water vapour transmission rate at a
steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

9.94 69.0 (1) 23.2 (0.1) 2.33E-07 (1.2E-09)
9.76 69.0 (1) 23.2 (0.1) 2.53E-07 (1.8E-09)
9.65 69.0 (1) 23.2 (0.1) 3.44E-07 (2.6E-09)
12.31 90.5 (2) 23.0 (0.3) 2.21E-07 (3.5E-09)
12.40 90.5 (2) 23.0 (0.3) 1.19E-07 (1.0E-09)
12.38 90.5 (2) 23.0 (0.3) 1.57E-07 (2.2E-09)


The average thickness of still air in the cups for both series is 15 mm

33
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M. K.,
A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water Vapour
Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

39


Derived Water Vapour Permeability
34



Table 4.6. The dependence of water vapour permeability of OSB 2 on relative humidity.

RH, % Permeability
kg m
-1
s
-1
Pa
-1

RH, % Permeability
kg m
-1
s
-1
Pa
-1

10
6.42E-14
60
8.11E-13
20
1.06E-13
70
1.35E-12
30
1.77E-13
80
2.27E-12
40
2.93E-13
90
3.83E-12
50
4.87E-13
100
6.54E-12




From the TableCurve statistics, the estimated uncertainty in the derived value of the permeability
may be higher than 50 %. The scatter in the WVT data for this product is unusually high for a
building material.




34
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

40


Water Absorption Coefficient
35
:

Four test specimens, 5 cm X 5 cm each, were used in these measurements. Water is maintained
at (22 1) C. The absorption is across the major surface. The numbers in parentheses give the
standard deviations.

Table 4.7. Water absorption data for OSB 2.

Square Root of
time, s


Water Absorption
kg m
-2

7.75 0.04 (0.01)
13.42 0.06 (0.02)
21.91 0.07 (0.02)
28.98 0.07 (0.02)
38.73 0.09 (0.02)
45.83 0.10 (0.03)
60.00 0.12 (0.03)
85.56 0.15(0.03)
106.77 0.18 (0.04)
127.28 0.21 (0.04)
140.71 0.23(0.04)
165.41 0.26(0.04)
288.58 0.46(0.07)
312.54 0.51(0.07)
335.41 0.55(0.08)
410.97 0.70(0.08)

Linear regression using all the data listed above

Water Absorption Coefficient for the major surface = 0.0016 0.00003 kg m
-2
s
-
.


35
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
B1115.13

41


Moisture Diffusivity:

Gamma ray method
36
is used to measure the distribution of moisture in three test
specimens, 6.5 cm X 25 cm each, during the moisture uptake in a direction parallel to the major
surfaces (that is across the edges). The principle of the methodology is described by Kumaran et.
al
37
. Marchand and Kumaran
38
have reported the procedure used for the data reduction.

The moisture diffusivity derived from the gamma ray measurements is given in Table 8.

Table 4.8. The dependence of moisture diffusivity of OSB 2 on moisture content; the moisture
transport is parallel to the major surfaces.

Moisture Content
kg kg
-1

Diffusivity
m
2
s
-1

Moisture Content
kg kg
-1

Diffusivity
m
2
s
-1

0.197 7.07E-10 0.424 2.03E-10
0.212 6.21E-10 0.439 1.92E-10
0.227 5.52E-10 0.455 1.83E-10
0.242 4.95E-10 0.470 1.74E-10
0.258 4.47E-10 0.485 1.66E-10
0.273 4.07E-10 0.500 1.58E-10
0.288 3.73E-10 0.515 1.51E-10
0.303 3.43E-10 0.530 1.45E-10
0.318 3.17E-10 0.545 1.39E-10
0.333 2.95E-10 0.561 1.34E-10
0.348 2.75E-10 0.576 1.29E-10
0.364 2.57E-10 0.591 1.24E-10
0.379 2.41E-10 0.606 1.19E-10
0.394 2.27E-10 0.621 1.15E-10
0.409 2.14E-10 0.636 1.11E-10


The uncertainty in the derived moisture diffusivity is estimated to be as high as 30 to 50 %.

36
Kumaran, M.K. and Bomberg, M.T., "A Gamma-spectrometer for determination of density
distribution and moisture distribution in building materials," Moisture and Humidity: Measurement
and Control in Science and Industry : Proceedings of International Symposium (Washington,
D.C., USA, 1985), pp. 485-90, 1985.
37
Kumaran, M.K., Mitalas, G.P., Kohonen, R., Ojanen, T, "Moisture transport coefficient of pine
from gamma ray absorption measurements," Collected Papers in Heat Transfer, 1989 : Winter
Annual Meeting of the ASME (San Francisco, CA, USA, 1989) pp. 179-183, 1989(ASME Heat
Transfer Division vol. 123).
38
Marchand, R.G. and Kumaran, M. K., "Moisture diffusivity of cellulose insulation," Journal of
Thermal Insulation and Building Envelopes, Vol. 17, pp. 362-377, 1994.
B1115.13

42


Air Permeability:
Bomberg and Kumaran
39
have reported the principle of the method used in these
measurements. Appendix XIII of the Client Report to ASHRAE, B-1115.3 A Thermal and
Moisture Transport Property Database for Common Building and Insulating Materials 1018-RP
dated 1 April 1999 reports the details. Three circular test specimens (thickness 9.60, 9.72 and
9.84 mm), each approximately 13 cm in diameter, are used in these measurements. The
measurements are conducted at a temperature = (22 1) C.
The summary of the statistical analyses of all data obtained from two series of
measurements on each specimen is shown in Figure 1 as three separate sets.

0
0.01
0.02
0.03
0.04
0.05
0.06
0.07
0 200 400 600 800
Pressure Difference, Pa
F
l
o
w
,

l

m
-
2

s
-
1

Data Points Mean Permeance
Upper Confidence Interval Lower Confidence Interval

Figure 4.1. The dependence of airflow rate on pressure difference for OSB 2.

For the range of pressure differences between 25 Pa and 600 Pa, the flow rate linearly
varies with the pressure difference. The air permeability is (9.8 1.4) E-10 kg m
-1
Pa
-1
s
-1
.



39
Bomberg, M. T. and Kumaran, M.K., " A Test method to determine air flow resistance of
exterior membranes and sheathings," Journal of Thermal Insulation, Vol.9, pp. 224-235,1986.
B1115.13

43


5. HYGROTHERMAL PROPERTIES OF ORIENTED STRAND
BOARD -3



The test specimens used for various measurements reported
here are taken from one board of a commercial product, 4 X
8 with a nominal thickness of 7/16. The strands of this
product are manufactured from birch, poplar and aspen.



Density: (650 ) 30) kg m
-3


Heat Capacity (From International Energy Agency Annex 24 Report
40
): 1880 J K
-1
kg
-1


Thermal Conductivity:
Measurements are according to ASTM Standard C518; 30.5 cm X 30.5 cm specimens are used
in these measurements. The temperatures of the plates are maintained within 0.04 C for these
measurements, for 12 h period to confirm steady state. Heat flow is perpendicular to the major
surfaces.
Table 5.1. Thermal Conductivity of OSB 3.
Specimen Thickness
mm
Hot Surface Temperature
C
Cold surface Temperature
C
Conductivity
W m
-1
K
-1

10.87 27.66 21.73 0.0866
10.87 3.24 -2.78 0.0844
10.98 27.28 21.74 0.102
19.50 2.80 -2.93 0.0965

Note: The heat flow meter apparatus is built to measure the heat transmission characteristics of
insulating materials and for those materials the measurement uncertainties are within 2 %. This
same uncertainty is applicable to OSB.

40
M K Kumaran, Final Report, Volume 3, Material Properties, International Energy Agency
Annex 24 Report, Published by K. U. Leuven Belgium, 1996
B1115.13

44


Sorption Desorption Measurements
41
:
Up to nine specimens, 40 mm X 40 mm each at the full board thickness are used in these
measurements; the numbers in parentheses indicate the experimental uncertainties.

Sorption:
Table 5.2. Sorption data for OSB 3.
RH, % Temperature, C Moisture Content, kg kg
-1

100, total saturation Lab at 22 (1) 1.58 (0.16), six specimens
100, total saturation Lab at 22 (1) 1.60 (0.10), nine specimens
48.9 (1) 23 (0.2) 0.054 (0.001), three specimens
69.1 (1) 23 (0.2) 0.082 (0.001), three specimens
88.6 (1) 23 (0.2) 0.147 (0.005), three specimens

Desorption:

Table 5.3. Desorption data for OSB 3.
RH, % Temperature, C Moisture Content, kg kg
-1

99.8(0.1) Lab at 22 (1) 0.627 (0.010), six specimens
99.3 (0.1) Lab at 22 (1) 0.391 (0.015), six specimens
90.3 (1) 23.0 (0.2) 0.174 (0.002), three specimens
69.4 (1) 23.0 (0.2) 0.099 (0.002), two specimens
49.9 (1) 23.0 (0.2) 0.079 (0.001), two specimens

Note:
Desorption measurements at the RH of 92.3% on the two specimens gave very different results
(0.15 and 0.55) for the equilibrium moisture content. The reason for this is unknown and the data
are excluded.


41
In the hygroscopic range, the measurements are done using the proposed procedure for ASTM
Standard C1498, which in turn is based on CEN 89 N 337 E, Hygroscopic Sorption Curve; at
the higher range the pressure plate method is used. Details of the pressure plate method are
given by: Hansen, M. H., "Retention Curves Measured Using Pressure Plate and Pressure
Membrane," Nordtest Technical Report 367, Danish Building Research Institute, 1998, p 63.
B1115.13

45


Water Vapour Transmission (WVT) Rate measurements
42
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used.

Table 5.4. Dry Cup Measurements on OSB 3 specimens: The numbers in parentheses indicate
the experimental uncertainties for RH and temperature; for WVT Rate the numbers indicate the
standard errors according to a linear regression of data on water vapour transmission rate at a
steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

10.54 49.3 (1) 23.1 (0.1) 5.71E-08 (6.5E-10)
10.58 49.3 (1) 23.1 (0.1) 7.79E-08 (1.3E-09)
10.71 49.3 (1) 23.2 (0.1) 9.84E-08 (1.6 E-09)
10.54 69.1 (1) 23.3 (0.1) 1.13E-07 (1.9E-09)
10.58 69.1 (1) 23.3 (0.1) 1.48E-07 (1.8E-09)
10.71 69.1 (1) 23.3 (0.1) 1.75E-07 (1.9 E-09)
10.54 92.7(2) 22.7 (0.2) 3.31E-07 (3.0E-09)
10.58 92.7 (2) 22.7 (0.2) 3.39E-07 (1.5E-09)
10.71 92.7 (2) 22.7 (0.2) 3.55E-07 (2.4E-09)



Table 5.5. Wet Cup Measurements on OSB 3 specimens: The numbers in parentheses indicate
the experimental uncertainties for RH and temperature; for WVT Rate the numbers indicate the
standard errors according to a linear regression of data on water vapour transmission rate at a
steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

10.81 69.1 (1) 23.2 (0.1) 3.26E-07 (3.2E-09)
10.90 69.1 (1) 23.2 (0.1) 2.81E-07 (4.5E-09)
10.85 69.1 (1) 23.2 (0.1) 2.89E-07 (3.6E-09)
10.81 91.9 (2) 23.3 (0.2) 3.12E-07 (4.5E-09)
10.90 91.9 (2) 23.3 (0.2) 1.22E-07 (1.6E-09)
10.85 91.9 (2) 23.3 (0.2) 9.06E-08 (8.6E-10)


The average thickness of still air in the cups for both series is 15 mm

42
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M. K.,
A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water Vapour
Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

46


Derived Water Vapour Permeability
43



Table 5.6. The dependence of water vapour permeability of OSB 3 on relative humidity.

RH, % Permeability
kg m
-1
s
-1
Pa
-1

RH, % Permeability
kg m
-1
s
-1
Pa
-1

10
2.56E-13
60
1.70E-12
20
4.01E-13
70
2.30E-12
30
6.02E-13
80
3.08E-12
40
8.73E-13
90
4.08E-12
50
1.23E-12
100
5.35E-12




From the TableCurve statistics, the estimated uncertainty in the derived value of the permeability
may be higher than 50 %. The scatter in the WVT data for this product is unusually high for a
building material.




43
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

47


Water Absorption Coefficient :
44

Four test specimens, 5 cm X 5 cm each, were used in these measurements. Water is maintained
at (22 1) C. The absorption is across the major surface. The numbers in parentheses give the
standard deviations.


Square Root of
time, s

Water Absorption
-2
7.75 0.05 (0.01)
13.42 0.06 (0.01)
18.97
24.49 0.09 (0.01)
0.10 (0.02)
42.43 0.12 (0.02)
54.77
Table 5.7. Water absorption data for OSB 3.
kg m
0.07 (0.02)
34.64
0.15 (0.03)
60.00 0.16 (0.03)
81.24 0.20 (0.03)
100.70 0.25 (0.04)
121.24 0.29 (0.04)
144.71 0.34 (0.04)
157.80 0.35 (0.05)
285.66 0.65 (0.10)
311.77 0.71 (0.11)
336.48 0.78 (0.11)

Linear regression using all the data listed above

Water Absorption Coefficient for the major surface = 0.0022 0.00002 kg m
-2
s
-
.


44
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
B1115.13

48


Moisture Diffusivity:

Gamma ray method
45
is used to measure the distribution of moisture in three test
specimens, 6.5 cm X 25 cm each, during the moisture uptake in a direction parallel to the major
surfaces (that is across the edges). The principle of the methodology is described by Kumaran et.
al
46
. Marchand and Kumaran
47
have reported the procedure used for the data reduction.

The moisture diffusivity derived from the gamma ray measurements is given in Table 8.

Table 5.8. The dependence of moisture diffusivity of OSB 3 on moisture content; the moisture
transport is parallel to the major surfaces.

Moisture Content
kg kg
-1

Diffusivity
m
2
s
-1

Moisture Content
kg kg
-1

Diffusivity
m
2
s
-1

0.200 4.17E-10 0.600 1.58E-10
0.231 3.57E-10 0.631 1.52E-10
0.262 3.15E-10 0.662 1.46E-10
0.292 2.84E-10 0.692 1.41E-10
0.323 2.59E-10 0.723 1.37E-10
0.354 2.4E-10 0.754 1.33E-10
0.385 2.24E-10 0.785 1.29E-10
0.415 2.1E-10 0.815 1.25E-10
0.446 1.98E-10 0.846 1.22E-10
0.477 1.88E-10 0.877 1.18E-10
0.508 1.79E-10 0.908 1.15E-10
0.538 1.71E-10 0.923 1.14E-10
0.569 1.64E-10


The uncertainty in the derived moisture diffusivity is estimated to be as high as 30 to 50 %.

45
Kumaran, M.K. and Bomberg, M.T., "A Gamma-spectrometer for determination of density
distribution and moisture distribution in building materials," Moisture and Humidity: Measurement
and Control in Science and Industry : Proceedings of International Symposium (Washington,
D.C., USA, 1985), pp. 485-90, 1985.
46
Kumaran, M.K., Mitalas, G.P., Kohonen, R., Ojanen, T, "Moisture transport coefficient of pine
from gamma ray absorption measurements," Collected Papers in Heat Transfer, 1989 : Winter
Annual Meeting of the ASME (San Francisco, CA, USA, 1989) pp. 179-183, 1989(ASME Heat
Transfer Division vol. 123).
47
Marchand, R.G. and Kumaran, M. K., "Moisture diffusivity of cellulose insulation," Journal of
Thermal Insulation and Building Envelopes, Vol. 17, pp. 362-377, 1994.
B1115.13

49


Air Permeability:
Bomberg and Kumaran
48
have reported the principle of the method used in these
measurements. Appendix XIII of the Client Report to ASHRAE, B-1115.3 A Thermal and
Moisture Transport Property Database for Common Building and Insulating Materials 1018-RP
dated 1 April 1999 reports the details. Three circular test specimens (thickness 10.91, 10.94 and
10.84 mm), each approximately 13 cm in diameter, are used in these measurements. The
measurements are conducted at a temperature = (22 1) C.
The summary of the statistical analyses of all data obtained from two series of
measurements on each specimen is shown in Figure 1 as three separate sets.

0
0.02
0.04
0.06
0.08
0.1
0.12
0 100 200 300 400 500
Pressure Difference, Pa
F
l
o
w
,

l

m
-
2

s
-
1
Data Points Mean Permeance
Upper Confidence Interval Lower Confidence Interval

Figure 5.1. The dependence of airflow rate on pressure difference for OSB 3.

For the range of pressure differences between 25 Pa and 400 Pa, the flow rate linearly
varies with the pressure difference. The air permeability is (2.2 1.0) E-09 kg m
-1
Pa
-1
s
-1
.

48
Bomberg, M. T. and Kumaran, M.K., " A Test method to determine air flow resistance of
exterior membranes and sheathings," Journal of Thermal Insulation, Vol.9, pp. 224-235,1986.
B1115.13

50


6. HYGROTHERMAL PROPERTIES OF PLYWOOD - 1



The test specimens used for various measurements reported
here are taken from one board of a commercial product, 4 X
8 with a nominal thickness of 3/4. The product is certified as
conforming to Canadian plywood manufacturing standard
CSA O151 Canadian Softwood Plywood.



Density: (445 ) 5) kg m
-3


Heat Capacity (From International Energy Agency Annex 24 Report
49
): 1880 J K
-1
kg
-1


Thermal Conductivity:
Measurements are according to ASTM Standard C518; 30.5 cm X 30.5 cm specimens are used
in these measurements. The temperatures of the plates are maintained within 0.04 C for these
measurements, for 12 h period to confirm steady state. Heat flow is perpendicular to the major
surfaces.
Table 6.1. Thermal Conductivity of Plywood 1.
Specimen Thickness
mm
Hot Surface Temperature
C
Cold surface Temperature
C
Conductivity
W m
-1
K
-1

17.93 27.23 21.04 0.0929
17.93 3.98 -3.35 0.0887
17.74 27.22 21.05 0.0911
19.50 4.04 -3.32 0.0870

Note: The heat flow meter apparatus is built to measure the heat transmission characteristics of
insulating materials and for those materials the measurement uncertainties are within 2 %. This
same uncertainty is applicable to Plywood.

49
M K Kumaran, Final Report, Volume 3, Material Properties, International Energy Agency
Annex 24 Report, Published by K. U. Leuven Belgium, 1996
B1115.13

51


Sorption Desorption Measurements
50
:
Up to nine specimens, 40 mm X 40 mm each at the full board thickness are used in these
measurements; the numbers in parentheses indicate the experimental uncertainties.
Sorption:
Table 6.2. Sorption data for Plywood 1.
RH, % Temperature, C Moisture Content, kg kg
-1

100, total saturation Lab at 22 (1) 1.8 (0.1), six specimens
100, total saturation Lab at 22 (1) 1.9 (0.1), nine specimens
48.9 (1) 23 (0.2) 0.067 (0.001), three specimens
69.1 (1) 23 (0.2) 0.101 (0.001), three specimens
88.6 (1) 23 (0.2) 0.176 (0.005), three specimens

Desorption:
Table 6.3. Desorption data for Plywood 1.
RH, % Temperature, C Moisture Content, kg kg
-1

99.8(0.1) Lab at 22 (1) 0.99 (0.01), three specimens
99.3 (0.1) Lab at 22 (1) 0.66 (0.05) , three specimens
92.3 (1) Lab at 22 (1) 0.207 (0.002), three specimens
90.3 (1) 23.0 (0.2) 0.193 (0.002), three specimens
69.4 (1) 23.0 (0.2) 0.113 (0.003), two specimens
49.9 (1) 23.0 (0.2) 0.089 (0.001), two specimens

Note: Pressure plate measurements at 22 C on four similar products gave the following results
for equilibrium moisture contents at relative humidity very close to 100 %.
Table 6.3a. Desorption data for four similar plywood products.
RH, % Moisture Content, kg kg
-1

99.98 1.23 (0.25), 12 specimens
99.93 0.94 (0.22), 12 specimens


50
In the hygroscopic range, the measurements are done using the proposed procedure for ASTM
Standard C1498, which in turn is based on CEN 89 N 337 E, Hygroscopic Sorption Curve; at
the higher range the pressure plate method is used. Details of the pressure plate method are
given by: Hansen, M. H., "Retention Curves Measured Using Pressure Plate and Pressure
Membrane," Nordtest Technical Report 367, Danish Building Research Institute, 1998, p 63.
B1115.13

52


Water Vapour Transmission (WVT) Rate measurements
51
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used.

Table 6.4. Dry Cup Measurements on Plywood 1 specimens: The numbers in parentheses
indicate the experimental uncertainties for RH and temperature; for WVT Rate the numbers
indicate the standard errors according to a linear regression of data on water vapour transmission
rate at a steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

17.84 50.2 (1) 23.2 (0.1) 5.06E-08 (3.3E-10)
17.82 50.2 (1) 23.2 (0.1) 4.86E-08 (2.8E-10)
17.86 50.2 (1) 23.2 (0.1) 6.48E-08 (3.2E-10)
17.84 69.0 (1) 23.3 (0.1) 1.00E-07 (1.9E-10)
17.82 69.0 (1) 23.3 (0.1) 1.09E-07 (1.2E-09)
17.86 69.0 (1) 23.3 (0.1) 1.25E-07 (8.8E-10)
17.84 90.0(2) 23.2 (0.2) 5.21E-07 (5.7E-09)
17.82 90.0(2) 23.2 (0.2) 4.73E-07 (8.4E-09)
17.86 90.0(2) 23.2 (0.2) 5.24E-07 (8.0E-09)



Table 6.5. Wet Cup Measurements on Plywood 1 specimens: The numbers in parentheses
indicate the experimental uncertainties for RH and temperature; for WVT Rate the numbers
indicate the standard errors according to a linear regression of data on water vapour transmission
rate at a steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

17.85 69.3 (1) 23.3 (0.1) 5.08E-07 (5.3E-09)
17.77 69.3 (1) 23.3 (0.1) 5.46E-07 (6.7E-09)
17.81 69.3 (1) 23.3 (0.1) 5.83E-07 (8.6E-09)
17.85 90.0 (2) 23.1 (0.2) 2.81E-07 (3.8E-09)
17.77 90.0 (2) 23.1 (0.2) 3.35E-07 (3.8E-09)
17.81 90.0 (2) 23.1 (0.2) 3.58E-07 (5.4E-09)


The average thickness of still air in the cups for both series is 15 mm

51
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M. K.,
A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water Vapour
Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

53


Derived Water Vapour Permeability
52



Table 6.6. The dependence of water vapour permeability of Plywood 1.

RH, % Permeability
kg m
-1
s
-1
Pa
-1

RH, % Permeability
kg m
-1
s
-1
Pa
-1

10
5.94E-14
60
3.87E-12
20
2.17E-13
70
6.12E-12
30
5.71E-13
80
9.20E-12
40
1.22E-12
90
1.33E-11
50
2.28E-12
100
1.88E-11




From the TableCurve statistics, the estimated uncertainty in the derived value of the permeability
is about 22 %.




52
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

54


Water Absorption Coefficient
53
:

Four test specimens, 5 cm X 5 cm each, were used in these measurements. Water is maintained at
(22 1) C. The absorption is across the major surface. The numbers in parentheses give the standard
deviations.

Table 6.7. Water absorption data for Plywood 1.

Square Root of
time, s


Water Absorption
kg m
-2

7.75 0.07 (0.01)
13.42 0.09 (0.02)
18.97 0.13 (0.03)
24.49 0.13 (0.03)
38.73 0.19 (0.05)
45.83 0.22 (0.06)
54.77 0.24 (0.07)
81.24 0.35 (0.14)
100.10 0.41 (0.16)
118.74 0.46 (0.17)
143.87 0.53 (0.20)
159.87 0.58 (0.20)
285.13 0.93 (0.27)
303.68 1.00 (0.27)
331.99 1.06 (0.28)

Linear regression using the data from the initial linear part of the above set gives:

Water Absorption Coefficient for the major surface = 0.0037 0.0002 kg m
-2
s
-
.


53
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
B1115.13

55


Moisture Diffusivity:

Gamma ray method
54
is used to measure the distribution of moisture in three test
specimens, 6.5 cm X 25 cm each, during the moisture uptake in a direction parallel to the major
surfaces (that is across the edges). The principle of the methodology is described by Kumaran et.
al
55
. Marchand and Kumaran
56
have reported the procedure used for the data reduction.

The moisture diffusivity derived from the gamma ray measurements is given in Table 8.

Table 6.8. The dependence of moisture diffusivity of Plywood 1 on moisture content; the moisture
transport is parallel to the major surfaces.

Moisture
Content
kg kg
-1

Diffusivity
m
2
s
-1

Moisture
Content
kg kg
-1

Diffusivity
m
2
s
-1

Moisture
Content
kg kg
-1

Diffusivity
m
2
s
-1

0.112 2.13E-08 0.472 2.11E-09 0.831 2.67E-09
0.135 1.99E-08 0.494 2.01E-09 0.854 2.27E-09
0.157 1.81E-08 0.517 1.94E-09 0.876 1.97E-09
0.180 1.61E-08 0.539 1.9E-09 0.899 1.73E-09
0.202 1.38E-08 0.562 1.9E-09 0.921 1.54E-09
0.225 1.16E-08 0.584 1.92E-09 0.944 1.39E-09
0.247 9.46E-09 0.607 1.99E-09 0.966 1.25E-09
0.270 7.59E-09 0.629 2.12E-09 0.989 1.14E-09
0.292 6.1E-09 0.652 2.33E-09 1.011 1.04E-09
0.315 4.96E-09 0.674 2.71E-09 1.034 9.51E-10
0.337 4.12E-09 0.697 3.47E-09 1.056 8.74E-10
0.360 3.5E-09 0.719 5.71E-09 1.079 8.05E-10
0.382 3.04E-09 0.764 6.5E-09 1.101 7.44E-10
0.404 2.7E-09 0.787 4.25E-09 1.124 6.89E-10
0.427 2.45E-09 0.809 3.26E-09 1.146 6.4E-10

The uncertainty in the derived moisture diffusivity is estimated to be as high as 30 to 50 %.

54
Kumaran, M.K. and Bomberg, M.T., "A Gamma-spectrometer for determination of density
distribution and moisture distribution in building materials," Moisture and Humidity: Measurement
and Control in Science and Industry : Proceedings of International Symposium (Washington,
D.C., USA, 1985), pp. 485-90, 1985.
55
Kumaran, M.K., Mitalas, G.P., Kohonen, R., Ojanen, T, "Moisture transport coefficient of pine
from gamma ray absorption measurements," Collected Papers in Heat Transfer, 1989 : Winter
Annual Meeting of the ASME (San Francisco, CA, USA, 1989) pp. 179-183, 1989(ASME Heat
Transfer Division vol. 123).
56
Marchand, R.G. and Kumaran, M. K., "Moisture diffusivity of cellulose insulation," Journal of
Thermal Insulation and Building Envelopes, Vol. 17, pp. 362-377, 1994.
B1115.13

56


Air Permeability:
Bomberg and Kumaran
57
have reported the principle of the method used in these
measurements. Appendix XIII of the Client Report to ASHRAE, B-1115.3 A Thermal and
Moisture Transport Property Database for Common Building and Insulating Materials 1018-RP
dated 1 April 1999 reports the details. Three circular test specimens (thickness 17.85, 17.88 and
17.90 mm), each approximately 13 cm in diameter, are used in these measurements. The
measurements are conducted at a temperature = (22 1) C.
The summary of the statistical analyses of all data obtained from two series of
measurements on each specimen is shown in Figure 1 as three separate sets. Two specimens
were almost identical in their responses.

0
0.005
0.01
0.015
0.02
0.025
0 2000 4000 6000 8000 10000 12000
Pressure Difference, Pa
F
l
o
w
,

l

m
-
2

s
-
1
Data Points Mean Permeance
Upper Confidence Interval Lower Confidence Interval

Figure 6.1. The dependence of airflow rate on pressure difference for Plywood 1.

For the range of pressure differences between 2000 Pa and 10 kPa, the flow rate linearly
varies with the pressure difference. The air permeability is (1.9 1.9) E-11 kg m
-1
Pa
-1
s
-1
.


57
Bomberg, M. T. and Kumaran, M.K., " A Test method to determine air flow resistance of
exterior membranes and sheathings," Journal of Thermal Insulation, Vol.9, pp. 224-235,1986.
B1115.13

57


7. HYGROTHERMAL PROPERTIES OF PLYWOOD - 2



The test specimens used for various measurements reported
here are taken from one board of a commercial product, 4 X
8 with a nominal thickness of 1/2. The product is certified as
conforming to Canadian plywood manufacturing standard
CSA O121 Douglas Fir Plywood.



Density: (470 ) 5) kg m
-3


Heat Capacity (From International Energy Agency Annex 24 Report
58
): 1880 J K
-1
kg
-1


Thermal Conductivity:
Measurements are according to ASTM Standard C518; 30.5 cm X 30.5 cm specimens are used
in these measurements. The temperatures of the plates are maintained within 0.04 C for these
measurements, for 12 h period to confirm steady state. Heat flow is perpendicular to the major
surfaces.
Table 7.1. Thermal Conductivity of Plywood 2.
Specimen Thickness
mm
Hot Surface Temperature
C
Cold surface Temperature
C
Conductivity
W m
-1
K
-1

12.03 27.38 20.89 0.0854
12.03 3.53 -2.71 0.0820
12.08 27.28 20.89 0.0862
12.08 3.43 -2.79 0.0808

Note: The heat flow meter apparatus is built to measure the heat transmission characteristics of
insulating materials and for those materials the measurement uncertainties are within 2 %. This
same uncertainty is applicable to Plywood.

58
M K Kumaran, Final Report, Volume 3, Material Properties, International Energy Agency
Annex 24 Report, Published by K. U. Leuven Belgium, 1996
B1115.13

58


Sorption Desorption Measurements
59
:
Up to nine specimens, 40 mm X 40 mm each at the full board thickness are used in these
measurements; the numbers in parentheses indicate the experimental uncertainties.

Sorption:
Table 7.2. Sorption data for Plywood 2.
RH, % Temperature, C Moisture Content, kg kg
-1

100, total saturation Lab at 22 (1) 1.25 (0.15), six specimens
100, total saturation Lab at 22 (1) 1.7 (0.15), nine specimens
48.9 (1) 23 (0.2) 0.070 (0.001), three specimens
69.1 (1) 23 (0.2) 0.092 (0.001), three specimens
88.6 (1) 23 (0.2) 0.158 (0.005), three specimens

Desorption:

Table 7.3. Desorption data for Plywood 2.
RH, % Temperature, C Moisture Content, kg kg
-1

99.8(0.1) Lab at 22 (1) 1.01 (0.05), three specimens
99.3 (0.1) Lab at 22 (1) 0.70 (0.05), three specimens
92.3 (1) Lab at 22 (1) 0.190 (0.003), three specimens
90.3 (1) 23.0 (0.2) 0.182 (0.002), three specimens
69.4 (1) 23.0 (0.2) 0.108 (0.003), two specimens
49.9 (1) 23.0 (0.2) 0.084 (0.001), two specimens



59
In the hygroscopic range, the measurements are done using the proposed procedure for ASTM
Standard C1498, which in turn is based on CEN 89 N 337 E, Hygroscopic Sorption Curve; at
the higher range the pressure plate method is used. Details of the pressure plate method are
given by: Hansen, M. H., "Retention Curves Measured Using Pressure Plate and Pressure
Membrane," Nordtest Technical Report 367, Danish Building Research Institute, 1998, p 63.
B1115.13

59


Water Vapour Transmission (WVT) Rate measurements
60
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used.

Table 7.4. Dry Cup Measurements on Plywood 2 specimens: The numbers in parentheses
indicate the experimental uncertainties for RH and temperature; for WVT Rate the numbers
indicate the standard errors according to a linear regression of data on water vapour transmission
rate at a steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

11.92 50.2 (1) 23.2 (0.1) 1.01E-07 (7.7E-10)
12.08 50.2 (1) 23.2 (0.1) 7.59E-08 (6.2E-11)
12.10 50.2 (1) 23.2 (0.1) 9.35E-08 (1.7E-09)
11.92 69.0 (1) 23.3 (0.1) 1.73E-07 (2.7E-09)
12.08 69.0 (1) 23.3 (0.1) 1.18E-07 (8.0E-10)
12.10 69.0 (1) 23.3 (0.1) 1.65E-07 (9.5E-10)
11.92 90.0(2) 23.2 (0.2) 3.84E-07 (6.0E-09)
12.08 90.0(2) 23.2 (0.2) 2.53E-07 (2.6E-09)
12.10 90.0(2) 23.2 (0.2) 3.57E-07 (3.6E-09)



Table 7.5. Wet Cup Measurements on Plywood 2 specimens: The numbers in parentheses
indicate the experimental uncertainties for RH and temperature; for WVT Rate the numbers
indicate the standard errors according to a linear regression of data on water vapour transmission
rate at a steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

11.92 69.3 (1) 23.3 (0.1) 3.94E-07 (3.1E-09)
11.89 69.3 (1) 23.3 (0.1) 4.52E-07 (5.5E-09)
11.75 69.3 (1) 23.3 (0.1) 4.08E-07 (3.8E-09)
11.92 90.0 (2) 23.1 (0.2) 2.62E-07 (3.2E-09)
11.89 90.0 (2) 23.1 (0.2) 2.99E-07 (3.3E-09)
11.75 90.0 (2) 23.1 (0.2) 3.09E-07 (1.5E-09)


The average thickness of still air in the cups for both series is 15 mm

60
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M. K.,
A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water Vapour
Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

60


Derived Water Vapour Permeability
61



Table 7.6. The dependence of water vapour permeability of Plywood 2.

RH, % Permeability
kg m
-1
s
-1
Pa
-1

RH, % Permeability
kg m
-1
s
-1
Pa
-1

10
1.93E-13
60
2.18E-12
20
3.51E-13
70
3.19E-12
30
5.93E-13
80
4.58E-12
40
9.48E-13
90
6.50E-12
50
1.46E-12
100
9.13E-12




From the TableCurve statistics, the estimated uncertainty in the derived value of the permeability
is estimated to be as high as 50 %.




61
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

61


Water Absorption Coefficient
62
:

Four test specimens, 5 cm X 5 cm each, were used in these measurements. Water is maintained
at (22 1) C. The absorption is across the major surface. The numbers in parentheses give the
standard deviations.

Table 7.7. Water absorption data for Plywood 2.

Square Root of
time, s


Water Absorption
kg m
-2

7.75 0.07 (0.03)
13.42 0.09 (0.03)
18.97 0.12 (0.05)
25.69 0.14 (0.06)
30.98 0.16 (0.06)
39.50 0.21 (0.07)
62.45 0.29 (0.11)
75.89 0.34 (0.13)
96.12 0.45 (0.15)
115.41 0.52 (0.20)
140.93 0.61 (0.24)
157.80 0.66 (0.27)
283.65 0.98 (0.41)
301.99 1.00 (0.42)
330.73 1.07 (0.44)

Linear regression using the data from the initial linear part of the above set gives:

Water Absorption Coefficient for the major surface = 0.0042 0.0001 kg m
-2
s
-
.

Note that the rather large standard deviations are not included in the regression. The uncertainty
in the derived value for water absorption coefficient can be much larger than 0.0001 kg m
-2
s
-
.


62
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
B1115.13

62


Moisture Diffusivity:

Gamma ray method
63
is used to measure the distribution of moisture in three test
specimens, 6.5 cm X 25 cm each, during the moisture uptake in a direction parallel to the major
surfaces (that is across the edges). The principle of the methodology is described by Kumaran et.
al
64
. Marchand and Kumaran
65
have reported the procedure used for the data reduction.

The moisture diffusivity derived from the gamma ray measurements is given in Table 8.

Table 7.8. The dependence of moisture diffusivity of Plywood 2 on moisture content; the moisture
transport is parallel to the major surfaces.

Moisture
Content
kg kg
-1

Diffusivity
m
2
s
-1

Moisture
Content
kg kg
-1

Diffusivity
m
2
s
-1

Moisture
Content
kg kg
-1

Diffusivity
m
2
s
-1

0.085 9.32E-09 0.383 2.18E-09 0.681 1.50E-09
0.106 4.70E-09 0.404 2.39E-09 0.702 1.39E-09
0.128 3.16E-09 0.426 2.62E-09 0.723 1.29E-09
0.149 2.47E-09 0.447 2.84E-09 0.745 1.21E-09
0.170 2.10E-09 0.468 2.98E-09 0.766 1.13E-09
0.191 1.89E-09 0.489 3.01E-09 0.787 1.05E-09
0.213 1.76E-09 0.511 2.92E-09 0.809 9.90E-10
0.234 1.69E-09 0.532 2.75E-09 0.830 9.32E-10
0.255 1.66E-09 0.553 2.53E-09 0.851 8.78E-10
0.277 1.67E-09 0.574 2.32E-09 0.872 8.30E-10
0.298 1.71E-09 0.596 2.12E-09 0.894 7.85E-10
0.319 1.77E-09 0.617 1.93E-09 0.915 7.44E-10
0.340 1.87E-09 0.638 1.77E-09 0.936 7.06E-10
0.362 2.01E-09 0.660 1.63E-09 0.957 6.71E-10

The uncertainty in the derived moisture diffusivity is estimated to be as high as 30 to 50 %.

63
Kumaran, M.K. and Bomberg, M.T., "A Gamma-spectrometer for determination of density
distribution and moisture distribution in building materials," Moisture and Humidity: Measurement
and Control in Science and Industry : Proceedings of International Symposium (Washington,
D.C., USA, 1985), pp. 485-90, 1985.
64
Kumaran, M.K., Mitalas, G.P., Kohonen, R., Ojanen, T, "Moisture transport coefficient of pine
from gamma ray absorption measurements," Collected Papers in Heat Transfer, 1989 : Winter
Annual Meeting of the ASME (San Francisco, CA, USA, 1989) pp. 179-183, 1989(ASME Heat
Transfer Division vol. 123).
65
Marchand, R.G. and Kumaran, M. K., "Moisture diffusivity of cellulose insulation," Journal of
Thermal Insulation and Building Envelopes, Vol. 17, pp. 362-377, 1994.
B1115.13

63


Air Permeability:
Bomberg and Kumaran
66
have reported the principle of the method used in these
measurements. Appendix XIII of the Client Report to ASHRAE, B-1115.3 A Thermal and
Moisture Transport Property Database for Common Building and Insulating Materials 1018-RP
dated 1 April 1999 reports the details. Three circular test specimens (thickness 11.75, 11.80 and
11.93 mm), each approximately 13 cm in diameter, are used in these measurements. The
measurements are conducted at a temperature = (22 1) C.
The summary of the statistical analyses of all data obtained from two series of
measurements on each specimen is shown in Figure 1 as three separate sets. Two specimens
were almost identical in their responses.

0
0.005
0.01
0.015
0.02
0.025
0.03
0.035
0.04
0 2000 4000 6000 8000
Pressure Difference, Pa
F
l
o
w
,

l

m
-
2

s
-
1
Data Points Mean Permeance
Upper Confidence Interval Lower Confidence Interval

Figure 7.1. The dependence of airflow rate on pressure difference for Plywood 2.

For the range of pressure differences between 2000 Pa and 7000 Pa, the flow rate
linearly varies with the pressure difference. The air permeability is (3.8 3.8) E-11 kg m
-1
Pa
-1
s
-1
.



66
Bomberg, M. T. and Kumaran, M.K., " A Test method to determine air flow resistance of
exterior membranes and sheathings," Journal of Thermal Insulation, Vol.9, pp. 224-235,1986.
B1115.13

64


8. HYGROTHERMAL PROPERTIES OF PLYWOOD - 3



The test specimens used for various measurements reported
here are taken from one board of a commercial product, 4 X
8 with a nominal thickness of 5/8. The product is certified as
conforming to Canadian plywood manufacturing standard
CSA O121 Douglas Fir Plywood.



Density: (550 ) 5) kg m
-3


Heat Capacity (From International Energy Agency Annex 24 Report
67
): 1880 J K
-1
kg
-1


Thermal Conductivity:
Measurements are according to ASTM Standard C518; 30.5 cm X 30.5 cm specimens are used
in these measurements. The temperatures of the plates are maintained within 0.04 C for these
measurements, for 12 h period to confirm steady state. Heat flow is perpendicular to the major
surfaces.
Table 8.1. Thermal Conductivity of Plywood 3.
Specimen Thickness
mm
Hot Surface Temperature
C
Cold surface Temperature
C
Conductivity
W m
-1
K
-1

15.08 26.86 21.06 0.102
15.08 3.61 -3.30 0.0968
15.25 26.75 21.04 0.106
15.25 3.38 -3.44 0.101

Note: The heat flow meter apparatus is built to measure the heat transmission characteristics of
insulating materials and for those materials the measurement uncertainties are within 2 %. This
same uncertainty is applicable to Plywood.

67
M K Kumaran, Final Report, Volume 3, Material Properties, International Energy Agency
Annex 24 Report, Published by K. U. Leuven Belgium, 1996
B1115.13

65


Sorption Desorption Measurements
68
:
Up to nine specimens, 40 mm X 40 mm each at the full board thickness are used in these
measurements; the numbers in parentheses indicate the experimental uncertainties.

Sorption:
Table 8.2. Sorption data for Plywood 3.
RH, % Temperature, C Moisture Content, kg kg
-1

100, total saturation Lab at 22 (1) 1.2 (0.2), six specimens
100, total saturation Lab at 22 (1) 1.4 (0.1), nine specimens
48.9 (1) 23 (0.2) 0.068 (0.001), three specimens
69.1 (1) 23 (0.2) 0.096 (0.001), three specimens
88.6 (1) 23 (0.2) 0.168 (0.005), three specimens

Desorption:

Table 8.3. Desorption data for Plywood 3.
RH, % Temperature, C Moisture Content, kg kg
-1

99.8(0.1) Lab at 22 (1) 0.79 (0.01) , three specimens
99.3 (0.1) Lab at 22 (1) 0.47 (0.06), three specimens
92.3 (1) Lab at 22 (1) 0.193 (0.005), two specimens
90.3 (1) 23.0 (0.2) 0.198 (0.001), three specimens
69.4 (1) 23.0 (0.2) 0.113 (0.001), two specimens
49.9 (1) 23.0 (0.2) 0.086 (0.001), two specimens



68
In the hygroscopic range, the measurements are done using the proposed procedure for ASTM
Standard C1498, which in turn is based on CEN 89 N 337 E, Hygroscopic Sorption Curve; at
the higher range the pressure plate method is used. Details of the pressure plate method are
given by: Hansen, M. H., "Retention Curves Measured Using Pressure Plate and Pressure
Membrane," Nordtest Technical Report 367, Danish Building Research Institute, 1998, p 63.
B1115.13

66


Water Vapour Transmission (WVT) Rate measurements
69
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used.

Table 8.4. Dry Cup Measurements on Plywood 3 specimens: The numbers in parentheses
indicate the experimental uncertainties for RH and temperature; for WVT Rate the numbers
indicate the standard errors according to a linear regression of data on water vapour transmission
rate at a steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

15.23 50.0 (1) 23.2 (0.1) 4.09E-08 (2.5E-10)
14.92 50.0 (1) 23.2 (0.1) 3.92E-08 (6.2E-10)
14.87 50.0 (1) 23.2 (0.1) 4.15E-08 (2.6E-10)
15.23 69.1 (1) 23.3 (0.1) 1.10E-07 (1.3E-09)
14.92 69.1 (1) 23.3 (0.1) 1.25E-07 (9.1E-10)
14.87 69.1 (1) 23.3 (0.1) 1.21E-07 (1.5E-09)
15.23 89.2(2) 23.4 (0.2) 2.93E-07 (4.7E-09)
14.92 89.2(2) 23.4 (0.2) 2.82E-07 (1.7E-09)
14.87 89.2(2) 23.4 (0.2) 2.47E-07 (3.2E-09)



Table 8.5. Wet Cup Measurements on Plywood 3 specimens: The numbers in parentheses
indicate the experimental uncertainties for RH and temperature; for WVT Rate the numbers
indicate the standard errors according to a linear regression of data on water vapour transmission
rate at a steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

14.84 69.3 (1) 23.3 (0.1) 4.11E-07 (3.6E-09)
14.88 69.3 (1) 23.3 (0.1) 3.40E-07 (6.0E-09)
15.00 69.3 (1) 23.3 (0.1) 3.48E-07 (6.6E-09)
14.84 90.1 (2) 23.1 (0.2) 2.09E-07 (1.8E-09)
14.88 90.1 (2) 23.1 (0.2) 2.50E-07 (1.9E-09)
15.00 90.1 (2) 23.1 (0.2) 3.44E-07 (4.3E-09)


The average thickness of still air in the cups for both series is 15 mm

69
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M. K.,
A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water Vapour
Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

67


Derived Water Vapour Permeability
70



Table 8.6. The dependence of water vapour permeability of Plywood 3.

RH, % Permeability
kg m
-1
s
-1
Pa
-1

RH, % Permeability
kg m
-1
s
-1
Pa
-1

10
1.55E-13
60
1.78E-12
20
2.52E-13
70
2.91E-12
30
4.10E-13
80
4.80E-12
40
6.67E-13
90
7.99E-12
50
1.09E-12
100
1.35E-11




From the TableCurve statistics, the estimated uncertainty in the derived value of the permeability
is estimated to be as high as 50 %.




70
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

68


Water Absorption Coefficient
71
:

Four test specimens, 5 cm X 5 cm each, were used in these measurements. Water is maintained
at (22 1) C. The absorption is across the major surface. The numbers in parentheses give the
standard deviations.

Table 8.7. Water absorption data for Plywood 3.

Square Root of
time, s


Water Absorption
kg m
-2

7.75 0.05 (0.01)
13.42 0.07 (0.01)
17.32 0.08 (0.01)
24.49 0.10 (0.02)
34.64 0.14 (0.02)
42.43 0.15 (0.02)
60.50 0.21 (0.03)
73.48 0.26 (0.05)
95.18 0.32 (0.06)
122.47 0.40 (0.07)
147.38 0.48 (0.08)
161.93 0.52 (0.08)
286.71 0.83 (0.10)
312.44 0.90 (0.10)
335.14 0.96 (0.11)

Linear regression using the data from the initial linear part of the above set gives:

Water Absorption Coefficient for the major surface = 0.0031 0.0001 kg m
-2
s
-
.



71
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
B1115.13

69


Moisture Diffusivity:

Gamma ray method
72
is used to measure the distribution of moisture in three test
specimens, 6.5 cm X 25 cm each, during the moisture uptake in a direction parallel to the major
surfaces (that is across the edges). The principle of the methodology is described by Kumaran et.
al
73
. Marchand and Kumaran
74
have reported the procedure used for the data reduction.

The moisture diffusivity derived from the gamma ray measurements is given in Table 8.

Table 8.8. The dependence of moisture diffusivity of Plywood 3 on moisture content; the moisture
transport is parallel to the major surfaces.

Moisture
Content
kg kg
-1

Diffusivity
m
2
s
-1

Moisture
Content
kg kg
-1

Diffusivity
m
2
s
-1

Moisture
Content
kg kg
-1

Diffusivity
m
2
s
-1

0.109 5.41E-09 0.382 5.87E-09 0.636 1.56E-09
0.127 5.35E-09 0.400 6.39E-09 0.655 1.45E-09
0.145 5.21E-09 0.418 7.22E-09 0.673 1.36E-09
0.164 5.06E-09 0.436 8.67E-09 0.691 1.26E-09
0.182 4.94E-09 0.455 1.20E-08 0.709 1.16E-09
0.200 4.85E-09 0.473 1.10E-08 0.727 1.06E-09
0.218 4.79E-09 0.491 9.49E-09 0.745 9.47E-10
0.236 4.76E-09 0.509 5.08E-09 0.764 8.38E-10
0.255 4.76E-09 0.527 3.55E-09 0.782 7.36E-10
0.273 4.79E-09 0.545 2.80E-09 0.800 6.45E-10
0.291 4.85E-09 0.564 2.35E-09 0.818 5.66E-10
0.309 4.94E-09 0.582 2.05E-09 0.836 4.98E-10
0.327 5.07E-09 0.600 1.84E-09 0.855 4.42E-10
0.345 5.26E-09 0.382 5.87E-09 0.873 3.95E-10

The uncertainty in the derived moisture diffusivity is estimated to be as high as 30 to 50 %.

72
Kumaran, M.K. and Bomberg, M.T., "A Gamma-spectrometer for determination of density
distribution and moisture distribution in building materials," Moisture and Humidity: Measurement
and Control in Science and Industry : Proceedings of International Symposium (Washington,
D.C., USA, 1985), pp. 485-90, 1985.
73
Kumaran, M.K., Mitalas, G.P., Kohonen, R., Ojanen, T, "Moisture transport coefficient of pine
from gamma ray absorption measurements," Collected Papers in Heat Transfer, 1989 : Winter
Annual Meeting of the ASME (San Francisco, CA, USA, 1989) pp. 179-183, 1989(ASME Heat
Transfer Division vol. 123).
74
Marchand, R.G. and Kumaran, M. K., "Moisture diffusivity of cellulose insulation," Journal of
Thermal Insulation and Building Envelopes, Vol. 17, pp. 362-377, 1994.
B1115.13

70


Air Permeability:
Bomberg and Kumaran
75
have reported the principle of the method used in these
measurements. Appendix XIII of the Client Report to ASHRAE, B-1115.3 A Thermal and
Moisture Transport Property Database for Common Building and Insulating Materials 1018-RP
dated 1 April 1999 reports the details. Three circular test specimens (thickness 15.2, 14.94 and
14.82 mm), each approximately 13 cm in diameter, are used in these measurements. The
measurements are conducted at a temperature = (22 1) C.
Two of the three specimens were rather permeable to air while the third was much less
permeable. Based on the three series of measurements (two on each test specimen), the air
permeability is approximately 1.0 E-09 kg m
-1
Pa
-1
s
-1
. The uncertainty can be more than 100 %.


75
Bomberg, M. T. and Kumaran, M.K., " A Test method to determine air flow resistance of
exterior membranes and sheathings," Journal of Thermal Insulation, Vol.9, pp. 224-235,1986.
B1115.13

71


9. HYGROTHERMAL PROPERTIES OF WOODFIBRE BOARD



The test specimens used for various measurements reported
here are taken from two boards of a commercial product, 4 X
8 with a nominal thickness of 7/16. Both major surfaces of
the boards are coated black.



Density: (320 ) 10) kg m
-3


Heat Capacity (From International Energy Agency Annex 24 Report
76
): 1880 J K
-1
kg
-1


Thermal Conductivity:
Measurements are according to ASTM Standard C518; 30.5 cm X 30.5 cm specimens are used
in these measurements. The temperatures of the plates are maintained within 0.04 C for these
measurements, for 12 h period to confirm steady state. Heat flow is perpendicular to the major
surfaces.
Table 9.1. Thermal Conductivity of OSB 2.
Specimen Thickness
mm
Hot Surface Temperature
C
Cold surface Temperature
C
Conductivity
W m
-1
K
-1

12.02 28.41 21.09 0.0535
12.02 5.59 -2.85 0.0512
12.00 29.00 19.98 0.0532
9.85 14.58 6.17 0.0519

Note: The heat flow meter apparatus is built to measure the heat transmission characteristics of
insulating materials and for those materials the measurement uncertainties are within 2 %. This
same uncertainty is applicable to this material.

76
M K Kumaran, Final Report, Volume 3, Material Properties, International Energy Agency
Annex 24 Report, Published by K. U. Leuven Belgium, 1996
B1115.13

72


Sorption Desorption Measurements
77
:

Up to nine specimens, 40 mm X 40 mm each at the full board thickness are used in these
measurements; the numbers in parentheses indicate the experimental uncertainties.

Sorption:
Table 9.2. Sorption data for fibreboard.
RH, % Temperature, C Moisture Content, kg kg
-1

100, total saturation Lab at 22 (1) 3.04 (0.03), nine specimens
50.6 (1) 23 (0.2) 0.046 (0.001), three specimens
70.5 (1) 23 (0.2) 0.074 (0.003), three specimens
91.1 (1) 23 (0.2) 0.158 (0.009), three specimens

Desorption:

Table 9.3. Desorption data for fibreboard.
RH, % Temperature, C Moisture Content, kg kg
-1

99.93(0.01) Lab at 22 (1) 2.3 (0.1), nine specimens
99.85(0.01) Lab at 22 (1) 2.3 (0.1), nine specimens
99.71 (0.01) Lab at 22 (1) 2.3 (0.1), nine specimens
90.6 (1) 23.0 (0.2) 0.150 (0.003), three specimens
71.1 (1) 23.0 (0.2) 0.074 (0.001), two specimens
50.6 (1) 23.0 (0.2) 0.039 (0.001), two specimens


Note: Pressure plate technique may not be applicable to this material.

77
In the hygroscopic range, the measurements are done using the proposed procedure for ASTM
Standard C1498, which in turn is based on CEN 89 N 337 E, Hygroscopic Sorption Curve; at
the higher range the pressure plate method is used. Details of the pressure plate method are
given by: Hansen, M. H., "Retention Curves Measured Using Pressure Plate and Pressure
Membrane," Nordtest Technical Report 367, Danish Building Research Institute, 1998, p 63.
B1115.13

73


Water Vapour Transmission (WVT) Rate measurements
78
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used.

Table 9.4. Dry Cup Measurements on fibreboard specimens: The numbers in parentheses
indicate the experimental uncertainties for RH and temperature; for WVT Rate the numbers
indicate the standard errors according to a linear regression of data on water vapour transmission
rate at a steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

11.71 50.5 (1) 22.9 (0.1) 1.37E-06 (9.1E-09)
11.75 50.5 (1) 22.9 (0.1) 1.40E-06 (6.2E-09)
11.83 50.5 (1) 22.9 (0.1) 1.52E-06 (6.2E-09)
11.71 70.6 (1) 22.9 (0.1) 1.95E-06 (9.2E-09)
11.75 70.6 (1) 22.9 (0.1) 2.01E-06 (7.8E-09)
11.83 70.6 (1) 22.9 (0.1) 2.14E-06 (7.3E-09)
11.71 91.4 (1) 22.7 (0.1) 2.65E-06 (8.0E-09)
11.75 91.4 (1) 22.7 (0.1) 2.72E-06 (9.0E-09)
11.83 91.4 (1) 22.7 (0.1) 2.89E-06 (7.4E-09)


Table 9.5. Wet Cup Measurements on fibreboard specimens: The numbers in parentheses
indicate the experimental uncertainties for RH and temperature; for WVT Rate the numbers
indicate the standard errors according to a linear regression of data on water vapour transmission
rate at a steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

11.93 70.6 (1) 22.9 (0.1) 1.04E-06 (9.4E-09)
11.92 70.6 (1) 22.9 (0.1) 1.02E-06 (1.7E-08)
11.89 70.6 (1) 22.9 (0.1) 1.08E-06 (1.9E-08)
11.93 90.4 (2) 22.8 (0.3) 3.80E-07 (4.1E-09)
11.92 90.4 (2) 22.8 (0.3) 3.73E-07 (6.3E-09)
11.89 90.4 (2) 22.8 (0.3) 3.90E-07 (5.6E-09)


The average thickness of still air in the cups for both series is 15 mm

78
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M. K.,
A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water Vapour
Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

74


Derived Water Vapour Permeability
79



Table 9.6. The dependence of water vapour permeability of fibreboard on relative humidity.

RH, % Permeability
kg m
-1
s
-1
Pa
-1

RH, % Permeability
kg m
-1
s
-1
Pa
-1

10
1.24E-11
60
1.57E-11
20
1.30E-11
70
1.64E-11
30
1.36E-11
80
1.72E-11
40
1.43E-11
90
1.81E-11
50
1.50E-11
100
1.90E-11




From the TableCurve statistics, the estimated uncertainty in the derived value of the permeability
is about 20 %.




79
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

75


Water Absorption Coefficient
80
:

Four test specimens, 5 cm X 5 cm each, were used in these measurements. Water is maintained
at (22 1) C. The absorption is across the major surface. The numbers in parentheses give the
standard deviations.

Table 9.7. Water absorption data for fibreboard.

Square Root of
time, s


Water Absorption
kg m
-2

7.75 0.008 (0.006)
13.42 0.011(0.0040
17.32 0.015 (0.005)
24.49 0.023 (0.006)
30.98 0.022 (0.003)
38.73 0.032 (0.004)
46.48 0.039 (0.006)
53.67 0.044 (0.004)
60.00 0.053 (0.004)
69.28 0.061 (0.004)
74.30 0.065 (0.003)
78.61 0.077 (0.006)
85.56 0.081 (0.004)
91.98 0.084 (0.004)
112.25 0.102 (0.006)
120.00 0.115 (0.006)
137.04 0.131 (0.013)
160.44 0.144 (0.010)
172.86 0.155 (0.008)
290.34 0.206 (0.008)

Linear regression using the data for the initial linear part of the absorption process gave:

Water Absorption Coefficient for the major surface = 0.00094 0.00003 kg m
-2
s
-
.


80
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
B1115.13

76


Moisture Diffusivity:

Gamma ray method
81
is used to measure the distribution of moisture in three test
specimens, 6.5 cm X 25 cm each, during the moisture uptake in a direction parallel to the major
surfaces (that is across the edges). The principle of the methodology is described by Kumaran et.
al
82
. Marchand and Kumaran
83
have reported the procedure used for the data reduction.

The moisture diffusivity derived from the gamma ray measurements is given in Table 8.

Table 9.8. The dependence of moisture diffusivity of fibreboard on moisture content; the moisture
transport is parallel to the major surfaces.

Moisture Content
kg kg
-1

Diffusivity
m
2
s
-1

Moisture Content
kg kg
-1

Diffusivity
m
2
s
-1

0.031 5.47E-10 0.219 1.94E-10
0.063 4.68E-10 0.250 1.83E-10
0.094 3.05E-10 0.281 1.73E-10
0.125 2.55E-10 0.313 1.64E-10
0.156 2.27E-10 0.344 1.56E-10
0.188 2.08E-10 0.375 1.49E-10


The uncertainty in the derived moisture diffusivity is estimated to be as high as 30 to 50 %.

81
Kumaran, M.K. and Bomberg, M.T., "A Gamma-spectrometer for determination of density
distribution and moisture distribution in building materials," Moisture and Humidity: Measurement
and Control in Science and Industry : Proceedings of International Symposium (Washington,
D.C., USA, 1985), pp. 485-90, 1985.
82
Kumaran, M.K., Mitalas, G.P., Kohonen, R., Ojanen, T, "Moisture transport coefficient of pine
from gamma ray absorption measurements," Collected Papers in Heat Transfer, 1989 : Winter
Annual Meeting of the ASME (San Francisco, CA, USA, 1989) pp. 179-183, 1989(ASME Heat
Transfer Division vol. 123).
83
Marchand, R.G. and Kumaran, M. K., "Moisture diffusivity of cellulose insulation," Journal of
Thermal Insulation and Building Envelopes, Vol. 17, pp. 362-377, 1994.
B1115.13

77


Air Permeability:
Bomberg and Kumaran
84
have reported the principle of the method used in these
measurements. Appendix XIII of the Client Report to ASHRAE, B-1115.3 A Thermal and
Moisture Transport Property Database for Common Building and Insulating Materials 1018-RP
dated 1 April 1999 reports the details. Three circular test specimens (thickness 11.71, 11.75 and
11.83 mm), each approximately 15 cm in diameter, are used in these measurements. The
measurements are conducted at a temperature = (22 1) C.
The summary of the statistical analyses of all data obtained from two series of
measurements on each specimen is shown in Figure 1 as three separate sets.

0
0.2
0.4
0.6
0.8
1
1.2
1.4
0 10 20 30 40 50 60 70
Pressure Difference, Pa
F
l
o
w
,

l

m
-
2

s
-
1
Data Points Mean Permeance
Upper Confidence Interval Lower Confidence Interval

Figure 9.1. The dependence of airflow rate on pressure difference for fibreboard.

For the range of pressure differences between 10 Pa and 70 Pa, the flow rate linearly
varies with the pressure difference. The air permeability is (2.52 0.04) E-07 kg m
-1
Pa
-1
s
-1
.


84
Bomberg, M. T. and Kumaran, M.K., " A Test method to determine air flow resistance of
exterior membranes and sheathings," Journal of Thermal Insulation, Vol.9, pp. 224-235,1986.
B1115.13

78


10. HYGROTHERMAL PROPERTIES OF EASTERN WHITE
CEDAR


The test specimens used for various measurements reported
here are taken from two planks of eastern white cedar lumber,
approximately 1 X 8 x 8 in size. The 8 X 8 surfaces of the
planks are referred to as the major surfaces in this report.


Density: (360 ) 20) kg m
-3


Heat Capacity (From International Energy Agency Annex 24 Report
85
): 1880 J K
-1
kg
-1


Thermal Conductivity:
Measurements are according to ASTM Standard C518; 30 cm X 30 cm specimens* are used in
these measurements. The temperatures of the plates are maintained within 0.04 C for these
measurements, for 12 h period to confirm steady state. Heat flow is perpendicular to the major
surfaces.
Table 10.1. Thermal Conductivity of Eastern White Cedar (EWC).
Specimen Thickness
mm
Hot Surface Temperature
C
Cold Surface Temperature
C
Conductivity
W m
-1
K
-1

19.35 33.63 13.42 0.0900
19.35 8.24 -8.41 0.0862
19.50 33.35 13.51 0.0961
19.50 7.83 -7.57 0.0922
19.50** 34.67 16.26 0.0984

Note: The heat flow meter apparatus is built to measure the heat transmission characteristics of
insulating materials and for those materials the measurement uncertainties are within 2 %. This
same uncertainty is applicable to EWC also.
*Each test specimen is an assembly of two slabs glued together using a very fine layer of
carpenters glue.
**Retested after 2 years storage in laboratory conditions. The specimen gained about 1.5 % of its
original mass during that period.

85
M K Kumaran, Final Report, Volume 3, Material Properties, International Energy Agency
Annex 24 Report, Published by K. U. Leuven Belgium, 1996
B1115.13

79


Sorption Desorption Measurements
86
:
Up to nine specimens, 41 mm X 41 mm X 6 mm each are used in these measurements; the
numbers in parentheses indicate the experimental uncertainties.
Sorption:
Table 10.2. Sorption data for EWC.
RH, % Temperature, C Moisture Content, kg kg
-1

100, total saturation Lab at 22 (1) 2.28 (0.10), nine specimens
49.8 (1) 23 (0.1) 0.034 (0.001), three specimens
70.0 (1) 23 (0.1) 0.076 (0.001), three specimens
88.5 (1) 23 (0.1) 0.128 (0.002), three specimens

Desorption:
Table 10.3. Desorption data for EWC.
RH, % Temperature, C Moisture Content, kg kg
-1

99.92 (0.01) Lab at 22 (1) 1.76 (0.08), nine specimens
99.85 (0.01) Lab at 22 (1) 1.58 (0.06), nine specimens
99.78(0.01)* Lab at 22 (1) 1.48 (0.1), three specimens
99.71(0.01) Lab at 22 (1) 1.41 (0.05), nine specimens
99.63(0.01) Lab at 22 (1) 1.18 (0.08), nine specimens
99.49(0.01) Lab at 22 (1) 1.12 (0.08), nine specimens
99.27(0.01) Lab at 22 (1) 0.97 (0.05), nine specimens
98.90(0.01) Lab at 22 (1) 0.85 (0.06), nine specimens
97.81(0.01) Lab at 22 (1) 0.71 (0.05), nine specimens
96.7(0.1) Lab at 22 (1) 0.61 (0.03), nine specimens
95.3 (0.1) Lab at 22 (1) 0.50 (0.02), nine specimens
88.7 (1) 23.0 (0.1) 0.119 (0.002), two specimens
70.5 (1) 23.0 (0.1) 0.074 (0.001), two specimens
50.0 (1) 23.0 (0.1) 0.017 (0.003), two specimens

* The measurement on the three specimens at RH = 99.78 % was after maintaining the pressure
difference for several weeks while all the other data, up to RH = 95.3 %, were obtained after
maintaining the pressure difference for 48 to 72 hr. It seems that the method worked for this
material. But the same method when applied to four other wood species did not yield reliable
results. The reason for this is unknown.

86
In the hygroscopic range, the measurements are done using the proposed procedure for ASTM
Standard C1498, which in turn is based on CEN 89 N 337 E, Hygroscopic Sorption Curve; at
the higher range the pressure plate method is used. Details of the pressure plate method are
given by: Hansen, M. H., "Retention Curves Measured Using Pressure Plate and Pressure
Membrane," Nordtest Technical Report 367, Danish Building Research Institute, 1998, p 63.
B1115.13

80


Water Vapour Transmission (WVT) Rate measurements
87
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used. The vapour flow
is perpendicular to the major surfaces.

Table 10.4. Dry Cup Measurements on EWC specimens: The numbers in parentheses indicate
the experimental uncertainties for RH and temperature; for WVT Rate the numbers indicate the
standard errors according to a linear regression of data on water vapour transmission rate at a
steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

19.38 49.8 (1) 23.1 (0.1) 1.16E-08 (5.0E-10)
19.36 49.8 (1) 23.1 (0.1) 7.87E-09 (3.0E-10)
19.74 49.8 (1) 23.1 (0.1) 1.25E-08 (3.3E-10)
19.38 70.8 (1) 23.2 (0.1) 1.20E-07 (3.9E-09)
19.36 70.8 (1) 23.2 (0.1) 1.24E-07 (1.4E-09)
19.74 70.8 (1) 23.2 (0.1) 1.20E-07 (1.3E-09)
19.38 88.4 (1) 23.3 (0.1) 2.46E-07 (2.9E-09)
19.36 88.4 (1) 23.3 (0.1) 2.22E-07 (2.9E-09)
19.74 88.4 (1) 23.3 (0.1) 2.41E-07 (2.8E-09)



Table 10.5. Wet Cup Measurements on EWC specimens: The numbers in parentheses indicate
the experimental uncertainties for RH and temperature; for WVT Rate the numbers indicate the
standard errors according to a linear regression of data on water vapour transmission rate at a
steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

19.31 69.5 (1) 23.3 (0.1) 6.32E-07 (5.7E-09)
19.42 69.5 (1) 23.3 (0.1) 6.22E-07 (1.1E-08)
19.46 69.5 (1) 23.3 (0.1) 6.12E-07 (9.8E-09)
19.31 88.2 (1) 23.2 (0.1) 5.04E-07 (5.5E-09)
19.42 88.2 (1) 23.2 (0.1) 5.50E-07 (3.8E-09)
19.46 88.2 (1) 23.2 (0.1) 5.35E-07 (4.3E-09)


The average thickness of still air in the cups in both series is 15 mm


87
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M. K.,
A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water Vapour
Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

81


Derived Water Vapour Permeability
88



Table 10.6. The dependence of water vapour permeability of EWC on relative humidity; the
vapour flow is perpendicular to the major surfaces.

RH, % Permeability
kg m
-1
s
-1
Pa
-1

RH, % Permeability
kg m
-1
s
-1
Pa
-1

10
1.26E-14
60
1.21E-12
20
3.13E-14
70
3.05E-12
30
7.80E-14
80
7.82E-12
40
1.94E-13
90
2.09E-11
50
4.85E-13
100
6.40E-11



From the TableCurve statistics, the estimated uncertainty in the derived value of the permeability
may be as high as 60 %.




88
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

82


Water Absorption Coefficient
89
:

Four test specimens, 5 cm X 5 cm X 2 cm each, were used in these measurements. Water is
maintained at (22 1) C. The absorption is across the major surface. The numbers in
parentheses give the standard deviations.

Table 10.7. Water absorption data for EWC.

Square Root of
time, s


Water Absorption
kg m
-2

7.75 0.07 (0.01)
13.42 0.08 (0.01)
18.97 0.10 (0.01)
27.93 0.11 (0.02)
42.43 0.13 (0.02)
57.45 0.15 (0.03)
82.70 0.19 (0.03)
100.70 0.21 (0.03)
136.16 0.26 (0.04)
149.00 0.28 (0.04)
159.69 0.30 (0.04)

Linear regression using all the data from the first linear part of the absorption process for the four
specimens gives:

Water Absorption Coefficient for the major surface = 0.0016 0.0003 kg m
-2
s
-
.


89
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
B1115.13

83


Moisture Diffusivity:

90
91 92


Table 10.8. The dependence of moisture diffusivity of EWC on moisture content; the moisture
transport is parallel to the major surfaces.

Moisture Content
Gamma ray method is used to measure the distribution of moisture in three test
specimens, 5 cm X 23 cm X 2 cm each, during the moisture uptake in a direction parallel to the
major surfaces, in the longitudinal direction. The principle of the methodology is described by
Kumaran et. al . Marchand and Kumaran have reported the procedure used for the data
reduction.
The moisture diffusivity derived from the gamma ray measurements is given in Table 8.
Diffusivity Moisture Content Diffusivity
kg kg
-1
m
2
s
-1
kg kg
-1
m s
2 -1
4.69E-08 0.475 2.30E-09
0.053 3.12E-08 0.501
0.079 1.51E-08 2.08E-09
0.106
0.026
2.19E-09
0.528
1.04E-08 0.554 1.99E-09
0.132 8.03E-09 0.580 1.90E-09
6.61E-09 0.607 1.82E-09
0.185 5.65E-09 0.633
0.211 4.95E-09 1.68E-09
0.237 0.686 1.62E-09
3.99E-09 0.712 1.56E-09
0.290
0.158
1.75E-09
0.660
4.42E-09
0.264
3.65E-09 0.739 1.50E-09
0.317 3.36E-09 0.765 1.45E-09
0.343 3.12E-09 0.792 1.40E-09
0.369 2.91E-09 0.818 1.35E-09
0.396 2.73E-09 0.844 1.31E-09
0.422 2.57E-09 0.871 1.27E-09
0.449 0.897 1.23E-09 2.43E-09


The uncertainty in the derived moisture diffusivity is estimated to be as high as 30 to 50 %.

90
Kumaran, M.K. and Bomberg, M.T., "A Gamma-spectrometer for determination of density
distribution and moisture distribution in building materials," Moisture and Humidity: Measurement
and Control in Science and Industry : Proceedings of International Symposium (Washington,
D.C., USA, 1985), pp. 485-90, 1985.
91
Kumaran, M.K., Mitalas, G.P., Kohonen, R., Ojanen, T, "Moisture transport coefficient of pine
from gamma ray absorption measurements," Collected Papers in Heat Transfer, 1989 : Winter
Annual Meeting of the ASME (San Francisco, CA, USA, 1989) pp. 179-183, 1989(ASME Heat
Transfer Division vol. 123).
92
Marchand, R.G. and Kumaran, M. K., "Moisture diffusivity of cellulose insulation," Journal of
Thermal Insulation and Building Envelopes, Vol. 17, pp. 362-377, 1994.
B1115.13

84


Air Permeability:
Bomberg and Kumaran
93
have reported the principle of the method used in these
measurements. Appendix XIII of the Client Report to ASHRAE, B-1115.3 A Thermal and
Moisture Transport Property Database for Common Building and Insulating Materials 1018-RP
dated 1 April 1999 reports the details. Three circular test specimens, each approximately 15 cm
in diameter, are used in these measurements. The measurements are conducted at a
temperature = (22 1) C. The thickness of each specimen is 19.5 mm and at that thickness
they are very resistant to airflow (perpendicular to the major surfaces). Pressure decay
measurements failed to give any insight for an estimation of air permeability of EWC.

93
Bomberg, M. T. and Kumaran, M.K., " A Test method to determine air flow resistance of
exterior membranes and sheathings," Journal of Thermal Insulation, Vol.9, pp. 224-235,1986.
B1115.13

85


11. HYGROTHERMAL PROPERTIES OF WESTERN RED CEDAR



The test specimens used for various measurements reported
here are taken from two planks of western red cedar lumber,
approximately 1 X 8 x 8 in size. The 8 X 8 surfaces of the
planks are referred to as the major surfaces in this report.

Density: (350 ) 20) kg m
-3


Heat Capacity (From International Energy Agency Annex 24 Report
94
): 1880 J K
-1
kg
-1


Thermal Conductivity:
Measurements are according to ASTM Standard C518; 30 cm X 30 cm specimens* are used in
these measurements. The temperatures of the plates are maintained within 0.04 C for these
measurements, for 12 h period to confirm steady state. Heat flow is perpendicular to the major
surfaces.
Table 11.1. Thermal Conductivity of Western Red Cedar (WRC).
Specimen Thickness
mm
Hot Surface Temperature
C
Cold Surface Temperature
C
Conductivity
W m
-1
K
-1

17.80 33.08 13.44 0.0871
17.80 7.37 -7.73 0.0835
17.76 32.99 13.31 0.0841
17.76 7.33 -7.81 0.0805
17.76** 34.82 15.84 0.0845

Note: The heat flow meter apparatus is built to measure the heat transmission characteristics of
insulating materials and for those materials the measurement uncertainties are within 2 %. This
same uncertainty is applicable to WRC also.
*Each test specimen is an assembly of two slabs glued together using a very fine layer of
carpenters glue.
**Retested after 2 years storage in laboratory conditions. The specimen gained about 1.5 % of its
original mass during that period.

94
M K Kumaran, Final Report, Volume 3, Material Properties, International Energy Agency
Annex 24 Report, Published by K. U. Leuven Belgium, 1996
B1115.13

86


Sorption Desorption Measurements
95
:
Up to nine specimens, 41 mm X 41 mm X 6 mm each are used in these measurements; the
numbers in parentheses indicate the experimental uncertainties.
Sorption:
Table 11.2. Sorption data for WRC.
RH, % Temperature, C Moisture Content, kg kg
-1

100, total saturation Lab at 22 (1) 2.28 (0.10), nine specimens
49.8 (1) 23 (0.1) 0.034 (0.001), three specimens
70.0 (1) 23 (0.1) 0.060 (0.002), three specimens
88.5 (1) 23 (0.1) 0.096 (0.010), three specimens

Desorption:
Table 11.3. Desorption data for WRC.
RH, % Temperature, C Moisture Content, kg kg
-1

99.78 (0.1)* Lab at 22 (1) 1.13 (0.01), two specimens
88.7 (1) 23.0 (0.1) 0.133 (0.001), two specimens
70.5 (1) 23.0 (0.1) 0.090 (0.001), two specimens
50.0 (1) 23.0 (0.1) 0.010 (0.001), two specimens

*Note: For the pressure plate apparatus measurements, equilibration took nearly four months and
further measurements were abandoned. A series of measurements after 48 hours of exposure at
each pressure differential gave the values listed in Table 4 for three test specimens. The results
show that they are far removed from equilibrium values.
Table 11.4. Desorption data for WRC.
RH, % Temperature, C Moisture Content, kg kg
-1

98.83 (0.01) Lab at 22 (1) 2.00 (0.01)
96.17 (0.01) Lab at 22 (1) 1.83 (0.05)
95.6 (0.1) Lab at 22 (1) 1.58 (0.15)
95.3 (0.1) Lab at 22 (1) 1.17 (0.16)


95
In the hygroscopic range, the measurements are done using the proposed procedure for ASTM
Standard C1498, which in turn is based on CEN 89 N 337 E, Hygroscopic Sorption Curve; at
the higher range the pressure plate method is used. Details of the pressure plate method are
given by: Hansen, M. H., "Retention Curves Measured Using Pressure Plate and Pressure
Membrane," Nordtest Technical Report 367, Danish Building Research Institute, 1998, p 63.
B1115.13

87


Water Vapour Transmission (WVT) Rate measurements
96
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used. The vapour flow
is perpendicular to the major surfaces.

Table 11.5. Dry Cup Measurements on WRC specimens: The numbers in parentheses indicate
the experimental uncertainties for RH and temperature; for WVT Rate the numbers indicate the
standard errors according to a linear regression of data on water vapour transmission rate at a
steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

17.76 49.8 (1) 23.1 (0.1) 7.95E-09 (2.5E-10)
17.79 49.8 (1) 23.1 (0.1) 7.18E-09 (2.4E-10)
17.78 49.8 (1) 23.1 (0.1) 1.15E-08 (2.6E-10)
17.76 70.8 (1) 23.2 (0.1) 5.49E-08 (6.7E-10)
17.79 70.8 (1) 23.2 (0.1) 5.38E-08 (5.2E-10)
17.78 70.8 (1) 23.2 (0.1) 5.54E-08 (7.8E-10)
17.76 88.4 (1) 23.3 (0.1) 7.67E-08 (1.2E-09)
17.79 88.4 (1) 23.3 (0.1) 7.73E-08 (6.7E-10)
17.78 88.4 (1) 23.3 (0.1) 7.58E-08 (7.1E-09)



Table 11.6. Wet Cup Measurements on WRC specimens: The numbers in parentheses indicate
the experimental uncertainties for RH and temperature; for WVT Rate the numbers indicate the
standard errors according to a linear regression of data on water vapour transmission rate at a
steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

17.84 69.6 (1) 23.3 (0.1) 1.22E-07 (1.4E-09)
17.81 69.6 (1) 23.3 (0.1) 2.75E-08 (------)*
17.78 69.6 (1) 23.3 (0.1) 1.10E-07 (1.0E-09)
17.84 88.2 (1) 23.3 (0.1) 3.77E-08 (1.4E-10)
17.81 88.2 (1) 23.3 (0.1) 4.00E-08 (3.0E-10)
17.78 88.2 (1) 23.3 (0.1) 3.59E-08 (7.0E-10)


The average thickness of still air in the cups in both series is 15 mm
* being an odd value not used in the analyses

96
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M. K.,
A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water Vapour
Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

88


Derived Water Vapour Permeability
97



Table 11.7. The dependence of water vapour permeability of WRC on relative humidity; the
vapour flow is perpendicular to the major surfaces.

RH, % Permeability
kg m
-1
s
-1
Pa
-1

RH, % Permeability
kg m
-1
s
-1
Pa
-1

10
1.06E-13
60
7.21E-13
20
1.56E-13
70
1.06E-12
30
2.28E-13
80
1.56E-12
40
3.35E-13
90
2.29E-12
50
4.91E-13
100
3.39E-12



From the TableCurve statistics, the estimated uncertainty in the derived value of the permeability
may be as high as 80 %.




97
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

89


Water Absorption Coefficient
98
:

Four test specimens, 5 cm X 5 cm X 2 cm each, were used in these measurements. Water is
maintained at (22 1) C. The absorption is across the major surface. The numbers in
parentheses give the standard deviations.

Table 11.8. Water absorption data for WRC.

Square Root of
time, s


Water Absorption
kg m
-2

7.75 0.04 (0.01)
10.95 0.05 (0.00)
17.32 0.05 (0.01)
25.69 0.06 (0.01)
35.50 0.07 (0.01)
46.48 0.08 (0.01)
60.50 0.08 (0.01)
85.21 0.10 (0.01)
102.47 0.11 (0.01)
137.48 0.13 (0.02)
150.20 0.15 (0.02)
160.81 0.15 (0.01)

Linear regression using all the data from the first linear part of the absorption process for the four
specimens gives:

Water Absorption Coefficient for the major surface = 0.0010 0.0002 kg m
-2
s
-
.


98
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
B1115.13

90


Moisture Diffusivity:

Gamma ray method
99
is used to measure the distribution of moisture in three test
specimens, 5 cm X 23 cm X 2 cm each, during the moisture uptake in a direction parallel to the
major surfaces, in the longitudinal direction. The principle of the methodology is described by
Kumaran et. al
100
. Marchand and Kumaran
101
have reported the procedure used for the data
reduction.

The moisture diffusivity derived from the gamma ray measurements is given in Table 9.

Table 11.9. The dependence of moisture diffusivity of WRC on moisture content; the moisture
transport is parallel to the major surfaces.

Moisture Content
kg kg
-1

Diffusivity
m
2
s
-1

Moisture Content
kg kg
-1

Diffusivity
m
2
s
-1

0.079 3.96E-09 0.529 4.08E-10
0.106 4.12E-09 0.556 3.78E-10
0.132 5.67E-09 0.582 3.52E-10
0.159 5.87E-09 0.608 3.3E-10
0.185 5.99E-09 0.635 3.11E-10
0.212 4.65E-09 0.661 2.8E-10
0.238 4.46E-09 0.688 2.67E-10
0.265 3.73E-09 0.714 2.55E-10
0.291 2.32E-09 0.741 2.45E-10
0.317 1.52E-09 0.767 2.35E-10
0.344 1.11E-09 0.794 2.27E-10
0.370 8.77E-10 0.820 2.19E-10
0.397 7.27E-10 0.847 2.11E-10
0.423 6.24E-10 0.873 2.11E-10
0.450 5.48E-10 0.899 2.04E-10
0.476 4.91E-10 0.926 1.98E-10
0.503 4.45E-10 0.952 1.92E-10


The uncertainty in the derived moisture diffusivity is estimated to be as high as 30 to 50 %.

99
Kumaran, M.K. and Bomberg, M.T., "A Gamma-spectrometer for determination of density
distribution and moisture distribution in building materials," Moisture and Humidity: Measurement
and Control in Science and Industry : Proceedings of International Symposium (Washington,
D.C., USA, 1985), pp. 485-90, 1985.
100
Kumaran, M.K., Mitalas, G.P., Kohonen, R., Ojanen, T, "Moisture transport coefficient of pine
from gamma ray absorption measurements," Collected Papers in Heat Transfer, 1989 : Winter
Annual Meeting of the ASME (San Francisco, CA, USA, 1989) pp. 179-183, 1989(ASME Heat
Transfer Division vol. 123).
101
Marchand, R.G. and Kumaran, M. K., "Moisture diffusivity of cellulose insulation," Journal of
Thermal Insulation and Building Envelopes, Vol. 17, pp. 362-377, 1994.
B1115.13

91


Air Permeability:
Bomberg and Kumaran
102
have reported the principle of the method used in these
measurements. Appendix XIII of the Client Report to ASHRAE, B-1115.3 A Thermal and
Moisture Transport Property Database for Common Building and Insulating Materials 1018-RP
dated 1 April 1999 reports the details. Three circular test specimens, each approximately 15 cm
in diameter, are used in these measurements. The measurements are conducted at a
temperature = (22 1) C. The thickness of each specimen is 17.8 mm and at that thickness
they are very resistant to airflow (perpendicular to the major surfaces). From pressure decay
measurements it is estimated that the air permeability is less than 1E-12 kg m
-1
s
-1
Pa
-1
.

102
Bomberg, M. T. and Kumaran, M.K., " A Test method to determine air flow resistance of
exterior membranes and sheathings," Journal of Thermal Insulation, Vol.9, pp. 224-235,1986.
B1115.13

92


12. HYGROTHERMAL PROPERTIES OF SPRUCE



The test specimens used for various measurements reported
here are taken from two planks of spruce lumber,
approximately 1 X 8 x 8 in size. The 8 X 8 surfaces of the
planks are referred to as the major surfaces in this report.

Density: (400 ) 50) kg m
-3


Heat Capacity (From International Energy Agency Annex 24 Report
103
): 1880 J K
-1
kg
-1


Thermal Conductivity:
Measurements are according to ASTM Standard C518; 30.5 cm X 30.5 cm specimens* are used
in these measurements. The temperatures of the plates are maintained within 0.04 C for these
measurements, for 12 h period to confirm steady state. Heat flow is perpendicular to the major
surfaces.
Table 12.1. Thermal Conductivity of Spruce.
Specimen Thickness
mm
Hot Surface Temperature
C
Cold Surface Temperature
C
Conductivity
W m
-1
K
-1

19.41 34.30 13.79 0.0819
19.41 10.25 -10.81 0.0771
19.50 33.81 13.09 0.0938
19.50 8.36 -9.67 0.0899
19.50** 33.59 15.99 0.0909

Note: The heat flow meter apparatus is built to measure the heat transmission characteristics of
insulating materials and for those materials the measurement uncertainties are within 2 %. This
same uncertainty is applicable to spruce also.
*Each test specimen is an assembly of two slabs glued together using a very fine layer of
carpenters glue.
**Retested after 2 years storage in laboratory conditions. The specimen lost about 6 % of its
original mass during that period.

103
M K Kumaran, Final Report, Volume 3, Material Properties, International Energy Agency
Annex 24 Report, Published by K. U. Leuven Belgium, 1996
B1115.13

93


Sorption Desorption Measurements
104
:
Up to nine specimens, 41 mm X 41 mm X 6 mm each are used in these measurements; the
numbers in parentheses indicate the experimental uncertainties.

Sorption:
Table 12.2. Sorption data for Spruce.
RH, % Temperature, C Moisture Content, kg kg
-1

100, total saturation Lab at 22 (1) 2.21 (0.15), nine specimens
100, total saturation (repeat) Lab at 22 (1) 2.28 (0.06), six specimens
49.8 (1) 23 (0.1) 0.041 (0.001), three specimens
70.0 (1) 23 (0.1) 0.092 (0.002), three specimens
88.5 (1) 23 (0.1) 0.167 (0.001), three specimens

Desorption:

Table 12.3. Desorption data for Spruce.
RH, % Temperature, C Moisture Content, kg kg
-1

99.78 (0.1) Lab at 22 (1) 1.87 (0.05), three specimens
95.96 (0.1) Lab at 22 (1) 1.48 (0.06), three specimens
23.0 (0.1) 0.177 (0.001), two specimens
70.5 (1) 23.0 (0.1) 0.113 (0.000), two specimens
50.0 (1) 23.0 (0.1) 0.049 (0.001), two specimens
88.7 (1)



104
In the hygroscopic range, the measurements are done using the proposed procedure for
ASTM Standard C1498, which in turn is based on CEN 89 N 337 E, Hygroscopic Sorption
Curve; at the higher range the pressure plate method is used. Details of the pressure plate
method are given by: Hansen, M. H., "Retention Curves Measured Using Pressure Plate and
Pressure Membrane," Nordtest Technical Report 367, Danish Building Research Institute, 1998,
p 63.
B1115.13

94


Water Vapour Transmission (WVT) Rate measurements
105
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used. The vapour flow
is perpendicular to the major surfaces.

Table 12.4. Dry Cup Measurements on Spruce specimens: The numbers in parentheses indicate
the experimental uncertainties for RH and temperature; for WVT Rate the numbers indicate the
standard errors according to a linear regression of data on water vapour transmission rate at a
steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

19.52 49.9 (1) 23.1 (0.1) 1.17E-07 (5.7E-10)
19.46 49.9 (1) 23.1 (0.1) 6.31E-08 (5.6E-10)
19.49 49.9 (1) 23.1 (0.1) 3.70E-08 (3.9E-10)
19.52 70.6 (1) 23.1 (0.1) 3.92E-07 (2.2E-09)
19.46 70.6 (1) 23.1 (0.1) 2.78E-07 (4.4E-09)
19.49 70.6 (1) 23.1 (0.1) 2.08E-07 (3.4E-09)
19.52 88.6 (1) 23.1 (0.1) 7.64E-07 (5.3E-09)
19.46 88.6 (1) 23.1 (0.1) 5.65E-07 (3.8E-09)
19.49 88.6 (1) 23.1 (0.1) 4.96E-07 (7.9E-09)



Table 12.5. Wet Cup Measurements on Spruce specimens: The numbers in parentheses indicate
the experimental uncertainties for RH and temperature; for WVT Rate the numbers indicate the
standard errors according to a linear regression of data on water vapour transmission rate at a
steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

19.46 69.5 (1) 23.1 (0.1) 8.33E-07 (4.5E-09)
19.41 69.5 (1) 23.1 (0.1) 8.27E-07 (5.7E-09)
19.46 69.5 (1) 23.1 (0.1) 8.60E-07 (5.7E-09)
19.46 89.5 (1) 23.1 (0.1) 6.51E-07 (5.3E-09)
19.41 89.5 (1) 23.1 (0.1) 6.01E-07 (6.2E-09)
19.46 89.5 (1) 23.1 (0.1) 6.43E-07 (9.1E-09)


The average thickness of still air in the cups is 15 mm

105
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M.
K., A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water
Vapour Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

95


Derived Water Vapour Permeability
106



Table 12.6. The dependence of water vapour permeability of Spruce on relative humidity; the
vapour flow is perpendicular to the major surfaces.

RH, % Permeability
kg m
-1
s
-1
Pa
-1

RH, % Permeability
kg m
-1
s
-1
Pa
-1

10
3.77E-13
60
5.36E-12
20
6.38E-13
70
9.27E-12
30
1.08E-12
80
1.63E-11
40
1.84E-12
90
2.95E-11
50
3.13E-12
100
5.68E-11



From the TableCurve statistics, the estimated uncertainty in the derived value of the permeability
may be as high as 60 %; however a numerical analysis using the lower and upper range of data
shows that the variability in the derived values for the permeability is about 25 %.




106
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

96


Water Absorption Coefficient
107
:

Four test specimens, 5 cm X 5 cm X 2 cm each, were used in these measurements. Water is maintained at
(22 1) C. The absorption is across the major surface. The numbers in parentheses give the standard
deviations.

Table 12.7. Water absorption data for Spruce.

Water Absorption Square Root of
time, s


kg m
-2

7.75 0.04 (0.01)
10.95 0.05 (0.01)
17.32 0.06 (0.02)
24.49 0.07 (0.02)
37.95 0.09 (0.02)
43.82 0.11 (0.02)
57.45 0.13 (0.02)
64.34 0.15 (0.02)
80.87 0.17 (0.03)
0.20 (0.03)
114.89 0.24 (0.03)
131.68 0.28 (0.04)
144.71 0.29 (0.04)
156.65 0.32 (0.05)
167.75 0.34 (0.05)
95.50

Linear regression using all the data from the first linear part of the absorption process for the
fourspecimens gives:


Water Absorption Coefficient for the major surface = 0.0020 0.0001 kg m
-2
s
-
.


107
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
B1115.13

97


Moisture Diffusivity:

Gamma ray method
108
is used to measure the distribution of moisture in three test
specimens, 5 cm X 23 cm X 2 cm each, during the moisture uptake in a direction parallel to the
major surfaces, in the longitudinal direction. The principle of the methodology is described by
Kumaran et. al
109
. Marchand and Kumaran
110
have reported the procedure used for the data
reduction.

The moisture diffusivity derived from the gamma ray measurements is given in Table 8.

Table 12.8. The dependence of moisture diffusivity of Spruce on moisture content; the moisture
transport is parallel to the major surfaces.

Moisture Content
kg kg
-1

Diffusivity
m
2
s
-1

Moisture Content
kg kg
-1

Diffusivity
m
2
s
-1

0.2 7.48E-10 0.8 1.92E-10
0.25 6.09E-10 0.85 1.87E-10
0.275 5.56E-10 0.9 1.78E-10
0.325 4.74E-10 0.95 1.7E-10
0.35 4.42E-10 1.00 1.64E-10
0.4 3.88E-10 1.05 1.59E-10
0.45 3.46E-10 1.10 1.55E-10
0.5 3.12E-10 1.15 1.53E-10
0.55 2.84E-10 1.175 1.53E-10
2.6E-10 1.20 1.53E-10
0.65 2.32E-10 1.225 1.54E-10
0.7 2.16E-10
0.6


The uncertainty in the derived moisture diffusivity is estimated to be as high as 30 to 50 %.

108
Kumaran, M.K. and Bomberg, M.T., "A Gamma-spectrometer for determination of density
distribution and moisture distribution in building materials," Moisture and Humidity: Measurement
and Control in Science and Industry : Proceedings of International Symposium (Washington,
D.C., USA, 1985), pp. 485-90, 1985.
109
Kumaran, M.K., Mitalas, G.P., Kohonen, R., Ojanen, T, "Moisture transport coefficient of pine
from gamma ray absorption measurements," Collected Papers in Heat Transfer, 1989 : Winter
Annual Meeting of the ASME (San Francisco, CA, USA, 1989) pp. 179-183, 1989(ASME Heat
Transfer Division vol. 123).
110
Marchand, R.G. and Kumaran, M. K., "Moisture diffusivity of cellulose insulation," Journal of
Thermal Insulation and Building Envelopes, Vol. 17, pp. 362-377, 1994.
B1115.13

98


Air Permeability:

Bomberg and Kumaran
111
have reported the principle of the method used in these
measurements. Appendix XIII of the Client Report to ASHRAE, B-1115.3 A Thermal and
Moisture Transport Property Database for Common Building and Insulating Materials 1018-RP
dated 1 April 1999 reports the details. Three circular test specimens, each approximately 15 cm
in diameter, are used in these measurements. The measurements are conducted at a
temperature = (22 1) C. The thickness of each specimen is 19.5 mm and at that thickness
they are very resistant to airflow (perpendicular to the major surfaces). From pressure decay
measurements it is estimated that the air permeability is approximately 5.0 E-11 kg m
-1
Pa
-1
s
-1
.

111
Bomberg, M. T. and Kumaran, M.K., " A Test method to determine air flow resistance of
exterior membranes and sheathings," Journal of Thermal Insulation, Vol.9, pp. 224-235,1986.
B1115.13

99


13. HYGROTHERMAL PROPERTIES OF EASTERN WHITE PINE


Conductivity



The test specimens used for various measurements reported
here are taken from two planks of eastern white pine lumber,
approximately 1 X 8 x 8 in size. The 8 X 8 surfaces of the
planks are referred to as the major surfaces in this report.

Density: (460 ) 60) kg m
-3

Heat Capacity (From International Energy Agency Annex 24 Report
112
): 1880 J K
-1
kg
-1


Thermal Conductivity:
Measurements are according to ASTM Standard C518; 30 cm X 30 cm specimens* are used in
these measurements. The temperatures of the plates are maintained within 0.04 C for these
measurements, for 12 h period to confirm steady state. Heat flow is perpendicular to the major
surfaces.
Table 13.1. Thermal Conductivity of Eastern White Pine (EWP).
Specimen Thickness
mm
Hot Surface Temperature
C
Cold Surface Temperature
C W m
-1
K
-1

18.81 32.02 14.41 0.100
18.81 7.13 -8.21 0.0946
13.47
18.84 7.55 -6.90 0.0870
18.84** 34.73 0.0909 15.71
18.84 33.50 0.0904

Note: The heat flow meter apparatus is built to measure the heat transmission characteristics of
insulating materials and for those materials the measurement uncertainties are within 2 %. This
same uncertainty is applicable to EWP also.
*Each test specimen is an assembly of two slabs glued together using a very fine layer of
carpenters glue.
**Retested after 2 years storage in laboratory conditions. The specimen gained about 1 % of its
original mass during that period.

112
M K Kumaran, Final Report, Volume 3, Material Properties, International Energy Agency
Annex 24 Report, Published by K. U. Leuven Belgium, 1996
B1115.13

100


Sorption Desorption Measurements
113
:
Up to nine specimens, 41 mm X 41 mm X 6 mm each are used in these measurements; the
numbers in parentheses indicate the experimental uncertainties.
Sorption:
Table 13.2. Sorption data for EWP.
RH, % Temperature, C Moisture Content, kg kg
-1

100, total saturation Lab at 22 (1) 1.59 (0.12), nine specimens
100, total saturation (repeat) Lab at 22 (1) 1.92 (0.12), six specimens
49.8 (1) 23 (0.1) 0.032 (0.001), three specimens
70.0 (1) 23 (0.1) 0.076 (0.001), three specimens
88.5 (1) 23 (0.1) 0.120 (0.010), three specimens

Desorption:
Table 13.3. Desorption data for EWP.
RH, % Temperature, C Moisture Content, kg kg
-1

99.78 (0.1)* Lab at 22 (1) 0.84 (0.01), three specimens
88.7 (1) 23.0 (0.1) 0.124 (0.01), two specimens
23.0 (0.1) 0.090 (0.001), two specimens
50.0 (1) 23.0 (0.1) 0.032 (0.001), two specimens
70.5 (1)

*Note: For the pressure plate apparatus measurements, equilibration took nearly four months and
further measurements were abandoned. A series of measurements after 48 hours of exposure at
each pressure differential gave the values listed in Table 4 for three test specimens. The results
show that they are far removed from equilibrium values.
Table 13.4. Desorption data for EWP.
RH, % Temperature, C Moisture Content, kg kg
-1

98.83 (0.01) Lab at 22 (1) 1.34 (0.14)
96.17 (0.01) Lab at 22 (1) 1.31 (0.15)
95.6 (0.1) Lab at 22 (1) 1.28 (0.10)
95.3 (0.1) Lab at 22 (1) 1.12 (0.15)


113
In the hygroscopic range, the measurements are done using the proposed procedure for
ASTM Standard C1498, which in turn is based on CEN 89 N 337 E, Hygroscopic Sorption
Curve; at the higher range the pressure plate method is used. Details of the pressure plate
method are given by: Hansen, M. H., "Retention Curves Measured Using Pressure Plate and
Pressure Membrane," Nordtest Technical Report 367, Danish Building Research Institute, 1998,
p 63.
B1115.13

101


Water Vapour Transmission (WVT) Rate measurements
114
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used. The vapour flow
is perpendicular to the major surfaces.

Table 13.5. Dry Cup Measurements on EWP specimens: The numbers in parentheses indicate
the experimental uncertainties for RH and temperature; for WVT Rate the numbers indicate the
standard errors according to a linear regression of data on water vapour transmission rate at a
steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

18.78 49.8 (1) 23.1 (0.1) 6.84E-09 (2.4E-10)
18.82 49.8 (1) 23.1 (0.1) 7.56E-09 (3.0E-10)
18.82 49.8 (1) 23.1 (0.1) 3.93E-08 (3.9E-10)
18.78 70.8 (1) 23.2 (0.1) 7.82E-08 (9.8E-10)
18.82 70.8 (1) 23.2 (0.1) 8.51E-07 (1.0E-09)
18.82 70.8 (1) 23.2 (0.1) 1.51E-07 (1.6E-09)
18.78 88.5 (1) 23.3 (0.1) 1.39E-07 (2.3E-09)
18.82 88.5 (1) 23.3 (0.1) 1.34E-07 (2.4E-09)
18.82 88.5 (1) 23.3 (0.1) 2.42E-07 (3.8E-09)



Table 13.6. Wet Cup Measurements on EWP specimens: The numbers in parentheses indicate
the experimental uncertainties for RH and temperature; for WVT Rate the numbers indicate the
standard errors according to a linear regression of data on water vapour transmission rate at a
steady state.
%

Specimen Thickness
mm
Chamber RH Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

18.77 69.7 (1) 23.3 (0.1) 3.28E-07 (4.0E-09)
18.82 69.7 (1) 23.3 (0.1) 3.38E-07 (3.3E-09)
18.83 69.7 (1) 23.3 (0.1) 3.82E-07 (2.6E-09)
18.77 88.2 (1) 23.3 (0.1) 2.37E-07 (2.3E-09)
18.82 88.2 (1) 23.3 (0.1) 2.44E-07 (2.0E-09)
18.83 88.2 (1) 23.3 (0.1) 2.38E-07 (1.3E-09)


The average thickness of still air in the cups in both series is 15 mm

114
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M.
K., A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water
Vapour Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

102


Derived Water Vapour Permeability
115



Table 13.7. The dependence of water vapour permeability of EWP on relative humidity; the
vapour flow is perpendicular to the major surfaces.

RH, % Permeability
kg m
-1
s
-1
Pa
-1

RH, % Permeability
kg m
-1
s
-1
Pa
-1

4.70E-14
60
1.31E-12
20
9.14E-14
70
2.58E-12
30
1.78E-13
80
5.08E-12
3.46E-13
90
1.02E-11
50
6.74E-13
100
2.10E-11
10
40






From the TableCurve statistics, the estimated uncertainty in the derived value of the permeability
may be as high as 80 %.


115
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

103


Water Absorption Coefficient
116
:

Four test specimens, 5 cm X 5 cm X 2 cm each, were used in these measurements. Water is
maintained at (22 1) C. The absorption is across the major surface. The numbers in
parentheses give the standard deviations.

Table 13.8. Water absorption data for EWP.

Square Root of
time, s


Water Absorption*
kg m
-2

13.42 0.14 (0.05)
(0.04)
24.49 0.24 (0.10)
37.95 0.32 (0.06)
48.99 0.39 (0.02)
64.34 0.48 (0.02)
81.98 0.57 (0.06)
103.92 0.70 (0.08)
124.66 0.80 (0.11)
136.38 0.86 (0.11)
148.80 0.91 (0.12)
160.44 0.96 (0.13)
295.47 1.50 (0.21)
7.75 0.13 (0.05)
17.32 0.15

Linear regression using all the data from the first linear part of the absorption process for the four
specimens gives:

* One of the four specimens behaved completely different from the other three specimens. The
data on that one specimen were not used for the analyses.

Water Absorption Coefficient for the major surface = 0.0066 0.0003 kg m
-2
s
-
.


116
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
B1115.13

104


Moisture Diffusivity:

Gamma ray method
117
is used to measure the distribution of moisture in three test
specimens, 5 cm X 23 cm X 2 cm each, during the moisture uptake in a direction parallel to the
major surfaces, in the longitudinal direction. The principle of the methodology is described by
Kumaran et. al
118
. Marchand and Kumaran
119
have reported the procedure used for the data
reduction.

The moisture diffusivity derived from the gamma ray measurements is given in Table 9.

Table 13.9. The dependence of moisture diffusivity of EWP on moisture content; the moisture
transport is parallel to the major surfaces.

Moisture Content
kg kg
-1

Diffusivity
m
2
s
-1

Moisture Content
kg kg
-1

Diffusivity
m
2
s
-1

0.024 1.19E-09 0.431 1.34E-09
0.048 1.36E-09 0.455 1.16E-09
0.072 1.49E-09 0.478 9.96E-10
1.59E-09 0.502 8.64E-10
0.120 1.67E-09 0.526 7.55E-10
0.144 1.75E-09 0.550 6.65E-10
0.167 1.82E-09 0.574 5.91E-10
1.90E-09 0.598 4.78E-10
0.215 1.96E-09 0.622 4.34E-10
0.239 2.03E-09 0.646 3.96E-10
0.263 2.08E-09 0.670 3.63E-10
0.287 2.11E-09 0.694 3.35E-10
0.311 2.11E-09 0.718 3.10E-10
0.335 2.06E-09 0.742 2.88E-10
0.359 1.94E-09 0.766 2.68E-10
0.383 1.76E-09 0.789 2.68E-10
0.407 1.55E-09 0.813 2.51E-10
0.096
0.191



The uncertainty in the derived moisture diffusivity is estimated to be as high as 30 to 50 %.

117
Kumaran, M.K. and Bomberg, M.T., "A Gamma-spectrometer for determination of density
distribution and moisture distribution in building materials," Moisture and Humidity: Measurement
and Control in Science and Industry : Proceedings of International Symposium (Washington,
D.C., USA, 1985), pp. 485-90, 1985.
118
Kumaran, M.K., Mitalas, G.P., Kohonen, R., Ojanen, T, "Moisture transport coefficient of pine
from gamma ray absorption measurements," Collected Papers in Heat Transfer, 1989 : Winter
Annual Meeting of the ASME (San Francisco, CA, USA, 1989) pp. 179-183, 1989(ASME Heat
Transfer Division vol. 123).
119
Marchand, R.G. and Kumaran, M. K., "Moisture diffusivity of cellulose insulation," Journal of
Thermal Insulation and Building Envelopes, Vol. 17, pp. 362-377, 1994.
B1115.13

105


Air Permeability:
Bomberg and Kumaran
120
have reported the principle of the method used in these
measurements. Appendix XIII of the Client Report to ASHRAE, B-1115.3 A Thermal and
Moisture Transport Property Database for Common Building and Insulating Materials 1018-RP
dated 1 April 1999 reports the details. Three circular test specimens, each approximately 15 cm
in diameter, are used in these measurements. The measurements are conducted at a
temperature = (22 1) C. The thickness of each specimen is 18.8 mm and at that thickness
they are very resistant to airflow (perpendicular to the major surfaces). From pressure decay
measurements it is estimated that the air permeability is approximately 1.5 E-12 kg m
-1
Pa
-1
s
-1
.

120
Bomberg, M. T. and Kumaran, M.K., " A Test method to determine air flow resistance of
exterior membranes and sheathings," Journal of Thermal Insulation, Vol.9, pp. 224-235,1986.
B1115.13

106


14. HYGROTHERMAL PROPERTIES OF SOUTHERN YELLOW
PINE




C
The test specimens used for various measurements reported
here are taken from two planks of southern yellow pine
lumber, approximately 1 X 8 x 8 in size. The 8 X 8 surfaces
of the planks are referred to as the major surfaces in this
report.

Density: (500 ) 40) kg m
-3

Heat Capacity (From International Energy Agency Annex 24 Report
121
): 1880 J K
-1
kg
-1


Thermal Conductivity:
Measurements are according to ASTM Standard C518; 30 cm X 30 cm specimens* are used in
these measurements. The temperatures of the plates are maintained within 0.04 C for these
measurements, for 12 h period to confirm steady state. Heat flow is perpendicular to the major
surfaces.
Table 14.1. Thermal Conductivity of Southern Yellow Pine (SYP).
Specimen Thickness
mm
Hot Surface Temperature
C
Cold Surface Temperature Conductivity
W m
-1
K
-1

12.36 0.126
19.15 8.13 -8.51 0.121
19.28 32.10 14.90 0.117
-7.63 0.113
19.29** 34.10 17.15 0.116
19.15 32.93
19.28 7.43

Note: The heat flow meter apparatus is built to measure the heat transmission characteristics of
insulating materials and for those materials the measurement uncertainties are within 2 %. This
same uncertainty is applicable to SYP also.
*Each test specimen is an assembly of two slabs glued together using a very fine layer of
carpenters glue.
**Retested after 2 years storage in laboratory conditions. The mass change was negligible during
that period.

121
M K Kumaran, Final Report, Volume 3, Material Properties, International Energy Agency
Annex 24 Report, Published by K. U. Leuven Belgium, 1996
B1115.13

107


Sorption Desorption Measurements
122
:
Up to nine specimens, 41 mm X 41 mm X 6 mm each are used in these measurements; the
numbers in parentheses indicate the experimental uncertainties.
Sorption:
Table 14.2. Sorption data for SYP.
RH, % Temperature, C Moisture Content, kg kg
-1

100, total saturation Lab at 22 (1) 1.85 (0.15), nine specimens
100, total saturation (repeat) Lab at 22 (1) 1.58 (0.04), six specimens
49.8 (1) 23 (0.1) 0.036 (0.001), three specimens
70.0 (1) 23 (0.1) 0.081 (0.002), three specimens
88.5 (1) 23 (0.1) 0.152 (0.002), three specimens

Desorption:
Table 14.3. Desorption data for SYP.
RH, % Temperature, C Moisture Content, kg kg
-1

99.78 (0.1)* Lab at 22 (1) 0.57 (0.13), three specimens
88.7 (1) 23.0 (0.1) 0.156, two specimens
70.5 (1) 23.0 (0.1) 0.100, two specimens
50.0 (1) 23.0 (0.1) 0.043, two specimens

*Note: For the pressure plate apparatus measurements, equilibration took nearly four months and
further measurements were abandoned. A series of measurements after 48 hours of exposure at
each pressure differential gave the values listed in Table 4 for one test specimen. The results
show that they are far removed from equilibrium values.
Table 14.4. Desorption data for SYP.
RH, % Temperature, C Moisture Content, kg kg
-1

98.83 (0.01) Lab at 22 (1) 1.54 (0.03)
96.17 (0.01) Lab at 22 (1) 1.35 (0.05)
95.6 (0.1) Lab at 22 (1) 1.08 (0.05)
Lab at 22 (1) 0.96 (0.05) 95.3 (0.1)


122
In the hygroscopic range, the measurements are done using the proposed procedure for
ASTM Standard C1498, which in turn is based on CEN 89 N 337 E, Hygroscopic Sorption
Curve; at the higher range the pressure plate method is used. Details of the pressure plate
method are given by: Hansen, M. H., "Retention Curves Measured Using Pressure Plate and
Pressure Membrane," Nordtest Technical Report 367, Danish Building Research Institute, 1998,
p 63.
B1115.13

108


Water Vapour Transmission (WVT) Rate measurements
123
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used. The vapour flow
is perpendicular to the major surfaces.

Table 14.5. Dry Cup Measurements on SYP specimens: The numbers in parentheses indicate
the experimental uncertainties for RH and temperature; for WVT Rate the numbers indicate the
standard errors according to a linear regression of data on water vapour transmission rate at a
steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

19.51 49.8 (1) 23.1 (0.1) 1.43E-08 (3.9E-10)
19.49 49.8 (1) 23.1 (0.1) 1.67E-08 (3.9E-10)
19.56 49.8 (1) 23.1 (0.1) 2.17E-08 (4.1E-10)
19.51 70.8 (1) 23.2 (0.1) 1.21E-07 (9.2E-10)
19.49 70.8 (1) 23.2 (0.1) 1.29E-07 (1.1E-09)
19.56 70.8 (1) 23.2 (0.1) 1.50E-07 (9.7E-10)
19.51 88.4 (1) 23.3 (0.1) 3.28E-07 (3.8E-09)
19.49 88.4 (1) 23.3 (0.1) 3.10E-07 (3.4E-09)
19.56 88.4 (1) 23.3 (0.1) 3.21E-07 (2.7E-09)



Table 14.6. Wet Cup Measurements on SYP specimens: The numbers in parentheses indicate
the experimental uncertainties for RH and temperature; for WVT Rate the numbers indicate the
standard errors according to a linear regression of data on water vapour transmission rate at a
steady state.

Specimen Thickness
mm
Chamber RH
% kg m
Chamber Temperature
C
WVT Rate
-2
s
-1

19.34 69.7 (1) 23.3 (0.1) 5.64E-07 (4.1E-09)
19.47 69.7 (1) 23.3 (0.1) 5.43E-07 (4.7E-09)
19.46 69.7 (1) 23.3 (0.1) 5.34E-07 (4.9E-09)
19.46 88.2 (1) 23.3 (0.1) 4.29E-07 (5.5E-09)
19.41 88.2 (1) 23.3 (0.1) 4.01E-07 (2.1E-09)
19.46 88.2 (1) 23.3 (0.1) 3.71E-07 (3.7E-09)


The average thickness of still air in the cups in both series is 15 mm

123
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M.
K., A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water
Vapour Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

109


Derived Water Vapour Permeability
124



Table 14.7. The dependence of water vapour permeability of SYP on relative humidity; the vapour
flow is perpendicular to the major surfaces.

RH, % Permeability
kg m
-1
s
-1
Pa
-1

RH, % Permeability
kg m
-1
s
-1
Pa
-1

10
1.20E-13
60
2.53E-12
20
2.20E-13
70
4.70E-12
30
4.04E-13
80
8.82E-12
40
7.43E-13
90
1.69E-11
50
1.37E-12
100
3.39E-11



From the TableCurve statistics, the estimated uncertainty in the derived value of the permeability
may be as high as 45 %.




124
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

110


Water Absorption Coefficient
125
:


Four test specimens, 5 cm X 5 cm X 2 cm each, were used in these measurements. Water is
maintained at (22 1) C. The absorption is across the major surface. The numbers in
parentheses give the standard deviations.

Table 14.8. Water absorption data for SYP.
Square Root of
time, s


Water Absorption
kg m
-2

7.75 0.07 (0.00)
10.95 0.09 (0.01)
13.42 0.11 (0.01)
17.32 0.14 (0.02)
21.91 0.19 (0.03)
25.69 0.25 (0.04)
30.98 0.34 (0.07)
36.33 0.43 (0.10)
43.13 0.55 (0.13)
47.12 0.62 (0.15)
54.77 0.75 (0.16)
63.40 0.86 (0.17)
74.70 1.01 (0.19)
(0.18)
110.63 1.36 (0.19)
127.98 1.52 (0.21)
141.35 1.63 (0.22)
153.56 1.73 (0.22)
(0.24)
90.33 1.16
164.86 1.83

Linear regression using all the data from the first linear part of the absorption process for the four
specimens gives:


Water Absorption Coefficient for the major surface = 0.0014 0.0001 kg m
-2
s
-
.


125
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
B1115.13

111


Moisture Diffusivity:

Gamma ray method
126
is used to measure the distribution of moisture in three test
specimens, 5 cm X 23 cm X 2 cm each, during the moisture uptake in a direction parallel to the
major surfaces, in the longitudinal direction. The principle of the methodology is described by
Kumaran et. al
127
. Marchand and Kumaran
128
have reported the procedure used for the data
reduction.

The moisture diffusivity derived from the gamma ray measurements is given in Table 9.

Table 14.9. The dependence of moisture diffusivity of SYP on moisture content; the moisture
transport is parallel to the major surfaces.

Moisture Content
kg kg
-1

Diffusivity
m
2
s
-1

Moisture Content
kg kg
-1

Diffusivity
m
2
s
-1

0.077 1.32E-08 0.579 9.16E-09
0.116 1.81E-08 0.598 1.04E-08
0.154 2.03E-08 0.618 1.22E-08
0.193 2.18E-08 0.637 1.22E-08
0.232 2.35E-08 0.656 1.52E-08
0.270 2.62E-08 0.676 2.08E-08
0.309 3.14E-08 0.695 3.34E-08
0.347 3.40E-08 0.714 7.71E-08
0.386 1.62E-08 0.753 3.72E-08
0.405 1.22E-08 0.772 1.88E-08
0.425 1.00E-08 0.792 1.18E-08
0.444 8.78E-09 0.811 8.29E-09
0.463 8.03E-09 0.830 6.19E-09
0.483 7.40E-09 0.849 4.83E-09
0.502 7.37E-09 0.869
7.52E-09 0.888
0.541 7.84E-09 0.907 2.69E-09
0.560 8.36E-09
3.89E-09
0.521 3.21E-09


The uncertainty in the derived moisture diffusivity is estimated to be as high as 30 to 50 %.

126
Kumaran, M.K. and Bomberg, M.T., "A Gamma-spectrometer for determination of density
distribution and moisture distribution in building materials," Moisture and Humidity: Measurement
and Control in Science and Industry : Proceedings of International Symposium (Washington,
D.C., USA, 1985), pp. 485-90, 1985.
127
Kumaran, M.K., Mitalas, G.P., Kohonen, R., Ojanen, T, "Moisture transport coefficient of pine
from gamma ray absorption measurements," Collected Papers in Heat Transfer, 1989 : Winter
Annual Meeting of the ASME (San Francisco, CA, USA, 1989) pp. 179-183, 1989(ASME Heat
Transfer Division vol. 123).
128
Marchand, R.G. and Kumaran, M. K., "Moisture diffusivity of cellulose insulation," Journal of
Thermal Insulation and Building Envelopes, Vol. 17, pp. 362-377, 1994.
B1115.13

112


Air Permeability:
Bomberg and Kumaran
129
have reported the principle of the method used in these
measurements. Appendix XIII of the Client Report to ASHRAE, B-1115.3 A Thermal and
Moisture Transport Property Database for Common Building and Insulating Materials 1018-RP
dated 1 April 1999 reports the details. Three circular test specimens, each approximately 15 cm
in diameter, are used in these measurements. The measurements are conducted at a
temperature = (22 1) C. The thickness of each specimen is 19.5 mm and at that thickness
they are very resistant to airflow (perpendicular to the major surfaces). From pressure decay
measurements it is estimated that the air permeability is approximately 3.0 E-11 kg m
-1
Pa
-1
s
-1
.

129
Bomberg, M. T. and Kumaran, M.K., " A Test method to determine air flow resistance of
exterior membranes and sheathings," Journal of Thermal Insulation, Vol.9, pp. 224-235,1986.
B1115.13

113


15. HYGROTHERMAL PROPERTIES OF COMPOSITE WOOD
SIDING



The test specimens used for various measurements reported
here are taken from a composite Wood Siding panel, 4 X 8.
The material is made out of high-density wood fibreboard and
one major surface coated with a paint (factory primed)at a
fraction of a mm thickness. The nominal thickness of the
panel is 7/16.




Hot Surface Temperature
Density: (740 ) 30) kg m
-3

Heat Capacity (From International Energy Agency Annex 24 Report
130
): 1880 J K
-1
kg
-1


Thermal Conductivity:
Measurements are according to ASTM Standard C518; 30 cm X 30 cm specimens are used in
these measurements. The temperatures of the plates are maintained within 0.04 C for these
measurements, for 12 h period to confirm steady state. Heat flow is perpendicular to the major
surfaces.
Table 15.1. Thermal Conductivity of Wood Siding.
Specimen Thickness
mm C
Cold Surface Temperature
C
Conductivity
W m
-1
K
-1

19.74 0.095
10.44 3.77 -3.51 0.092
10.65 28.26 21.28 0.096
10.65 2.68 -3.56
10.44 27.14
0.091

Note: The heat flow meter apparatus is built to measure the heat transmission characteristics of
insulating materials and for those materials the measurement uncertainties are within 2 %. This
same uncertainty is applicable to Wood Siding also.


130
M K Kumaran, Final Report, Volume 3, Material Properties, International Energy Agency
Annex 24 Report, Published by K. U. Leuven Belgium, 1996
B1115.13

114


Sorption Desorption Measurements
131
:
Up to nine specimens, 41 mm X 41 mm X 6 mm each are used in these measurements; the
numbers in parentheses indicate the experimental uncertainties.
Sorption:
Table 15.2. Sorption data for Wood Siding.
RH, % Temperature, C Moisture Content, kg kg
-1

Lab at 22 (1) 0.90 (0.03), nine specimens
50.3 (1) 23 (0.1) 0.047 (0.001), three specimens
69.6 (1) 23 (0.1) 0.069 (0.001), three specimens
91.3 (1) 23 (0.1) 0.131 (0.003), three specimens
100, total saturation

Desorption:
Table 15.3. Desorption data for Wood Siding.
RH, % Temperature, C Moisture Content, kg kg
-1

99.78(0.01)* Lab at 22 (1) 0.38 (0.02), three specimens
91.3 (1) 23.0 (0.1) 0.134 (0.003), two specimens
69.2 (1) 23.0 (0.1) 0.076 (0.002), two specimens
50.3(1) 23.0 (0.1) 0.044 (0.000), two specimens


* It took more than 15 weeks for equilibration. So subsequent measurements in progress, and not
yet at equilibrium after several weeks, were abandoned.

131
In the hygroscopic range, the measurements are done using the proposed procedure for
ASTM Standard C1498, which in turn is based on CEN 89 N 337 E, Hygroscopic Sorption
Curve; at the higher range the pressure plate method is used. Details of the pressure plate
method are given by: Hansen, M. H., "Retention Curves Measured Using Pressure Plate and
Pressure Membrane," Nordtest Technical Report 367, Danish Building Research Institute, 1998,
p 63.
B1115.13

115


Water Vapour Transmission (WVT) Rate measurements
132
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used. The vapour flow
is perpendicular to the major surfaces.

Table 15.4. Dry Cup Measurements on Wood Siding specimens: The numbers in parentheses
indicate the experimental uncertainties for RH and temperature; for WVT Rate the numbers
indicate the standard errors according to a linear regression of data on water vapour transmission
rate at a steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

10.85 50.7 (1) 23.0 (0.1) 5.19E-07 (2.3E-09)
10.80 50.7 (1) 23.0 (0.1) 5.46E-07 (2.2E-09)
10.82 50.7 (1) 23.0 (0.1) 5.52E-07 (3.9E-09)
10.85 70.5 (1) 23.1 (0.1) 7.62E-07 (5.5E-09)
10.80 70.5 (1) 23.1 (0.1) 8.03E-07 (5.4E-09)
70.5 (1) 23.1 (0.1) 8.13E-07 (5.8E-09)
10.85 90.4 (1) 23.0 (0.1) 9.90E-07 (1.2E-08)
10.80 90.4 (1) 23.0 (0.1) 1.03E-06 (1.4E-08)
10.82 90.4 (1) 23.0 (0.1) 1.04E-06 (7.6E-09)
10.82



Table 15.5. Wet Cup Measurements on Wood Siding specimens: The numbers in parentheses
indicate the experimental uncertainties for RH and temperature; for WVT Rate the numbers
indicate the standard errors according to a linear regression of data on water vapour transmission
rate at a steady state.

Chamber Temperature Specimen Thickness
mm
Chamber RH
% C
WVT Rate
kg m
-2
s
-1

10.68 70.5 (1) 23.1 (0.1) 4.02E-07 (4.5E-09)
10.42 70.5 (1) 23.1 (0.1) 3.64E-07 (4.8E-09)
10.35 70.5 (1) 23.1 (0.1) 3.27E-07 (3.7E-09)
10.68 90.9 (1) 23.0 (0.1) 2.20E-07 (1.3E-09)
10.42 90.9 (1) 23.0 (0.1) 2.03E-07 (8.9E-10)
10.35 90.9 (1) 23.0 (0.1) 1.94E-07 (1.9E-09)


The average thickness of still air in the cups in both series is 15 mm


132
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M.
K., A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water
Vapour Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

116


Derived Water Vapour Permeability
133



Table 15.6. The dependence of water vapour permeability of Wood Siding on relative humidity;
the vapour flow is perpendicular to the major surfaces.

RH, % Permeability
kg m
-1
s
-1
Pa
-1

RH, % Permeability
kg m
-1
s
-1
Pa
-1

10
3.92E-12
60
4.88E-12
20
4.09E-12
70
5.10E-12
30
4.28E-12
80
5.34E-12
40
4.47E-12
90
5.58E-12
50
4.67E-12
100
5.83E-12



From the TableCurve statistics, the estimated uncertainty in the derived value of the permeability
may be as high as 45 %.





133
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

117


Water Absorption Coefficient
134
:

Four test specimens, 5 cm X 5 cm X 2 cm each, were used in these measurements. Water is
maintained at (22 1) C. The absorption is across that major surface with the paint coating. The
numbers in parentheses give the standard deviations.

Table 15.7. Water absorption data for Wood Siding.

Square Root of
time, s


Water Absorption
kg m
-2

10.95 0.02 (0.00)
18.97 0.02 (0.01)
30.98 0.03 (0.00)
43.13 0.04 (0.00)
72.66 0.05 (0.00)
89.33 0.06 (0.00)
121.74 0.08 (0.01)
158.18 0.11 (0.01)
281.10 0.21 (0.01)
406.64 0.30 (0.01)

Linear regression using all the data from the first linear part of the absorption process for the four
specimens gives:

Water Absorption Coefficient for the major coated surface = 0.00072 0.00002 kg m

-2
s
-
.


134
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
B1115.13

118


Moisture Diffusivity:

Gamma ray method
135
is used to measure the distribution of moisture in three test
specimens, 5 cm X 23 cm X 2 cm each, during the moisture uptake in a direction parallel to the
major surfaces, in the longitudinal direction. The principle of the methodology is described by
Kumaran et. al
136
. Marchand and Kumaran
137
have reported the procedure used for the data
reduction.

The moisture diffusivity derived from the gamma ray measurements is given in Table 8.

Table 15.8. The dependence of moisture diffusivity of Wood Siding on moisture content; the
moisture transport is parallel to the major surfaces.

Moisture Content
kg kg
-1

Diffusivity
m
2
s
-1

Moisture Content
kg kg
-1

Diffusivity
m
2
s
-1

0.081 5.53E-11
5.11E-11 0.405 3.89E-11
0.108 4.83E-11 0.419 3.9E-11
0.122 4.63E-11 0.432 3.92E-11
0.135 4.47E-11 0.446 3.92E-11
0.149 4.36E-11 0.459 3.94E-11
0.162 4.26E-11 0.473 3.96E-11
0.176 4.18E-11 0.486 3.98E-11
0.189 4.12E-11 0.500 4.01E-11
0.203 4.07E-11 0.514 4.04E-11
0.216 4.03E-11 0.527 4.08E-11
0.230 3.99E-11 0.541 4.12E-11
0.243 3.96E-11 0.554 4.16E-11
0.257 3.93E-11 0.568 4.21E-11
0.270 3.91E-11 0.581 4.27E-11
0.284 3.90E-11 0.595 4.33E-11
0.297 3.88E-11 0.608 4.40E-11
0.311 3.87E-11 0.622 4.48E-11
0.324 3.87E-11 0.635 4.57E-11
0.338 3.86E-11 0.649
3.86E-11 0.662 4.8E-11
0.365 3.87E-11 0.676 4.95E-11
0.378 3.87E-11 0.689
0.392 3.88E-11
0.095
4.68E-11
0.351
5.12E-11

The uncertainty in the derived moisture diffusivity is estimated to be as high as 30 to 50 %.

135
Kumaran, M.K. and Bomberg, M.T., "A Gamma-spectrometer for determination of density
distribution and moisture distribution in building materials," Moisture and Humidity: Measurement
and Control in Science and Industry : Proceedings of International Symposium (Washington,
D.C., USA, 1985), pp. 485-90, 1985.
136
Kumaran, M.K., Mitalas, G.P., Kohonen, R., Ojanen, T, "Moisture transport coefficient of pine
from gamma ray absorption measurements," Collected Papers in Heat Transfer, 1989 : Winter
Annual Meeting of the ASME (San Francisco, CA, USA, 1989) pp. 179-183, 1989(ASME Heat
Transfer Division vol. 123).
137
Marchand, R.G. and Kumaran, M. K., "Moisture diffusivity of cellulose insulation," Journal of
Thermal Insulation and Building Envelopes, Vol. 17, pp. 362-377, 1994.
B1115.13

119


Air Permeability:
Bomberg and Kumaran
138
have reported the principle of the method used in these
measurements. Appendix XIII of the Client Report to ASHRAE, B-1115.3 A Thermal and
Moisture Transport Property Database for Common Building and Insulating Materials 1018-RP
dated 1 April 1999 reports the details. Three circular test specimens (thickness 10.50, 10.60 and
10.50 mm), each approximately 13 cm in diameter, are used in these measurements. The
measurements are conducted at a temperature = (22 1) C.
The summary of the statistical analyses of all data obtained from two series of
measurements on each specimen is shown in Figure 1 as three separate sets.

0
0.02
0.04
0.06
0.08
0.1
0.12
0.14
0 50 100 150 200 250 300 350
Pressure Difference, Pa
F
l
o
w
,

l

m
-
2

s
-
1
Data Points Mean Permeance
Upper Confidence Interval Lower Confidence Interval

Figure 15.1. The dependence of airflow rate on pressure difference for Wood Siding.



For the range of pressure differences between 25 Pa and 300 Pa, the flow rate linearly
varies with the pressure difference. The air permeability is (4.5 1.2) E-09 kg m
-1
Pa
-1
s
-1
.

138
Bomberg, M. T. and Kumaran, M.K., " A Test method to determine air flow resistance of
exterior membranes and sheathings," Journal of Thermal Insulation, Vol.9, pp. 224-235,1986.
B1115.13

120


16 HYGROTHERMAL PROPERTIES OF CLAY BRICK



The properties reported here are obtained on one type of clay brick. It is
manufactured in Canada and is identified as Charleston Brick. Test
specimens are prepared from several 72 mm X 78 mm X 250 mm samples
from one production batch. The bricks are light reddish brown in colour
and referred to as Extruded Clay Brick.



Density: (1980 30) kg m
-3


Thermal Conductivity:
C
Heat Capacity (From International Energy Agency Annex 24 Report
139
): 840 J K
-1
kg
-1


Measurements are according to ASTM Standard C518; one 30 cm X 30 cm specimen,
assembled from several 10 cm X 20 cm blocks are used in these measurements. The
temperatures of the plates are maintained within 0.04 C for these measurements, for 12 h period
to confirm steady state. Heat flow is perpendicular to the major surfaces.
Table 16.1. Thermal Conductivity of brick.
Specimen Thickness
mm
Hot Surface Temperature Cold surface Temperature
C
Conductivity
W m
-1
K
-1

12.17 27.09 21.70 0.42
12.02 14.52 7.98 0.41

Note: The heat flow meter apparatus is built to measure the heat transmission characteristics of
insulating materials and for those materials the measurement uncertainties are within 2 %. Brick
being highly conductive and the test specimen being assembled from several blocks that have
been friction fitted, the uncertainty in these measurements can be as high as 5 to 10 %.

139
M K Kumaran, Final Report, Volume 3, Material Properties, International Energy Agency
Annex 24 Report, Published by K. U. Leuven Belgium, 1996
B1115.13

121


Sorption Desorption Measurements
140
:

Up to nine specimens, 40 mm X 40 mm each at the full board thickness are used in these
measurements; the numbers in parentheses indicate the experimental uncertainties.

Sorption:
Table 16.2. Sorption data for brick.
RH, % Temperature, C Moisture Content, kg kg
-1

100, total saturation Lab at 22 (1) 0.099 (0.002), nine specimens
50.0 (1) 23 (0.2) 0.0008 (0.0001), three specimens
69.1 (1) 23 (0.2) 0.0012 (0.002), three specimens
91.2 (1) 23 (0.2) 0.0010 (0.002), three specimens

Desorption:

Table 16.3. Desorption data for brick.
RH, % Temperature, C Moisture Content, kg kg
-1

99.93(0.01) Lab at 22 (1) 0.091 (0.003), nine specimens
99.85(0.01) Lab at 22 (1) 0.086 (0.003), nine specimens
Lab at 22 (1) 0.082 (0.004), nine specimens
99.63 (0.01) Lab at 22 (1) 0.060 (0.010), nine specimens
99.49 (0.01) Lab at 22 (1) 0.056 (0.010), nine specimens
99.27 (0.01) Lab at 22 (1) 0.050 (0.010), nine specimens
98.90 (0.01)
91.2 (1)
23.0 (0.2)
99.71 (0.01)
Lab at 22 (1) 0.045 (0.010), nine specimens
23.0 (0.2) 0.00, two specimens
69.1 (1) 0.00, two specimens
50.0 (1) 23.0 (0.2) 0.00, two specimens



140
In the hygroscopic range, the measurements are done using the proposed procedure for
ASTM Standard C1498, which in turn is based on CEN 89 N 337 E, Hygroscopic Sorption
Curve; at the higher range the pressure plate method is used. Details of the pressure plate
method are given by: Hansen, M. H., "Retention Curves Measured Using Pressure Plate and
Pressure Membrane," Nordtest Technical Report 367, Danish Building Research Institute, 1998,
p 63.
B1115.13

122


Water Vapour Transmission (WVT) Rate measurements
141
:
For each test condition, 3 rectangular specimens, each 20 cm X 8 cm, are used.

Table 16.4. Dry Cup Measurements on brick specimens: The numbers in parentheses indicate
the experimental uncertainties for RH and temperature; for WVT Rate the numbers indicate the
standard errors according to a linear regression of data on water vapour transmission rate at a
steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
-2 -1
12.37 50.5 (1) 22.9 (0.1) 4.66E-07 (6.4E-09)
12.35 50.5 (1) 22.9 (0.1) 4.84E-07 (5.5E-09)
12.41 50.5 (1) 22.9 (0.1) 4.77E-07 (4.9E-09)
12.37 70.6 (1) 22.9 (0.1) 6.90E-07 (1.0E-09)
12.35 70.6 (1) 22.9 (0.1) 7.12E-07 (1.7E-09)
12.41 70.6 (1) 22.9 (0.1) 7.01E-07 (2.1E-09)
12.37 90.6 (1) 22.9 (0.1) 8.96E-07 (2.1E-09)
12.35 90.6 (1) 22.9 (0.1) 9.19E-07 (1.1E-09)
12.41 90.6 (1) 22.9 (0.1) 9.00E-07 (4.6E-10)
kg m s


Table 16.5. Wet Cup Measurements on brick specimens: The numbers in parentheses indicate
the experimental uncertainties for RH and temperature; for WVT Rate the numbers indicate the
standard errors according to a linear regression of data on water vapour transmission rate at a
steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

12.46 70.6 (1) 22.9 (0.1) 3.59E-07(2.3E-09)
12.26 70.6 (1) 22.9 (0.1) 3.54E-07 (1.7E-09)
12.41 70.6 (1) 22.9 (0.1) 3.40E-07 (1.6E-09)
12.46 91.4 (2) 22.7 (0.3) 1.20E-07 (2.0E-09)
12.26 91.4 (2) 22.7 (0.3) 1.20E-07 (1.3E-09)
12.41 91.4 (2) 22.7 (0.3) 1.17E-07 (1.4E-09)


The average thickness of still air in the cups for both series is 15 mm

141
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M.
K., A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water
Vapour Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

123


Derived Water Vapour Permeability
142



Table 16.6. The dependence of water vapour permeability of brick on relative humidity.

RH, % Permeability
kg m
-1
s
-1
Pa
-1

RH, % Permeability
kg m
-1
s
-1
Pa
-1

10 4.14E-12 60 4.94E-12
20 4.29E-12 70 5.12E-12
30 4.44E-12 80 5.31E-12
40 4.60E-12 90 5.50E-12
50 4.77E-12 100 5.70E-12




From the TableCurve statistics, the estimated uncertainty in the derived value of the permeability
is about 20 %.




142
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

124


Water Absorption Coefficient
143
:

Four test specimens, 5 cm X 5 cm each (thickness 12 mm), were used in these measurements.
Water is maintained at (22 1) C. The absorption is across the major surface. The numbers in
parentheses give the standard deviations.

Table 16.7. Water absorption data for brick.

Square Root of
time, s


Water Absorption
kg m
-2

7.75 1.30 (0.24)
13.42 1.56 (0.14)
18.97 1.65 (0.07)
30.98 1.68 (0.07)
43.13 1.67 (0.07)
60.50 1.68 (0.07)

The absorption process was very fast. From the above data it is estimated that


Water Absorption Coefficient for this brick is approximately 0.17 kg m
-2
s
-
.


143
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
B1115.13

125


Moisture Diffusivity:

Gamma ray method
144
is used to measure the distribution of moisture in three test
specimens, 6.5 cm X 20 cm each (1 cm thick), during a moisture uptake process. The principle
of the methodology is described by Kumaran et. al
145
. Marchand and Kumaran
146
have reported
the procedure used for the data reduction.

The moisture diffusivity derived from the gamma ray measurements is given in Table 8.

Table 16.8. The dependence of moisture diffusivity of brick on moisture content.

Moisture Content
kg kg
-1

Diffusivity
m
2
s
-1

Moisture Content
kg kg
-1

Diffusivity
m
2
s
-1

0.005 2.26E-08 0.045 2.37E-07
0.010 4.57E-08 0.051 2.75E-07
0.015 6.94E-08 0.056 3.19E-07
0.020 9.38E-08 0.061 3.74E-07
0.025 1.19E-07 0.066 4.5E-07
1.46E-07 0.071 5.74E-07
0.035 1.74E-07 0.076 9.01E-07
0.040 2.04E-07
0.030

The uncertainty in the derived moisture diffusivity is estimated to be as high as 30 to 50 %.

144
Kumaran, M.K. and Bomberg, M.T., "A Gamma-spectrometer for determination of density
distribution and moisture distribution in building materials," Moisture and Humidity: Measurement
and Control in Science and Industry : Proceedings of International Symposium (Washington,
D.C., USA, 1985), pp. 485-90, 1985.
145
Kumaran, M.K., Mitalas, G.P., Kohonen, R., Ojanen, T, "Moisture transport coefficient of pine
from gamma ray absorption measurements," Collected Papers in Heat Transfer, 1989 : Winter
Annual Meeting of the ASME (San Francisco, CA, USA, 1989) pp. 179-183, 1989(ASME Heat
Transfer Division vol. 123).
146
Marchand, R.G. and Kumaran, M. K., "Moisture diffusivity of cellulose insulation," Journal of
Thermal Insulation and Building Envelopes, Vol. 17, pp. 362-377, 1994.
B1115.13

126


Air Permeability:
Bomberg and Kumaran
147
have reported the principle of the method used in these
measurements. Appendix XIII of the Client Report to ASHRAE, B-1115.3 A Thermal and
Moisture Transport Property Database for Common Building and Insulating Materials 1018-RP
dated 1 April 1999 reports the details. Three rectangular test specimens, 20 cm X 8 cm (thickness
12.46, 12.26 and 12.41 mm), are used in these measurements. The measurements are
conducted at a temperature = (22 1) C. No measurable airflow resulted for pressure
differences up to 3 kPa. From pressure decay measurements on a number of brick specimens it
is estimated that the air permeability of bricks is about 1.5 to 5.0 E-10 kg m
-1
Pa
-1
s
-1
.


147
Bomberg, M. T. and Kumaran, M.K., " A Test method to determine air flow resistance of
exterior membranes and sheathings," Journal of Thermal Insulation, Vol.9, pp. 224-235,1986.
B1115.13

127


17. HYGROTHERMAL PROPERTIES OF MORTAR



The properties reported are obtained on one masonry cement mortar mix,
type N: 1 part by volume of masonry cement type N and 2 to 3 parts by
volume of aggregate.



Density: (1600 30) kg m
-3


Heat Capacity (From International Energy Agency Annex 24 Report 840 J K
W m
148
):
-1
kg
-1


Thermal Conductivity:
Measurements are according to ASTM Standard C518; two 30 cm X 30 cm specimens were used
in these measurements. The temperatures of the plates are maintained within 0.04 C for these
measurements, for 12 h period to confirm steady state.
Table 16.1. Thermal Conductivity of mortar.
Specimen Thickness
mm
Hot Surface Temperature
C
Cold surface Temperature
C
Conductivity
-1
K
-1

18.73 24.72 19.51 0.46
18.73 1.33 -3.34 0.45
18.96 24.92 19.87 0.48
18.96 1.74 -3.20 0.45

Note: The heat flow meter apparatus is built to measure the heat transmission characteristics of
insulating materials and for those materials the measurement uncertainties are within 2 %. Mortar
being highly conductive the uncertainty in these measurements can be as high as 5 to 10 %.

148
M K Kumaran, Final Report, Volume 3, Material Properties, International Energy Agency
Annex 24 Report, Published by K. U. Leuven Belgium, 1996
B1115.13

128


Sorption Desorption Measurements
149
:

Up to nine specimens, 40 mm X 40 mm each at the full board thickness are used in these
measurements; the numbers in parentheses indicate the experimental uncertainties.

Sorption:
Table 16.2. Sorption data for mortar.
RH, % Temperature, C Moisture Content, kg kg
-1

100, total saturation Lab at 22 (1) 0.26 (0.02), nine specimens
49.9 (1) 23 (0.2) 0.0042 (0.002), three specimens
70.1 (1) 23 (0.2) 0.023 (0.003), three specimens
89.9 (1) 23 (0.2) 0.053 (0.009), three specimens

Desorption:

Table 16.3. Desorption data for mortar.
RH, % Temperature, C Moisture Content, kg kg
-1

99.93(0.01) Lab at 22 (1) 0.25 (0.01), three specimens
99.71 (0.01) Lab at 22 (1) 0.25 (0.02), three specimens
99.63 (0.01) Lab at 22 (1) 0.22 (0.01), three specimens
99.49 (0.01) Lab at 22 (1) 0.20 (0.02), three specimens
99.27 (0.01) Lab at 22 (1) 0.19 (0.01), three specimens
98.90 (0.01) Lab at 22 (1) 0.17 (0.03), three specimens
89.9 (1) 23.0 (0.2) 0.061 (0.000), two specimens
70.2 (1) 23.0 (0.2) 0.044 (0.000), two specimens
49.9 (1) 23.0 (0.2) 0.034 (0.000), two specimens



149
In the hygroscopic range, the measurements are done using the proposed procedure for
ASTM Standard C1498, which in turn is based on CEN 89 N 337 E, Hygroscopic Sorption
Curve; at the higher range the pressure plate method is used. Details of the pressure plate
method are given by: Hansen, M. H., "Retention Curves Measured Using Pressure Plate and
Pressure Membrane," Nordtest Technical Report 367, Danish Building Research Institute, 1998,
p 63.
B1115.13

129


Water Vapour Transmission (WVT) Rate measurements
150
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used.

Table 16.4. Dry Cup Measurements on mortar specimens: The numbers in parentheses indicate
the experimental uncertainties for RH and temperature; for WVT Rate the numbers indicate the
standard errors according to a linear regression of data on water vapour transmission rate at a
steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

13.43 49.8 (1) 23.1 (0.1) 1.32E-06 (9.0E-09)
13.15 49.8 (1) 23.1 (0.1) 1.22E-06 (6.7E-09)
12.74 49.8 (1) 23.1 (0.1) 1.18E-06 (8.5E-09)
13.43 70.8 (1) 23.2 (0.1) 2.63E-06 (3.3E-09)
13.15 70.8 (1) 23.2 (0.1) 2.48E-06 (8.3E-09)
12.74 70.8 (1) 23.2 (0.1) 2.47E-06 (4.9E-09)
13.43 89.2 (1) 23.1 (0.1) 3.45E-06 (9.0E-09)
13.15 89.2 (1) 23.1 (0.1) 3.28E-06 (1.2E-08)
12.74 89.2 (1) 23.1 (0.1) 3.25E-06 (1.4E-08)


Table 16.5. Wet Cup Measurements on mortar specimens: The numbers in parentheses indicate
the experimental uncertainties for RH and temperature; for WVT Rate the numbers indicate the
standard errors according to a linear regression of data on water vapour transmission rate at a
steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

12.95 71.0 (1) 23.2 (0.1) 1.18E-06 (1.0E-08)
13.06 71.0 (1) 23.2 (0.1) 1.26E-06 (7.7E-09)
13.21 71.0 (1) 23.2 (0.1) 1.09E-06 (6.5E-09)
12.95 89.1 (1) 23.1 (0.1) 3.63E-07 (3.1E-09)
13.06 89.1 (1) 23.1 (0.1) 4.68E-07 (3.0E-09)
13.21 89.1 (1) 23.1 (0.1) 4.00E-07 (1.8E-09)


The average thickness of still air in the cups for both series is 15 mm

150
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M.
K., A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water
Vapour Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

130


Derived Water Vapour Permeability
151



Table 16.6. The dependence of water vapour permeability of mortar on relative humidity.

RH, % Permeability
kg m
-1
s
-1
Pa
-1

RH, % Permeability
kg m
-1
s
-1
Pa
-1

10
1.36E-11
60
2.22E-11
1.50E-11
70
2.45E-11
30
1.65E-11
80
2.72E-11
40
1.82E-11
90
3.02E-11
50
2.01E-11
100
3.36E-11
20




From the TableCurve statistics, the estimated uncertainty in the derived value of the permeability
is about 40 %.




151
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

131


Water Absorption Coefficient
152
:

Four test specimens, 5 cm X 5 cm each (thickness 13 mm), were used in these measurements.
Water is maintained at (22 1) C. The absorption is across the major surface. The numbers in
parentheses give the standard deviations.

Table 16.7. Water absorption data for mortar.

Square Root of
time, s


Water Absorption
kg m
-2

7.75 0.41 (0.02)
10.95 0.48 (0.02)
15.49 0.57 (0.02)
20.49 0.65 (0.02)
26.83 0.75 (0.02)
(0.03)
42.43 0.97 (0.03)
7.75
36.33 0.89
0.41 (0.02)

There is no clear initial linear part in the absorption process.


Water Absorption Coefficient for mortar is approximately (0.02 0.01) kg m
-2
s
-
.


152
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
B1115.13

132


Moisture Diffusivity:

Diffusivity
Gamma ray method
153
is used to measure the distribution of moisture in three test
specimens, 6.5 cm X 20 cm each (1 cm thick), during a moisture uptake process. The principle
of the methodology is described by Kumaran et. al
154
. Marchand and Kumaran
155
have reported
the procedure used for the data reduction.

The moisture diffusivity derived from the gamma ray measurements is given in Table 8.

Table 16.8. The dependence of moisture diffusivity of mortar on moisture content.

Moisture Content
kg kg
-1

Diffusivity
m
2
s
-1

Moisture Content
kg kg
-1

m
2
s
-1

8.96E-09 0.081 3.73E-09
0.019 4.74E-09 0.088 4.52E-09
0.025 3.53E-09 0.094 7.07E-09
0.031 3.12E-09 0.100 5.19E-09
0.038 2.93E-09 0.106 2.24E-09
0.044 2.86E-09 0.113 1.61E-09
2.84E-09 0.119 1.25E-09
2.88E-09 0.125 9.00E-10
2.96E-09 0.131 6.13E-10
3.10E-09 0.138 4.29E-10
0.075 3.33E-09 0.144 3.19E-10
0.013
0.050
0.056
0.063
0.069

The uncertainty in the derived moisture diffusivity is estimated to be as high as 30 to 50 %.

153
Kumaran, M.K. and Bomberg, M.T., "A Gamma-spectrometer for determination of density
distribution and moisture distribution in building materials," Moisture and Humidity: Measurement
and Control in Science and Industry : Proceedings of International Symposium (Washington,
D.C., USA, 1985), pp. 485-90, 1985.
154
Kumaran, M.K., Mitalas, G.P., Kohonen, R., Ojanen, T, "Moisture transport coefficient of pine
from gamma ray absorption measurements," Collected Papers in Heat Transfer, 1989 : Winter
Annual Meeting of the ASME (San Francisco, CA, USA, 1989) pp. 179-183, 1989(ASME Heat
Transfer Division vol. 123).
155
Marchand, R.G. and Kumaran, M. K., "Moisture diffusivity of cellulose insulation," Journal of
Thermal Insulation and Building Envelopes, Vol. 17, pp. 362-377, 1994.
B1115.13

133


Air Permeability:
Bomberg and Kumaran
156
have reported the principle of the method used in these
measurements. Appendix XIII of the Client Report to ASHRAE, B-1115.3 A Thermal and
Moisture Transport Property Database for Common Building and Insulating Materials 1018-RP
dated 1 April 1999 reports the details. Three circular test specimens, 15 cm in diameter
(thickness 13.43, 13.15 and 13.06 mm), are used in these measurements. The measurements
are conducted at a temperature = (22 1) C.
The summary of the statistical analyses of all data obtained from two series of
measurements on each specimen is shown in Figure 1 as three separate sets.

0
0.02
0.04
0.06
0.08
0.1
0.12
0.14
0.16
0.18
0 200 400 600 800 1000 1200 1400
Pressure Difference, Pa
F
l
o
w
,

l

m
-
2

s
-
1
Data Points Mean Permeance
Upper Confidence Interval Lower Confidence Interval

Figure 16.1. The dependence of airflow rate on pressure difference for mortar.


For the range of pressure differences between 100 Pa and 1300 Pa, the flow rate linearly
varies with the pressure difference. The air permeability is (1.5 0.5) E-09 kg m
-1
Pa
-1
s
-1
.

156
Bomberg, M. T. and Kumaran, M.K., " A Test method to determine air flow resistance of
exterior membranes and sheathings," Journal of Thermal Insulation, Vol.9, pp. 224-235,1986.
B1115.13

134


18. HYGROTHERMAL PROPERTIES OF STUCCO




The properties reported are obtained on one regular Portland stucco mix.
Slabs were prepared and allowed to cure for 28 days as suggested by the
manufacturer. No lath was embedded in these samples.



Density: (1985 30) kg m
-3

Heat Capacity (From International Energy Agency Annex 24 Report
157
): 840 J K
-1
kg
-1


Thermal Conductivity:
Measurements are according to ASTM Standard C518; two 30 cm X 30 cm specimen were used
in these measurements. The temperatures of the plates are maintained within 0.04 C for these
measurements, for 12 h period to confirm steady state.
Table 18.1. Thermal Conductivity of stucco.
Specimen Thickness
mm
Hot Surface Temperature
C
Cold surface Temperature
C
Conductivity
W m
-1
K
-1

19.93 0.41
14.69 2.77 -2.28 0.39
12.87 24.62 20.04 0.41
12.87 2.26 -1.86 0.39
14.69 25.00

Note: The heat flow meter apparatus is built to measure the heat transmission characteristics of
insulating materials and for those materials the measurement uncertainties are within 2 %. Stucco
being highly conductive the uncertainty in these measurements can be as high as 5 to 10 %.

157
M K Kumaran, Final Report, Volume 3, Material Properties, International Energy Agency
Annex 24 Report, Published by K. U. Leuven Belgium, 1996
B1115.13

135


Sorption Desorption Measurements
158
:

Up to nine specimens, 40 mm X 40 mm each at the full board thickness are used in these
measurements; the numbers in parentheses indicate the experimental uncertainties.

Sorption:
Table 18.2. Sorption data for stucco.
RH, % Temperature, C Moisture Content, kg kg
-1

100, total saturation Lab at 22 (1) 0.120 (0.002), nine specimens
50.0 (1) 23 (0.2) 0.030 (0.001), three specimens
70.3 (1) 23 (0.2) 0.037 (0.001), three specimens
89.9 (1) 23 (0.2) 0.058 (0.001), three specimens

Desorption:

Table 18.3. Desorption data for stucco.
RH, % Temperature, C Moisture Content, kg kg
-1

Lab at 22 (1) 0.117 (0.001), six specimens
99.85 (0.01) Lab at 22 (1) 0.117 (0.002), six specimens
99.71 (0.01) Lab at 22 (1) 0.117 (0.002), six specimens
99.63 (0.01) Lab at 22 (1) 0.117 (0.002), six specimens
99.49 (0.01) Lab at 22 (1) 0.116 (0.002), six specimens
99.27 (0.01) Lab at 22 (1) 0.116 (0.002), six specimens
98.90 (0.01) Lab at 22 (1) 0.116 (0.002), six specimens
97.81 (0.01) Lab at 22 (1) 0.104 (0.002), six specimens
96.74 (0.01) Lab at 22 (1) 0.103 (0.002), six specimens
95.29 (0.01) Lab at 22 (1) 0.103 (0.002), six specimens
90.3 (1) 23.0 (0.2) 0.070 (0.01), two specimens
70.3 (1) 23.0 (0.2) 0.052 (0.01), two specimens
50.0 (1) 23.0 (0.2) 0.042 (0.01), two specimens
99.93(0.01)



158
In the hygroscopic range, the measurements are done using the proposed procedure for
ASTM Standard C1498, which in turn is based on CEN 89 N 337 E, Hygroscopic Sorption
Curve; at the higher range the pressure plate method is used. Details of the pressure plate
method are given by: Hansen, M. H., "Retention Curves Measured Using Pressure Plate and
Pressure Membrane," Nordtest Technical Report 367, Danish Building Research Institute, 1998,
p 63.
B1115.13

136


Water Vapour Transmission (WVT) Rate measurements
159
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used.

Table 18.4. Dry Cup Measurements on stucco specimens: The numbers in parentheses indicate
the experimental uncertainties for RH and temperature; for WVT Rate the numbers indicate the
standard errors according to a linear regression of data on water vapour transmission rate at a
steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

13.60 50.0 (1) 23.1 (0.1) 9.52E-08 (1.3E-09)
14.03 50.0 (1) 23.1 (0.1) 8.58E-08 (1.0E-09)
13.28 50.0 (1) 23.1 (0.1) 1.12E-07 (7.7E-10)
13.60 70.0 (1) 23.3 (0.1) 2.00E-07 (2.4E-09)
14.03 70.0 (1) 23.3 (0.1) 1.89E-07 (3.6E-09)
13.28 70.0 (1) 23.3 (0.1) 2.19E-07 (2.8E-09)
13.60 90.2 (1) 22.9 (0.1) 2.98E-07 (4.7E-09)
14.03 90.2 (1) 22.9 (0.1) 2.85E-07 (3.0E-09)
13.28 90.2 (1) 22.9 (0.1) 3.24E-07 (3.4E-09)


Table 18.5. Wet Cup Measurements on stucco specimens: The numbers in parentheses indicate
the experimental uncertainties for RH and temperature; for WVT Rate the numbers indicate the
standard errors according to a linear regression of data on water vapour transmission rate at a
steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

12.37 70.2 (1) 23.2 (0.1) 1.54E-07 (8.7E-10)
14.88 70.2 (1) 23.2 (0.1) 9.37E-08 (1.9E-09)
14.69 70.2 (1) 23.2 (0.1) 1.13E-07 (2.4E-09)
12.37 89.6 (1) 23.1 (0.1) 8.65E-08 (1.5E-09)
14.88 89.6 (1) 23.1 (0.1) 3.94E-08 (4.8E-10)
14.69 89.6 (1) 23.1 (0.1) 5.20E-08 (4.5E-10)


The average thickness of still air in the cups for both series is 15 mm

159
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M.
K., A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water
Vapour Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

137


Derived Water Vapour Permeability
160



Table 18.6. The dependence of water vapour permeability of stucco on relative humidity.

RH, % Permeability
kg m
-1
s
-1
Pa
-1

RH, % Permeability
kg m
-1
s
-1
Pa
-1

10
8.14E-13
60
1.94E-12
20
9.68E-13
70
2.31E-12
30
1.15E-12
80
2.74E-12
40
1.37E-12
90
3.26E-12
50
1.63E-12
100
3.88E-12




From the TableCurve statistics, the estimated uncertainty in the derived value of the permeability
is about 25 %.




160
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

138


Water Absorption Coefficient
161
:

Four test specimens, 5 cm X 5 cm each (thickness 13 mm), were used in these measurements.
Water is maintained at (22 1) C. The absorption is across the major surface. The numbers in
parentheses give the standard deviations.

Table 18.7. Water absorption data for stucco.

Square Root of
time, s


Water Absorption
kg m
-2

7.75 0.16 (0.01)
13.42 0.21 (0.01)
18.97 0.26 (0.01)
24.49 0.33 (0.01)
30.00 0.40 (0.02)
34.64 0.46 (0.02)
42.43 0.56 (0.02)
59.50 0.78 (0.02)
76.29 0.97 (0.03)
86.95 1.09 (0.03)
96.75 1.20 (0.04)
114.89 1.41 (0.05)
136.38 1.61 (0.07)
146.77 1.69 (0.08)
156.84 1.76 (0.09)

A linear regression of data from the initial part of the process gives;


Water Absorption Coefficient for stucco is (0.012 0.001) kg m
-2
s
-
.


161
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
B1115.13

139


Moisture Diffusivity:

Gamma ray method
162
is used to measure the distribution of moisture in three test
specimens, 6.5 cm X 20 cm each (1 cm thick), during a moisture uptake process. The principle
of the methodology is described by Kumaran et. al
163
. Marchand and Kumaran
164
have reported
the procedure used for the data reduction.

The moisture diffusivity derived from the gamma ray measurements is given in Table 8.

Table 18.8. The dependence of moisture diffusivity of stucco on moisture content.

Moisture Content
kg kg
-1

Diffusivity
m
2
s
-1

Moisture Content
kg kg
-1

Diffusivity
m
2
s
-1

0.005 6.64E-10 0.087 1.86E-09
0.010 1.64E-09 0.092 1.17E-09
0.015 3.31E-09 0.097 8.38E-10
0.020 7.00E-09 0.102 6.45E-10
0.025 1.48E-08 0.107 5.20E-10
1.18E-08 0.112 4.33E-10
0.036 9.01E-09 0.117 3.69E-10
0.041 7.88E-09 0.122 3.21E-10
7.43E-09 0.127 2.83E-10
7.35E-09 0.132 2.52E-10
7.57E-09 0.137 2.27E-10
0.061 8.13E-09 0.142 2.06E-10
0.066 9.32E-09 0.148 1.89E-10
0.071 1.23E-08 0.153 1.74E-10
0.081 3.96E-09 0.158 1.61E-10
0.031
0.046
0.051
0.056

The uncertainty in the derived moisture diffusivity is estimated to be as high as 30 to 50 %.

162
Kumaran, M.K. and Bomberg, M.T., "A Gamma-spectrometer for determination of density
distribution and moisture distribution in building materials," Moisture and Humidity: Measurement
and Control in Science and Industry : Proceedings of International Symposium (Washington,
D.C., USA, 1985), pp. 485-90, 1985.
163
Kumaran, M.K., Mitalas, G.P., Kohonen, R., Ojanen, T, "Moisture transport coefficient of pine
from gamma ray absorption measurements," Collected Papers in Heat Transfer, 1989 : Winter
Annual Meeting of the ASME (San Francisco, CA, USA, 1989) pp. 179-183, 1989(ASME Heat
Transfer Division vol. 123).
164
Marchand, R.G. and Kumaran, M. K., "Moisture diffusivity of cellulose insulation," Journal of
Thermal Insulation and Building Envelopes, Vol. 17, pp. 362-377, 1994.
B1115.13

140


Air Permeability:
Bomberg and Kumaran
165
have reported the principle of the method used in these
measurements. Appendix XIII of the Client Report to ASHRAE, B-1115.3 A Thermal and
Moisture Transport Property Database for Common Building and Insulating Materials 1018-RP
dated 1 April 1999 reports the details. Three circular test specimens, 15 cm in diameter
(thickness 13.60, 14.03 and 13.28 mm), are used in these measurements. The measurements
are conducted at a temperature = (22 1) C. No measurable airflow resulted for pressure
differences up to 3 kPa. From pressure decay measurements on the specimens it is estimated
that the air permeability of stucco is approximately 1 E-11 kg m
-1
Pa
-1
s
-1
.




165
Bomberg, M. T. and Kumaran, M.K., " A Test method to determine air flow resistance of
exterior membranes and sheathings," Journal of Thermal Insulation, Vol.9, pp. 224-235,1986.
B1115.13

141


19. HYGROTHERMAL PROPERTIES OF FIBRE CEMENT
SHEATHING BOARD


Cold surface Temperature



All test specimens used for the measurements reported here are prepared
from one board of a commercial product with a nominal thickness of 5/16.

Density: (1380 40) kg m
-3

Heat Capacity (From International Energy Agency Annex 24 Report
166
): 840 J K
-1
kg
-1


Thermal Conductivity:
Measurements are according to ASTM Standard C518; two 30 cm X 30 cm specimens were used
in these measurements. The temperatures of the plates are maintained within 0.04 C for these
measurements, for 12 h period to confirm steady state.
Table 19.1. Thermal Conductivity of fibre cement board.
Specimen Thickness
mm
Hot Surface Temperature
C C
Conductivity
W m
-1
K
-1

7.82 26.95 23.07 0.25
7.82 3.15 -0.47 0.24
7.86 25.91 22.09 0.25
7.86 1.49 -2.16 0.24

Note: The heat flow meter apparatus is built to measure the heat transmission characteristics of
insulating materials and for those materials the measurement uncertainties are within 2 %. Fibre
cement being more conductive than insulation materials the uncertainty in these measurements
can be as high as 5 %.

166
M K Kumaran, Final Report, Volume 3, Material Properties, International Energy Agency
Annex 24 Report, Published by K. U. Leuven Belgium, 1996
B1115.13

142


Sorption Desorption Measurements
Temperature, C
167
:

Up to nine specimens, 40 mm X 40 mm each at the full board thickness are used in these
measurements; the numbers in parentheses indicate the experimental uncertainties.

Sorption:
Table 19.2. Sorption data for fibre cement.
RH, % Moisture Content, kg kg
-1

100, total saturation Lab at 22 (1) 0.347 (0.018), nine specimens
70.4 (1) 23 (0.2) 0.058 (0.009), three specimens
89.9 (1) 23 (0.2) 0.168 (0.020), three specimens
50.6 (1) 23 (0.2) 0.040 (0.001), three specimens

Desorption:
Table 19.3. Desorption data for fibre cement.
RH, % Temperature, C Moisture Content, kg kg
-1

99.93(0.01) Lab at 22 (1) 0.339 (0.018), nine specimens
99.85 (0.01) Lab at 22 (1) 0.333 (0.018), nine specimens
99.78 (0.01) Lab at 22 (1) 0.330 (0.018), nine specimens
99.71 (0.01) Lab at 22 (1) 0.329 (0.018), nine specimens
99.63 (0.01) Lab at 22 (1) 0.327 (0.018), nine specimens
99.49 (0.01) Lab at 22 (1) 0.325 (0.017), nine specimens
99.27 (0.01) Lab at 22 (1) 0.322 (0.017), nine specimens
98.90 (0.01) Lab at 22 (1) 0.324 (0.017), nine specimens
97.81 (0.01) Lab at 22 (1) 0.318 (0.017), nine specimens
96.74 (0.01) Lab at 22 (1) 0.320 (0.018), nine specimens
95.32 (0.01) Lab at 22 (1) 0.313 (0.018), nine specimens
90.6 (1) 23.0 (0.2) 0.196 (0.001), two specimens
70.5 (1) 23.0 (0.2) 0.123 (0.002), two specimens
50.5 (1) 23.0 (0.2) 0.066 (0.000), two specimens



167
In the hygroscopic range, the measurements are done using the proposed procedure for
ASTM Standard C1498, which in turn is based on CEN 89 N 337 E, Hygroscopic Sorption
Curve; at the higher range the pressure plate method is used. Details of the pressure plate
method are given by: Hansen, M. H., "Retention Curves Measured Using Pressure Plate and
Pressure Membrane," Nordtest Technical Report 367, Danish Building Research Institute, 1998,
p 63.
B1115.13

143


Water Vapour Transmission (WVT) Rate measurements
168
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used.

Table 19.4. Dry Cup Measurements on fibre cement specimens: The numbers in parentheses
indicate the experimental uncertainties for RH and temperature; for WVT Rate the numbers
indicate the standard errors according to a linear regression of data on water vapour transmission
rate at a steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

7.80 50.4 (1) 22.9 (0.1) 1.76E-07 (1.6E-09)
7.74 50.4 (1) 22.9 (0.1) 1.17E-07 (1.5E-09)
7.86 50.4 (1) 22.9 (0.1) 2.20E-07 (2.0E-09)
70.4 (1) 22.9 (0.1) 3.15E-07 (3.3E-09)
7.74 70.4 (1) 22.9 (0.1) 2.49E-07 (2.8E-09)
7.86 70.4 (1) 22.9 (0.1) 3.84E-07 (3.3E-09)
7.80 91.3 (1) 22.7 (0.1) 6.66E-07 (7.0E-09)
7.74 91.3 (1) 22.7 (0.1) 6.64E-07 (6.4E-09)
7.86 91.3 (1) 22.7 (0.1) 8.65E-07 (4.8E-09)
7.80


Table 19.5. Wet Cup Measurements on fibre cement specimens: The numbers in parentheses
indicate the experimental uncertainties for RH and temperature; for WVT Rate the numbers
indicate the standard errors according to a linear regression of data on water vapour transmission
rate at a steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

7.71 70.3 (1) 22.9 (0.1) 1.05E-06 (1.4E-08)
70.3 (1) 22.9 (0.1) 1.14E-06 (6.7E-09)
70.3 (1) 22.9 (0.1) 9.43E-07 (1.5E-09)
91.2 (1) 22.7 (0.1) 8.17E-07 (7.4E-09)
8.03 91.2 (1) 22.7 (0.1) 8.21E-07 (6.0E-09)
7.93 91.2 (1) 22.7 (0.1) 6.72E-07 (8.3E-09)
8.03
7.93
7.71


The average thickness of still air in the cups for both series is 15 mm

168
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M.
K., A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water
Vapour Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

144


Derived Water Vapour Permeability
169


kg m

Table 19.6. The dependence of water vapour permeability of fibre cement on relative humidity.

RH, % Permeability
-1
s
-1
Pa
-1

RH, % Permeability
kg m
-1
s
-1
Pa
-1

10
2.10E-13
60
2.76E-12
20
3.49E-13
70
4.71E-12
30
5.82E-13
80
8.21E-12
40
9.74E-13
90
1.48E-11
50
1.63E-12
100
2.89E-11


From the TableCurve statistics, the estimated uncertainty in the derived value of the permeability
may be as high as 80 %; the measured water vapour transmission rate is strong function of RH
(in the high RH range) and this is the reason for the rather large uncertainty.




169
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

145


Water Absorption Coefficient
170
:

Four test specimens, 5 cm X 5 cm each, were used in these measurements. Water is maintained
at (22 1) C. The absorption is across the major surface. The numbers in parentheses give the
standard deviations.


Table 19.7. Water absorption data for fibre cement.
Square Root of
time, s


Water Absorption
kg m
-2

7.75 0.26 (0.03)
10.95 0.34 (0.04)
15.49 0.45 (0.06)
18.97 0.54 (0.07)
24.49 0.69 (0.09)
30.98 0.84 (0.10)
46.48 1.21 (0.12)
54.77 1.40 (0.13)
71.83 1.77 (0.15)
(0.14)
116.45 2.45 (0.08)
135.50 2.51 (0.04)
93.91 2.21

From a linear regression using the data from the initial stage of the process:


Water Absorption Coefficient for fibre cement is (0.025 0.001) kg m
-2
s
-
.


170
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
B1115.13

146


Moisture Diffusivity:

Gamma ray method
171
is used to measure the distribution of moisture in three test
specimens, 6.5 cm X 22 cm each, during a moisture uptake process across the edge. The
principle of the methodology is described by Kumaran et. al
172
. Marchand and Kumaran
173
have
reported the procedure used for the data reduction.

The moisture diffusivity derived from the gamma ray measurements is given in Table 8.

Table 19.8. The dependence of moisture diffusivity of fibre cement on moisture content.

Moisture Content
kg kg
-1

Diffusivity
m
2
s
-1

Moisture Content
kg kg
-1

Diffusivity
m
2
s
-1

0.029 1.04E-10 0.116 1.13E-09
0.036 1.26E-10 0.130 1.68E-09
0.043 1.54E-10 0.145 2.51E-09
0.051 1.88E-10 0.159 3.74E-09
0.058 2.30E-10 0.174 5.57E-09
0.065 2.81E-10 0.188 8.29E-09
0.072 3.42E-10 0.203 1.23E-08
0.087 5.10E-10 0.217 1.84E-08
0.101 7.59E-10 0.223 2.16E-08

The uncertainty in the derived moisture diffusivity is estimated to be as high as 30 to 50 %.

171
Kumaran, M.K. and Bomberg, M.T., "A Gamma-spectrometer for determination of density
distribution and moisture distribution in building materials," Moisture and Humidity: Measurement
and Control in Science and Industry : Proceedings of International Symposium (Washington,
D.C., USA, 1985), pp. 485-90, 1985.
172
Kumaran, M.K., Mitalas, G.P., Kohonen, R., Ojanen, T, "Moisture transport coefficient of pine
from gamma ray absorption measurements," Collected Papers in Heat Transfer, 1989 : Winter
Annual Meeting of the ASME (San Francisco, CA, USA, 1989) pp. 179-183, 1989(ASME Heat
Transfer Division vol. 123).
173
Marchand, R.G. and Kumaran, M. K., "Moisture diffusivity of cellulose insulation," Journal of
Thermal Insulation and Building Envelopes, Vol. 17, pp. 362-377, 1994.
B1115.13

147


Air Permeability:
Bomberg and Kumaran
174
have reported the principle of the method used in these
measurements. Appendix XIII of the Client Report to ASHRAE, B-1115.3 A Thermal and
Moisture Transport Property Database for Common Building and Insulating Materials 1018-RP
dated 1 April 1999 reports the details. Three circular test specimens, 15 cm in diameter
(thickness 7.80, 7.74 and 7.77 mm), are used in these measurements. The measurements are
conducted at a temperature = (22 1) C.
The fibre cement board specimens are very resistant to airflow and no airflow is
detectable for pressure differences up to 3 kPa . From a set of pressure decay measurements it
is estimated that the air permeability is approximately 3E-12 kg m
-1
Pa
-1
s
-1
.


174
Bomberg, M. T. and Kumaran, M.K., " A Test method to determine air flow resistance of
exterior membranes and sheathings," Journal of Thermal Insulation, Vol.9, pp. 224-235,1986.
B1115.13

148


20. HYGROTHERMAL PROPERTIES OF CEMENT BOARD
All test specimens used for the measurements reported here are prepared
from two boards, 4 X 8, of a commercial product with a nominal thickness
of 1/2. The product is used as an exterior sheathing member in EIFS walls.







Density: (1130 50) kg m
-3

Heat Capacity (From International Energy Agency Annex 24 Report
175
): 840 J K
-1
kg
-1


Thermal Conductivity:
Measurements are according to ASTM Standard C518; two 61 cm X 61 cm specimen was used
in these measurements. The temperatures of the plates are maintained within 0.04 C for these
measurements, for 12 h period to confirm steady state.
Table 20.1. Thermal Conductivity of cement board.
Specimen Thickness
mm
Hot Surface Temperature
C
Cold surface Temperature
C
Conductivity
W m
-1
K
-1

12.52 26.49 22.85 0.25
12.52 31.66 28.02 0.26

Note: The heat flow meter apparatus is built to measure the heat transmission characteristics of
insulating materials and for those materials the measurement uncertainties are within 2 %.
Cement board being more conductive than insulation materials the uncertainty in these
measurements can be as high as 5 %.

175
M K Kumaran, Final Report, Volume 3, Material Properties, International Energy Agency
Annex 24 Report, Published by K. U. Leuven Belgium, 1996
B1115.13

149


Sorption Desorption Measurements
176
:

Up to nine specimens, 40 mm X 40 mm each at the full board thickness are used in these
measurements; the numbers in parentheses indicate the experimental uncertainties.

Sorption:
Table 20.2. Sorption data for cement board.
RH, % Temperature, C Moisture Content, kg kg
-1

100, total saturation Lab at 22 (1) 0.427 (0.006), nine specimens
43.0 (1) Lab at 22 (1) 0.010 (0.000), three specimens
70.0 (1) Lab at 22 (1) 0.019 (0.000), three specimens
81.0 (1) Lab at 22 (1) 0.034 (0.000), three specimens
93.0 (1) Lab at 22 (1) 0.061 (0.000), three specimens

Desorption:
Table 20.3. Desorption data for cement board.
RH, % Temperature, C Moisture Content, kg kg
-1

99.93(0.01) Lab at 22 (1) 0.28 (0.03), nine specimens
99.85 (0.01) Lab at 22 (1) 0.26 (0.03), nine specimens
99.78 (0.01) Lab at 22 (1) 0.25 (0.02), nine specimens
99.71 (0.01) Lab at 22 (1) 0.23 (0.03), nine specimens
99.63 (0.01) Lab at 22 (1) 0.20 (0.03), nine specimens
99.49 (0.01) Lab at 22 (1) 0.19 (0.02), nine specimens
99.27 (0.01) Lab at 22 (1) 0.18 (0.02), nine specimens
93.0 (1) Lab at 22 (1) 0.062 (0.000), three specimens
81.0 (1) Lab at 22 (1) 0.046 (0.000), three specimens
70.0 (1) Lab at 22 (1) 0.032 (0.000), three specimens
43.0 (1) Lab at 22 (1) 0.016 (0.000), three specimens



176
In the hygroscopic range, the measurements are done using the proposed procedure for
ASTM Standard C1498, which in turn is based on CEN 89 N 337 E, Hygroscopic Sorption
Curve; at the higher range the pressure plate method is used. Details of the pressure plate
method are given by: Hansen, M. H., "Retention Curves Measured Using Pressure Plate and
Pressure Membrane," Nordtest Technical Report 367, Danish Building Research Institute, 1998,
p 63.
B1115.13

150


Water Vapour Transmission (WVT) Rate measurements
177
:
Note: Data generated in a previous project on the same material are used to derive the water
vapour permeability listed below. The raw data are not available in the usual format and hence
are not reported.

Derived Water Vapour Permeability
178


Table 20.4. The dependence of water vapour permeability of cement board on relative humidity.

RH, % Permeability
kg m
-1
s
-1
Pa
-1

RH, % Permeability
kg m
-1
s
-1
Pa
-1

10 7.44E-12 60 1.05E-11
20 7.44E-12 70 1.22E-11
30 7.44E-12 80 1.36E-11
40 8.31E-12 90 1.61E-11
50 9.30E-12 100 1.86E-11




From the TableCurve statistics, the estimated uncertainty in the derived value of the permeability
may be as high as 40 %.



177
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M.
K., A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water
Vapour Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
178
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

151


Water Absorption Coefficient
179
:

Three test specimens, 5 cm X 5 cm each, were used in these measurements. Water is
maintained at (22 1) C. The absorption is across the major surface. The numbers in
parentheses give the standard deviations.

Table 20.5. Water absorption data for cement board.

Square Root of
time, s


Water Absorption
kg m
-2

7.75 0.28 (0.02)
13.42 0.37 (0.02)
18.97 0.44 (0.01)
30.98 0.60 (0.01)
(0.02)
60.50 0.98 (0.02)
83.43 1.23 (0.02)
123.69 1.62 (0.03)
43.13 0.77

From a linear regression using the data from the initial stage of the process:


Water Absorption Coefficient for cement board is (0.013 0.001) kg m
-2
s
-
.


179
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
B1115.13

152


Moisture Diffusivity:

Gamma ray method
180
is used to measure the distribution of moisture in three test
specimens, 6.5 cm X 22 cm each, during a moisture uptake process across the edge. The
principle of the methodology is described by Kumaran et. al
181
. Marchand and Kumaran
182
have
reported the procedure used for the data reduction.

The moisture diffusivity derived from the gamma ray measurements is given in Table 6.

Table 20.6. The dependence of moisture diffusivity of cement board on moisture content.


Moisture content
kg kg
-1

Moisture Diffusivity
m
2
s
-1

Moisture content
kg kg
-1

Moisture diffusivity
m
2
s
-1

0.001 1.49E-11 0.081 9.84E-10
0.002 5.07E-11 0.088 1.11E-09
0.004 8.74E-11 0.095 1.26E-09
0.006 1.22E-10 0.104 1.49E-09
0.008 1.56E-10 0.113 1.87E-09
0.122 2.48E-09
0.016 2.78E-10 0.125 2.74E-09
0.023 3.59E-10 0.127 3.03E-09
0.030 4.35E-10 0.130 3.53E-09
0.040 5.35E-10 0.133 4.13E-09
0.054 6.63E-10 0.136 5.11E-09
8.41E-10 0.139 6.72E-09
0.075 9.09E-10 0.141 9.40E-09
0.012 2.19E-10
0.070

The uncertainty in the derived moisture diffusivity is estimated to be as high as 30 to 50 %.

180
Kumaran, M.K. and Bomberg, M.T., "A Gamma-spectrometer for determination of density
distribution and moisture distribution in building materials," Moisture and Humidity: Measurement
and Control in Science and Industry : Proceedings of International Symposium (Washington,
D.C., USA, 1985), pp. 485-90, 1985.
181
Kumaran, M.K., Mitalas, G.P., Kohonen, R., Ojanen, T, "Moisture transport coefficient of pine
from gamma ray absorption measurements," Collected Papers in Heat Transfer, 1989 : Winter
Annual Meeting of the ASME (San Francisco, CA, USA, 1989) pp. 179-183, 1989(ASME Heat
Transfer Division vol. 123).
182
Marchand, R.G. and Kumaran, M. K., "Moisture diffusivity of cellulose insulation," Journal of
Thermal Insulation and Building Envelopes, Vol. 17, pp. 362-377, 1994.
B1115.13

153


Air Permeability:
Bomberg and Kumaran
183
have reported the principle of the method used in these
measurements. Appendix XIII of the Client Report to ASHRAE, B-1115.3 A Thermal and
Moisture Transport Property Database for Common Building and Insulating Materials 1018-RP
dated 1 April 1999 reports the details. Five circular test specimens, 13 cm in diameter (thickness
12.19, 11.98,12.35,12.17 and 12.41 mm), are used in these measurements. The measurements
are conducted at a temperature = (22 1) C.

The summary of the statistical analyses of all data obtained from two series of
measurements on each specimen is shown in Figure 1 as five separate sets.

0
0.2
0.4
0.6
0.8
1
1.2
1.4
1.6
0 50 100 150 200 250
Pressure Difference, Pa
F
l
o
w
,

l

m
-
2

s
-
1
Data Points Mean Permeance

Figure 20.1. The dependence of airflow rate on pressure difference for cement board; the
variation from specimen to specimen is rather large.
For the range of pressure differences between 25 Pa and 200 Pa, the flow rate linearly
varies with the pressure difference. The mean air permeability is 3E-08 kg m
-1
Pa
-1
s
-1
. The
uncertainty is as high as 100 %.

183
Bomberg, M. T. and Kumaran, M.K., " A Test method to determine air flow resistance of
exterior membranes and sheathings," Journal of Thermal Insulation, Vol.9, pp. 224-235,1986.
B1115.13

154


21. HYGROTHERMAL PROPERTIES OF LIMESTONE



Specimen Thickness


The test specimens used for various measurements reported
here are taken from two slabs of Georgian Bay Limestone.


Density: (2500 ) 100) kg m
-3

Heat Capacity (From International Energy Agency Annex 24 Report
184
): 840 J K
-1
kg
-1


Thermal Conductivity:
Measurements are according to ASTM Standard C518; 32 cm X 32 cm specimens are used in
these measurements. The temperatures of the plates are maintained within 0.04 C for these
measurements, for 12 h period to confirm steady state. Heat flow is perpendicular to the major
surfaces.
Table 21.1. Thermal Conductivity of Limestone.
mm
Hot Surface Temperature
C
Cold Surface Temperature
C
Conductivity
W m
-1
K
-1

27.45 26.40 22.43 0.93
27.45 1.97 -1.31 0.86
20.93 26.10 0.57 22.34
20.93 0.38 -3.75 0.53

Note: The heat flow meter apparatus is built to measure the heat transmission characteristics of
insulating materials and for those materials the measurement uncertainties are within 2 %. The
thermal conductivity of limestone being much higher than insulating materials, the errors in the
above measurements may be 5 to 10 %.
The two specimens differed in their bulk densities by 200 kg m
-3
. The specimen with lower
density showed relatively lower thermal conductivity.

184
M K Kumaran, Final Report, Volume 3, Material Properties, International Energy Agency
Annex 24 Report, Published by K. U. Leuven Belgium, 1996
B1115.13

155


Sorption Desorption Measurements
185
:
Up to nine specimens, 41 mm X 41 mm X 6 mm each are used in these measurements; the
numbers in parentheses indicate the experimental uncertainties.

Sorption:
Table 21.2. Sorption data for Spruce.
RH, % Temperature, C Moisture Content, kg kg
-1

100, total saturation Lab at 22 (1) 0.016 (0.001), nine specimens
100, total saturation (repeat) Lab at 22 (1) 0.016 (0.001), six specimens
50.0 (1) 23 (0.1) 0.000, three specimens
70.0 (1) 23 (0.1) 0.000, three specimens
88.5 (1) 23 (0.1) 0.001, three specimens

Desorption:

Table 21.3. Desorption data for Spruce.
RH, % Temperature, C Moisture Content, kg kg
-1

99.93 (0.01) Lab at 22 (1) 0.013 (0.001), three specimens
99.85 (0.01) Lab at 22 (1) 0.012 (0.001), three specimens
99.78 (0.01) Lab at 22 (1) 0.012 (0.001), three specimens
99.71 (0.01) Lab at 22 (1) 0.011 (0.001), three specimens
99.63 (0.01) Lab at 22 (1) 0.010 (0.000), three specimens
99.49 (0.01) Lab at 22 (1) 0.008 (0.001), three specimens
99.27 (0.01) Lab at 22 (1) 0.006 (0.002), three specimens
98.90 (0.01) Lab at 22 (1) 0.005 (0.002), three specimens
97.81 (0.01) Lab at 22 (1) 0.004 (0.001), three specimens
96.74 (0.01) Lab at 22 (1) 0.0029 (0.0008), three specimens
95.3 (0.1) Lab at 22 (1) 0.0021 (0.0003), three specimens
88.6 (1) 23.0 (0.1) 0.001, two specimens
70.5 (1) 23.0 (0.1) 0.000, two specimens
23.0 (0.1) 0.000, two specimens 49.9 (1)


185
In the hygroscopic range, the measurements are done using the proposed procedure for
ASTM Standard C1498, which in turn is based on CEN 89 N 337 E, Hygroscopic Sorption
Curve; at the higher range the pressure plate method is used. Details of the pressure plate
method are given by: Hansen, M. H., "Retention Curves Measured Using Pressure Plate and
Pressure Membrane," Nordtest Technical Report 367, Danish Building Research Institute, 1998,
p 63.
B1115.13

156


Water Vapour Transmission (WVT) Rate measurements

186
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used.

Table 21.4. Dry Cup Measurements on limestone specimens: The numbers in parentheses
indicate the experimental uncertainties for RH and temperature; for WVT Rate the numbers
indicate the standard errors according to a linear regression of data on water vapour transmission
rate at a steady state.
Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

20.88 49.9 (1) 23.1 (0.1) 3.44E-09 (1.3E-10)
20.39 49.9 (1) 23.1 (0.1) 2.82E-09 (1.4E-10)
24.59 49.9 (1) 23.1 (0.1) 1.26E-08 (2.3E-10)
20.88 70.9 (1) 23.2 (0.1) 1.01E-08 (2.0E-10)
20.39 70.9 (1) 23.2 (0.1) 9.34E-09 (2.1E-10)
24.59 70.9 (1) 23.2 (0.1) 1.41E-08 (3.3E-10)
20.88 88.6 (1) 23.2 (0.1) 1.17E-08 (1.7E-10)
20.39 88.6 (1) 23.2 (0.1) 9.77E-09 (2.7E-10)
24.59 88.6 (1) 23.2 (0.1) 3.83E-08 (5.0E-10)



Table 21.5. Wet Cup Measurements on limestone specimens: The numbers in parentheses
indicate the experimental uncertainties for RH and temperature; for WVT Rate the numbers
indicate the standard errors according to a linear regression of data on water vapour
transmission rate at a steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

18.70 69.5 (1) 23.3 (0.1) 2.62E-07 (3.5E-09)
69.5 (1) 23.3 (0.1) 2.53E-07 (1.5E-09)
24.81 69.5 (1) 23.3 (0.1) 2.26E-07 (3.0E-09)
18.70 88.4 (2) 23.1 (0.2) 2.56E-07 (4.7E-09)
19.54 88.4 (2) 23.1 (0.2) 2.53E-07 (4.0E-09)
24.81 88.4 (2) 23.1 (0.2) 2.30E-07 (1.6E-09)
19.54


The average thickness of still air in the cups in both series is 15 mm

186
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M.
K., A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water
Vapour Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

157


Derived Water Vapour Permeability
187



Table 21.6. The dependence of water vapour permeability of limestone on relative humidity.

RH, % Permeability
kg m
-1
s
-1
Pa
-1

RH, % Permeability
kg m
-1
s
-1
Pa
-1

30 2.56E-13 93 4.17E-13
40 2.56E-13 94 6.94E-13
50 2.56E-13 95 1.45E-12
60 2.56E-13 96 3.54E-12
70 2.56E-13 97 9.47E-12
80 2.56E-13 98 2.76E-11
90 2.64E-13 99 9.99E-11
2.78E-13 2E-10
92 3.15E-13
91 100


From the TableCurve statistics, the estimated uncertainty in the derived value of the permeability
may be as high as 100 % as the RH approaches 100 %; most of this large uncertainty is due to a
substantial (exponential) increase in the water vapour transmission rate very close to 100 % RH.
Note that the limestone is highly resistant to water vapour transmission, below 90 % RH.




187
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

158


Water Absorption Coefficient
188
:

Four test specimens, 5 cm X 5 cm X 2 cm each, were used in these measurements. Water is
maintained at (22 1) C. The absorption is across the major surface. The numbers in
parentheses give the standard deviations.

Table 21.7. Water absorption data for limestone.

Square Root of
time, s


Water Absorption
kg m
-2

7.75 0.020 (0.011)
13.42 0.020 (0.011)
18.97 0.023 (0.012)
(0.014)
41.71 0.032 (0.018)
66.63 0.041 (0.022)
77.85 0.043 (0.024)
93.91 0.047 (0.027)
103.05 0.049 (0.028)
122.47 0.053 (0.030)
136.38 0.053 (0.030)
153.56 0.053 (0.032)
160.81 0.054 (0.033)
286.91 0.074 (0.044)
334.07 0.080 (0.049)
413.01 0.098 (0.058)
30.00 0.025

Linear regression using all the data from the first linear part of the absorption process for the four
specimens gives:


Water Absorption Coefficient for limestone = 0.00033 0.00002 kg m
-2
s
-
.


188
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
B1115.13

159


Moisture Diffusivity:



Gamma ray method
189
did not reveal any measurable moisture uptake (see the very low water
absorption coefficient). From the water absorption coefficient and the measured moisture
concentration at full saturation, it is estimated that the moisture diffusivity of limestone is
approximately 7E-11 m
2
s
-1
.


Air Permeability:

The test specimens yielded no measurable air permeance.

189
Kumaran, M.K. and Bomberg, M.T., "A Gamma-spectrometer for determination of density
distribution and moisture distribution in building materials," Moisture and Humidity: Measurement
and Control in Science and Industry : Proceedings of International Symposium (Washington,
D.C., USA, 1985), pp. 485-90, 1985.
B1115.13

160


22. HYGROTHERMAL PROPERTIES OF LOW DENSITY GLASS
FIBER BATT INSULATION





The test specimens used for the measurements reported here
are taken from a roll of a commercial product with a nominal
thickness of 4. The fibers are held together using a binder.


Thickness: (88 ) 3) mm
Density: (11.5 ) 1.5) kg m
-3

Heat Capacity (FromInternational Energy Agency Annex 24 Report
190
): 840 J K
-1
kg
-1


Thermal Conductivity:
Measurements are according to ASTM Standard C518; 60 cm X 60 cm specimens are used in
these measurements. The temperatures of the plates are maintained within 0.04 C for these
measurements, for 12 h period to confirm steady state.
Table 1. Thermal conductivity of low-density glassfibre insulation.
Specimen Thickness
mm
Hot Surface Temperature
C
Cold Surface Temperature
C
Conductivity
W m
-1
K
-1

88.5 35.25 12.84 0.0430

International round robin measurements show that results obtained on thermal insulation
products at the Institute for Research in Construction using heat flow meter apparatus are
accurate within 2 %.
Note: According to the Report to ASHRAE, dated 21 August 2000, based on the Table on
Thermal Conductivity of glass fiber insulation on page 92 the thermal conductivity of the product
reported here shall be between 0.0460 and 0.0411 W m
-1
K
-1
. The temperature coefficient of
thermal conductivity for this product will be approximately 2.5E-04 W m
-1
K
-2
.

190
M K Kumaran, Final Report, Volume 3, Material Properties, International Energy Agency
Annex 24 Report, Published by K. U. Leuven Belgium, 1996
B1115.13

161


Sorption Desorption Measurements
191
:
Three specimens, weighing approximately 12 g each, are used in these measurements at each
set of experimental conditions; the numbers in parentheses indicate the experimental
uncertainties.
Table 22.2. Sorption/ desorption results on low-density glassfibre insulation.
Sorption:
RH, % Temperature, C Moisture Content, kg kg
-1

88.1 (0.2) 3.2 (0.1) 0.0075 (0.0008)
71.5 (0.1) 22.8 (0.1) 0.0034 (0.0005)
50.6 (0.1) 22.9 (0.1) 0.0021 (0.0009)

Desorption:
RH, % Temperature, C Moisture Content, kg kg
-1

88.2 (0.2) 23.3 (0.1) 0.0067 (0.0005)
71.4 (0.2) 22.8 (0.1) 0.0035 (0.0003)
50.4(0.2) 23.0 (0.1) 0.0024 (0.0001)

Pressure plate measurements were not applicable for this material.

191
Measurements are done using the proposed procedure for ASTM Standard C1498, which in
turn is based on CEN 89 N 337 E, Hygroscopic Sorption Curve.
B1115.13

162


Water Vapour Transmission (WVT) Rate measurements :
192

Table 22.3. Dry Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature; for WVT Rate the numbers indicate the standard errors
according to a linear regression of data on water vapour transmission rate at a steady state.
kg m s
-1
For each test condition, 3 circular specimens, each 15 cm in diameter, are used.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
88.8 50.5 (1) 23.0 (0.1) 2.22E-06 (1.0E-08)
85.1 50.5 (1) 23.0 (0.1) 2.21E-06 (1.2E-08)
89.3 50.5 (1) 23.0 (0.1) 2.14E-06 (5.0E-09)
88.8 71.4 (1) 22.8 (0.1) 3.25E-06 (2.2E-08)
85.1 71.4 (1) 22.8 (0.1) 3.35E-06 (1.7E-08)
89.3 71.4 (1) 22.8 (0.1) 3.16E-06 (1.5E-08)
88.8 87.8 (1) 23.3 (0.1) 4.10E-06 (2.2E-08)
85.1 87.8 (1) 23.0 (0.1) 4.19E-06 (3.1E-08)
89.3 87.8 (1) 23.0 (0.1) 3.98E-06 (2.4E-08)
-2



Table 22.4. Wet Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature; for WVT Rate the numbers indicate the standard errors
according to a linear regression of data on water vapour transmission rate at a steady state.


Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m s
-1

88.9 71.4 (1) 22.8 (0.1) 1.37E-06 (5.5E-09)
87.2 71.4 (1) 22.8 (0.1) 1.35E-06 (4.3E-09)
89.4 71.4 (1) 22.8 (0.1) 1.37E-06 (7.4E-09)
88.9 87.9 (1) 23.3 (0.1) 5.84E-07 (1.7E-09)
87.2 87.9 (1) 23.3 (0.1) 5.96E-07 (1.7E-09)
89.4 87.9 (1) 23.3 (0.1) 5.87E-07 (3.4E-09)
-2


The average thickness of still air in the cup 9 mm

192
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M.
K., A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water
Vapour Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

163


Derived Water Vapour Permeability
193


Table 22.5. Water vapour permeability of low-density glassfibre insulation.

RH, % Permeability
kg m
-1
s
-1
Pa
-1

RH, % Permeability
kg m
-1
s
-1
Pa
-1

10
1.72E-10
60
1.72E-10
20
1.72E-10
70
1.72E-10
30
1.72E-10
80
1.72E-10
40
1.72E-10
90
1.72E-10
50
1.72E-10
100
1.72E-10


From the TableCurve statistics, the estimated uncertainty in the derived value of the permeability
is less than 5 %.

Air Permeability:

The high open porosity of this material makes it difficult to build up measurable pressure
differences across the test specimens for the practical flow rates used in the tests. Estimates
made from measurements done by stacking three test specimens give :
Air permeability of the glass fibre insulation is approximately 2.5 E-04 kg m
-1
s
-1
Pa
-1
.

193
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

164


23. HYGROTHERMAL PROPERTIES OF CELLULOSE FIBRE
INSULATION



The test specimens used for the measurements reported here
are taken from samples prepared by blowing a commercial
cellulose insulation product according to the manufacturers
directions. The product is prepared by a dry fiberization
technology with recycled newspaper as the starting material.
The fire retardant and fungicide also are applied as dry raw
materials during the process.




Applied Density: ( 30 ) 4) kg m
-3

Heat Capacity (According to I E A Annex 24 Report
194
): 1880 J K
-1
kg
-1


Thermal Conductivity:
Measurements are according to ASTM Standard C518; 60 cm X 60 cm specimens are used in
these measurements. The temperatures of the plates are maintained within 0.04 C for these
measurements, for 12 h period to confirm steady state.
Table 23.1. Thermal conductivity of cellulose fibre insulation.
Specimen Thickness
mm
Hot Surface Temperature
C
Cold Surface Temperature
C
Conductivity
W m
-1
K
-1

88.53 35.44 12.45 0.0376
88.53 11.40 -11.51 0.0339


International round robin measurements show that results obtained on thermal insulation
products at the Institute for Research in Construction using heat flow meter apparatus are
accurate within 2 %.

194
M K Kumaran, Final Report, Volume 3, Material Properties, International Energy Agency
Annex 24 Report, Published by K. U. Leuven Belgium, 1996
B1115.13

165


Sorption Desorption Measurements
195
:
Three specimens, weighing approximately 18 g each, are used in these measurements at each
set of experimental conditions; the numbers in parentheses indicate the experimental
uncertainties or mean deviations.

Table 23.2. Sorption/ desorption results on cellulose fibre insulation.
Sorption:

RH, % Temperature, C Moisture Content, kg kg
-1

50.5 (1) 22.9 (0.1) 0.061 (0.001)
71.5 (1) 22.8 (0.1) 0.096 (0.001)
88.1 (1) 23.3 (0.1) 0.24 (0.01)

Desorption:

RH, % Temperature, C Moisture Content, kg kg
-1

88.0 (1) 23.3 (0.1) 0.26 (0.07)
72.8 (1) 22.5 (0.1) 0.12 (0.04)
50.2 (1) 23.0 (0.1) 0.05 (0.03)

Pressure plate measurements were not applicable for this material.

195
Measurements are done using the proposed procedure for ASTM Standard C1498, which in
turn is based on CEN 89 N 337 E, Hygroscopic Sorption Curve.
B1115.13

166


Water Vapour Transmission (WVT) Rate measurements
196
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used. Coarse wire
mesh supported the fibres in the test assembly.

Table 23.3. Dry Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature; for WVT Rate the numbers indicate the standard errors
according to a linear regression of data on water vapour transmission rate at a steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

64.5 50.2 (1) 23.1 (0.1) 2.32E-06 (1.7E-08)
64.5 50.2 (1) 23.1 (0.1) 2.22E-06 (1.4E-08)
64.5 50.2 (1) 23.1 (0.1) 2.25E-06 (1.6E-08)
64.5 69.6 (1) 23.3 (0.1) 3.51E-06 (1.2E-08)
64.5 69.6 (1) 23.3 (0.1) 3.50E-06 (8.2E-09)
64.5 69.6 (1) 23.3 (0.1) 3.38E-06 (1.3E-08)
64.5 88.9 (1) 23.2 (0.1) 4.64E-06 (7.8E-09)
64.5 88.9 (1) 23.2 (0.1) 4.65E-06 (9.3E-09)
64.5 88.9 (1) 23.2 (0.1) 4.54E-06 (1.1E-08)



Table 23.4. Wet Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature; for WVT Rate the numbers indicate the standard errors
according to a linear regression of data on water vapour transmission rate at a steady state.


Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

64.5 69.2 (1) 23.3 (0.1) 1.71E-06 (1.4E-08)
64.5 69.2 (1) 23.3 (0.1) 1.64E-06 (1.3E-08)
64.5 69.2 (1) 23.3 (0.1) 1.67E-06 (1.5E-08)
64.5 89.4 (1) 23.1 (0.1) 7.92E-07 (1.7E-08)
64.5 89.4 (1) 23.1 (0.1) 8.31E-07 (1.4E-08)
64.5 89.4 (1) 23.1 (0.1) 8.53E-07 (1.1E-08)


The average thickness of still air in the cup 15 mm

196
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M.
K., A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water
Vapour Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

167


Derived Water Vapour Permeability
197


Table 23.5. Dependence of water vapour permeability of cellulose insulation on relative humidity.

RH, % Permeability
kg m
-1
s
-1
Pa
-1

RH, % Permeability
kg m
-1
s
-1
Pa
-1

10
1.12E-10
60
1.63E-10
20
1.29E-10
70
1.68E-10
30
1.40E-10
80
1.73E-10
40
1.49E-10
90
1.78E-10
50
1.56E-10
100
1.82E-10


From the TableCurve statistics, the estimated uncertainty in the derived value of the permeability
is about 13 %.

Air Permeability:
The high open porosity of this material makes it difficult to build up measurable pressure
differences across the test specimens for the practical flow rates used in the tests. Estimates
made from measurements done by stacking three test specimens give:
Air permeability of cellulose insulation is approximately 2.9 E-04 kg m
-1
s
-1
Pa
-1
.


197
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

168


Water Absorption Coefficient:


Four 5cm X 5 cm X 5 cm plexiglas containers were filled with cellulose insulation at
approximately 30 kg m
-3
density. The top of the container was fully open while the base carried a
wire mesh to hold the cellulose particle in place. Water, maintained at (22 ) 1) *C was allowed
just to immerse the mesh and make contact with the cellulose. The results from the
measurements are listed below. The numbers in parentheses give the mean deviations.

Table 4. Water absorption by cellulose insulation.
Square Root of
time, s


Water Absorption
kg m
-2

7.75 0.24 (0.10)
10.95 0.45(0.12)
15.49 0.95(0.16)
18.97 1.42(0.25)
21.91 1.82(0.35)
24.49 2.14(0.37)
27.93 2.44(0.55)
30.98 2.81(0.40)
33.76 2.80(0.46)
36.33 3.23(0.53)
38.73 3.25(0.43)
41.71 3.62(0.40)
44.50 3.84(0.60)
47.12 3.92(0.34)
48.99 3.94(0.33)
54.77 4.55(0.30)
60.00 4.84(0.48)
64.81 4.97(0.39)
69.28 5.18(0.49)
73.08 5.26(0.44)
88.66 5.75(0.26)
98.89 5.67(0.38)

Linear regression using the data from the initial stages of the process for the four specimens
gives:

Water Absorption Coefficient for cellulose insulation = 0.10 0.01 kg m
-2
s
-
.

B1115.13

169


24. HYGROTHERMAL PROPERTIES OF EXPANDED
POLYSTYRENE INSULATION


The test specimens used for the measurements reported here
are taken from one type (Type 1) of expanded polystyrene.


Density: (14.8 0.2) kg m
-3

Heat Capacity (According to I E A Annex 24 Report
198
): 1470 J K
-1
kg
-1

Thermal Conductivity:
Measurements are according to ASTM Standard C518; 30 cm X 30 cm specimens are used in
these measurements. The temperatures of the plates are maintained within 0.04 C for these
measurements, for 12 h period to confirm steady state.
Table 24.1. Thermal conductivity of the expanded polystyrene insulation.
Specimen Thickness
mm
Hot Surface Temperature
C
Cold Surface Temperature
C
Conductivity
W m
-1
K
-1

25.52 34.75 13.33 0.0379
25.52 11.14 -10.64 0.0346

Sorption Desorption Measurements
199
:
A stack of three specimens, 15 cm X 15 cm X 2 mm each, is used in these measurements at
each set of experimental conditions; the stack is weighed as one unit. The temperature in each
case is (23.0 ) 0.2)* C
Table 24.2. Results from sorption desorption measurements

Relative humidity
%
Sorption
kgkg
-1

Desorption
kgkg
-1

50.1 0.004
67.9 0.005
87.9 0.005
50.4 0.004
68.3 0.003
88.3 0.002

Pressure plate measurements were not applicable for this material.

198
M K Kumaran, Final Report, Volume 3, Material Properties, International Energy Agency
Annex 24 Report, Published by K. U. Leuven Belgium, 1996
B1115.13

170


Water Vapour Transmission (WVT) Rate measurements
200
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used.

Table 24.3. Dry Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature; for WVT Rate the numbers indicate the standard errors
according to a linear regression of data on water vapour transmission rate at a steady state

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

24.28 32.6 (1) 22.6 (0.1) 1.29E-07 (1.4E-09)
24.27 32.6 (1) 22.6 (0.1) 1.29E-07 (1.4E-09)
24.30 32.6 (1) 22.6 (0.1) 1.30E-07 (1.0E-09)
24.28 70.7(1) 24.6 (0.1) 2.79E-07 (5.8E-10)
24.27 70.7(1) 24.6 (0.1) 2.77E-07 (4.9E-10)
24.30 70.7(1) 24.6 (0.1) 2.78E-07 (3.4E-09)
24.28 91.1 (1) 22.8 (0.1) 4.01E-07 (1.4E-09)
24.27 91.1 (1) 22.8 (0.1) 3.96E-07 (1.4E-09)
24.30 91.1 (1) 22.8 (0.1) 3.98E-07 (1.0E-09)

Table 24.4. Wet Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature; for WVT Rate the numbers indicate the standard errors
according to a linear regression of data on water vapour transmission rate at a steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

24.28 50.2 (1) 23.0 (0.1) 2.56E-07 (7.7E-10)
24.27 50.2 (1) 23.0 (0.1) 2.51E-07 (6.9E-10)
24.30 50.2 (1) 23.0 (0.1) 2.49E-07 (8.8E-10)
24.28 71.7 (1) 24.3 (0.1) 1.75E-07 (1.0E-09)
24.27 71.7 (1) 24.3 (0.1) 1.71E-07 (2.1E-10)
24.30 71.7 (1) 24.3 (0.1) 1.69E-07 (6.3E-10)
24.28 90.3(1) 23.3 (0.1) 8.80E-08 (1.0E-09)
24.27 90.3(1) 23.3 (0.1) 8.76E-07 (1.3E-09)
24.30 90.3(1) 23.3 (0.1) 3.98E-07 (2.0E-09)


The average thickness of still air in the cup is 15 mm

199
Measurements are done using the proposed procedure for ASTM Standard C1498, which in
turn is based on CEN 89 N 337 E, Hygroscopic Sorption Curve.
200
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M.
K., A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water
Vapour Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

171


Derived Water Vapour Permeability
201

Table 24.5. Water vapour permeability of the insulation at various relative humidities.

RH, % Permeability
kg m
-1
s
-1
Pa
-1

RH, % Permeability
kg m
-1
s
-1
Pa
-1

10
2.85E-12
60
4.30E-12
20
3.09E-12
70
4.66E-12
30
3.36E-12
80
5.07E-12
40
3.64E-12
90
5.50E-12
50
3.96E-12
100
5.98E-12

From the TableCurve statistics, the estimated uncertainty in the derived value of the permeability
is about 22 %.

Air Permeability:
The results obtained on the same three test specimens used in the water vapour
permeance measurements and the statistical analyses of the data are shown in Figure 1. Two
series of measurements were performed on each specimen at (22 ) 1)* C.
0
0.02
0.04
0.06
0.08
0.1
0.12
0.14
0 50 100 150 200 250 300 350
Pressure Difference, Pa
F
l
o
w
,

l

m
-
2

s
-
1

Data Points Mean Permeance
Upper Confidence Interval Lower Confidence Interval

Figure 24.1. Airflow across the expanded polystyrene test specimens at various pressure
differences.

201
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

172


The air permeability of the expanded polystyrene insulation, for pressure differences
between 25 and 300 Pa, is (1.1 ) 0.1) E-08 kg m
-1
s
-1
Pa
-1
.


B1115.13

173


25. HYGROTHERMAL PROPERTIES OF EXTRUDED
POLYSTYRENE INSULATION


The test specimens used for the measurements reported here are
taken from one board (Type 4) of a commercial product, 4 thick.


Density: (28.6 0.2) kg m
-3

Heat Capacity (According to I E A Annex 24 Report
202
): 1470 J K
-1
kg
-1


Thermal Conductivity:
Measurements are according to ASTM Standard C518; 60 cm X 60 cm specimens are used in
these measurements. The temperatures of the plates are maintained within 0.04 C for these
measurements, for 12 h period to confirm steady state.

Thermal Conductivity:
Table 25.1. Thermal conductivity of extruded polystyrene.
Specimen Thickness
mm
Hot Surface Temperature
C
Cold Surface Temperature
C
Conductivity
W m
-1
K
-1

35.10 12.83 0.0264
103.7 11.17 -11.59 0.0239
103.7
After 2 yr further aging
35.30 13.62 0.0279
103.7 (2 years after
manufacture)

All subsequent test specimens are prepared from the aged board (approximately four years after
manufacture).

A stack of three specimens, 20 cm X 20 cm X 2 mm each, is used in these measurements at
each set of experimental conditions; the stack is weighed as one unit. The temperature in each
case is (23.0 ) 0.2)* C

Sorption Desorption Measurements
203
:



202
M K Kumaran, Final Report, Volume 3, Material Properties, International Energy Agency
Annex 24 Report, Published by K. U. Leuven Belgium, 1996
B1115.13

174



Table 25.2. Results from sorption desorption measurements

Relative humidity
%
Sorption
kgkg
-1

Desorption
kgkg
-1

50.1 0.005
67.9 0.005
87.9 0.004
50.4 0.006
68.3 0.005
88.3 0.004

Pressure plate measurements were not applicable for this material.

Water Vapour Transmission (WVT) Rate measurements
204
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used.

Table 25.3. Dry Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature; for WVT Rate the numbers indicate the standard errors
according to a linear regression of data on water vapour transmission rate at a steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

25.45 50.5 (1) 22.9 (0.1) 6.60E-08 (5.5E-10)
50.5 (1) 22.9 (0.1) 6.51E-08 (7.8E-10)
25.59 50.5 (1) 22.9 (0.1) 6.46E-08 (4.7E-10)
25.45 71.5 (1) 22.8 (0.1) 9.36E-08 (1.4E-09)
25.40 71.5 (1) 22.8 (0.1) 9.01E-08 (6.9E-10)
25.59 71.5 (1) 22.8 (0.1) 9.17E-08 (4.7E-10)
25.45 88.0 (1) 23.3 (0.1) 1.21E-07 (1.4E-09)
25.40 88.0 (1) 23.3 (0.1) 1.18E-07 (1.7E-09)
25.59 88.0 (1) 23.3 (0.1) 1.16E-07 (1.3E-09)
25.40






203
Measurements are done using the proposed procedure for ASTM Standard C1498, which in
turn is based on CEN 89 N 337 E, Hygroscopic Sorption Curve.
204
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M.
K., A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water
Vapour Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

175






Table 25.4. Wet Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature; for WVT Rate the numbers indicate the standard errors
according to a linear regression of data on water vapour transmission rate at a steady state.


Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

25.84 71.5 (1) 22.8 (0.1) 3.88E-08 (4.5E-10)
25.74 71.5 (1) 22.8 (0.1) 3.66E-08 (4.6E-10)
25.69 71.5 (1) 22.8 (0.1) 3.76E-08 (5.6E-10)
25.84 88.3 (1) 23.2 (0.1) 1.41E-08 (1.6E-10)
25.74 88.3 (1) 23.2 (0.1) 1.60E-08 (2.3E-10)
25.69 88.3 (1) 23.2 (0.1) 2.00E-08 (1.0E-10)


The average thickness of still air in the cups for both series is 10 mm


Derived Water Vapour Permeability
205


Table 25.5. Dependence of water vapour permeability of extruded polystyrene on relative
humidity.

RH, % Permeability
kg m
-1
s
-1
Pa
-1

RH, % Permeability
kg m
-1
s
-1
Pa
-1

10
1.22E-12
60
1.22E-12
20
1.22E-12
70
1.22E-12
30
1.22E-12
80
1.22E-12
40
1.22E-12
90
1.22E-12
50
1.22E-12
100
1.22E-12

From the TableCurve statistics, the estimated uncertainty in the derived value of the permeability
is less than 2 %.


Air Permeability:
The test specimens are impermeable and no measurable airflow was obtained for
pressure differences up to several kPa.


205
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

176


26. HYGROTHERMAL PROPERTIES OF SPRAYED
POLYURETHANE FOAM INSULATION



The test specimens used for the measurements reported here
are taken from one sprayed sample (3 passes) of a
commercial product, approximately 6 thick.




Hot Surface Temperature Cold Surface Temperature
Density: (39.0 2) kg m
-3

Heat Capacity (According to I E A Annex 24 Report
206
): 1470 J K
-1
kg
-1

Thermal Conductivity:
Measurements are according to ASTM Standard C518; 60 cm X 60 cm specimens are used in
these measurements. The temperatures of the plates are maintained within 0.05 C for these
measurements, for 12 h period to confirm steady state.

Table 26.1. Thermal conductivity of sprayed polyurethane foam insulation.

Specimen Thickness
mm C C
Conductivity
W m
-1
K
-1

47.1 (prepared from a
product aged for 1 year)
35.14 11.99 0.0227
47.1 (further aged for 1
yr)
34.96 12.57 0.0265

All subsequent specimens are prepared from the 2 yr aged specimen.


Sorption Desorption Measurements
207
:
A stack of three specimens, 20 cm X 20 cm X 2 mm each, is used in these measurements at
each set of experimental conditions; the stack is weighed as one unit. The temperature in each
case is (23.0 ) 0.2)* C


206
M K Kumaran, Final Report, Volume 3, Material Properties, International Energy Agency
Annex 24 Report, Published by K. U. Leuven Belgium, 1996
207
Measurements are done using the proposed procedure for ASTM Standard C1498, which in
turn is based on CEN 89 N 337 E, Hygroscopic Sorption Curve.
B1115.13

177




Table 26.2. Results from sorption desorption measurements

Relative humidity
%
Sorption
kgkg
-1

Desorption
kgkg
-1

50.1 0.011
67.9 0.015
87.9 0.018
50.4 0.013
68.3 0.017
88.4 0.020

Pressure plate measurements were not applicable for this material.

Water Vapour Transmission (WVT) Rate measurements
208
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used.

Table 26.3. Dry Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature; for WVT Rate the numbers indicate the standard errors
according to a linear regression of data on water vapour transmission rate at a steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

25.60 50.5 (1) 22.9 (0.1) 1.34E-07 (1.9E-09)
25.11 50.5 (1) 22.9 (0.1) 1.35E-07 (1.9E-09)
25.69 50.5 (1) 22.9 (0.1) 1.33E-07 (1.6E-09)
25.60 71.5 (1) 22.8 (0.1) 2.00E-07 (1.4E-09)
25.11 71.5 (1) 22.8 (0.1) 2.01E-07 (1.4E-09)
25.69 71.5 (1) 22.8 (0.1) 1.97E-07 (1.3E-09)
25.60 88.0 (1) 23.3 (0.1) 2.65E-07 (9.4E-10)
25.11 88.0 (1) 23.3 (0.1) 2.66E-07 (1.9E-09)
25.69 88.0 (1) 23.3 (0.1) 2.53E-07 (3.2E-09)





208
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M.
K., A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water
Vapour Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

178


Table 26.4. Wet Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature; for WVT Rate the numbers indicate the standard errors
according to a linear regression of data on water vapour transmission rate at a steady state.


Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

26.19 71.4 (1) 22.8 (0.1) 8.35E-08 (4.5E-10)
25.87 71.4 (1) 22.8 (0.1) 8.89E-08 (4.6E-10)
25.89 71.4 (1) 22.8 (0.1) 8.77E-08 (5.6E-10)
26.19 88.0 (1) 23.3 (0.1) 4.12E-08 (5.7E-10)
25.87 88.0 (1) 23.3 (0.1) 4.52E-08 (4.6E-10)
25.89 88.0 (1) 23.3 (0.1) 4.96E-08 (7.6E-10)


The average thickness of still air in the cups for both series is 10 mm


Derived Water Vapour Permeability
209


Table 26.5. Dependence of water vapour permeability of sprayed polyurethane foam insulation
on relative humidity.

RH, % Permeability
kg m
-1
s
-1
Pa
-1

RH, % Permeability
kg m
-1
s
-1
Pa
-1

10
2.34E-12
60
2.86E-12
20
2.44E-12
70
2.97E-12
30
2.54E-12
80
3.09E-12
40
2.64E-12
90
3.22E-12
50
2.75E-12
100
3.35E-12


From the TableCurve statistics, the estimated uncertainty in the derived value of the permeability
is about 30 %.

Air Permeability:
The test specimens are nearly impermeable and no noticeable airflow was obtained for
pressure differences up to 10 kPa. From the available data on one of the three tested specimens
it appears that the permeability is approximately 1 x 10E-11 kg m
-1
s
-1
Pa
-1
.


B1115.13

179


27. HYGROTHERMAL PROPERTIES OF POLYISOCYANURATE
INSULATION



The test specimens used for the measurements reported here
are taken from one board of a commercial product, 3 thick.


Density: (26.5 0.2) kg m

mm
-3

Heat Capacity (According to I E A Annex 24 Report
210
): 1470 J K
-1
kg
-1


Thermal Conductivity:
Measurements are according to ASTM Standard C518; 60 cm X 60 cm specimens are used in
these measurements. The temperatures of the plates are maintained within 0.04 C for these
measurements, for 12 h period to confirm steady state.
Table 27.1. Thermal conductivity of polyisocyanurate insulation.
Specimen Thickness Hot Surface Temperature
C
Cold Surface Temperature
C
Conductivity
W m
-1
K
-1

13.12 0.0210
(After 3 yr aging)
68.85 mm
35.17 13.77 0.0275
68.58 34.87

All subsequent test specimens are prepared from the 3 yr aged board.


Sorption Desorption Measurements
211
:

A stack of three specimens, 20 cm X 20 cm X 2 mm each, is used in these measurements at
each set of experimental conditions; the stack is weighed as one unit. The temperature in each
case is (23.0 ) 0.2)* C



209
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
210
M K Kumaran, Final Report, Volume 3, Material Properties, International Energy Agency
Annex 24 Report, Published by K. U. Leuven Belgium, 1996
211
Measurements are done using the proposed procedure for ASTM Standard C1498, which in
turn is based on CEN 89 N 337 E, Hygroscopic Sorption Curve.
B1115.13

180




Table 27.2. Results from sorption desorption measurements

Relative humidity
%
Sorption
kgkg
-1

Desorption
kgkg
-1

50.1 0.011
67.9 0.015
87.9 0.019
50.4 0.013
68.3 0.017
88.3 0.021

Pressure plate measurements were not applicable for this material.


mm
Water Vapour Transmission (WVT) Rate measurements
212
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used.
Table 27.3. Dry Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature; for WVT Rate the numbers indicate the standard errors
according to a linear regression of data on water vapour transmission rate at a steady state.

Specimen Thickness Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

25.70 50.5 (1) 22.9 (0.1) 2.39E-07(1.2E-09)
25.55 50.5 (1) 22.9 (0.1) 2.40E-07(1.7E-09)
25.69 50.5 (1) 22.9 (0.1) 2.36E-07(1.1E-09)
25.70 71.5 (1) 22.8 (0.1) 3.63E-07(1.0E-09)
25.55 71.5 (1) 22.8 (0.1) 3.64E-07(1.4E-09)
25.69 71.5 (1) 22.8 (0.1) 3.59E-07(1.5E-09)
25.70 88.0 (1) 23.3 (0.1) 4.85E-07(1.1E-09)
25.55 88.0 (1) 23.3 (0.1) 4.73E-07(2.0E-09)
25.69 88.0 (1) 23.3 (0.1) 4.72E-07(1.6E-09)






212
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M.
K., A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water
Vapour Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

181






Table 27.4. Wet Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature; for WVT Rate the numbers indicate the standard errors
according to a linear regression of data on water vapour transmission rate at a steady state.


Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

26.02 71.4 (1) 22.8 (0.1) 1.71E-07(1.6E-09)
25.64 71.4 (1) 22.8 (0.1) 1.77E-07(1.7E-09)
26.08 71.4 (1) 22.8 (0.1) 1.76E-07(2.2E-09)
26.02 88.0 (1) 23.3 (0.1) 9.36E-08 (1.1E-09)
25.64 88.0 (1) 23.3 (0.1) 1.02E-07 (1.2E-09)
26.08 88.0 (1) 23.3 (0.1) 9.87E-08 (1.4E-09)


The average thickness of still air in the cups for both series is 10 mm


Derived Water Vapour Permeability
213


Table 27.5. Dependence of water vapour permeability of polyisocyanurate insulation on relative
humidity.

RH, % Permeability
kg m
-1
s
-1
Pa
-1

RH, % Permeability
kg m
-1
s
-1
Pa
-1

10
4.04E-12
60
5.46E-12
20
4.29E-12
70
5.80E-12
30
4.56E-12
80
6.16E-12
40
4.84E-12
90
6.55E-12
50
5.14E-12
100
6.96E-12

From the TableCurve statistics, the estimated uncertainty in the derived value of the permeability
is about 28 %.


Air Permeability:
The test specimens are impermeable and no measurable airflow was obtained for
pressure differences up to 3 kPa.


213
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

182


28. HYGROTHERMAL PROPERTIES OF LOW-DENSITY
SPRAYED PLOYURETHANE FOAM INSULATION





The test specimens used for the measurements reported here
are taken from one 4 x 4 sample of a commercial product
sprayed to 8 to 10 height.

Density: 6.5 to 8.5 kg m
-3

Heat Capacity (According to I E A Annex 24 Report
214
): 1470 J K
-1
kg
-1


Thermal Conductivity:
Measurements are according to ASTM Standard C518; 30 cm X 30 cm specimens are used in
these measurements. The temperatures of the plates are maintained within 0.04 C for these
measurements, for 12 h period to confirm steady state.

Table 28.1. Thermal conductivity of low-density polyurethane foam insulation.

Specimen
Thickness, mm
Average Density
kg m
-3

Hot Surface
Temperature, C
Cold Surface
Temperature, C
Conductivity
W m
-1
K
-1

20.7 7.0 35.53 13.62 0.0423
20.7 7.0 11.11 -10.62 0.0372
19.7 8.4 35.65 13.50 0.0370
19.7 8.4 11.49 -10.66 0.0332



Sorption Desorption Measurements
215
:
A stack of ninel slices (to form a dry specimen with approximate weight 4 g), 15 cm X 15 cm X 2
to 3 mm each, is used in these measurements at each set of experimental conditions; the stack is
weighed as one unit. The temperature in each case is (23.0 ) 0.2)* C



214
M K Kumaran, Final Report, Volume 3, Material Properties, International Energy Agency
Annex 24 Report, Published by K. U. Leuven Belgium, 1996
215
Measurements are done using the proposed procedure for ASTM Standard C1498, which in
turn is based on CEN 89 N 337 E, Hygroscopic Sorption Curve.
B1115.13

183




Table 28.2. Results from sorption desorption measurements

Relative humidity
%
Sorption
kgkg
-1

Desorption
kgkg
-1

50.5 0.010
70.9 0.021
91.3 0.070
50.4 0.005
70.2 0.010
90.3 0.016

Pressure plate measurements were not applicable for this material.

Water Vapour Transmission (WVT) Rate measurements
216
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used.

Table 28.3. Dry Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature; for WVT Rate the numbers indicate the standard errors
according to a linear regression of data on water vapour transmission rate at a steady state.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

23.10 50.3 (1) 22.9 (0.1) 3.52E-06 (2.3E-08)
23.84 50.5 (1) 22.9 (0.1) 3.55E-06 (2.1E-08)
24.87 50.5 (1) 22.9 (0.1) 3.49E-06 (7.3E-09)
23.10 70.3 (1) 23.0 (0.1) 5.08E-06 (1.2E-08)
23.84 70.3 (1) 23.0 (0.1) 5.02E-06 (3.2E-08)
24.87 70.3 (1) 23.0 (0.1) 4.82E-06 (3.1E-08)
23.10 89.7 (1) 22.9 (0.1) 7.18E-06 (1.3E-08)
23.84 89.7 (1) 22.9 (0.1) 7.14E-06 (2.7E-08)
24.87 89.7 (1) 22.9 (0.1) 6.79E-06 (2.9E-08)






216
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M.
K., A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water
Vapour Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

184



Table 28.4. Wet Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature; for WVT Rate the numbers indicate the standard errors
according to a linear regression of data on water vapour transmission rate at a steady state.


Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

21.38 70.4 (1) 22.9 (0.1) 2.13E-06 (5.2E-09)
21.88 70.4 (1) 22.9 (0.1) 2.17E-06 (4.1E-09)
22.11 70.4 (1) 22.9 (0.1) 2.06E-06 (8.2E-09)
21.38 90.0 (1) 22.9 (0.1) 7.78E-07 (1.0E-08)
21.88 90.0 (1) 22.9 (0.1) 7.94E-07 (1.0E-08)
22.11 90.0 (1) 22.9 (0.1) 7.43E-07 (1.1E-08)


The average thickness of still air in the cups for both series is 15 mm


Derived Water Vapour Permeability
217


Table 28.5. Dependence of water vapour permeability of low-density polyurethane foam
insulation on relative humidity.

RH, % Permeability
kg m
-1
s
-1
Pa
-1

RH, % Permeability
kg m
-1
s
-1
Pa
-1

8.75E-11
60
8.75E-11
20
8.75E-11
70
8.75E-11
30
8.75E-11
80
8.75E-11
40
8.75E-11
90
8.75E-11
50
8.75E-11
100
8.75E-11
10


From the TableCurve statistics, the estimated uncertainty in the derived value of the permeability
is about 8 %.



217
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

185


Air Permeability:

Three circular test specimens (thickness 23.10 mm, 23.84 mm, 21.38 mm), each
approximately 15 cm in diameter, are used in these measurements. The measurements are
conducted at a temperature = (22 1) C.
The summary of the statistical analyses of all data obtained from two series of
measurements on each specimen is shown in Figure 1 as three separate sets.
0
0.05
0.1
0.15
0.2
0.25
0 200 400 600 800 1000
Pressure Difference, Pa
F
l
o
w

,

l

m
-
2

s
-
1
Data Points Mean Permeance
Upper Confidence Interval Lower Confidence Interval


Figure 28.1. The dependence of airflow rate on pressure difference for low density foam.

For the range of pressure differences between 25 Pa and 1000 Pa, the flow rate linearly
varies with the pressure difference. The air permeability is (4.2 2.9) E-09 kg m
-1
Pa
-1
s
-1
.


B1115.13

186


29. HYGROTHERMAL PROPERTIES OF BITUMINOUS PAPER
(#15 FELT)

The test specimens used for the measurements reported here
are taken from a roll of a commercial product.
Water Vapour Transmission (WVT) Rate measurements

Thickness: (0.72 ) 0.03) mm
Mass per Area: 515 g m
-2

218
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used.

Table 29.1. Dry Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature and standard errors for WVT rate.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

0.737 49.0 (1) 23.2 (0.1) 4.04E-07 (5.0E-10)
0.752 49.0 (1) 23.2 (0.1) 4.30E-07 (4.0E-10)
0.727 49.0 (1) 23.2 (0.1) 4.10E-07 (5.0E-10)
0.737 68.8 (1) 23.3 (0.1) 5.14E-07 (1.6E-09)
0.752 68.8 (1) 23.3 (0.1) 5.45E-07 (3.0E-10)
0.727 68.8 (1) 23.3 (0.1) 5.16E-07 (1.6E-09)
0.737 89.7 (1) 23.1 (0.1) 7.75E-07 (2.9E-09)
0.752 89.7 (1) 23.1(0.1) 8.25E-07 (9.0E-09)
0.727 89.7 (1) 23.1 (0.1) 7.97E-07 (9.8E-09)

Table 29.2. Wet Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature and standard errors for WVT rate.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

0.691 68.8 (1) 23.3 (0.1) 7.21E-07 (2.6E-09)
0.712 68.8 (1) 23.3 (0.1) 7.03E-07 (2.3E-09)
0.730 68.8 (1) 23.3 (0.1) 7.08E-07 (3.0E-09)
0.691 90.9 (2) 23.0 (0.2) 2.69E-07 (1.8E-09)
0.712 90.9 (2) 23.0 (0.2) 2.82E-07 (2.6E-09)
0.730 90.9 (2) 23.0 (0.2) 2.98E-07 (3.6E-09)
The average thickness of still air in the cups in both series is 20 mm

218
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M.
K., A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water
Vapour Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

187


Derived Water Vapour Permeance
219


Table 29.3. Dependence of water vapour permeance of #15 Felt on relative humidity.

RH, % Permeance
kg m
-2
s
-1
Pa
-1

RH, % Permeance
kg m
-2
s
-1
Pa
-1

60
2.95E-10
20
2.91E-10
70
3.98E-10
30
2.91E-10
80
5.81E-10
40
2.91E-10
90
1.17E-09
50
2.91E-10
100
3.11E-09
10
2.91E-10

From the TableCurve statistics, the estimated uncertainty in the derived value of the permeance
may be as high as 40 %.

Three circular test specimens, each approximately 15 cm in diameter are used in these
measurements. The summary of the statistical analyses of all data obtained from two series of
measurements on each specimen is shown in Figure 1.
Air Permeance
220
:
0
0.05
0.1
0.15
0.2
0.25
0.3
0.35
0.4
0.45
0.5
0 50 100 150 200
Pressure Difference, Pa
F
l
o
w

,

l

m
-
2

s
-
1
Data Points Mean Permeance
Upper Confidence Interval Lower Confidence Interval

Figure 29.1. The dependence of airflow rate on pressure difference for #15 Felt.

219
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
220
Bomberg, M. T. and Kumaran, M.K., " A Test method to determine air flow resistance of
exterior membranes and sheathings," Journal of Thermal Insulation, Vol.9, pp. 224-235,1986.
B1115.13

188


For the range of pressure differences between 25 and 175 Pa, the flow rate linearly varies with
the pressure difference. The air permeance of #15 Felt is (2.5 ) 0.6) E-06 kg m
-2
s
-1
Pa
-1
.


Square Root of
time, s
Water Absorption Coefficient
221
:

Four test specimens, 5 cm X 5 cm each, were prepared as follows. The membrane was attached
to the major surface of a 5 cm X 5 cm OSB using a thin (less than 1 mm) layer of drywall
compound and allowed to dry. The sides were then sealed using wax. Water was maintained at
(22 1) C and allowed to touch the exposed surface of the membrane. The results from the
water absorption measurements are listed in Table 4. The numbers in parentheses give the
standard deviations.

Table 29.4. Water absorption data for #15 Felt.


Water Absorption
kg m
-2

(0.003)
(0.004)
17.3 0.019 (0.003)
21.9 0.030 (0.002)
27.9 0.029 (0.002)
38.7 0.031 (0.003)
52.0 0.040 (0.002)
(0.003)
78.6 0.054 (0.004)
93.3 0.062 (0.005)
106.8 0.070 (0.002)
128.2 0.077 (0.004)
(0.004)
158.2 0.094 (0.007)
7.7 0.012
11.0 0.018
60.0 0.042
140.7 0.083




Linear regression using all data for the four specimens gives:
Water Absorption Coefficient for the major surfaces = 0.00051 0.00002 kg m
-2
s
-
.





221
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
B1115.13

189


30. HYGROTHERMAL PROPERTIES OF ASPHALT
IMPREGNATED PAPER RATED AS 10 min PAPER

The test specimens used for the measurements reported here
are taken from a roll of a commercial product, Grade D.
Thickness: (0.20 ) 0.01) mm
Mass per Area: 170 g m
-2

Water Vapour Transmission (WVT) Rate measurements
222
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used.

Table 30.1. Dry Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature and standard errors for WVT rate.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

0.201 49.0 (1) 23.2 (0.1) 7.43E-07 (2.1E-09)
0.197 49.0 (1) 23.2 (0.1) 7.49E-07 (1.8E-09)
0.198 49.0 (1) 23.2 (0.1) 7.99E-07 (1.8E-09)
0.201 68.8 (1) 23.3 (0.1) 1.08E-06 (2.8E-09)
0.197 68.8 (1) 23.3 (0.1) 1.05E-06 (3.1E-09)
0.198 68.8 (1) 23.3 (0.1) 1.10E-06 (9.0E-10)
0.201 89.7 (1) 23.1 (0.1) 1.78E-06 (7.0E-09)
89.7 (1) 23.1(0.1) 1.77E-06 (1.3E-08)
0.198 89.7 (1) 23.1 (0.1)
0.197
1.79E-06 (1.6E-08)

Table 30.2. Wet Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature and standard errors for WVT rate.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

0.198 68.8 (1) 23.3 (0.1) 1.73E-06 (7.2E-09)
0.203 68.8 (1) 23.3 (0.1) 1.83E-06 (1.3E-08)
0.199 68.8 (1) 23.3 (0.1) 1.79E-06 (1.6E-08)
0.198 90.9 (2) 23.0 (0.2) 4.04E-07 (1.4E-09)
0.203 90.9 (2) 23.0 (0.2) 4.86E-07 (4.9E-09)
0.199 90.9 (2) 23.0 (0.2) 4.99E-07 (2.1E-09)
The average thickness of still air in the cups in both series is 20 mm

222
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M.
K., A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water
Vapour Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

190


Derived Water Vapour Permeance
223


Table 30.3. Dependence of water vapour permeance of 10 min paper on relative humidity.

RH, % Permeance
kg m
-2
s
-1
Pa
-1

RH, % Permeance
kg m
-2
s
-1
Pa
-1

10
2.38E-10
60
1.07E-09
20
3.17E-10
70
1.48E-09
30
4.25E-10
80
2.10E-09
40
5.73E-10
90
3.06E-09
50
7.78E-09
100
4.71E-09

From the TableCurve statistics, the estimated uncertainty in the derived value of the permeance
is 25 %.

Air Permeance
224
:
Three circular test specimens, each approximately 15 cm in diameter are used in these
measurements. The summary of the statistical analyses of all data obtained from two series of
measurements on each specimen is shown in Figure 1.
0
0.02
0.04
0.06
0.08
0.1
0.12
0.14
0.16
0.18
0.2
0 50 100 150 200
Pressure Difference (Pa)
F
l
o
w

,

l

m
-
2

s
-
1
Data Points Mean Permeance
Upper Confidence Interval Lower Confidence Interval

Figure 30.1. The dependence of airflow rate on pressure difference for 10 min Paper.

223
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

191


For the range of pressure differences between 25 and 175 Pa, the flow rate linearly varies with
the pressure difference. The air permeance of 10 min Paper is (1.1 ) 0.1) E-06 kg m
-2
s
-1
Pa
-1
.


Water Absorption Coefficient
225
:

Four test specimens, 5 cm X 5 cm each, were prepared as follows. The membrane was attached
to the major surface of a 5 cm X 5 cm OSB using a thin (less than 1 mm) layer of drywall
compound and allowed to dry. The sides were then sealed using wax. Water was maintained at
(22 1) C and allowed to touch the exposed surface of the membrane. The results from the
water absorption measurements are listed in Table 4. The numbers in parentheses give the
standard deviations.

Table 30.4. Water absorption data for 10 min Paper.
Square Root of
time, s


Water Absorption
kg m
-2

11.0 0.031(0.005)
15.5 0.034 (0.006)
20.5 0.039 (0.009)
27.9 0.039 (0.003)
32.9 0.047 (0.002)
37.1 0.057 (0.007)
43.1 0.063 (0.005)
53.1 0.075 (0.008)
61.0 0.073 (0.005)
81.2 0.092 (0.004)
90.7 0.107 (0.004)
102.8 0.120 (0.005)
123.2 0.143 (0.003)
137.0 0.153 (0.004)

Linear regression using all data for the four specimens gives:


Water Absorption Coefficient for the major surfaces = 0.00099 0.00003 kg m
-2
s
-
.



224
Bomberg, M. T. and Kumaran, M.K., " A Test method to determine air flow resistance of
exterior membranes and sheathings," Journal of Thermal Insulation, Vol.9, pp. 224-235,1986.
225
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
B1115.13

192


31. HYGROTHERMAL PROPERTIES OF ASPHALT
IMPREGNATED PAPER RATED AS 30 min PAPER

The test specimens used for the measurements reported here
are taken from a roll of a commercial product, Grade D.
Thickness: (0.22 ) 0.01) mm
Mass per Area: 200 g m
-2

Water Vapour Transmission (WVT) Rate measurements
226
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used.

Table 31.1. Dry Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature and standard errors for WVT rate.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

0.213 49.0 (1) 23.2 (0.1) 1.16E-06 (4.6E-09)
0.212 49.0 (1) 23.2 (0.1) 1.43E-06 (5.6E-09)
49.0 (1) 1.16E-06 (6.9E-09)
0.213 68.8 (1) 23.3 (0.1) 1.53E-06 (3.5E-09)
0.212 68.8 (1) 23.3 (0.1) 1.85E-06 (5.7E-09)
0.209 68.8 (1) 23.3 (0.1) 1.52E-06 (7.4E-09)
0.213 89.7 (1) 23.1 (0.1) 2.48E-06 (1.8E-08)
0.212 89.7 (1) 23.1(0.1) 2.97E-06 (1.5E-08)
0.209 89.7 (1) 23.1 (0.1) 2.43E-06 (2.5E-08)
0.209 23.2 (0.1)

Table 31.2. Wet Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature and standard errors for WVT rate.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

68.8 (1) 23.3 (0.1) 2.32E-06 (1.2E-08)
0.219 68.8 (1) 23.3 (0.1) 2.49E-06 (1.1E-08)
0.219 68.8 (1) 23.3 (0.1) 2.61E-06 (2.0E-08)
0.214 90.9 (2) 23.0 (0.2) 4.81E-07 (3.9E-09)
0.219 90.9 (2) 23.0 (0.2) 5.26E-07 (4.7E-09)
0.219 90.9 (2) 23.0 (0.2) 5.11E-07 (3.2E-09)
0.214
The average thickness of still air in the cups for both series is 20 mm.

226
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M.
K., A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water
Vapour Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

193


Derived Water Vapour Permeance
227


Table 31.3. Dependence of water vapour permeance of 30 min paper on relative humidity.

RH, % Permeance
kg m
-2
s
-1
Pa
-1

RH, % Permeance
kg m
-2
s
-1
Pa
-1

10
4.41E-10
60
1.70E-09
20
5.70E-10
70
2.31E-09
30
7.40E-10
80
3.22E-09
40
9.67E-10
90
4.67E-09
50
1.28E-09
100
7.23E-09

From the TableCurve statistics, the estimated uncertainty in the derived value of the permeance
may be as high as 40 %.

Air Permeance
228
:
Three circular test specimens, each approximately 15 cm in diameter are used in these
measurements. The summary of the statistical analyses of all data obtained from two series of
measurements on each specimen is shown in Figure 1.
0
0.2
0.4
0.6
0.8
1
1.2
1.4
1.6
1.8
0 50 100 150 200 250 300
Pressure Difference, Pa
F
l
o
w
,

l

m
-
2

s
-
1

Data Points Mean Permeance
Upper Confidence Interval Lower Confidence Interval

Figure 31.1. The dependence of airflow rate on pressure difference for 30 min Paper.

227
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
228
Bomberg, M. T. and Kumaran, M.K., " A Test method to determine air flow resistance of
exterior membranes and sheathings," Journal of Thermal Insulation, Vol.9, pp. 224-235,1986.
B1115.13

194


For the range of pressure differences between 25 and 250 Pa, the flow rate linearly varies with
the pressure difference. The air permeance of 10 min Paper is (6.6 ) 0.3) E-06kg m
-2
s
-1
Pa
-1
.



kg m
Water Absorption Coefficient
229
:

Four test specimens, 5 cm X 5 cm each, were prepared as follows. The membrane was attached
to the major surface of a 5 cm X 5 cm OSB using a thin (less than 1 mm) layer of drywall
compound and allowed to dry. The sides were then sealed using wax. Water was maintained at
(22 1) C and allowed to touch the exposed surface of the membrane. The results from the
water absorption measurements are listed in Table 4. The numbers in parentheses give the
standard deviations.
Table 31.4. Water absorption data for 30 min Paper.
Square Root of
time, s


Water Absorption
-2

11.0 0.039 (0.012)
13.4 0.031 (0.009)
17.3 0.034 (0.008)
24.5 0.039 (0.007)
30.0 0.042 (0.003)
34.6 0.058 (0.008)
38.7 0.062 (0.008)
49.0 0.070 (0.004)
55.9 0.073 (0.005)
64.8 0.085 (0.008)
73.1 0.086 (0.004)
79.4 0.091 (0.006)
93.9 0.108 (0.006)
0.144 (0.005)
150.0 0.154 (0.005)
105.4 0.114 (0.007)
(0.008)
137.3
165.6 0.171 (0.007)
Linear regression using all data for the four specimens gives:


Water Absorption Coefficient for the major surfaces = 0.00093 0.00005 kg m
-2
s
-
.
117.7 0.137


229
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
B1115.13

195


32. HYGROTHERMAL PROPERTIES OF ASPHALT
IMPREGNATED PAPER RATED AS 60 min PAPER

The test specimens used for the measurements reported here
are taken from a roll of a commercial product, Grade D.
C
Thickness: (0.34 ) 0.01) mm
Mass per Area: 280 g m
-2

Water Vapour Transmission (WVT) Rate measurements :
230
For each test condition, 3 circular specimens, each 15 cm in diameter, are used.

Table 32.1. Dry Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature and standard errors for WVT rate.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature WVT Rate
kg m
-2
s
-1

0.338 49.0 (1) 23.2 (0.1) 2.47E-06 (1.8E-08)
0.331 49.0 (1) 23.2 (0.1) 2.30E-06 (2.0E-08)
0.333 49.0 (1) 23.2 (0.1) 2.06E-06 (1.5E-08)
0.338 68.8 (1) 23.3 (0.1) 2.95E-06 (6.6E-09)
0.331 68.8 (1) 23.3 (0.1) 2.78E-06 (8.3E-09)
0.333 23.3 (0.1) 2.52E-06 (7.7E-09)
0.338 89.7 (1) 23.1 (0.1) 5.05E-06 (3.9E-08)
0.331 89.7 (1) 23.1(0.1) 4.69E-06 (4.6E-08)
0.333 89.7 (1) 23.1 (0.1) 4.28E-06 (4.7E-08)
68.8 (1)

Table 32.2. Wet Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature and standard errors for WVT rate.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

0.337 68.8 (1) 23.3 (0.1) 2.59E-06 (1.6E-08)
0.333 68.8 (1) 23.3 (0.1) 2.38E-06 (1.5E-08)
0.219 68.8 (1) 23.3 (0.1) 2.63E-06 (1.6E-08)
0.337 90.9 (2) 23.0 (0.2) 5.62E-07 (4.3E-09)
0.333 90.9 (2) 23.0 (0.2) 6.10E-07 (7.2E-09)
0.219 90.9 (2) 23.0 (0.2) 5.73E-07 (6.9E-09)
The average thickness of still air in the cups for both series is 20 mm

230
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M.
K., A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water
Vapour Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

196


Derived Water Vapour Permeance
231


Table 32.3. Dependence of water vapour permeance of 60 min paper on relative humidity.

RH, % Permeance
kg m
-2
s
-1
Pa
-1

RH, % Permeance
kg m
-2
s
-1
Pa
-1

10
1.51E-09
60
2.78E-09
20
1.70E-09
70
3.18E-09
30
1.91E-09
80
3.66E-09
40
2.16E-09
90
4.24E-09
50
2.44E-09
100
4.95E-09

From the TableCurve statistics, the estimated uncertainty in the derived value of the permeance
may be as high as 40 %.
Air Permeance
232
:
Three circular test specimens, each approximately 15 cm in diameter are used in these
measurements. The summary of the statistical analyses of all data obtained from two series of
measurements on each specimen is shown in Figure 1.
0
0.2
0.4
0.6
0.8
1
1.2
1.4
1.6
1.8
0 50 100 150 200 250 300
Pressure Difference, Pa
F
l
o
w
,

l

m
-
2

s
-
1
Data Points Mean Permeance
Upper Confidence Interval Lower Confidence Interval

Figure 32.1. The dependence of airflow rate on pressure difference for 60 min Paper.

231
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

197


For the range of pressure differences between 25 and 250 Pa, the flow rate linearly varies with
the pressure difference. The air permeance of 10 min Paper is (7.1 ) 0.5) E-06 kg m
-2
s
-1
Pa
-1
.


Water Absorption Coefficient
233
:

Four test specimens, 5 cm X 5 cm each, were prepared as follows. The membrane was attached
to the major surface of a 5 cm X 5 cm OSB using a thin (less than 1 mm) layer of drywall
compound and allowed to dry. The sides were then sealed using wax. Water was maintained at
(22 1) C and allowed to touch the exposed surface of the membrane. The results from the
water absorption measurements are listed in Table 4. The numbers in parentheses give the
standard deviations.

Table 32.4. Water absorption data for 60 min Paper.
Square Root of
time, s


Water Absorption
kg m
-2

7.7 0.017 (0.004)
11.0 0.029 (0.002)
17.3 0.033 (0.005)
21.9 0.040 (0.006)
30.0 0.051 (0.008)
38.7 0.056 (0.005)
49.0 0.068 (0.005)
57.4 0.077 (0.003)
67.1 0.090 (0.007)
75.1 0.098 (0.008)
89.3 0.111 (0.007)
101.9 0.124 (0.007)
114.1 0.137 (0.005)
134.6 0.157 (0.007)
147.0 0.168 (0.005)
163.4 0.179 (0.002)

Linear regression using all data for the four specimens gives:


Water Absorption Coefficient for the major surfaces = 0.0011 0.00005 kg m
-2
s
-
.



232
Bomberg, M. T. and Kumaran, M.K., " A Test method to determine air flow resistance of
exterior membranes and sheathings," Journal of Thermal Insulation, Vol.9, pp. 224-235,1986.
233
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
B1115.13

198


33. HYGROTHERMAL PROPERTIES OF SPUN BONDED
POLYOLEFIN MEMBRANE (SBP)

The test specimens used for the measurements reported here
are taken from a roll of a commercial product.

Thickness: 0.14 to 0.15 mm
Mass per Area: (65 ) 5) g m
-2

Water Vapour Transmission (WVT) Rate measurements
234
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used.

Table 33.1. Dry Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature and standard errors for WVT rate.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

0.142 49.0 (1) 23.2 (0.1) 3.67E-06 (5.8E-08)
0.146 49.0 (1) 23.2 (0.1) 3.40E-06 (2.1E-08)
0.141 49.0 (1) 23.2 (0.1) 3.18E-06 (3.9E-08)
0.142 68.6 (1) 23.4 (0.1) 5.57E-06 (1.6E-08)
0.146 68.6 (1) 23.4 (0.1) 5.40E-06 (2.0E-08)
0.141 68.6 (1) 23.4 (0.1) 5.09E-06 (2.6E-08)
0.142 87.6 (1) 23.5 (0.2) 7.94E-06 (5.4E-08)
0.146 87.6 (1) 23.5(0.2) 7.43E-06 (3.1E-08)
0.141 87.6 (1) 23.5 (0.2) 7.15E-06 (3.6E-08)

Table 33.2. Wet Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature and standard errors for WVT rate.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

0.147 68.9 (1) 23.4 (0.1) 2.59E-06 (1.1E-08)
0.151 68.9 (1) 23.4 (0.1) 2.44E-06 (2.0E-08)
0.153 68.9 (1) 23.4 (0.1) 2.40E-06 (3.4E-08)
0.147 89.5 (2) 23.2 (0.2) 5.94E-07 (8.1E-09)
0.151 89.5 (2) 23.2 (0.2) 6.12E-07 (6.4E-09)
0.153 89.5 (2) 23.2 (0.2) 5.19E-07 (4.9E-09)
The average thickness of still air in the cups for both series is 15 mm

234
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M.
K., A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water
Vapour Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

199


Derived Water Vapour Permeance
235


Table 33.3. Dependence of water vapour permeance of SBP on relative humidity.

RH, % Permeance
kg m
-2
s
-1
Pa
-1

RH, % Permeance
kg m
-2
s
-1
Pa
-1

10
4.37E-09
60
4.37E-09
20
4.37E-09
70
4.37E-09
30
4.37E-09
80
4.37E-09
40
4.37E-09
90
4.37E-09
50
4.37E-09
100
4.37E-09

From the TableCurve statistics, the estimated uncertainty in the derived value of the permeance
is less than 5 %.
Air Permeance
236
:
Three circular test specimens, each approximately 15 cm in diameter are used in these
measurements. The summary of the statistical analyses of all data obtained from two series of
measurements on each specimen is shown in Figure 1.
0
0.02
0.04
0.06
0.08
0.1
0.12
0.14
0.16
0.18
0.2
0 50 100 150 200 250 300
Pressure Difference, Pa
F
l
o
w
,

l

m
-
2

s
-
1
Data Points Mean Permeance
Upper Confidence Interval Lower Confidence Interval

Figure 33.1. The dependence of airflow rate on pressure difference for SBP.

235
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

200


For the range of pressure differences between 25 and 250 Pa, the flow rate linearly varies with
the pressure difference. The air permeance of SBP is (4.6 ) 2.5) E-07 kg m
-2
s
-1
Pa
-1
.


Water Absorption Coefficient
237
:

Four test specimens, 5 cm X 5 cm each, were prepared as follows. The membrane was attached
to the major surface of a 5 cm X 5 cm OSB using a thin (less than 1 mm) layer of drywall
compound and allowed to dry. The sides were then sealed using wax. Water was maintained at
(22 1) C and allowed to touch the exposed surface of the membrane. The results from the
water absorption measurements are listed in Table 4. The numbers in parentheses give the
standard deviations.

Table 33.4. Water absorption data for SBP.
Square Root of
time, s


Water Absorption
kg m
-2

7.7 0.013 (0.004)
13.4 0.015 (0.006)
17.3 0.015 (0.007)
24.5 0.015 (0.005)
34.6 0.013 (0.005)
49.0 0.016 (0.005)
61.0 0.020 (0.004)
75.5 0.028 (0.007)
89.7 0.034 (0.004)
112.5 0.043 (0.007)
127.5 0.048 (0.005)
144.1 0.057 (0.002)
155.3 0.059 (0.004)

Linear regression using all data for the four specimens gives:


Water Absorption Coefficient for the major surfaces = 0.00031 0.00003 kg m
-2
s
-
.



236
Bomberg, M. T. and Kumaran, M.K., " A Test method to determine air flow resistance of
exterior membranes and sheathings," Journal of Thermal Insulation, Vol.9, pp. 224-235,1986.
237
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
B1115.13

201


34. HYGROTHERMAL PROPERTIES OF SPUN BONDED
POLYOLEFIN MEMBRANE WITH CRINKLED SURFACE (SBPC)


The test specimens used for the measurements reported here
are taken from a roll of a commercial product.
Thickness: 0.097 to 0.112 mm
Mass per Area: (67 ) 2) g m
-2

Water Vapour Transmission (WVT) Rate measurements
238
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used.

Table 34.1. Dry Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature and standard errors for WVT rate.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

0.101 49.0 (1) 23.2 (0.1) 3.57E-06 (1.8E-08)
0.112 49.0 (1) 23.2 (0.1) 3.28E-06 (2.5E-08)
0.106 49.0 (1) 23.2 (0.1) 3.00E-06 (2.6E-08)
0.101 68.6 (1) 23.4 (0.1) 5.13E-06 (6.1E-09)
0.112 68.6 (1) 23.4 (0.1) 4.94E-06 (1.1E-08)
0.106 68.6 (1) 23.4 (0.1) 4.27E-06 (1.3E-08)
0.101 87.6 (1) 23.5 (0.2) 7.59E-06 (1.6E-08)
0.112 87.6 (1) 23.5(0.2) 7.21E-06 (2.8E-08)
0.106 87.6 (1) 23.5 (0.2) 6.16E-06 (3.8E-09)

Table 34.2. Wet Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature and standard errors for WVT rate.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

0.101 68.9 (1) 23.4 (0.1) 2.15E-06 (7.4E-09)
0.103 68.9 (1) 23.4 (0.1) 2.30E-06 (1.2E-08)
0.097 68.9 (1) 23.4 (0.1) 2.22E-06 (1.6E-08)
0.101 89.5 (2) 23.2 (0.2) 3.94E-07 (4.5E-09)
89.5 (2) 23.2 (0.2) 4.77E-07 (3.3E-09)
0.097 89.5 (2) 23.2 (0.2) 4.37E-07 (4.6E-09)
0.103
The average thickness of still air in the cups for both series is 15 mm

238
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M.
K., A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water
Vapour Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

202


Derived Water Vapour Permeance
239


Table 34.3. Dependence of water vapour permeance of SBPC on relative humidity.

RH, % Permeance
kg m
-2
s
-1
Pa
-1

RH, % Permeance
kg m
-2
s
-1
Pa
-1

10
3.17E-09
60
3.17E-09
20
3.17E-09
70
3.17E-09
30
3.17E-09
80
3.17E-09
40
3.17E-09
90
3.17E-09
50
3.17E-09
100
3.17E-09

From the TableCurve statistics, the estimated uncertainty in the derived value of the permeance
is about 15 %.
240
: Air Permeance
Three circular test specimens, each approximately 15 cm in diameter are used in these
measurements. The summary of the statistical analyses of all data obtained from two series of
measurements on each specimen is shown in Figure 1.
0
0.02
0.04
0.06
0.08
0.1
0.12
0 100 200 300 400
Pressure Difference, Pa
F
l
o
w
,

l

m
-
2

s
-
1
Data Points Mean Permeance
Upper Confidence Interval Lower Confidence Interval

Figure 34.1. The dependence of airflow rate on pressure difference for SBPC.

239
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

203


For the range of pressure differences between 25 and 250 Pa, the flow rate linearly varies with
the pressure difference. The air permeance of SBPC is (3.0 ) 1) E-07 kg m
-2
s
-1
Pa
-1
.


Water Absorption Coefficient
241
:

Four test specimens, 5 cm X 5 cm each, were prepared as follows. The membrane was attached
to the major surface of a 5 cm X 5 cm OSB using a thin (less than 1 mm) layer of drywall
compound and allowed to dry. The sides were then sealed using wax. Water was maintained at
(22 1) C and allowed to touch the exposed surface of the membrane. The results from the
water absorption measurements are listed in Table 4. The numbers in parentheses give the
standard deviations.

Table 34.4. Water absorption data for SBPC.
Square Root of
time, s


Water Absorption
kg m
-2

7.7 0.010 (0.005)
13.4 0.011 (0.009)
17.3 0.010 (0.002)
24.5 0.013 (0.002)
30.0 0.013 (0.002)
37.9 0.015 (0.003)
44.5 0.009 (0.002)
49.6 0.015 (0.000)
72.7 0.016 (0.002)
83.4 0.023 (0.003)
96.4 0.029 (0.002)
118.0 0.036 (0.004)
132.4 0.039 (0.003)
148.0 0.042 (0.003)
158.7 0.046 (0.004)

Linear regression using all data for the four specimens gives:


Water Absorption Coefficient for the major surfaces = 0.00024 0.00003 kg m
-2
s
-
.



240
Bomberg, M. T. and Kumaran, M.K., " A Test method to determine air flow resistance of
exterior membranes and sheathings," Journal of Thermal Insulation, Vol.9, pp. 224-235,1986.
241
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
B1115.13

204


35. HYGROTHERMAL PROPERTIES OF VINYL WALLPAPER

Mass per Area: 170 g m


The test specimens used for the measurements reported here
are taken from a roll of a commercial product.

Thickness: (0.205 ) 0.008) mm
-2

Water Vapour Transmission (WVT) Rate measurements
242
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used.
Table 35.1. Dry Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature and standard errors for WVT rate.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

0.203 50.4 (1) 22.9 (0.1) 2.13E-07 (5.0E-10)
0.208 50.4 (1) 22.9 (0.1) 2.15E-07 (4.0E-10)
0.197 50.4 (1) 22.9 (0.1) 2.22E-07 (5.0E-10)
0.203 70.2 (1) 22.9 (0.1) 3.16E-07 (1.6E-09)
0.208 70.2 (1) 22.9 (0.1) 3.18E-07 (3.0E-10)
0.197 70.2 (1) 22.9 (0.1) 3.32E-07 (1.6E-09)
0.203 91.2 (1) 22.7 (0.1) 4.53E-07 (2.9E-09)
0.208 91.2 (1) 22.7 (0.1) 4.55E-07 (9.0E-09)
0.197 91.2 (1) 22.7 (0.1) 4.88E-07 (9.8E-09)

Table 35.2. Wet Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature and standard errors for WVT rate.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

0.202 70.4 (1) 22.9 (0.1) 4.78E-07 (2.6E-09)
0.209 70.4 (1) 22.9 (0.1) 3.77E-07 (2.3E-09)
0.210 70.4 (1) 22.9 (0.1) 3.73E-07 (3.0E-09)
0.202 90.5 (2) 22.8 (0.2) 1.92E-07 (1.8E-09)
0.209 90.5 (2) 22.8 (0.2) 1.42E-07 (2.6E-09)
0.210 90.5 (2) 22.8 (0.2) 1.39E-07 (3.6E-09)
The average thickness of still air in the cups in both series is 15 mm

242
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M.
K., A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water
Vapour Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

205


Derived Water Vapour Permeance
243


Table 35.3. Dependence of water vapour permeance of vinyl wallpaper on relative humidity.

RH, % Permeance
kg m
-2
s
-1
Pa
-1

RH, % Permeance
kg m
-2
s
-1
Pa
-1

10
8.48E-11
60
2.59E-10
20
1.06E-10
70
3.16E-10
30
1.35E-10
80
3.82E-10
40
1.69E-10
90
4.60E-10
50
2.10E-10
100
5.51E-10

From the TableCurve statistics, the estimated uncertainty in the derived value of the permeance
may be as high as 30 %.



Air Permeance
244
:
Three circular test specimens, each approximately 15 cm in diameter were used in these
measurements. No measurable airflow was recorded for pressures differences up to several
kPa. Pressure decay measurements resulted in an estimate of 5E-09 kg m
-2
s
-1
Pa
-1
for the air
permeance of vinyl wall paper.
Water Absorption Coefficient
245
:

Four test specimens, 5 cm X 5 cm each, were prepared as follows. The wallpaper was attached
to the major surface of a 5 cm X 5 cm gypsum board using a thin (less than 1 mm) layer of
drywall compound and allowed to dry. The sides were then sealed using wax. Water was
maintained at (22 1) C and allowed to touch the exposed surface of the wallpaper. The results
from the water absorption measurements are listed in Table 4. The numbers in parentheses give
the standard deviations.

243
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
244
Bomberg, M. T. and Kumaran, M.K., " A Test method to determine air flow resistance of
exterior membranes and sheathings," Journal of Thermal Insulation, Vol.9, pp. 224-235,1986.
245
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
B1115.13

206



Table 35.4. Water absorption data for vinyl wall paper.

Square Root of
time, s


Water Absorption
kg m
-2

7.75 0.002 (0.002)
13.42 0.005 (0.002)
17.32 0.006 (0.002)
18.97 0.009 (0.003)
42.43 0.012 (0.004)
54.77 0.016 (0.006)
85.56 0.023 (0.004)
95.18 0.021 (0.007)
115.41 0.029 (0.006)
142.41 0.026 (0.007)
156.65 0.027 (0.008)
(0.004)
316.45 0.030 (0.004)
332.26 0.039 (0.010)
1043.55 0.035 (0.004)
280.89 0.035


Linear regression of data from the initial stage of the process gives:

Water Absorption Coefficient for the major surfaces = 0.00025 0.00002 kg m
-2
s
-
.


B1115.13

207


36. HYGROTHERMAL PROPERTIES OF PRIMER AND PAINT ON
A GYPSUM BOARD AS A SUBSTRATE


The test specimens used for the measurements reported here
are taken from the following three:
1. Interior Gypsum Board (one 4 x 8 board); same product
used in Chapter 2B.
2. Part of the above Gypsum Board coated with one coat of a
Primer
3. Part of the above Gypsum Board coated with one coat of
Primer and two coats of a Latex Paint

1. Gypsum Board

Water Vapour Transmission (WVT) Rate measurements
246
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used.

Table 36.1. Dry Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

12.50 50.3 (1) 22.9(0.1) 2.99E-06 (1.3E-08)
12.48 50.3 (1) 22.9(0.1) 2.93E-06 (5.2E-09)
12.44 50.3 (1) 22.9(0.1) 2.94E-06 (9.0E-09)
12.50 70.3 (1) 23.0(0.1) 4.12E-06 (1.1E-08)
12.48 70.3 (1) 23.0(0.1) 4.18E-06 (1.3E-08)
12.44 70.3 (1) 23.0(0.1) 4.28E-06 (1.6E-08)
12.50 89.8 (1) 22.9(0.1) 5.65E-06 (2.0E-08)
12.48 89.8 (1) 22.9(0.1) 5.85E-06 (6.1E-09)
12.44 89.8 (1) 22.9(0.1) 5.77E-06 (1.1E-08)


246
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M.
K., A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water
Vapour Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

208



Table 36.2. Wet Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature WVT Rate
C kg m
-2
s
-1

12.51 70.4 (1) 22.9(0.1) 2.44E-06 (1.2E-08)
12.50 70.4 (1) 22.9(0.1) 2.47E-06 (1.2E-08)
12.43 70.4 (1) 22.9(0.1) 2.53E-06 (1.5E-08)
12.51 90.0 (1) 22.9(0.1) 1.02E-06 (1.3E-08)
12.50 90.0 (1) 22.9(0.1) 1.03E-06 (1.2E.08)
12.43 90.0 (1) 22.9(0.1) 1.02E-06 (1.1E-08)
The average thickness of still air in the cups for both series is 15 mm



Water Absorption Coefficient
247
:

Four test specimens, 51 mm X 51 mm each, were used in these measurements. Water is
maintained at (22 1) C. The numbers in parentheses give the standard deviations.

Table 36.3. Water absorption across the major surface.
Square Root of
time, s


Water Absorption
kg m
-2

7.7 0.03 (0.01)
13.4 0.05 (0.01)
19.0 0.06 (0.02)
25.7 0.08 (0.01)
34.6 0.09 (0.01)
42.4 0.10 (0.01)
52.0 0.13 (0.01)
62.4 0.14 (0.01)
84.9 0.16 (0.02)
105.4 0.19 (0.01)
115.9 0.20 (0.02)
130.8 0.23 (0.02)
0.24(0.02) 143.2

Linear regression of the data from the first linear part of the absorption process gives:



Water Absorption Coefficient for the major surfaces = 0.0019 0.0001 kg m
-2
s
-
.

Air Permeance:
From the airflow measurements the air permeance of the gypsum board is (3.33 ) 0.05) E-07
kg m
-2
s
-1
Pa
-1
(see chapter 2.).


247
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
B1115.13

209





2. Gypsum Board + One Coat of the Primer

Water Vapour Transmission (WVT) Rate measurements
248
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used.

Table 36.4. Dry Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

12.69 50.3 (1) 22.9 (0.1) 1.41E-06 (3.2E-09)
12.71 50.3 (1) 22.9 (0.1) 1.50E-06 (2.7E-09)
12.63 50.3 (1) 22.9 (0.1) 1.48E-06 (3.3E-09)
12.69 70.3(1) 23.0 (0.1) 2.39E-06 (3.3E-09)
12.71 70.3(1) 23.0 (0.1) 2.52E-06 (5.5E-09)
12.63 70.3(1) 23.0 (0.1) 2.48E-06 (5.9E-09)
12.69 89.8 (1) 22.9 (0.1) 4.26E-06 (1.9E-08)
12.71 89.8 (1) 22.9 (0.1) 4.34E-06 (2.8E-08)
12.63 89.8 (1) 22.9 (0.1) 4.36E-06 (2.1E-08)


Table 36.5. Wet Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties
Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

12.47 70.4 (1) 22.9 (0.1) 1.84E-06 (4.7E-09)
12.44 70.4 (1) 22.9 (0.1) 1.93E-06 (1.0E-08)
12.42 70.4 (1) 22.9 (0.1) 1.97E-06 (1.1E-08)
12.47 90.0 (1) 22.9 (0.1) 9.66E-07 (1.9E-08)
12.44 90.0 (1) 22.9 (0.1) 9.76E-07 (1.1E-08)
12.42 90.0 (1) 22.9 (0.1) 9.62E-07 (1.0E-08)

The average thickness of still air in the cups for both series is 15 mm





248
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M.
K., A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water
Vapour Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

210





Water Absorption Coefficient
249
:

Four test specimens, 51 mm X 51 mm each, were used in these measurements. Water is
maintained at (22 1) C. The numbers in parentheses give the standard deviations.

Table 36.6. Water absorption across the major surface.
Square Root of
time, s


Water Absorption
kg m
-2

7.7 0.03 (0.00)
(0.01)
19.0 0.05 (0.02)
23.2 0.06 (0.03)
30.0 0.08 (0.04)
(0.05)
44.5 0.11 (0.05)
52.0 0.12 (0.06)
73.5 0.17 (0.06)
84.5 0.18 (0.07)
93.9 0.19 (0.07)
107.9 0.21 (0.07)
120.0 0.23 (0.07)
135.7 0.24 (0.07)
148.4 0.27 (0.07)
13.4 0.04
37.9 0.10
61.0 0.14 (0.07)

Linear regression of the data from the first linear part of the absorption process gives:



Water Absorption Coefficient for the major surfaces = 0.0020 0.0001 kg m
-2
s
-
.


Air Permeance:
The specimens gave no measurable airflow for pressure differences up to several kPa. From a
pressure decay experiment in which the pressure inside the chamber that carries the test
specimens was increased by approximately 100 kPa and the change in pressure with time was
measured, the air permeance of gypsum board coated with the Primer is estimated to be (2.2 )
0.7) E-08 kg m
-2
s
-1
Pa
-1
.

249
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
B1115.13

211


3. Gypsum Board + One Coat of the Primer + Two Coats of the Latex Paint

mm
WVT Rate
Water Vapour Transmission (WVT) Rate measurements
250
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used.

Table 36.7. Dry Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties.

Specimen Thickness Chamber RH
%
Chamber Temperature
C kg m
-2
s
-1

12.57 50.4 (1) 22.9 (0.1) 3.23E-07 (2.7E-09)
12.52 50.4 (1) 22.9 (0.1) 3.24E-07 (2.9E-09)
50.4 (1) 22.9 (0.1) 3.29E-07 (1.7E-09)
12.57 70.2(1) 22.9 (0.1) 5.43E-07 (2.9E-09)
12.52 70.2(1) 22.9 (0.1) 5.40E-07 (3.6E-09)
12.47 70.2(1) 22.9 (0.1) 5.42E-07 (3.4E-09)
12.57 91.2 (1) 22.7 (0.1) 1.93E-06 (1.4E-08)
12.52 91.2 (1) 22.7 (0.1) 1.91E-06 (6.9E-09)
12.47 91.2 (1) 22.7 (0.1) 1.92E-06 (1.2E-08)
12.47


Table 36.8. Wet Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

12.59 70.4 (1) 22.9 (0.1) 1.05E-06 (1.7E-09)
12.53 70.4 (1) 22.9 (0.1) 1.07E-06 (2.8E-09)
12.56 70.4 (1) 22.9 (0.1) 1.07E-06 (1.6E-09)
12.59 90.6 (1) 22.8 (0.1) 6.22E-07 (7.2E-09)
12.53 90.6 (1) 22.8 (0.1) 6.24E-07 (3.8E-09)
12.56 90.6 (1) 22.8 (0.1) 6.24E-07 (3.8E-09)

The average thickness of still air in the cups for both series is 15 mm







250
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M.
K., A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water
Vapour Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

212





Square Root of
time, s
Water Absorption Coefficient
251
:
Four test specimens, 51 mm X 51 mm each, were used in these measurements. Water is
maintained at (22 1) C. The numbers in parentheses give the standard deviations.

Table 36.9. Water absorption across the major surface.


Water Absorption
kg m
-2

7.7 0.01 (0.00)
11.0 0.01 (0.01)
15.5 0.02 (0.01)
20.5 0.02 (0.01)
24.5 0.03 (0.01)
30.0 0.05 (0.01)
37.9 0.06 (0.01)
45.2 0.08 (0.01)
56.4 0.09 (0.02)
68.8 0.11 (0.01)
81.2 0.14 (0.02)
91.3 0.14 (0.02)
105.6 0.16 (0.02)
117.7 0.17 (0.02)
133.7 0.20 (0.02)

Linear regression of the data from the first linear part of the absorption process gives:


The specimens gave no measurable airflow for pressure differences up to several kPa. From a
pressure decay experiment in which the pressure inside the chamber that carries the test
specimens was increased by approximately 100 kPa and the change in pressure with time was
measured, the air permeance of gypsum board coated with the Primer (one coat) and Latex Paint
(two coats) is estimated to be (2.5 ) 2.5) E-09 kg m


Water Absorption Coefficient for the major surfaces = 0.0016 0.0001 kg m
-2
s
-
.


Air Permeance:
-2
s
-1
Pa
-1
.

251
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
B1115.13

213


Derived Water Vapour Permeance


252
:
Table 36.10. Dependence of vapour permeances of Gypsum Board, Primer and Latex Paint on
relative humidity.

RH, %
Permeance of Gypsum

kg m
-2
s
-1
Pa
-1

Permeance of Gypsum
+ Primer (one coat)
kg m
-2
s
-1
Pa
-1

Permeance of Gypsum +
Primer (one coat) +
Latex Paint (two coats)
kg m
-2
s
-1
Pa
-1

10
2.34E-09 6.83E-10 1.08E-10
20
2.52E-09 1.11E-09 1.50E-10
30
2.72E-09 1.49E-09 2.08E-10
40
2.95E-09 1.85E-09 2.89E-10
50
3.19E-09 2.2E-09 4.04E-10
60
3.46E-09 2.54E-09 5.65E-10
70
3.76E-09 2.89E-09 7.97E-10
80
4.09E-09 3.24E-09 1.14E-09
90
4.47E-09 3.59E-09 1.65E-09
100
4.90E-09 3.96E-09 2.46E-09



252
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
B1115.13

214


37. HYGROTHERMAL PROPERTIES OF EIFS (BASE COAT AND
FINISH COAT ON EPS)


The test specimens used for the measurements reported here
are prepared from an EIFS wall specimen built at the Institute
for Research in Construction. The base coat is polymer
cement and the finish coat is Latex Acrylic.

Thickness of Base Coat + Finish Coat: (4.4 ) 0.1) mm
Bulk Density of Base Coat + Finish Coat: (1140 ) 50) kg m
-3


Note:



The test specimens being a composite material, thermal conductivity and equilibrium moisture
content measurements were not performed. However, five test specimens, 5 cm X 5 cm, were
prepared and the EPS layer was removed from each specimen using a solvent. The specimens
devoid of EPS were dried at 60 C to constant mass and the average thickness and bulk density
of Base Coat + Finish Coat, as reported above, were determined. Then the specimens were
soaked in water for 72 h. The water uptake was then determined as (0.090 0.004) kg kg
-1
.
Water Vapour Transmission (WVT) Rate measurements
253
:
For each test condition, 3 circular specimens, each 15 cm in diameter, are used. Each specimen
is a composite of Base Coat + Finish Coat + EPS. The average thickness of the EPS layer is
(34.3 ) 0.3) mm. The density of the EPS is (15 1) kg m
-3
.

Table 37.1. Dry Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature and standard errors for WVT rate.
Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

38.94 72.7 (1) 22.6 (0.1) 1.65E-07 (5.3E-10)
38.37 72.7 (1) 22.6 (0.1) 1.81E-07 (4.6E-10)
38.46 72.7 (1) 22.6 (0.1) 1.91E-07 (3.5E-10)


253
Measurements are done as described by: Lackey, J. C., Marchand, R. G., and Kumaran, M.
K., A Logical Extension of the ASTM Standard E96 to Determine the Dependence of Water
Vapour Transmission on Relative Humidity, Insulation Materials: Testing And Applications: Third
Volume, ASTM STP 1320, R. S. Graves and R. R. Zarr, Eds, American Society for Testing and
Materials, West Conshohocken, PA, 1997, pp 456-470.
B1115.13

215


Table 37.2. Wet Cup Measurements: The numbers in parentheses indicate the experimental
uncertainties for RH and temperature and standard errors for WVT rate.

Specimen Thickness
mm
Chamber RH
%
Chamber Temperature
C
WVT Rate
kg m
-2
s
-1

38.68 72.7 (1) 22.6 (0.1) 5.34E-08 (1.1E-09)
38.55 72.7 (1) 22.6 (0.1) 5.69E-08 (1.6E-09)
72.7 (1) 22.6 (0.1) 4.90E-08 (7.9E-10) 39.05

The average thickness of still air in the cups in both series is 15 mm. The finish coat surface is in
contact with the chamber air.

Derived Water Vapour Permeance
254


Table 37.3. Dependence of water vapour permeance of the composite test specimens on relative
humidity.

RH, % Permeance
kg m
-2
s
-1
Pa
-1

RH, % Permeance
kg m
-2
s
-1
Pa
-1

10
9.47E-11
60
9.47E-11
20
9.47E-11
70
9.47E-11
30
9.47E-11
80
9.47E-11
40
9.47E-11
90
9.47E-11
50
9.47E-11
100
9.47E-11

From the TableCurve statistics, the estimated uncertainty in the derived value of the permeance
is 10 %.


Air Permeance
255
:
Three circular test specimens, each approximately 15 cm in diameter were used in these
measurements. No measurable airflow was recorded for pressures differences up to several
kPa. Pressure decay measurements did not yield an estimate for the air permeance of the
composite test specimens.





254
The analysis is done as described in : Kumaran, M. K., An Alternative Procedure for the
Analysis of Data from the Cup Method Measurements for Determination of Water Vapour
Transmission Properties, Journal of Testing and Evaluation, JTVEA, Vol. 26 , pp. 575-581, 1998.
255
Bomberg, M. T. and Kumaran, M.K., " A Test method to determine air flow resistance of
exterior membranes and sheathings," Journal of Thermal Insulation, Vol.9, pp. 224-235,1986.
B1115.13

216



Four composite test specimens, 5 cm X 5 cm each, were prepared. Water was maintained at (22
1) C and allowed to touch the exposed surface of the Finish Coat. The results from the water
absorption measurements are listed in Table 4. The numbers in parentheses give the standard
deviations.

Water Absorption Coefficient
256
:


Table 37.4. Water absorption data for the Finish Coat surface.
Square Root of
time, s


Water Absorption
kg m
-2

7.75 0.01 (0.00)
13.42 0.02 (0.00)
17.32 0.03 (0.00)
24.49 0.03 (0.00)
42.43 0.03 (0.00)
(0.00)
84.14 0.06 (0.00)
101.00 0.06 (0.01)
117.47 0.07 (0.01)
132.14 0.09 (0.01)
146.97 0.09 (0.01)
157.99 0.10 (0.01)
172.34 0.11 (0.01)
(0.02)
325.24 0.18 (0.02)
340.91 0.19 (0.01)
60.00 0.05
290.86 0.16


Linear regression of data from the initial stage of the process gives:



Water Absorption Coefficient for the major surface with the Finish Coat = 0.00053 0.00003 kg
m
-2
s
-
.






256
The procedure used is based on: CEN/TC 89/WG 10 N95 Determination of water absorption
coefficient, 1994-07-07.
B1115.13

217


APPENDIX I. How Well Should One Know the Hygrothermal
Properties of Building Materials?

Kumar Kumaran and Jinkai Wang

Building Envelope and Structure, Institute for Research in Construction, National
Research Council of Canada, Ottawa K1A 0R6, Canada
E-mail: kumar.kumaran@nrc.ca, jinkai.wang@nrc.ca


Abstract

Hygrothermal models enable us to analyze the hygrothermal behaviour of building envelope
components. Knowledge on several hygrothermal properties is a prerequisite for the application
of such models. Often the question is asked: How well should one know the properties? This
paper makes an attempt to provide some facts that may assist one to answer the question. A
well-controlled drying experiment was conducted on a cement board used as exterior sheathing
member in North America. All hygrothermal properties of the material have been determined
through well-known test procedures. The experimental data were used to benchmark an
advanced hygrothermal model called hygIRC. The model was subsequently used to conduct a
parametric analysis of the drying behaviour of the cement board. In the analysis, three
hygrothermal properties that affect the drying process were systematically varied. These
properties are: sorption/suction isotherm, water vapour permeability and moisture diffusivity. The
results show that the sorption/suction isotherm has to be determined as precisely as possible
according to current procedures. A 50 % variation in the vapour permeability has noticeable effect
on the drying behaviour of the cement board. But a 50 % variation in the moisture diffusivity has
insignificant effect on the drying details.
Key words: drying, vapour permeability, sorption/suction isotherm, moisture diffusivity,
hygrothermal models.
Introduction

Heat, air and moisture transport models[1] are powerful tools in the hands of building
practitioners. These models can assess the long-term hygrothermal performance of a given
building envelope assembly that operates in a specific geographic location and provides a
specific indoor environment. The models shall include all the known aspects of building physics
and the numerical techniques used shall be reliable. In addition, the following hygrothermal
properties of various materials in the assembly shall be representative of current products:
thermal conductivity as a function of temperature and moisture content, heat capacity as a
function of temperature and moisture content, equilibrium moisture content as a function of
B1115.13

218


relative humidity, water vapour permeability as a function of relative humidity, moisture diffusivity
as a function of moisture content, water absorption coefficient and air permeabilty as a function of
pressure difference and moisture content.
Determination of these properties is a challenging task due to a variety of uncertainties and
practical difficulties. Some are inherent to the procedures. The others are induced by the material
non-homogeneity and product variability. To give an example, ten plywood products were
subjected to the cup measurements to determine their water vapour permeabilities at a mean RH
equal to 86 %. The deviation of the results from an average value of 9.5E-12 kg m
28 %. So, how well one has to know the above properties to make acceptable predictions?
Results from systematic parametric analyses using reliable hygrothermal models that have been
properly benchmarked may answer this question.

-1
s
-1
Pa
-1
was
A drying experiment to benchmark models

Three 30 cm X 30 cm test specimens were cut from a cement board that is used as a sheathing
member in walls in North America. The average thickness of the product is 12.5 mm. The
hygrothermal properties of the product determined at the Institute for Research in Construction in
an earlier investigation are listed in Table 1.
The specimens, with edges sealed using a mixture of waxes impermeable to moisture,
were saturated by keeping under water for 24 h. The initial increases in weight were recorded and
the specimens were vertically placed on one of their edges in a chamber maintained at 25 *C and
70 % RH. Air was circulated over the major surfaces with velocities between 0.1 and 0.3 m/s. The
specimens were periodically removed from the chamber and the decrease in weight recorded
until equilibrium was attained. The average drying curve for the three test specimens is given in
Table 2.
Table 1. Hygrothermal properties of the cement board.
Density = 1130 kg m
-3
Heat capacity = 840 J kg
-1
K
-1

Thermal conductivity = 0.25 W m
-1
K
-1

Sorption/suction curve Moisture diffusivity Vapour permeability
RH Moisture content
(Fraction) (kg/kg)
0.02 8.77E-03
0.14 1.21E-02
0.26 1.44E-02
0.38 1.67E-02
0.50 1.94E-02
0.52 2.00E-02
0.64 2.37E-02
0.76 2.93E-02
0.88 4.03E-02
1.00 1.25E-01

Moisture Diffusivity
(kg/kg) (m
2
/s)
0.00 1.00E-13
0.02 1.00E-13
0.03 1.00E-13
0.05 5.00E-12
0.06 8.55E-10
0.06 8.89E-10
0.08 1.15E-09
0.09 1.60E-09

RH permeability
(Fraction) (kg m
-1
.Pa
-1
.s
-1
)
0.00 7.80E-12
0.12 8.09E-12
0.24 8.40E-12
0.37 8.78E-12
0.49 9.32E-12
0.51 9.43E-12
0.63 1.04E-11
0.76 1.22E-11
0.88 1.76E-11
1.00 2.68E-11

0.11 2.68E-09
0.13 9.14E-09
B1115.13

219



Table 2. The average drying curve for the three test specimens
Time, h Moisture content, g Time, h Moisture content, g
0 189.90 11.5 80.09
1 177.85 23.75 46.90
2 166.41 28.5 42.93
3 154.38 29.5 40.21
4 143.22 33.4 38.13
5.5 127.79 47.75 34.00
6.5 116.02 51.5 33.02
7.5 108.47 58.15 32.16
8.5 99.67 73.9 31.61
9.55 91.00 100 30.37
10.5 85.31 123.5 29.84

Results from a simulation of the drying process

An advanced hygrothermal model, hygIRC, developed at the Institute was used to simulate the
drying experiment exactly. Since the specimens were immersed in water for 24 h, it was assumed
that they were at a uniform initial RH =100 %. The results from the simulation are compared with
the measurements in Figure 1.
0
50
100
150
200
0 2 4 6
TIME, day
M
O
I
S
T
U
R
E
,

g
Measured
Simulated
Figure 1. Comparison of the simulated and measured drying curves.

Though the measured initial moisture content was slightly higher than the simulated, the
overall agreement between the measured and simulated drying curves is acceptable in terms of
the duration of the process and the shape of the drying curve.
B1115.13

220



Parametric analysis and discussion

The hygrothermal properties as listed in Table 1 were used in the original simulation referred to in
Figure 1. Eight other simulations were carried out as coded below, by systematically varying three
hygric properties: sorption/suction curve, vapour permeability and moisture diffusivity.
Code Variation from the properties listed in Table 1
vap 50 The vapour permeability was reduced by 50 % of the original
vap 150 The vapour permeability was increased by 50 % of the original
dfl 50 The moisture diffusivity was reduced by 50 % of the original
dfl 150 The moisture diffusivity was increased by 50 % of the original
sorp 50 The sorption curve was reduced by 50 % of the original
sorp 150 The sorption curve was increased by 50 % of the original
all 50 All three properties were reduced by 50 % of the original
all 150 All three properties were increased by 50 % of the original

Figure 2 compares the results from these simulations with the original drying curve
shown in Figure 1. The moisture contents are normalized against the initial moisture content.
There is very little difference among the results for the initial part of the drying curve, until the
moisture content reaches 50 % of the initial value.
B1115.13

221


0
0.05
0.1
0.15
0.2
0.25
0.3
0.35
0.4
0.45
0.5
0 1 2 3 4
TIME, day
M
O
I
S
T
U
R
E
,

(
-
)
sorp 50
sorp 150
all 50
vap 50
all 150
vap 150
dfl 50
original
dfl 150
Figure 2. Results from the parametric analysis compared with the original drying curve

A 50 % uncertainty in moisture diffusivity alone has insignificant effect on the details of
the drying curve. A 50 % uncertainty in the vapour permeability changes the shape of the curve
by affecting the duration of the process, especially when it is underestimated. A 50 % uncertainty
in the sorption curve, as one would expect, affects the shape of the drying curve significantly. The
reason for this is that all model calculations assume local equilibrium at all time. 50%
uncertainties in all three properties will result is very erroneous results, in terms of the shape of
the drying curve as well as the duration of the process.

Concluding remarks

Comparison of the simulated and measured drying curves in this investigation confirms that the
physics of the drying process is captured well by the hygrothermal model developed at the
Institute. Also the numerical techniques used are sound. The properties of the material being well
determined, the agreement between the two drying curves is acceptable in terms of the shape
and time frame.
Parametric analysis of the drying process investigated here leads to the following remarks.
A proper knowledge of the order of magnitude of the moisture diffusivity may give acceptable
B1115.13

222


drying curves. It is desirable that the vapour permeability is known at least within 20 % of the
actual value. However, the sorption curve has to be known rather well, maybe within 5 %.

Reference
[1] Hens, H., Heat, Air and Moisture Transport, Final Report, Volume 1, Task 1: Modelling,
International Energy Agency Annex 24, Laboratorium Bouwfysica, K. U.-Leuven, Belgium, 1996.

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APPENDIX II
Weight
Experimental and Analytical Investigations on the Drying Process
Undergone by Aerated Concrete

Fitsum Tariku and Mavinkal K Kumaran

INTRODUCTION
Two series of drying process of aerated concrete, one in a conditioned room and the
other in a well-controlled humidity chamber are investigated through experiment and computer
simulations. In the first case, drying in a conditioned room, the moisture profile along the length of
the specimen is measured using a gamma-ray apparatus, at various intervals. In the second
case, drying in the humidity chamber, the total moisture content of the specimen is measured
gravimetrically. Both experiments are compared with simulation results with IRCs advanced
hygrothermal model (hygIRC), using the same initial and boundary conditions as the experiment.
The concrete is the same as that reported in Chapter 2 of the main report. Therefore all relevant
hygrothermal properties are known. The main objective of the investigation is to assess the
suitability of using moisture diffusivity that has been determined from a moisture uptake process
to describe drying processes.
DRYING IN A CONDITIONED ROOM
Drying Experiment using Gamma-ray
Three samples are prepared from the aerated concrete. The physical dimensions of the
samples and bulk densities are given in Table 1 below.
Table 1. Physical dimension of the three samples of aerated concrete.
Sample Thickness
(mm)
Height
(mm)
Width
(mm) g
Density
(kg/m
3
)
A 17.5 210 64 111.17 473
B 17.1 209 64 105.36 461
64 465 C 17.8 209 110.69

In this experiment drying (moisture transfer) is allowed only at the top and bottom surfaces of the
specimen. To satisfy this condition the other four longitudinal surfaces are wrapped with
polyethylene sheet to prevent moisture transfer, Figure 1.
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224


f
f

Wrapped
Unwrapped



Figure 1. Samples preparation

After preparing the samples a reference gamma-ray measurement, which represents the
condition of the dry sample with respect to moisture content, along the centerline of the dry and
wrapped samples are taken. The detailed procedure of this test method is discussed by Kumaran
and Bomberg [1]
To determine the initial condition of the specimens, moisture content at capillary saturation state,
the samples are unwrapped and fully soaked in water until saturation is attained. The wetted
samples are weighed again to determine the moisture content at capillary saturation. Table 2
shows the moisture content of the samples.
Table 2. Moisture gain of the samples after capillary saturation.
Samples Dry weight
(g)
Wet weight
(g)
Water gain
(g)
Moisture
concentration
(kg/m
3
)
Moisture
content
(kg/kg)
A 111.17 183.56 72.39 308.35 0.651
105.36 175.70 70.34 308.07 0.668
C 110.69 183.41 72.72 305.76
B
0.657

Based on the moisture retention curve of aerated concrete, which is shown in Figure 2 below, the
saturation level is equivalent to approximately 99.6% relative humidity.
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Moisture retention curve of Aerated Concrete
0.00
0.20
0.40
0.60
0.80
1.00
1.20
1.40
1.60
1.80
2.00
97.5 98 98.5 99 99.5 100
RH (%)
M
o
s
t
u
r
r
e

c
o
n
t
e
n
t

(
k
g
/
k
g
)
Figure 2. Moisture retention curve of aerated concrete

After knowing the total moisture gains of the samples, the length of the specimens is reduced to
125 mm for practical reasons and they are wrapped as discussed above with polyethylene sheet,
exposing only the top and bottom surfaces to the room conditions to facilitate drying. The
moisture content change with time and space is captured by doing a series of measurements
using the gamma-ray apparatus, which basically measures the average density change at a point
due to the change in the amount of water content in that particular point. The test room was at a
temperature of 21
o
C and relative humidity of 40 %. The average air velocity measured was
0.01m/s. The average moisture content of the three samples with position and time (drying
curves) is shown in Figure 3 below, at four stages of the drying process of five weeks.

Computer Simulation with the advanced hygrothermal model (hygIRC)

The drying process of wetted aerated concrete in a conditioned room is simulated using
the advanced hygrothermal model (hygIRC), which is developed in-house at IRC. Knowledge of
material properties more importantly moisture diffusivity, vapor permeability and sorption isotherm
are required to do computer simulation of this drying process using IRCs model. The physical
dimension of aerated concrete used in the simulation is the same as the experimentally
investigated specimen (given in Table 1).
The boundary conditions for the simulation are the conditioned room temperature and
relative humidity, which are 21
o
C and 40 %, respectively. The initial conditions of the specimen
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are the same as the initial conditions of the experiment and are 99.6 % relative humidity
(equivalent to 0.66 kg/kg moisture content) and temperature of 21
o
C. All surfaces except the
bottom and top surfaces are assumed to be adiabatic and closed to mass transfer across them.
The experimental and simulation results of the drying process are compared in Figure 3 below.

Aerated Concrete
0
50
100
150
200
250
300
350
400
0 0.02 0.04 0.06 0.08 0.1 0.12
Height, m
M
o
i
s
t
u
r
e

C
o
n
t
e
n
t
,

k
g

m
-
3
Day 1
Day 8
Day 23
Day 34
Day 1--Computed
Day 8--Computed
Day 23--Computed
Day 34--Computed

Figure 3. Drying curves of aerated concrete in a conditioned room; comparison of
experimental and simulation results; the hygroscopic range is assumed to be till 97 % RH
and the diffusivity is 80 % of the diffusivity values determined from a moisture uptake
process.
It has been observed that in addition to the moisture diffusivity (determined from a wetting
process) three other parameters play important roles in the simulation of the drying process.
These are the heat and mass transfer coefficients and the upper limit of the hygroscopic range
(referred to as break point in this document) above which liquid transport is active. The mass
transfer coefficient is assumed to be very small in the simulation. This is based on the fact that
the room in which the experiment is carried out is conditioned using very low velocity airflow and
also the top and bottom surfaces are relatively small to calculate meaningful heat and mass
transfer coefficients. The more important parameter which is the break point above which the
liquid transport is active is investigated by simulating the drying process using 96 %, 97 % and 98
% relative humidity as the break point and compared with the experimental results. A break point
of 97 % relative humidity and moisture diffusivity that is 80 % of the diffusivity that has been
determined from the wetting process is found to be a reasonable assumption, as shown in Figure
3.
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227


DRYING IN A HUMIDITY CHAMBER

Drying Experiment using Gravimetric Method
257


As a second exercise, the drying process of aerated concrete in a humidity chamber is
performed, and again compared with the simulation result of the IRCs advanced hygrothermal
model (hygIRC). Nine cubes of aerated concrete with approximate dimension 50 mm X 50 mm X
50 mm are prepared. Four of the six surfaces are pained with wax to block moisture transfer
to/from those surfaces from/to the humidity chamber. The specimens are soaked in water to
reach capillary saturation. The physical dimensions and the initial moisture contents of the
specimen are given in Table 3 below.
Table 3 Physical dimensions and initial moisture contents of the nine cubes of aerated concrete.
Initial Initial
Moisture Moisture
Side 1 Side 2 Side 3 Volume Weight Density Concentration content
Specimen cm g kg/kg cm cm cm
3
kg/m
3
kg/m
3
A 5.1 5.0 5.0 131.3 62.3 474 275 0.570
B 5.1 5.0 5.0 133.8 63.5 474 244 0.514
C 5.1 5.0 5.0 130.8 61.8 472 269 0.569
D 5.1 5.0 5.0 130.9 61.9 473 278 0.588
E 5.1 5.1 5.1 134.9 63.9 473 234 0.494
F 5.1 5.1 5.0 133.5 62.7 469 249 0.530
5.1 5.0 5.0 133.5 62.9 471 239
H 5.1 5.1 5.1 135.0 64.4 477 236 0.494
5.1 5.1 5.0 134.7 63.7 472 227 0.481
G 0.507
I


The samples are placed in a very well controlled humidity chamber [2] that is kept at
approximately 50 % relative humidity and 23
o
C temperature. The drying process of the nine
samples, which undergo weight changes due to moisture transfer from the samples to the
chamber, is measured gravimetrically. The weight and time of measurement are recorded
repeatedly at various time intervals, where as the condition of the chamber (relative humidity and
temperature) are recorded using a data acquisition system. The weight of the samples and the
condition of the chamber for a test period of 22 days are given in Table 6 below.

257
The authors are grateful to Mr. Xiaochuan Qiu for performing the gravimetric experiments.

B1115.13

228


Table 6. Moisture concentration of the nine specimens and conditions of the humidity
chamber during the test period.

Time Temperature RH
Moisture concentration
kg/m
3

Days
o
C % A B C D I
0.819 22.6
1.159 22.5 51.6
50.6
109.5
78.7 85.4 88.7
81.0
69.1
54.0
63.2
41.0
39.1
23.3
8.4
14.7

E F G H
0.000 22.8 51.8 275.5 244.0 268.7 278.3 233.9 248.8 238.8 235.6 227.3
51.7 188.9 168.5 198.7 201.2 178.3 175.8 179.7 182.0 161.9
168.9 154.5 175.0 178.4 157.7 160.3 162.6 162.5 146.0
1.820 22.8 51.8 143.0 134.3 148.2 150.5 131.6 137.9 138.8 135.5 125.3
2.143 22.9 133.7 126.3 138.7 141.3 122.3 129.2 129.8 125.7 117.4
2.821 22.9 50.6 118.4 112.3 122.5 125.2 106.2 114.4 114.7 103.1
3.264 22.9 50.6 110.1 104.6 113.7 116.5 97.7 106.7 106.5 100.7 95.3
3.820 22.9 50.6 101.0 96.1 104.5 107.3 88.1 97.8 97.4 90.9 86.7
4.896 22.9 50.7 86.5 82.1 89.2 92.2 73.2 83.5 83.2 75.6 73.2
5.196 23.0 50.5 83.1 69.3 79.9 79.3 71.5 69.6
5.896 23.0 50.5 75.5 71.2 77.5 61.3 72.5 72.1 63.6 62.4
6.236 22.9 50.6 72.1 68.0 73.8 77.4 57.7 68.5 59.8 59.0
6.819 22.9 50.6 66.8 62.7 68.1 71.7 51.9 63.7 63.2 53.8
7.269 22.9 50.5 59.1 64.1 68.0 48.1 59.9 59.3 50.1 49.7
7.855 22.9 50.6 58.5 54.3 59.0 62.8 43.4 55.2 54.4 44.8 45.7
9.228 22.9 50.6 48.8 44.8 48.8 53.2 33.3 45.2 45.0 35.2 36.8
9.845 22.9 50.5 45.0 41.1 44.6 49.3 29.5 41.2 31.4 33.2
10.124 22.9 50.6 43.2 39.3 42.9 47.5 27.9 39.5 39.4 29.6 31.5
10.837 22.9 50.5 35.5 38.6 43.2 23.7 35.4 35.3 26.0 27.6
11.1 21.0 21.5 13.0 15.4
14.848 22.7 50.6 20.9 18.3 19.1 24.7 17.1 17.7 10.2 12.5
15.833 22.9 50.6 17.5 15.1 15.7 21.1 6.5 13.9 8.4
16.831 22.9 50.6 14.5 12.5 12.5 18.0 5.6 11.0 11.8 7.4 7.7
17.825 22.9 50.5 12.0 10.3 9.7 15.0 5.0 9.0 9.5 7.0 6.3
21.956 23.0 50.5 6.3 6.5 5.0 8.2 4.1 5.8 5.2 6.4 5.0
13.865 22.8 50.5 24.8 21.7 28.3
9.6

Computer Simulation with the advanced hygrothermal model (hygIRC)
A series of computer simulations is done to simulate the drying process of the wetted
aerated concrete sample in the well-controlled environment (humidity chamber) using hygIRC. In
the simulations, the average initial moisture content of the nine specimens is used as an initial
condition, which is 0.53 kg/kg and the corresponding relative humidity is 98.85 %. The average
relative humidity and temperature of the humidity chamber, which are 50.7 % and 22.8
o
C
respectively, are used as boundary conditions. Based on the air velocity measurement in the
chamber adjacent to the drying surfaces (approximately 0.01 m/s) the heat and mass transfer
coefficients are determined using the empirical formula suggested in ASHRAE Handbook of
Fundamentals and Lewis relation, respectively. Again, the break point (relative humidity above
which the liquid transport is assumed to be active) has influence in the simulation results. A break
point between 97 and 98% relative humidity gives very good agreement with the experiment.
Figure 4 shows the experimental results (drying curves) of the nine samples and simulation
results of the advanced hygrothermal model using 97 and 98 % relative humidity as the break
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229




points. The moisture diffusivity used in these calculations are same as those determined from the
wetting experiments.
Aerated concrete drying curves
0
50
100
150
200
250
300
0 10 20 30
Days
M
o
s
t
u
r
e

c
o
n
t
e
n
t

(
k
g
/
m
3
)
--A--
--B--
--C--
--D--
--E--
--F--
--G--
--H--
--I--
97% RH Break point
98% RH Break point

Figure 4. Drying curves of the nine samples and comparison with the simulation
results.

CONCLUDING REMARK:
The moisture diffusivity determined from a moisture uptake process is known only within
30 to 50 %. Both series of investigations reported here suggest that the diffusivity determined
from a wetting process describes the drying process with reasonable accuracy.
References

[1] M.K. Kumaran and M. Bomberg, A Gamma-Spectrometer for Determination of
Density Distribution and Moisture Distribution in Building Materials, Proceedings of the
international symposium on moisture and humidity, Washington D.C., 1985, pp. 485-490,
1985
[2] J. C. Lackey, R. G. Marchand and M. K. Kumaran, A Logical Extension of the ASTM
Standard E 96 to Determine the Dependence of Water Vapour Transmission on Relative
Humidity, Insulation Materials: Testing and Applications: Third Volume, ASTM STP 1320, pp.
456-470, 1997.

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