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DOI 10.1007/s12517-014-1381-3
ORIGINAL PAPER
Abstract This paper reports the relationship between electrical resistivity and rock failure during uniaxial compression.
Experiments of rock samples on an electro-hydraulic servocontrolled testing machine show that the variation of electrical
resistivity is closely related to rock deformation. Near to rock
fracture, microcracks appear and change the microstructure of
rock mass, causing the rupture of mineral crystal lattice, and
the electrical resistivity has a rapid variation with the growth
of cracks. The experimental result shows that rapid variation
of electrical resistivity occurs at the critical point with stress
level of approximately 7585 % relative to the peak strength
in uniaxial compression. This research may be useful to indirectly detecting the critical point of rock fracture.
Keywords Rock failure . Electrical resistivity . Critical
information . Identification
Introduction
The behavior of rock failure may be reflected in rock stressstrain curves and other physical parameters (Chen and Lin
2004). Under an external load, rock cracking or porosity
varies with the received pressure; consequently, the evolution
of stress-strain state and other physical parameters are
affected.
Q. Sun (*) : S. Zhu
School of Resources and Geosciences, China University of Mining
and Technology, Xuzhou, Jiangsu Province 221116,
Peoples Republic of China
e-mail: sunqiang04@126.com
Q. Sun : L. Xue
Key Laboratory of Engineering Geomechanics, Institute of Geology
and Geophysics, Chinese Academy of Sciences, Beijing 100029,
Peoples Republic of China
Arab J Geosci
U MN
I
K A=L
Where, is the rock resistivity; K is a coefficient determined by device; A is the cross-sectional area of rock sample;
L is the distance between MN; UMN is the potential difference between MN; and I is current.
Arab J Geosci
No of rock
samples
Rock type
Pinot D
Pinot C
Resistivity variation
characteristics
Stress/
MPa
Strain/
%
Stress level/%
Strain level/%
1
2
3
4
5
6
7
8
Mudstone
Mudstone
Mudstone
Sandstone
Limestone
Limestone
Limestone
Limestone
13.0
11.4
13.2
35.2
67.5
79.2
25.2
62.9
4.82
2.13
2.25
4.12
1.23
1.31
0.63
0.92
81.3
84.6
80.2
85.4
84.5
86.5
85.7
78.7
73.6
65.6
90.3
73.2
91.7
88.2
77.2
76.8
Decrease-increase
Decrease-increase
Decrease-increase
Continuous decline
Stationarydecrease
Continuous decline
Stationarydecrease
Continuous decline
9
10
11
12
Limestone
Limestone
Limestone
Limestone
Average
60.8
54.4
87.3
60.7
1.32
1.42
1.55
1.27
84.6
87.0
82.3
81.3
83.5
71.1
94.2
84.6
78.2
80.4
Increase-decrease
Continuous decline
Stationarydecrease
Stationarydecrease
Arab J Geosci
Fig. 2 Schematic diagram of the
experimental system for stress,
strain, and electrical resistance of
rock under uniaxial compression
Standard
resistance R
Pressure board
Insulation board
Electrode A of power supplying
Switch K
Potential electrode M
Potential electrode N
Insulation board
Electrode B of power supplying
Pressure board
Rock smaple
100
130
Strain level
90
120
80
Axial strain /%
60
100
50
90
40
30
Resistivity /%
110
70
80
Resistivity
20
70
10
0
60
10
20
30
40
50
60
Stress level /%
70
80
90
100
(a)
100
350
325
90
Strain level
300
80
Axial strain /%
250
60
225
50
200
40
175
30
150
20
125
Resistivity
100
10
75
0
0
10
20
30
40
50
60
Stress level /%
(b)
70
80
90
100
Resistivity /%
275
70
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100
100
90
100
110
90
100
80
90
90
Resistivity
80
80
50
60
Strain level
40
50
30
Resistivity
60
70
50
60
50
40
Strain level
30
40
40
20
30
10
0
20
30
40
50
60
Stress level /%
70
80
90
20
30
10
20
10
20
10
100
10
20
30
(a) No.4
110
70
80
90
110
90
100
80
90
70
80
60
70
100
Strain level
60
80
50
70
40
60
Axial strain /%
70
Resistivity /%
90
60
Resistivity
50
50
40
40
30
30
50
Resistivity
20
0
10
20
30
40
50
60
Stress level /%
Strain level
20
10
0
100
100
90
Axial strain /%
40
50
60
Stress level /%
(b) No.6
100
80
Resistivity /%
60
Axial strain /%
70
70
Resistivity /%
Axial strain /%
70
70
80
90
40
10
30
100
Resistivity /%
80
30
20
10
10
(c) No.8
20
30
40
50
60
Stress level /%
70
80
90
100
(d) No.10
Fig. 4 Relationship between strain, stress, and resistivity of rock a No. 4 (sandstone), b No. 6 (limestone), c No. 8 (limestone), d No. 10 (limestone)
onset of fracture coalescence starts at stress levels of approximately 7585 % of the peak strength. For rock samples with
high moisture content near the narrow fracture zone and
conductivity of water within the fissures, the electrical resistivity sharply decrease; in the absence of water, the resistivity
sharply increases. Therefore, the steep change of resistivity at
the yield point in this phase is closely related to the development of fractures and volumetric dilatation.
The resistivity sharply changes near the yield point (steep
down or steep up), and the resistivity-stress curve falls into
four types before the failure. The stress and strain corresponding to the yield point C are represented as (c,c) respectively,
and the peak stress and strain at the point D are taken as
reference values, then we have
c
c
c
100% ; c 100%
d
d
Case studies
Case 1: uniaxial compression test of different samples
Rock samples (the rock type is shown in Table 2) were cut into
50100 mm cylinders. Two symmetrically located 958
1 mm strip-shaped electrodes were made by putting gelatin
mixed with copper powder along the axial direction on the
surface of each sample. Rock samples were uniaxially loaded
at rock samples that were uniaxially loaded at electrohydraulic servo-controlled testing machine (MTS815). The
electrical resistivity was measured with a digital electrical
instrument (SYSCAL-R2) (Liu et al. 2009a, b).
Arab J Geosci
100
150
90
145
140
80
135
70
120
115
40
Resistivity
30
110
105
20
100
10
95
0
0
10
20
30
40
50
60
Stress level /%
70
80
90
100
(a) No.5
100
440
90
400
80
360
320
60
Strain level
280
50
240
40
Resistivity /%
Axial strain /%
70
200
30
Resistivity
20
160
10
120
0
0
10
20
30
40
50
60
Stress level /%
70
80
90
100
(b) No.12
The test result is shown in Figs. 9, 10, 11, 12, 13, and 14.
Based on the level of resistivity change vs. stress level (the
100
112
90
110
80
108
70
Axial strain /%
106
60
Resistivity
104
50
40
102
30
100
Strain level
20
98
10
96
0
0
10
20
30
40
50
60
Stress level /%
70
80
90
100
Resistivity /%
Axial strain /%
125
50
Resistivity /%
130
Strain level
60
stress level is normalized relative to their peak value respectively, and the resistivity changing level refers to the value of
resistivity normalized by the initial resistivity) obtained from
experiments on rock samples, the variation of resistivity with
stress level can be divided into four types according to the
mode of variation of electrical resistivity with stress level: (1)
decrease-increase, (2) continuous decline, (3) approximate
stationarydecrease, and (4) increase-decrease (as shown by
Table 2), consistent with (Li et al. 1999).
Three phases can be identified in the stress-strain curve
with different characteristics of electrical resistivity variation
during the compression process of rock specimens before the
peak strength is reached, as shown in Fig. 7. (1) The compaction and elastic phase O-A (shown in Fig. 7). (2) The elasticstable cracking phase (AC). (3) The yielding phase CD. Near
Point C, plenty of micro cracks initiate and grow rapidly, and
micro breaking is developed spatially in rows along the potential breaking planes until the micro cracks eventually become connected with each other, as indicated by the localization of strain, and accelerated increase of volumetric strain at
the cracks. In this phase, the resistivity sharply changes near
the yield point (steep down or steep up).
From Table 2, we can get the average value of stress level
for point C of 75.1 %. It also suggests that the variation of rock
resistivity can reflect the changes of stress state, which may
provide very useful information on rock stability.
Axial stress
Fig. 7 Stress-strain-resistivity
diagram showing the stages of
crack development
Peak
Resistivity
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Resistivity
(wet)
yield point
C
Stress
Crack closure
Resistivity
(dry)
Lateral strain %
Dilation Volumetric Contraction
strain
Axial strain %
Crack
closure
Elastic
region
Yield
region
Total measured
volumetric strain
Calculated crack
volumetric strain
Crack
closure
Crack
growth
(a)
(b)
(c)
(d)
Arab J Geosci
Table 2 Summary of yield stress
level from laboratory test by
electrical resistivity
No of rock samples
Rock type
1
2
3
4
5
Mudstone
Sandstone
Sandstone
Sanding mudstone
Limestone
69.8
80.2
74.8
72.5
71.6
Stationarydecrease
Decrease-increase
Increase-decrease
Continuous decline
Increase-decrease
6
7
8
9
Average
Limestone
Limestone
Coal petrography
Quartz sandstone
75.4
72.9
79.8
78.9
75.1
Increase-decrease
Increase-decrease
Decrease-increase
Continuous decline
as shown in Figs. 18, 19, and 20. (1) The compaction and
elastic phase. The resistivity was increasing with the increase
of stress level. (2) The elastic-stable cracking phase. The
resistivity changes slightly with the increase of stress level.
(3) The yielding phase. In this phase, the resistivity sharply
decreased with the increase of stress level.
When the ratio between the loading stress and peak stress is
70~85 %, the resistivity varies sharply with a jump in the
vicinity of the yield point, indicating accelerated variation and
accelerated decrease of the resistivity.
Theoretical analysis
100
90
100
100
180
90
90
160
80
40
80
30
60
20
Axial strain /%
100
Resistivity /%
Axial strain /%
Point C
Resistivity
50
Resistivity
70
140
120
80
Point C
70
Strain level
Where, =Vp/V is the rock void ratio (Vp is the rock pore
volume, V is the rock total volume), S=Vw/Vp is the rock
saturation (Vw is the volume of water).
80
60
S
m
n
mln nlnS ;
70
60
60
50
50
Strain level
40
40
30
30
20
20
10
10
Resistivity /%
(1) The compaction and elastic phase O-A (shown in Fig. 7).
40
10
0
0
10
20
30
40
50
60
Stress level /%
70
80
90
20
100
10
20
30
40
50
60
Stress level /%
70
80
90
0
100
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100
800
90
100
700
80
50
400
40
300
30
20
Strain level
Resistivity /%
500
60
Resistivity /%
Axial strain /%
90
600
Resistivity
70
100
0
10
20
30
40
50
60
Stress level /%
70
Point C
70
200
Point C
10
0
80
80
90
60
0
100
50
0
nm V V w
V w
a
n
an
V
Vw
Vw
10
20
30
40
50
60
Stress level /%
70
80
90
100
nm V V w
nm V
a
n
;
a
V
Vw
nm V V w
V W
a
n
mln a n
mln
V
Vw
VW
7
where, <1, m<0, Vw >0. The resistivity decreased sharply with a jump in the vicinity of the yield point. In the testing
process, the change of S is very small, so, the nlnS can be
ignored, which does not affect the results of above analysis.
100
118
116
95
114
112
Resistivity /%
Resistivity /%
90
85
80
Point C
110
108
106
Point C
104
75
102
100
70
0
10
20
30
40
50
60
Stress level /%
70
80
90
100
10
20
30
40
50
60
Stress level /%
70
80
90
100
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Press
machine
100
98
96
Monitoring sensor
Rock smaple
Resistivity /%
94
92
Press
machine
90
88
Constant
current
source
86
Point C
84
Galvanometer
82
Elctrical
instrument
Oscillograph
of 16 ray
Acoustic
detector
80
0
10
20
30
40
50
60
Stress level /%
70
80
90
100
strain
indicator
Conclusions
To assess crack initiation and crack damage stress levels in
rock mass, the characteristics of resistivity variation during the
100
130
Point C
95
R1
R2
R3
125
90
Resistivity /%
Resistivity /%
120
85
80
75
70
115
110
105
65
100
60
0
10
20
30
40
50
60
70
80
90
100
Stress level /%
10
20
30
40
50
60
Stress level /%
70
80
90
100
Arab J Geosci
128
124
R1
R2
R3
Resistivity /%
120
116
112
108
104
100
0
10
20
30
40
50
60
Stress level /%
70
80
90
100
140
120
Resistivity /%
100
80
60
R1
R2
R3
R4
40
20
0
10
20
30
40
50
60
Stress level /%
70
80
90
100
Fig. 20 Relationship between resistivity and stress level (An et al. 1996)
References
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changes under uniaxial pressure and water replenishment (in
Chinese). Earthquake Res China 12(3):300306
Arab J Geosci
Wang JX (2012) Theoretical and experimental research on resistivity
properties of rock under loading (in Chinese). Chongqing: Master.
Thesis, Chongqing University
Wang YH, Liu YF, Ma HT (2012) Changing regularity of rock damage
variable and resistivity under loading condition. Safety Sci 50:718
7227
Wong TF (1982) Micromechanics of faulting in Westerly granite. Int J
Rock Mech Min Sci Geomech Abstr 19:4964
Xiu JG, Chen DY (1987) Test of the saturation effect on rock apparent
resistivity under uniaxial pressure (in Chinese). Earthquake 7(2):38
45