Rheometric Scientific SR5 Manual

In s tru m e n t
M a n u a l
9 0 2 -3 0 0 1 4
R e v is io n X 1
2 4 O c to b e r 1 9 9 7
This document is to be used solely by owners of the

Rheometric Scientific SR5. Reproduction is prohibited
without permission of Rheometric Scientific, Inc. The
products described herein are under continuous
development. Consequently, product operation may vary
from that described. All information is subject to change
without notice.
Rheometric Scientific, Inc.

One Possumtown Road
Piscataway, NJ 08854, USA
Voice: 732-560-8550
Fax: 732-560-7451
Service: 732-560-8990
http://www.rheosci.com
SR5 INSTRUMENT MANUAL Revision X1 24 October 1997
GENERAL INFORMATION
NOTICES
Disclaimer Rheometric Scientific, Inc. has taken due care in the preparation of this
document. Insofar as specific mention is made of particular product features,

Rheometric Scientific believes the information to be true and representative of
the stated product at the time this document was published. No warranty is
made regarding the veracity of such material. In no event will Rheometric
Scientific be liable for damages of any kind, incidental or consequential, in regard
to or arising out of the performance, form, or application of the material contained
in this document. No representation is made regarding the suitability of this
product information for any particular purpose. Rheometric Scientific reserves
the right to revise this document and to make changes in its content without
obligation to notify any person of such revision or change.
Instrument Although this document is intended to describe the initial production version of
Development the SR5, all information is based upon a prototype evaluation instrument.
All products described herein are currently under continuous development.

Therefore, product operation may vary from that described in this document.
Document This document, and RSI Orchestrator Online Help, are the only Rheometric
Propriety Scientific authorized publications concerning operation and calibration of this
instrument.
Copyright 1997, Rheometric Scientific, Inc.
TERMS AND SYMBOLS USED IN THIS MANUAL

Term or Symbol
Meaning
DANGER
An immediately hazardous situation that, if not avoided, will result in either

personal injury or death.
WARNING
A potentially hazardous situation that, if not avoided, will result in either

personal injury or death.
CAUTION
A situation that, if not avoided, will result in damage to either this instrument or
other inanimate property.
NOTE
Information that is emphasized by being placed prior to the procedural step to

which it pertains.
General identification symbol for safety notices. Also defines information
pertaining to the portion of the instrument to which the symbol is affixed.
SAFETY
Service Do not attempt to service this instrument, as it contains no user-serviceable
components.
Electrical Do not make physical contact with any component inside the instrument unless a
Hazards set of procedural steps specifically instructs you to do so. In such cases, follow
the procedure step-by-step.
Required While operating this instrument, you must wear eye protection that either meets
Equipment or exceeds ANSI Z87.1 standards. Additionally, wear protective clothing that has
been approved for protection against the materials under test and the test
temperatures.
Safety Notices The following safety notices that appear throughout this document are repeated
here for emphasis.
Page 8
CAUTION
POSSIBLE DAMAGE TO INSTRUMENT
The membrane air dryer must be connected between your house air and the Test
Station. Failure to do so will result in extensive damage to this instrument.
Page 10
CAUTION
The Stress Head uses a precision air bearing that must be

operated with instrument-quality air at a pressure of 60 psi
(4.1 bar).
The Anvil (left) is an integral part of the bearing. Movement of
the Anvil when no air is applied will score the air bearing,
causing extensive damage to the instrument.
If the air supply is accidentally interrupted, do not touch the
Anvil, or otherwise allow it to move, until air is restored.
ANVIL
The instrument is shipped with a bearing lock that prevents

movement of the Anvil. If the air supply must be intentionally
interrupted, as when transporting the instrument, install the
bearing lock prior to removing air.
Page 10
CAUTION
Read the operating and maintenance instructions that were supplied with your air dryer.
Failure to properly maintain the dryer, moisture-trap, and coalescing filters will result in
extensive damage to this instrument.
Pages 15 and 32
DANGER
POSSIBLE PERSONAL INJURY
Turn OFF the Circulator prior to removing or installing any Lower Fixture. The Fluid
Bath is an open vat of fluid that is sealed only when a Lower Fixture is installed. Failure
to turn OFF the Circulator prior to fixture removal and installation will cause the Fluid
Bath to overflow, resulting in possible injury and extensive damage to this instrument.
Page 32
WARNING
TOXICITY
In Table 5-1 below, SF 96-50 silicon fluid emits toxic fumes when heated to a
temperature greater than +140C. Use SF 96-50 silicon fluid above +140C only if an
externally-vented exhaust hood is installed above the circulator. Ensure that exhaust
airflow is adequate to expel fumes emitted from the circulator. Failure to heed this
warning may result in injury or death.
Page 37
DANGER
Turn OFF the Circulator prior to removing or installing the Peltier Fixture. The Fluid
Bath is an open vat of fluid that is sealed only when the Peltier Fixture is installed.
Failure to turn OFF the Circulator prior to fixture removal and installation will cause the
Fluid Bath to overflow, resulting in possible injury and extensive damage to this
instrument.
CONTENTS
1 INTRODUCTION ....................................................................................................................................... 7
1-1 OVERVIEW...................................................................................................................................... 7
1-1.1 Organization ........................................................................................................................... 7
1-1.2 Related Sources of Information .............................................................................................. 7
1-2 DESCRIPTION OF INSTRUMENT .................................................................................................. 7
1-2.1 General Principle .................................................................................................................... 7
1-3 SPECIFICATIONS ........................................................................................................................... 8
1-3.1 Base System .......................................................................................................................... 8
1-3.2 Environmental Control Systems ............................................................................................. 8
1-4 REQUIREMENTS ............................................................................................................................ 8
1-4.1 Pneumatic .............................................................................................................................. 8
2 COMPONENT OPERATION ..................................................................................................................... 9
2-1 MODULES ....................................................................................................................................... 9
2-2 REQUIRED READING: PREVENTING DAMAGE TO THE INSTRUMENT .................................. 10
2-2.1 Air Bearing ............................................................................................................................ 10
2-2.2 Air Dryer ............................................................................................................................... 10
2-3 TEST STATION COMPONENTS .................................................................................................. 11
2-3.1 Stage .................................................................................................................................... 12
2-3.2 User Interface ....................................................................................................................... 12
2-3.3 Anvil Components ................................................................................................................ 12
2-4 ENVIRONMENTAL CONTROLLER .............................................................................................. 13
2-4.1 Overview .............................................................................................................................. 13
2-4.2 Status Panel ......................................................................................................................... 13
3 FROM FIXTURE INSTALLATION TO SAMPLE LOADING ................................................................... 14
3-1 OVERVIEW.................................................................................................................................... 14
3-2 FIXTURE INSTALLATION AND REMOVAL .................................................................................. 15
3-2.1 Lower Fixture ........................................................................................................................ 15
3-2.2 Upper Fixture ........................................................................................................................ 17
3-3 ZEROING NORMAL FORCE......................................................................................................... 17
3-4 AUTOCAL ...................................................................................................................................... 18
3-4.1 Overview .............................................................................................................................. 18
3-4.2 Procedure ............................................................................................................................. 18
3-5 TRACK MODE ............................................................................................................................... 19
3-5.1 Overview .............................................................................................................................. 19
3-5.2 Procedure ............................................................................................................................. 19
3-6 ZEROING AND SETTING THE GAP............................................................................................. 19
3-6.1 Overview .............................................................................................................................. 19
3-6.2 Zeroing the Gap ................................................................................................................... 19
3-6.3 Setting the Gap .................................................................................................................... 20
3-7 SAMPLE LOADING GUIDELINES ................................................................................................ 20
3-7.1 Parallel Plate ........................................................................................................................ 20
3-7.1.1 Gap Setting ................................................................................................................. 20

3-7.1.2 Loading ....................................................................................................................... 20
3-7.2 Cone and Plate ..................................................................................................................... 21
3-7.2.1 Gap Setting ................................................................................................................. 21
3-7.2.2 Test Temperatures...................................................................................................... 21
3-7.2.3 Loading ....................................................................................................................... 21
3-7.3 Couette ................................................................................................................................. 22
4 CALIBRATION ........................................................................................................................................ 23
4-1 OVERVIEW.................................................................................................................................... 23
4-1.1 Operations ............................................................................................................................ 23
4-1.2 Calibration Kit ....................................................................................................................... 24
4-2 TORQUE CALIBRATION............................................................................................................... 25
4-2.1 Overview .............................................................................................................................. 25
4-2.2 Procedure ............................................................................................................................. 25
4-3 SPIN CORRECTION ..................................................................................................................... 28
4-3.1 Overview .............................................................................................................................. 28
4-3.2 Procedure ............................................................................................................................. 28
4-4 EXAMINATION OF CAL CURVE................................................................................................... 29
4-4.1 Overview .............................................................................................................................. 29
4-4.2 Procedure ............................................................................................................................. 29
4-5 NORMAL FORCE CALIBRATION ................................................................................................. 30
4-5.1 Overview .............................................................................................................................. 30
4-5.2 Procedure ............................................................................................................................. 30
5 APPENDICES ......................................................................................................................................... 31
5-1 OVERVIEW.................................................................................................................................... 31
5-1.1 Purpose ................................................................................................................................ 31
5-1.2 Content ................................................................................................................................. 31
5-2 FLUID BATH ENVIRONMENTAL CONTROL SYSTEM................................................................ 32
5-2.1 Principle ................................................................................................................................ 32
5-2.2 Circulator Connection ........................................................................................................... 32
5-2.3 Filling the Circulator .............................................................................................................. 32
5-2.4 RSI Orchestrator Fluid Bath Configuration ........................................................................... 34
5-3 PELTIER ENVIRONMENTAL CONTROL SYSTEM...................................................................... 35
5-3.1 Principle ................................................................................................................................ 35
5-3.2 Tentative Specifications ....................................................................................................... 36
5-3.3 Selecting a Thermal Operating Range ................................................................................. 36
5-3.4 Installation ............................................................................................................................ 37
5-3.5 Circulator Options ................................................................................................................. 39
5-3.6 RSI Orchestrator Peltier Configuration ................................................................................. 39
5-4 HUMIDITY COVER ........................................................................................................................ 39
5-4.1 Principle ................................................................................................................................ 40
5-4.2 Usage ................................................................................................................................... 40
1
INTRODUCTION
1-1 OVERVIEW
1-1.1 This manual describes instrument-specific features of the Rheometric Scientific
Organization Universal Stress Rheometer SR5. The following information is contained herein:
Chapter 1 Introduction
Provides an overview of your documentation and the instrument, and lists
instrument performance specifications.
Chapter 2 Component Operation
Identifies and describes components of the base instrument.
Chapter 3 From Fixture Installation to Sample Loading
Details, in sequence, procedures that you must perform prior to conducting a
test.
Chapter 4 Calibration
Contains instrument calibration procedures.
Chapter 5 Appendices
Add-on sections that describe Environmental Control Systems and various
options as they become available.
1-1.2
Related Sources
of Information
This instrument is operated using Rheometric Scientific RSI Orchestrator

software for Microsoft Windows 95 and NT. The dynamic nature of RSI
Orchestrator has necessitated that, wherever possible, all technical information
concerning the software be segregated from hard copy and supplied in the form
of Windows Online Help. Please refer to the following sources concerning RSI
Orchestrator:
RSI Orchestrator Startup Guide 902-30010 Current Revision
Installation instructions, general procedures, and a brief tour of the software.
RSI Orchestrator Online Help Current Revision
Online WinHelp guide to software reference and operational information.
1-2 DESCRIPTION OF INSTRUMENT

1-2.1
General
Principle
The SR5 is a controlled-stress rheometer, i.e., the instrument deforms a sample

by applying the controlled stress that you specify. The resultant angular
deflection (strain) required to apply the stress is then measured. All material
properties are then calculated by analysis of the applied stress and resulting
strain.
Controlled stress is applied to the sample by the Stress Head. This is essentially
a drag cup motor mounted on a precision air bearing. Position sensors mounted
on the motor provide angular deflection (strain) information for any applied
stress.
Selected tests also allow you to choose a strain (desired angular deflection) to
which the sample is subjected, thereby allowing test conditions to be specified as
they would using a controlled-strain rheometer.
1-3 SPECIFICATIONS
1-3.1
Torque Range
Base System
0.01 to 500 gcm (0.001 to 50 mNm)
Rotation Rate
0 to 100 radians per second
Dynamic Frequency Range
0.00005 to 500 radians per second
Angular Resolution
When the instrument is in Track Mode, an

angular displacement of better than 1
microradian can be resolved around the starting
position (see paragraph 3-5 TRACK MODE on
page 19).
Normal Force Range
5 to 2000 grams
1-3.2
Environmental Fluid Bath
Control Systems
See paragraph 5-2.3 Filling the Circulator on

page 32
Peltier
See paragraph 5-3.2 Tentative Specifications on

page 36
Electrically Heated Plates
Ambient to +350C (preliminary specification)
Furnace
-150C to +500C (preliminary specification)
1-4 REQUIREMENTS
1-4.1 Air Pressure Into the
Pneumatic Instrument
60 psi (4.1 bar)
Air Flow Into the Instrument
2.5 scfm
Air Quality Into the

Membrane Dryer
Instrument-quality air with a dew point of -40C,

and containing particles no larger than 5 microns
in diameter.
CAUTION
The membrane air dryer must be connected between your house air and the Test
Station. Failure to do so will result in extensive damage to this instrument.
2
COMPONENT OPERATION
2-1 MODULES
Throughout this manual, references are made to the following instrument modules:
Test Station
The Test Station (Figure 2-1) is the single chassis comprising the SR5 Base
System. It houses the Stress Head, Fluid Bath, and all support electronics.
TEST
STATION
ENVIRONMENTAL
CONTROLLER
Figure 2-1 Test Station and Environmental Controller
Environmental Controller
The Environmental Controller (Figure 2-1) contains all support electronics
necessary to operate optional environmental control systems. Although not
needed to operate the Fluid Bath, the Environmental Controller is supplied with
options such as Peltier.
Personal Computer (PC)
The Personal Computer (IBM -compatible PC) operates RSI Orchestrator
software. Please refer to the manufacturers literature for hardware-specific
details concerning your PC. For minimum PC requirements, refer to the
current revision of the RSI Orchestrator Startup Guide 902-30010.
2-2 REQUIRED READING: PREVENTING DAMAGE TO THE INSTRUMENT

2-2.1 The Stress Head contains a precision air bearing, which is essentially a journal
Air Bearing that rotates within a race. A column of air less than 0.001 inch separates the
two, providing almost friction-free rotation during testing. If air flow to this
instrument is interrupted, rotating the Stress Head will result in incredibly
expensive damage to this instrument. Note the following caution.
CAUTION
The Stress Head uses a precision air bearing that must be

operated with instrument-quality air at a pressure of 60 psi
(4.1 bar).
The Anvil (left) is an integral part of the bearing. Movement of
the Anvil when no air is applied will score the air bearing,
causing extensive damage to the instrument.
If the air supply is accidentally interrupted, do not touch the
Anvil, or otherwise allow it to move, until air is restored.
ANVIL
The instrument is shipped with a bearing lock that prevents

movement of the Anvil. If the air supply must be intentionally
interrupted, as when transporting the instrument, install the
bearing lock prior to removing air.
2-2.2 This instrument is supplied with a membrane-type air dryer that blocks moisture
Air Dryer by passing air through a filter that blocks water molecules.
Moist air is continuously purged from the dryer through a series of purge holes.
The amount of purge can be adjusted by rotating the purge knob on the dryer.
Settings range from zero (no purge and, hence, no drying) to 3 (high purge and
maximum drying). We recommend a setting of 2. Do not set the purge below 2,
as this will not sufficiently dry the air into the instrument.
Depending upon the membrane dryer you receive, the dryer may require periodic
maintenance. Preceding and in line with the air dryer are a moisture-trap filter
and a coalescing filter. It is vital that you maintain both the moisture-trap and
coalescing filters in accordance with the instructions provided with the filters. In
general, maintenance of these filters usually involves no more than draining them
at the intervals specified by the manufacturer. Note the following caution.
CAUTION
Read the operating and maintenance instructions that were supplied with your air dryer.
Failure to properly maintain the dryer, moisture-trap, and coalescing filters will result in
extensive damage to this instrument.
10
2-3 TEST STATION COMPONENTS

Refer to Figure 2-2 during the following discussion of Test Station Components.
USER INTERFACE
STAGE
ANVIL STOP
ANVIL
ANVIL STOP CONTROL
Figure 2-2 Test Station Components
11
2-3.1 The stage is a motorized platform that supports the Stress Head. The stage can
Stage be manually raised and lowered using the Stage Control on the User Interface
(next topic), or automatically adjusted to a specific height using RSI Orchestrator

(see paragraph 3-6 ZEROING AND SETTING THE GAP on page 19).
To raise the Stage to maximum height:
Perform the following steps using RSI Orchestrator:
a. Click either the Gap Control Panel function (Control menu), or the Gap
Control button
. The Gap Control dialog box is displayed.
b. Click Send To Top.
2-3.2 The User Interface is a control panel that allows control and display of selected
User Interface Test Station functions, as described in Figure 2-3.
Stage Control
Press
To move Stage
Up slowly
Up quickly
Down slowly
Down quickly
Power
Illuminated when power is
applied to the instrument
Figure 2-3 User Interface
Environmental Off
Press to unconditionally remove power from the Environmental Control
System.
Display
Temperature currently being measured by the Environmental Control
System
Gap between Upper and Lower Fixtures, relative to a zero reference
established when you zero the Gap (see paragraph 3-6 ZEROING AND
SETTING THE GAP on page 19)
2-3.3
Anvil
Components
Upper Test Fixtures mount onto the Anvil. As mentioned in paragraph 2-2.1 Air
Bearing (page 10), the Anvil is an extension of the air bearing that rotates during
testing. The Anvil Stop, essentially a pneumatic piston, steadies the Anvil
during Upper Fixture installation and sample loading. To hold the Anvil in its
current position, turn the Anvil Stop Control to the Lock position. To allow the
Anvil to rotate freely, turn the Anvil Stop Control to the Unlock position.
Fixture installation procedures are given in paragraph 3-2 FIXTURE
INSTALLATION AND REMOVAL on page 15.
12
2-4 ENVIRONMENTAL CONTROLLER

2-4.1 Used with Environmental Control options other than the Fluid Bath, the
Overview Environmental Controller contains all electronics necessary to operate and
monitor Environmental Control systems such as Peltier and Heated Plates.
2-4.2 Although all Environmental Control functions are initiated using RSI Orchestrator,
Status Panel the Environmental Controller provides the following monitoring on the
Environmental Control Status Panel (Figure 2-4).
Each LED is illuminated when...

...the Peltier environmental control system is
decreasing temperature
increasing temperature
...power is applied to the Lower Heated Plate
...power is applied to the Upper Heated Plate
...nitrogen purge is enabled
...the Heated Plates environmental control
system is enabled
...all SR5 environmental control system
electronics are ready for use
...the Test Station electronics can
communicate with the Environmental
Controller
enabled
Figure 2-4 Environmental Control Status Panel
13
3
FROM FIXTURE INSTALLATION
TO SAMPLE LOADING
3-1 OVERVIEW
This chapter contains procedures that must be performed prior to executing a test using RSI Orchestrator
software. Perform these procedures in the sequence presented, as outlined below:
Fixture Installation and Removal
Instructions are provided to install and remove Upper and Lower Fixtures used
in conjunction with the base (standard) instrument.
Zeroing Normal Force
A method is given to establish a zero reference normal force.
AutoCal
General information concerning AutoCal (Automatic Fixture Inertia Calculation)
is provided with instructions for implementation.
Track Mode
A procedure is given to use Track Mode, which allows the instrument to
provide optimum angular resolution.
Zeroing and Setting the Gap
Separate procedures are given for manually adjusting the gap, or allowing RSI
Orchestrator to adjust the gap for you.
Sample Loading Guidelines
Guidelines to use while loading samples are provided for each geometry.
Geometry constants and formulas used for data calculation are included in RSI
Orchestrator Online Help (see the Reference Guide in the Online Help Table
of Contents).
14
3-2 FIXTURE INSTALLATION AND REMOVAL

3-2.1 The following procedure describes Lower Fixture installation when tests are
Lower Fixture conducted using the Fluid Bath, which is supplied with all instruments. For
procedures covering Environmental Control options, please see the relevant

Appendix.
DANGER
Refer to Figure 3-1 during the following procedures.
Installation
a. Raise the stage to maximum height (see paragraph 2-3.1 Stage on page 12).
b. Push the Lower Fixture fully into the base, aligning the four captive screws
with the holes in the base.
c. Tighten the four captive screws in the Lower Fixture (do not over-torque).
Removal
b. Loosen the four captive screws in the Lower Fixture.
c. Pull the Lower Fixture from the base.
15
VIEW LOOKING DOWNWARD FROM

THE TOP OF THE INSTRUMENT
NOTE
Early production units are
equipped with eight mounting
holes.
If your unit is so
equipped, align the captive
screws on the Lower Fixture
with the holes shown (at left)
filled in black.
FRONT OF INSTRUMENT
CAPTIVE SCREWS
LOWER FIXTURE
Figure 3-1 Lower Fixture Installation onto Fluid Bath
16
3-2.2 The following procedure describes Upper Fixture installation for all Environmental
Upper Fixture Control options.
Refer to Figure 3-2 during the following procedure.
Installation
a. Raise the stage to maximum height
(see paragraph 2-3.1 Stage on page
12).
b. Hold the Anvil in its current position by
turning the Anvil Stop Control to the
Lock position (see paragraph 2-3.3
Anvil Components on page 12).
c. Align the tapped hole in the fixture with
the threaded rod in the anvil.
d. Fasten the fixture to the anvil by rotating
the threaded rod until it draws the
fixture fully upward into the anvil (hand
tighten only).
e. If you are about to load a sample, keep
the Anvil Stop Control locked;
otherwise, turn it to the Unlock position.
THREADED ROD
ANVIL
FIXTURE
Figure 3-2 Upper Fixture

Removal
Installation
a. Raise the stage to maximum height
(see paragraph 2-3.1 Stage on page 12).
b. Hold the Anvil in its current position by turning the Anvil Stop Control to the
Lock position (see paragraph 2-3.3 Anvil Components on page 12).
c. While holding the fixture, rotate the threaded rod until it disengages the
fixture.
3-3 ZEROING NORMAL FORCE

Normal (Axial) Force sensed by the instrument must next be set to zero. Do this
clicking the Zero Normal Force function in the Control menu of RSI
Orchestrator software.
17
3-4 AUTOCAL
3-4.1 AutoCal (Automatic Fixture Inertia Calculation) is a function that measures the
Overview mass of an Upper Fixture, and adds this mass to the mass of the air bearing and
its associated components. The inertia of the total mass is then calculated for
use in compensating for inertia during testing. The inertia value is stored with the
geometry information and can be used in all subsequent experiments using that
Upper Fixture.
During Dynamic testing, accurate angular displacement of the Upper Fixture can
be achieved only if the fixtures inertia is overcome at each peak deflection point.
Inertia compensation therefore becomes more important as the Dynamic test
frequency (and consequently inertia) increases.
AutoCal must be performed prior to the first time an Upper Fixture is used to run
tests. Subsequent use of the same fixture does not require AutoCal.
3-4.2 Perform the following procedure to AutoCal:

Procedure
a. Install an Upper Fixture (see paragraph 3-2.2 Upper Fixture on page 17).
b. Release the Anvil by turning the Anvil Stop Control to the Unlock position
(see paragraph 2-3.3 Anvil Components on page 12). The Anvil must be free
to rotate.
b. Select the Start Test function. The Edit/Start Test dialog box is displayed.
c. From the displayed list, select the geometry that corresponds to the Upper
Fixture in use. Click Edit Geometry. The form for the selected geometry type
is displayed.
d. Click Options. The AutoCal dialog box (Figure 3-3) is displayed.
Figure 3-3 AutoCal Dialog Box

e. Ensure that the Upper Fixture meets the following conditions:
1. It is clear of obstructions and free to rotate.
2. It is either not rotating (ideal condition), or rotating at a rate of less than 1/4
revolution per second.
f. Click AutoCal, then wait until the inertia value is displayed (Figure 3-3).
g. Save the inertia value by clicking Ok. The form for the selected geometry is
again displayed.
h. Return to the Edit/Start Test dialog box by clicking Ok.
18
3-5 TRACK MODE

3-5.1 Activating the RSI Orchestrator Track Mode function synchronizes the
Overview instruments position control sensors. When the instrument is in Track Mode, an
angular displacement of better than 1 microradian can be resolved around the
starting position.
When the instrument is not in Track Mode, the angular resolution depends upon
the absolute position of the stress head.
You must activate Track Mode under the following conditions:
Immediately after applying power to the instrument (the instrument discards
Track Mode information after power has been removed)
If your test requires resolving an angular displacement of less than 1
microradian
Unless you must begin a test at a certain angular position, we recommend that
you activate Track Mode prior to making contact between the Upper Fixture and
the sample.
3-5.2 Prior to making contact between the Upper Fixture and the sample, activate
Procedure Track Mode by clicking the Track Mode function (Control menu) of RSI
Orchestrator. The Anvil subsequently rotates to a fixed position that it maintains

until a test begins.
3-6 ZEROING AND SETTING THE GAP

3-6.1 You must zero and set the Gap between Upper and Lower fixtures when using
Overview Parallel Plate or Cone and Plate fixtures.
The RSI Orchestrator Gap Control Panel function provides a single dialog box
that allows you to both zero and set the Gap.
3-6.2 If conducting tests at other than ambient temperature, ensure that the fixtures are
Zeroing the Gap at the starting or working temperature prior to proceeding.
a. Ensure that a sample is not loaded and the upper and lower fixtures are
clean.
b. Using the Stage Control on the User Interface (see paragraph 2-3.2 User
Interface on page 12), lower the stage to achieve a Gap of about 0.5 mm (as
judged visually).
c. Click either the Gap Control Panel function (Control menu), or the Gap
Control button
. The Gap Control dialog box is displayed.
d. Click Zero Fixture. An information form is displayed showing the duration
(Elapsed Time) of the zeroing operation. The present gap is displayed in the
Current Gap field, which updates at one second intervals. The following
events occur during the zeroing operation:
1. The stage lowers to achieve contact between fixtures.
2. Following contact, Current Gap is zeroed, and the information form is no
longer displayed.
e. In preparation for loading the sample, raise the Stage to maximum height by
clicking Send to Top.
f. Remain in the Gap Control Panel and proceed to the next paragraph Setting
the Gap.
19
3-6.3 After zeroing the Gap, set it as follows:

Setting the Gap
a. Place the sample onto the lower fixture (see paragraph 3-7
SAMPLE
LOADING GUIDELINES on page 20).
b. Enter the following information:
1. Commanded Gap Position
Enter the desired Gap in millimeters.
2. Max Allowed Force
Enter the maximum Normal Force (in grams-force) that will be generated
while the sample is being compressed during the gap setting operation.
When Normal Force exceeds this value, the stage stops descending until
Normal Force relaxes and drops below this value. Stage movement then
resumes.
c. Click Set Gap. An information form appears, indicating the time elapsed
since the button was clicked. The Stage should descend relatively quickly
(typically 5 mm/sec) until the Upper Fixture is 3 mm from the Commanded
Gap Position, at which time it will slow its rate of descent until the Gap is
achieved. The gap is set when the information form is no longer displayed.
3-7 SAMPLE LOADING GUIDELINES

3-7.1 Prior to loading the sample, ensure that all previous procedures in this chapter
Parallel Plate have been performed (if applicable, as indicated within each procedure).
3-7.1.1
Gap Setting
The recommended Gap setting between Parallel Plates is between 0.5 and 2
millimeters.
3-7.1.2
Loading
Perform the following procedure to load samples using the Parallel Plate fixtures.
In general, Figure 3-4 shows properly loaded Calibration Samples, included in
the Calibration Kit (see paragraph 4-1.2 Calibration Kit on page 24), which are
representative of most samples. At the left is the PDMS Calibration Sample, at
the right is the 100 cP Calibration Sample. Note that samples such as PDMS
should bulge somewhat from the edges of the plates, while the 100 cP fluid
should taper downward from the bottom edge of the Upper Fixture.
UPPER FIXTURE
SAMPLE
LOWER FIXTURE
Figure 3-4 Parallel Plates with Sample Loaded

a. Zero the gap (see paragraph 3-6.2 Zeroing the Gap on page 19).
b. Raise the Stage to maximum height (see paragraph 2-3.1 Stage on page 12).
c. Activate Track Mode (please read paragraph 3-5 TRACK MODE on page
19).
d. Hold the Anvil in its current position by turning the Anvil Stop Control to the
e. Place the sample onto the Lower Fixture.
NOTE
20
In the next step:

Although loading technique will vary depending
on the sample, we generally recommend
lowering the stage to within about 50 microns of
the desired gap, trimming the edges sample,
then lowering to the desired gap.
f. Set the gap (see paragraph 3-6.3 Setting the Gap on page 20).
g. Release the Anvil by turning the Anvil Stop Control to the Unlock position.
3-7.2 Prior to loading the sample, ensure that all previous procedures in this chapter
Cone and Plate have been performed (if applicable, as indicated within each procedure).
3-7.2.1
Gap Setting
The actual gap setting for each Cone and Plate fixture is stated on the
Certificate of Calibration that is included in the fixture kit. If no Certificate of
Calibration is available, contact our Technical Service department.
3-7.2.2
Test Temperatures
Use Cone and Plate for isothermal testing only. Transitions to elevated
temperatures cause expansion of the fixture. Since the nominal gap setting for
cone and plate geometry is 50 microns (0.05 millimeter), thermal expansion can
cause contact between fixtures, resulting in erroneous test data.
3-7.2.3
Loading
Perform the following procedure to load samples using Cone and Plate fixtures.
In general, Figure 3-5 shows properly loaded Calibration Samples, included in
the Calibration Kit (see paragraph 4-1.2 Calibration Kit on page 24), which are
representative of most samples. At the left is the PDMS Calibration Sample, at
the right is the 100 cP Calibration Sample. Note that samples such as PDMS
should bulge somewhat from the edges of the plates, while the 100 cP fluid
should taper downward from the bottom edge of the Upper Fixture.
UPPER FIXTURE
SAMPLE
LOWER FIXTURE
Figure 3-5 Cone and Plate with Sample Loaded

a. Zero the gap (see paragraph 3-6.2 Zeroing the Gap on page 19).
b. Raise the Stage to maximum height (see paragraph 2-3.1 Stage on page 12).
c. Activate Track Mode (please read paragraph 3-5 TRACK MODE on page
19).
d. Hold the Anvil in its current position by turning the Anvil Stop Control to the
e. Place the sample onto the Lower Fixture.
NOTE
In the next step:
Although loading technique will vary depending
on the sample, we generally recommend
lowering the stage to within about 50 microns of
the desired gap, trimming the edges sample,
then lowering to the desired gap.
f. Set the gap (see paragraph 3-6.3 Setting the Gap on page 20).
21
g. Release the Anvil by turning the Anvil Stop Control to the Unlock position.
3-7.3 Prior to loading the sample, ensure that all previous procedures in this chapter,
Couette except Zeroing and Setting the Gap, have been performed (if applicable, as
indicated within each procedure). You need not set the gap when using a
Couette.
The following sample loading procedure supports both standard and DIN
Couettes.
a. Raise the Stage to maximum height (see paragraph 2-3.1 Stage on page 12).
b. Activate Track Mode (please read paragraph 3-5 TRACK MODE on page
19).
c. Hold the Anvil in its current position by turning the Anvil Stop Control to the
d. Pour the sample into the Cup (Lower Fixture).
e. Using the Stage Control buttons on
UPPER SURFACE
the User Interface (see paragraph 2OF BOB
3.2 User Interface on page 12),
UPPER SURFACE
lower the Bob into the Cup until the
OF CUP
sample level reaches the upper
surface of the Bob, and the following
criteria are met (see Figure 3-6):
1. The sample forms a meniscus
BOB
CUP
between the edges of the Bob
and Cup, but does not flow over
the upper surface of the Bob.
2. The upper surface of the Bob is
between zero and 5 millimeters
below the upper surface of the
SAMPLE
Cup. If this is not the case,
adjust the sample volume
accordingly.
f. Release the Anvil by turning the
Figure 3-6 Couette with Sample
Anvil Stop Control to the Unlock
Loaded
position.
22
4
CALIBRATION
4-1 OVERVIEW
4-1.1 This chapter contains calibration operations that you should perform. Table 4-1
Operations lists these operations in the required order of performance and the mandatory or
recommended frequency of performance.
Table 4-1 Calibration Operations

Operation
in required order of performance
Frequency of Performance
Torque Calibration
Mandatory:
During instrument installation
Following replacement of stress head
Recommended once per month
Spin Correction
Mandatory:
Following movement and re-leveling of
the instrument
Recommended following Torque Calibration
Examination of Cal Curve
Mandatory during instrument installation

Recommended following Spin Correction
Normal Force Calibration
Mandatory:
Following replacement of stress head
Recommended once per month
23
4-1.2 This instrument is supplied with a Calibration Kit. It should contain the items
Calibration Kit listed in Table 4-2.
Table 4-2 Calibration Kit
Item
Description and Purpose
Calibration Fixture
Upper Fixture used to apply a known mass to the stress

head during Torque and Normal Force Calibration.
Hex Key Set
Six-piece (1.5- to 5-mm) metric balldriver set.
Level
Circular bubble level used to level the instrument.
Monofilament Line
Five-pound-test fishing line used to hang Weight from

Calibration Fixture during Torque Calibration.
Pulley
Pulley that supports the monofilament line during torque

calibration (used to reduce friction).
Screw (extra Bearing
M4 X 0.7 X 8-mm machine screw supplied as an extra

bearing lock screw, which must be installed when air is
not applied to the instrument.
Lock Screw)
Calibration Samples
(used to provide a
known viscosity)
Weights
100 centiPoise calibration sample (2 ounce bottle).

10 centiPoise calibration sample (2 ounce bottle).
GE# SE-30 PDMS viscoelastic sample (1 ounce bottle).
Precision weights used to apply a known mass to the
stress head during Torque and Normal Force
Calibration.
Torque Calibration Weight: 50 grams
Normal Force Calibration Weight: 1000 grams
24
4-2 TORQUE CALIBRATION

4-2.1 Torque Calibration involves hanging a precision weight from the Calibration
Overview Fixture, which provides a 2.5 centimeter moment of torque. The instrument then
determines and applies the corresponding counter-torque required to support the
weight.
4-2.2 Using the items provided in your Calibration Kit, perform Torque Calibration as
Procedure follows:
b. Release the Anvil by turning the Anvil Stop Control to the Unlock position
(see paragraph 2-3.3 Anvil Components on page 12). The Anvil must be free
to rotate.
c. Install the Calibration Fixture as shown in Figure 4-1. Note that the rod must
be positioned to the rear of the instrument, and must fit into the channel as
shown.
d. Insert the Pulley into the Test Station frame as shown in Figure 4-1, ensuring
that the flat machined into the Pulley shaft faces toward the left.
Secure the Pulley by tightening the setscrew in the access hole using a hex
wrench.
e. Prepare a piece of monofilament line with a knot at one end and a loop at the
other end.
f. Perform the following steps (refer to Figure 4-2):
1. Place the knotted end of the line through the slot in the Calibration Fixture,
and place the line in the groove of the pulley.
2. Hang the 50 gram weight (part number 613-02061) from the loop in the
line, ensuring that the weight hangs freely. The weight should cause the
Calibration Fixture to rotate counterclockwise (as viewed from the top of
the instrument), pulling the rod to rest against the left side of the channel
(as viewed facing the front of the instrument).
3. Adjust the line so it rests neither on the upper nor the lower surface of the
calibration fixture, as shown in Figure 4-2.
4. Ensure that the weight is free to hang without obstruction, and that the
weight is steady (not swinging from side-to-side).
g. Using RSI Orchestrator software, select Calibrate Instrument (Utilities
menu). The Transducer Setup form is displayed.
h. Click XducerCal. A calibration information form is displayed.
i. Click Torque Calibration. Yet another information form is displayed.
j. Click Ok. Calibration is complete when the following events have taken
place:
From the starting position, the Calibration Fixture should rotate clockwise,
moving the rod to the right. When calibration is complete, the rod should
return to the starting position, and the numbers in the Torque Calibration
Value and Motor Temp Reference fields should change value.
k. Exit the calibration by clicking Ok.
l. Remove the weight, line, pulley, and Calibration Fixture.
25
ROD
CALIBRATION FIXTURE
PULLEY
Figure 4-1 Installation of Calibration Fixture and Pulley
26
CALIBRATION FIXTURE
LINE
WEIGHT
CALIBRATION FIXTURE
UPPER SURFACE
LOWER SURFACE
LINE
Figure 4-2 Applying Torque Using Calibration Weight
27
4-3 SPIN CORRECTION

4-3.1 Spin Correction compensates for any air bearing rotation that may occur due to
Overview air flow or precession.
4-3.2 Before proceeding, ensure that Torque Calibration (paragraph 4-2 on page 25)
Procedure has been performed, and the instrument has been properly leveled.
a.
b.
c.
d.
e.
f.
f.
g.
h.
i.
j.
k.
Raise the Stage to maximum height (see paragraph 2-3.1 Stage on page 12).
Install a 25 mm Parallel Plate fixture.
Zero the Gap (see paragraph 3-6.2 Zeroing the Gap on page 19).
Load a quantity of the 10cP Calibration Sample from the Calibration Kit (see
paragraph 3-7.1 Parallel Plate on page 20). The quantity should be sufficient
to set a Gap of 1 millimeter.
Ensure that the Anvil Stop Control is in the Unlock position (see paragraph
2-3.3 Anvil Components on page 12). The Anvil must be free to rotate.
Set the Gap to 1 millimeter (see paragraph 3-6.3 Setting the Gap on page
20).
Using RSI Orchestrator software, select the Calibrate Instrument function
(Utilities menu). The Transducer Setup form is displayed.
Click SpinCorr. An information form is displayed, notifying you that Spin
Correction is about to begin.
Begin Spin Correction by clicking Ok. An information form is displayed,
notifying you that the instrument should not be disturbed during Spin
Correction.
Wait until Spin Correction is complete, as indicated by both of the following
events:
1. The information screen is no longer displayed.
2. The number in the Spin Correction field of the Transducer Setup form
changes value.
Click Ok.
Raise the stage to maximum height, then remove the Calibration Sample and
(if desired) Parallel Plate.
28
4-4 EXAMINATION OF CAL CURVE

4-4.1 During Spin Correction, the instrument generates a Cal Curve, which is a profile
Overview of stress head rotational characteristics at selected positions. A Cal Curve that is
within tolerances specified in step b of this procedure indicates that the
instrument is properly leveled and is a confirmation of the overall integrity of the
stress head and support electronics.
Before proceeding, ensure that the following calibration operations have been
performed in the order listed:
Torque Calibration (paragraph 4-2 on page 25)
Spin Correction (paragraph 4-3 on page 28)
4-4.2 Examine the Cal Curve as follows:

Procedure
a. Using RSI Orchestrator, select the Get Stress Head Cal Curve function
(Utilities: Service menu). The Cal Curve is displayed.
b. Ensure that Cal Curve parameters are within tolerances (subject to change
without notice), as follows (see Figure 4-3 for a definition of the parameters):
1. Amplitude (maximum peak-to-peak amplitude of the Cal Curve) must be
less than 12 mgcm.
2. Variation (maximum point-to-point deviation along the Cal Curve) must be
less than 2 mgcm.
Figure 4-3 Cal Curve Parameters
29
4-5 NORMAL FORCE CALIBRATION

4-5.1 Normal Force Calibration involves hanging a precision weight from a hook
Overview mounted to the Calibration Fixture. The instrument then scales the weight to
ensure accurate Normal Force measurement.
4-5.2 Using the items provided in your Calibration Kit, perform Normal Force
Procedure Calibration as follows:
b. Install the Calibration Fixture in the same manner as for the Torque
Calibration (see Figure 4-1). Do not install the pulley.
c. Ensure that the Anvil Stop Control is in the Unlock position (see paragraph
2-3.3 Anvil Components on page 12). The Anvil must be free to rotate.
d. Using RSI Orchestrator software, select Calibrate Instrument (Utilities
menu). The Transducer Setup form is displayed.
e. Click XducerCal. A Calibration information form is displayed.
f. Click NormalCal.
g. Click Zero. An information form is displayed, notifying you that Normal Force
is being zeroed. Before proceeding, wait until the Transducer Setup form is
again displayed.
h. Hang the 1000 gram weight from the hook that is mounted to the bottom of
the Calibration Fixture.
i. Click NormCal. A form is displayed, prompting you to enter the applied
weight.
j. Enter 1000.
k. Click Calibrate. Calibration is complete when the Transducer Setup form is
again displayed.
l. Exit the calibration by clicking Ok.
m. Remove the weight and Calibration Fixture.
30
5
APPENDICES
5-1 OVERVIEW
5-1.1 The Appendices in this chapter describe instrument options and provide
Purpose instructions that do not necessarily apply to operation and calibration of the base
instrument.
5-1.2 Topics following topics are currently included in this chapter:

Content
FLUID BATH ENVIRONMENTAL CONTROL SYSTEM
(paragraph 5-2, page 32)
PELTIER ENVIRONMENTAL CONTROL SYSTEM

HUMIDITY COVER
31
5-2 FLUID BATH ENVIRONMENTAL CONTROL SYSTEM

5-2.1 The Fluid Bath environmental control system continuously cycles fluid through an
Principle open transfer system between a circulator and the Fluid Bath, which is located
directly beneath the Lower Fixture.
DANGER
5-2.2 Fluid and electrical connections to the circulator are shown in Figure 5-1. At the
Circulator time this document was published, it was determined that the fluid hoses should
be pushed over the Circulator fluid nozzles and secured with hose clamps.
Connection
5-2.3 Depending on the desired operating range of the circulator, fill the circulator with
Filling the fluid as specified in Table 5-1.
Circulator
WARNING
TOXICITY
In Table 5-1 below, SF 96-50 silicon fluid emits toxic fumes when heated to a
temperature greater than +140C. Use SF 96-50 silicon fluid above +140C only if an
externally-vented exhaust hood is installed above the circulator. Ensure that exhaust
airflow is adequate to expel fumes emitted from the circulator. Failure to heed this
warning may result in injury or death.
Table 5-1 Circulator Operating Ranges and Fluids
Desired Circulator Operating Range
(bath range is slightly less)
Fluid
-20C
to +30C
100% Dow Corning Syltherm XLT
+1C
to +99C
100% water
-5C
to +90C
20% ethylene glycol / 80% water
to +130C
100% ethylene glycol
+40C
0C to +200C
(see WARNING above)
32
100% SF 96-50 silicon fluid
Figure 5-1 Circulator Connections
33
5-2.4 Prior to using RSI Orchestrator software to control circulator temperature, ensure
RSI Orchestrator that RSI Orchestrator Instrument Testing Limits are set to use the bath as
follows:
Fluid Bath
Configuration
a. Select the Instrument Configuration function (Utilities: Service menu).
The Instrument Options dialog box (Figure 5-2) is displayed.
Figure 5-2 Bath Instrument Configuration

b. Select the following items from the drop lists:
Instrument Setup ............... Temperature Control
Temperature Control ............. Bath (Instrument Controlled Only)
c. Enter the Maximum and Minimum Temperatures corresponding to the
desired circulator operating range and fluid (see paragraph 5-2.3 Filling the
Circulator on page 32).
d. Select either Temperature Loop Control option, using the following
information as a guideline:
1. Circulator Temperature
When selected, the temperature of the fluid in the circulator is maintained
at the commanded temperature. This is monitored independent of the
instrument.
Commanded temperature will be achieved faster than
selecting Tool Temperature (below), but Bath temperature will differ
slightly from that commanded.
2. Tool Temperature
When selected, the temperature of the lower test fixture is maintained at
the commanded temperature. Tool Temperature is the recommended
setting for general testing. Compared to Circulator Temperature (above),
bath temperature will more closely match that commanded, but it will
require 20 to 30 minutes for the commanded temperature to be achieved.
34
5-3 PELTIER ENVIRONMENTAL CONTROL SYSTEM

5-3.1 The Peltier environmental control system utilizes a solid-state heat pump
Principle (thermopile) to control the temperature of the lower fixture, which is an integral
part of the Peltier assembly. In general, the solid state heat pump consists of
multiple semiconductor devices in series, each composed of an N-P junction.
The devices are placed between the lower fixture and a heat sink (Figure 5-3).
Figure 5-3 Solid State Heat Pump (Peltier Element) Schematic

A DC voltage is applied across the semiconductors to either heat or cool the
lower fixture, depending on the polarity of the voltage. The semiconductors
transfer thermal energy between the lower fixture and the heat sink, which is
essentially a heat exchanger through which fluid (typically water) is circulated.
The fluid temperature determines the amount of thermal energy that the heat sink
can source to or sink from the lower fixture. The fluid temperature thereby
determines the Peltier system thermal operating range (see paragraph 5-3.3
Selecting a Thermal Operating Range on page 36).
35
5-3.2
Tentative Temperature Range
Specifications
-40C to +210C, depending on circulator fluid

temperature (see the next paragraph 5-3.3 Selecting a
Thermal Operating Range)
Ramp Rate
50C per minute from 0C to +100C

(at 20C circulator fluid temperature)
Stability
0.1C
5-3.3 Thermal operating range is the Peltier system temperature range at a given
Selecting a fluid temperature. To select a thermal operating range, fluid temperature must
be set in accordance with the following guideline.
Thermal
NOTE
Operating Range
The temperature differentials given below are
estimated.
Assuming that the ambient temperature in the vicinity of the heat sink is +20C, a
differential (T) of -40C exists between the fluid temperature and the lower limit
of the thermal operating range. A T of +80C exists between the fluid
temperature and the upper limit of the thermal operating range.
To determine thermal operating range, add these differentials to the fluid
temperature. For example, at a fluid temperature of +20C, the thermal
operating range of the Peltier system is -20C to +100C, calculated as follows:
Lower Limit
Upper Limit
T + (+20C) =
-40C + (+20C) = -20C
T + (+20C) =
+80C + (+20C) = +100C
At a fluid temperature of +40C, the thermal operating range of the Peltier system
is 0C to +120C, calculated as follows:
Lower Limit
Upper Limit
T + (+40C) =
-40C + (+40C) = 0C
T + (+40C) =
+80C + (+40C) = +120C
36
5-3.4 The Peltier Fixture is a self-contained unit that simply mounts onto the base of
Installation the instrument.
DANGER
Turn OFF the Circulator prior to removing or installing the Peltier Fixture. The Fluid
Bath is an open vat of fluid that is sealed only when the Peltier Fixture is installed.
Failure to turn OFF the Circulator prior to fixture removal and installation will cause the
Fluid Bath to overflow, resulting in possible injury and extensive damage to this
instrument.
Refer to Figure 5-4 during the following procedure.
Installation
b. Push the Peltier Fixture fully into the base, aligning the four captive screws
with the tapped holes in the base.
c. Tighten the four captive screws in the Peltier Fixture (do not over-torque).
d. Connect the cable to the receptacle.
Removal
b. Disconnect the cable from the receptacle.
c. Loosen the four captive screws in the Peltier Fixture.
c. Pull the Peltier Fixture from the base.
NOTE
The Peltier fixture is a Lower Fixture for use only
with Parallel Plate or Cone and Plate Upper
Fixtures.
37
VIEW LOOKING DOWNWARD FROM

THE TOP OF THE INSTRUMENT
NOTE
Early production units are
equipped with eight mounting
holes.
If your unit is so
equipped, align the captive
screws on the Peltier Fixture
with the holes shown (at left)
filled in black.
FRONT OF INSTRUMENT
CAPTIVE SCREWS
PELTIER FIXTURE
RECEPTACLE
(connected to
Environmental
Controller)
CABLE
Figure 5-4 Installation of Peltier System
5-3.5 Supply fluid to the Peltier system by connecting the fluid source to the instrument
38
Circulator Bath hoses (see Figure 5-1).

Options You have a choice of two fluid sources, depending upon your needs:
Peltier Circulator (specifications not yet available)
Manufactured by Rheometric Scientific, the Peltier Circulator is an effective
yet inexpensive means of providing recirculant. Instructions for use of the
Peltier Circulator are printed on the label that is affixed to the circulator.
Commercial Circulator
A commercial fluid circulator must be used to operate the Peltier system over
its entire specified temperature range. For information concerning fluid
connection to the instrument, as well as fluids for use in achieving specified
temperature ranges, see the following paragraphs:
Paragraph 5-2.2 Circulator Connection on page 32
Paragraph 5-2.3 Filling the Circulator on page 32
5-3.6 Prior to using RSI Orchestrator software to control circulator temperature, ensure
RSI Orchestrator that RSI Orchestrator Instrument Testing Limits are set to use the bath as
follows:
Peltier
Configuration
a. Select the Instrument Configuration function (Utilities: Service menu).
The Instrument Options dialog box is displayed.
Figure 5-5 Peltier Instrument Configuration

b. Select the following items from the drop lists:
Instrument Setup ............... Temperature Control
Temperature Control ............. Peltier (Thermopile Heat Pump)
c. Enter the Maximum and Minimum Temperatures in accordance with the
heat sink fluid temperature and the corresponding thermal operating range
(see paragraphs 5-3.1 Principle on page 35, and 5-3.3 Selecting a Thermal
Operating Range on page 36).
For example, if the fluid temperature is +20C, Set the Minimum Temperature
to -20C, and the Maximum Temperature to +100C.
5-4 HUMIDITY COVER
39
5-4.1 When used with the Fluid Bath or Peltier Environmental Control Systems, the
Principle Humidity Cover helps prevent evaporation of samples and/or solvents. This
device consists of the following components (see Figure 5-6):

a. Cover
The two-piece Cover is placed onto the Lower Fixture, providing a more
closed environment than open atmosphere.
b. Well
The steel Well is placed onto the Cover. The solvent for the sample under
test is placed in the Well, which is removable for cleaning.
c. Trap
The spring-loaded Trap is placed onto the Upper Fixture. After the sample is
loaded and the Gap set, the Trap is lowered until immersed in the solventfilled Well.
WELL
TRAP
(REMOVABLE)
COVER
(LEFT HALF)
COVER
(RIGHT HALF)
Figure 5-6 Humidity Cover

The Cover, Well, and Trap form a relatively sealed chamber. As the sample
and/or solvent evaporates, the atmosphere within the chamber nears saturation,
thus slowing evaporation.
5-4.2 To use the Humidity Cover, perform the following steps:

Usage
a. Install the Trap onto the Upper Fixture as follows:
1. Separate the two halves of the Trap by removing the spring that holds
them together.
2. Place each half on either side of the fixture shaft, and fasten the halves
together by replacing the spring.
3. Push the Trap as far as it will go toward the top of the fixture.
b. Install the Upper Fixture.
c. Perform AutoCal (see paragraph 3-4 AUTOCAL on page 18). This is
necessary because the Trap has added mass to the Upper Fixture.
d. Load the sample (complete procedures are contained in Chapter 3, which
begins on page 14).
e. Place the left and right halves of the Cover onto the Lower Fixture, and seal
the two halves by pressing them together.
40
f. If you wish to purge the internal atmosphere of the Cover, connect a nitrogen
gas purge line to the connector (not shown) that is mounted on the Cover.
g. Place the Well onto the Cover.
h. Fill the Well with the sample solvent.
NOTE
In the next step, do not allow the Trap to touch
the Well. The Upper Fixture must be able to
rotate freely.
i. Push the Trap downward until it is submersed in the solvent that is contained
in the Well.
41
INDEX
Air Bearing
caution concerning instrument damage, 10
Air Dryer
caution concerning instrument damage, 10
Anvil
identification, 12
locking and unlocking, 12
Anvil Stop Control, 12
AutoCal (Automatic Fixture Inertia Calculation),
18
Cal Curve, 29
Calibration
Cal Curve Examination, 29
Kit, 24
list of required calibrations, 23
Normal Force, 30
Spin Correction, 28
Torque, 25
Cone and Plate
Gap setting, 21
loading samples, 21
test temperatures, 21
Couette
loading samples, 22
Environmental Controller
monitoring, 13
Fixtures
Lower, installation/removal, 15
Upper, installation and removal, 17
Fluid Bath
configuration, 34
filling the circulator, 32
principle, 32
Gap
setting, 20
zeroing, 19
Humidity Cover
principle of operation, 40
usage, 40
Instrument description, 7
Manual Organization, 7
Normal Force
Calibration, 30
Parallel Plate
Gap setting (recommended), 20
loading samples, 20
Peltier Option
circulator options, 39
configuration, 39
installation, 37
specifications, 36
thermal operating range, 36
Peltier System
principle of operation, 35
RSI Orchestrator Online Help, 7
Specifications, instrument, 8
Spin Correction, 28
Stage, 12
Test Station
component identification, 11
Torque
Calibration, 25
Track Mode, 19
User Interface, 12
42

Rheometric Scientific SR5 Manual

Uploaded by

Document Information

Copyright

Available Formats

Share this document

Share or Embed Document

Sharing Options

Did you find this document useful?

Is this content inappropriate?

Copyright:

Available Formats

Rheometric Scientific SR5 Manual

Uploaded by

Copyright:

Available Formats

In s tru m e n t

This document is to be used solely by owners of the

Rheometric Scientific, Inc.

SR5 INSTRUMENT MANUAL Revision X1 24 October 1997

document. Insofar as specific mention is made of particular product features,

All products described herein are currently under continuous development.

TERMS AND SYMBOLS USED IN THIS MANUAL

An immediately hazardous situation that, if not avoided, will result in either

A potentially hazardous situation that, if not avoided, will result in either

Information that is emphasized by being placed prior to the procedural step to

SR5 INSTRUMENT MANUAL Revision X1 24 October 1997

The Stress Head uses a precision air bearing that must be

The instrument is shipped with a bearing lock that prevents

SR5 INSTRUMENT MANUAL Revision X1 24 October 1997

SR5 INSTRUMENT MANUAL Revision X1 24 October 1997

SR5 INSTRUMENT MANUAL Revision X1 24 October 1997

3-7.1.1 Gap Setting ................................................................................................................. 20

SR5 INSTRUMENT MANUAL Revision X1 24 October 1997

This instrument is operated using Rheometric Scientific RSI Orchestrator

1-2 DESCRIPTION OF INSTRUMENT

The SR5 is a controlled-stress rheometer, i.e., the instrument deforms a sample

SR5 INSTRUMENT MANUAL Revision X1 24 October 1997

0.01 to 500 gcm (0.001 to 50 mNm)

0 to 100 radians per second

Dynamic Frequency Range

0.00005 to 500 radians per second

When the instrument is in Track Mode, an

Normal Force Range

See paragraph 5-2.3 Filling the Circulator on

See paragraph 5-3.2 Tentative Specifications on

Electrically Heated Plates

Ambient to +350C (preliminary specification)

-150C to +500C (preliminary specification)

60 psi (4.1 bar)

Air Flow Into the Instrument

Air Quality Into the

Instrument-quality air with a dew point of -40C,

SR5 INSTRUMENT MANUAL Revision X1 24 October 1997

SR5 INSTRUMENT MANUAL Revision X1 24 October 1997

2-2 REQUIRED READING: PREVENTING DAMAGE TO THE INSTRUMENT

The Stress Head uses a precision air bearing that must be

The instrument is shipped with a bearing lock that prevents

SR5 INSTRUMENT MANUAL Revision X1 24 October 1997

2-3 TEST STATION COMPONENTS

ANVIL STOP CONTROL

Figure 2-2 Test Station Components

SR5 INSTRUMENT MANUAL Revision X1 24 October 1997

(next topic), or automatically adjusted to a specific height using RSI Orchestrator

Figure 2-3 User Interface

SR5 INSTRUMENT MANUAL Revision X1 24 October 1997

2-4 ENVIRONMENTAL CONTROLLER

Each LED is illuminated when...

Figure 2-4 Environmental Control Status Panel

SR5 INSTRUMENT MANUAL Revision X1 24 October 1997

SR5 INSTRUMENT MANUAL Revision X1 24 October 1997

3-2 FIXTURE INSTALLATION AND REMOVAL

procedures covering Environmental Control options, please see the relevant

SR5 INSTRUMENT MANUAL Revision X1 24 October 1997

VIEW LOOKING DOWNWARD FROM

Figure 3-1 Lower Fixture Installation onto Fluid Bath

SR5 INSTRUMENT MANUAL Revision X1 24 October 1997

Figure 3-2 Upper Fixture

3-3 ZEROING NORMAL FORCE

SR5 INSTRUMENT MANUAL Revision X1 24 October 1997