Professional Documents
Culture Documents
SYLLABUS
(For the Academic year 2014 - 2015)
V and VI Semester B. E.
CHEMICAL ENGINEERING
3. Faculty List:
Sl.
Name of the Faculty
No.
1
G. A. Shareef
2
Dr. Archna
3
V.Venkatesham
4
S. Swaminathan
5
Ravi Sadasivan
6
K.A. Badarinarayana
7
Dr.G. M. Madhu
8
Dr. Brijesh
9
Rajeswari M. Kulkarni
10
Ramasivakiran Reddy
11
Koteswara Rao Jammula
12
V. Shravanthi
Qualification
Designation
M.Tech., (Ph.D.)
M.E, Ph.D.
M. E., (Ph.D.)
M. E.
M.Sc.(Engg.), (Ph.D.)
M.Tech.
M.E., Ph.D.
M.Tech., Ph.D.
M.Tech., (Ph.D.)
M.Tech. (Ph.D.)
M.Tech., (Ph.D.)
M.Tech., (Ph.D.)
graduates with problem solving abilities, teamwork, and communication skills necessary throughout
their careers. They are consistent with the following Educational Objectives:
1. To provide a strong foundation and understanding of the fundamental principles of mathematics,
science, and engineering enabling graduates to pursue their careers as practicing chemical engineers in
Chemical and Allied Engineering Industries.
2.
To produce graduates who are prepared to pursue their post graduation and Research in the fields of
Chemical Engineering and Petrochemicals, Material Science, Biotechnology, Nanotechnology,
Environmental Engineering, any emerging allied areas and Business.
3. To produce graduates who posses skills with contemporary grounding in professional responsibility,
ethics, global and societal impact of engineering decisions to assume professional leadership roles and
administrative positions.
4.
To provide students with opportunities to participate in various multidisciplinary teams and to develop
and practice written and oral communication skills.
10. Process of deriving POs:
The Programme outcomes are defined by taking feedback from faculty, alumni, Industry, professional
bodies, guidelines suggested by regulatory bodies (UGC, AICTE, VTU) and graduate attributes
suggested by National Board of Accreditation. The established PEOs are in line with programme
educational objectives. The following Figure indicates the information flow.
a
x
b
x
x
x
x
Programme Outcomes
e
f
g
h
i
x
x
x
x
x
x
x
x
x
x
x
x
l
x
x
x
x
Subject
Code
Credits
(L:T:P)
Teaching
Dept.
Marks
End Exam
(Hrs)
CIE
SEE
Total
CH501
3:1:0
CH
03
50
50
100
CH502
Mass Transfer-I
3:1:0
CH
03
50
50
100
CH503
3:0:0
CH
03
50
50
100
CH504
3:0:0
CH
03
50
50
100
CH505
3:0:0
CH
03
50
50
100
CH506
1:1:0
CH
03
50
50
100
CHPE01x
*Elective A
3:0:0
CH
03
50
50
100
CHL504
0:0:2
CH
03
50
50
100
CHL506
0:0:2
CH
03
50
50
100
19
26
*Elective Group A
CHPE011 Petroleum Technology
CHPE012 Green Technology
CHPE013 Cheminformatics
CHPE014 Hazard Analysis and Risk Management
CHPE015 Process Instrumentation and Data Analysis
Subject
Code
Credits
(L:T:P)
Teaching
Dept.
Marks
End Exam
(Hrs)
CIE
SEE
Total
AL601
2:0:0
AL
03
50
50
100
CH601
3:1:0
CH
03
50
50
100
CH602
Mass Transfer-II
3:1:0
CH
03
50
50
100
CH603
Biochemical Engineering
3:0:0
CH
03
50
50
100
CHPE02x
*Elective-B
3:0:0
CH
03
50
50
100
CH604
1:1:2
CH
04
50
50
100
CHL601
0:0:2
CH
03
50
50
100
CHL602
0:0:2
CH
03
50
50
100
16
24
*Elective Group B
CHPE021
Natural Gas Engineering and Transportation
CHPE022
Non-Conventional Energy Sources and Technology
CHPE023
Composite Materials
CHPE024
Advanced Thermodynamics
CHPE025
Operations Research
Legend: CH-Chemical Engineering, AL-Any Department, L-Lecture, T-Tutorial, P-Practical, CIE-Continuous Internal Evaluation, SEESemester End Examination.
V Semester
CHEMICAL REACTION ENGINEERING-I
Sub Code:
Credit:
CIE:
CH501
3:1:0
50 Marks
Contact Hours: 70
SEE:
50 Marks
10
11
MASS TRANSFER-I
Sub Code:
Credit:
CIE:
CH502
3:1:0
50 Marks
Contact Hours: 70
SEE:
50 Marks
Unit III
Drying: Drying Equilibria. Drying rate curves. Mechanism of drying. Calculation of batch
and continuous drying. Equipments for drying. Design of continuous rotary dryer.
Unit IV
Crystallization: Factors governing nucleation and crystal growth rates. Controlled growth of
crystals. Yield calculations and energy balance. Different types of crystallizer equipments.
Fractional crystallization.
Unit V
Adsorption: Theories of adsorption. Isotherms, Industrial adsorbents. Stagewise operations,
Adsorptions calculations and equipments.
Ion exchange: Process & equipment.
12
Text Books:
1. Treybal, R.E., Mass Transfer Operations, 3rd Edition, McGraw Hill, 1981.
2. Ananthraman, K.M. Begum, M.S., Mass Transfer Theory and Practice, PHI New Delhi,
2011.
Reference Books:
1. Coulson JM, Richardson JF and Sinnott RK, Chemical Engineering Vol I, II, IV and V,
4th Edition, Pergmen Press, 1998.
2. Badger & Banchero, Introduction to Chemical Engineering, TMH, 6th Reprint, 1998.
3. Geankoplis, C. J., Transport Processes and Unit Operation, Prentice Hall(I), 2000.
Course Outcomes: On successful completion of this course the students will be able to
1. Explain the concept of Stages, Transfer Units and efficiency stages.
2. Analyze diffusion of fluids and related mass transfer theories.
3. .Explain principles of mass transfer operations humidification, drying, crystallization and
adsorption.
4. Perform material and energy balance calculations in mass transfer operations
humidification, drying, crystallization and adsorption.
5. Design the equipments for humidification, drying, crystallization and adsorption
operations.
13
Sub Code:
Credit:
CIE:
Pre-requisites: Nil
Course coordinator: Chemical Engineering Department
Course Objectives: The students will
1. Learn about the various utilities used in the process industries.
2. Learn to evaluate the utility requirements in process industries.
3. Design utility transportation systems.
4. Learn about various methods and instruments used for such purposes.
5. Perform energy audits in plants.
Course Content:
Unit I
Introduction: Different utilities. Role of utilities in process plant operations and criteria for
selection and estimation of suitable utilities.
Water: Water resources. Process water, Cooling water, drinking water and boiler feed water
Quality Standards. Water treatment processes for drinking, process and boiler feed. Storage
and handling of water. Types and selection of pumps, piping and accessories. Water pre
treatment , reuse and recycling.
Unit II
Steam and Power: Steam generation in chemical plants. Types of boilers and waste heat
boilers. Fuels-types, emissions and global warming, green fuels. Calorific value. Proximate
and ultimate analysis. HHV, LHV and related calculations. Cogeneration power plants. CHPs
and Boiler performance. Related Calculations. Economy of steam generation with different
fuels, related calculation. Steam storage and handling-piping and accessories.
Unit III
Air: Compressed air, blower air, fan air. Types of compressor and vacuum pumps and
selection. Power requirements, performance and related calculations. Booster and receivers.
Quality of compressed air for instruments and processes. Compressed air distribution systempiping and accessories.
Air-water vapour system: humidification/ dehumidification and
evaporative cooling-related calculations.
Unit IV
Refrigeration: Different refrigeration systems and their characteristics. Air-conditioning
systems. Coefficient of performance. Power requirements and refrigeration effect- related
calculations for each type of refrigeration system. Refrigerant properties and selection. Some
commonly used refrigerants and secondary refrigerants. Air-conditioning.
Insulation: Insulation Materials and Selection- Economics of insulation. Insulating factors.
Properties & Classification. Cold insulation and cryogenic insulation.
14
Unit V
Energy Audit: Energy scenario, Energy audit need, types of energy audit Preliminary audit,
detailed audit, Steps in audit, bench marking, energy performance, energy audit instruments.
15
Sub Code:
Credit:
CIE:
from chemical industries. Origin, control methods, and equipment used in typical industries
Thermal power plants, metallurgical industries, and cement industries. Carbon credits.
Unit IV
Solid waste treatment: Origin. Classification and microbiology. Properties and their
variation. Engineered systems for solid waste management generation, onsite handling,
storage, collection, transfer and transport, composting, sanitary land filling.
Unit V
Noise control: Sources and definitions. Determination of noise levels. Noise control criteria
and noise exposure index. Administrative and engineering controls. Acoustic absorptive
materials.
Safety: Introduction to Process Safety- Intrinsic & Extrinsic Safety. The Hazards- Toxicity,
Flammability, Fire, Explosions. Sources of ignition, Pressure.
Safety devices: Pressure relief valves. Ruptures discs. Blow down systems. Flare systems.
Flame arrestors. Deflagration arrestors and explosion suppression. Personal safety devices.
Process safety analysis: HAZAN and HAZOP comparison. Sequence of operability study.
Risk analysis and estimation. Safety check list. Computer based quantitative risk analysis.
ISO and OSHAS.
Text Books:
1. Rao, C.S., Environmental Pollution Control Engineering, New Age International, Reprint
2002.
2. Mahajan, S.P., Pollution Control in Process Industries, Tata McGraw Hill, 1999.
Reference Books:
1. Perkins, H.C., Air Pollution, McGraw Hill,1974.
2. Hagerty. D.J., Solid Waste Management, Van Nostrand Reinhold,1973.
Metcalf and Eddy, Waste Water Engineering, Treatment, Disposal & Reuse, Tata McGraw
Hill, 4th Edition, 2003.
Course Outcomes: On successful completion of this course, the student
1. Understands the nutrient and hydrological cycles.
2. Become well versed with characterization of pollutions in water, air, and soil.
3. Knows about the various acts enacted by the State and Pollution Control Boards.
4. Will be able to sample and analyze the pollutants in the laboratory.
5. Will be able to design the treatment systems for effluents from various industry.
6. Will be able to design for prevention and control of air pollution.
7. Are enabled to analyze the Solid Waste treatment and processing.
8. Are familiarized with noise pollution; they can formulate treatment strategies for waste
water, air & solid waste to be within the ambit of legal implications and environmental
regulations.
9. Will be able to analyze risks and understand functioning of safety devices.
17
CH505
3:0:0
50 Marks
Contact Hours: 42
SEE:
50 Marks
Pre-requisites: Nil
Course coordinator: Chemical Engineering Department
Course Objectives: The students will
1. Study the process industries such as organic, inorganic, natural, synthetic, metallurgical
industries.
2. Learn to write flow chart symbols and flow charts for typical chemical processes.
3. Understand the use of various unit process and unit operations involved in various
process industries and also learn in writing line/ pipe line diagrams.
4. Learn to generate process flow diagrams for a given set of operations.
Course Content:
Unit I
Sulfur: Elemental Sulfur mining, Sulfur from ores, Oxides of Sulfur (SO2, SO3).
Industrial Gases: CO2, H2, O2, N2, Water gas and Shift gas.
Acids: Sulfuric, Nitric, Hydrochloric, phosphoric acid.
Unit II
Chlor-Alkali Industries: Sodium chloride, Soda ash, Caustic soda, Chlorine, Bleaching
powder.
Fertilizers: Ammonia, Urea, Ammonium chloride, Ammonium nitrate, Ammonium
phosphate, Ammonium sulfate, DAP, Biofertilizers.
Unit III
Phosphorous Industries: Manufacture of white and Red Phosphorus, Pentoxide, Phosphatic
Fertilizers, Super Phosphate and Triple Super Phosphate.
Fermentation Industries: Production of alcohol, acetic acid and citric, penicillin.
Unit IV
Petroleum Industries: Constituents of crude petroleum refining and processing. Production
of Ethylene, Propylene.
Unit V
Polymers and Rubber: Polymerization, PVC, LDPE, Polyproylene, cross linked polymers,
natural rubber, synthetic rubber and rubber compounding.
Miscellaneous Industries: Paints, Pigments, Vanishes, Enamel, Lacquers - White Lead and
Zinc oxide, Hydrogen peroxide (H2O2), Silicon carbide (SiC), Glass, Cement (Types,
manufacture of portland cement, slag cement).
18
Text Books:
1. Shreves, Chemical Process Industries, McGraw Hill, 4th Edition.
2. Rao Gopal & Sittig Marshall, Dryden Outlines of Chemical Technology for 21st
Century, 3rd Edition, EWP.
Reference Book:
1. Bose, P.K., Chemical Engineering Technology, Vol. 1,2, Books and Allied (Pvt) Ltd,
2011.
2. Desikan and Sivakumar , Unit Processes in Organic Chemical Industries (Eds.), CEDC,
IITM, 1982.
19
Batch Reactor, PFR, CSTR (Calculations based on performance equation). (Algorithm and C
Program).
Unit V
MATLAB: Introduction, Array, Matrix algebra, Polynomials, Integral and Differential
Equations, Two and Three dimensional plots.
Text Books:
1. Rajaraman, V., Computer Oriented Numerical Methods, Prentice Hall of India.
2. Mickley, Sherwood, and Reed, Applied Mathematics in Chemical Engineering, Tata
McGraw Hill.
Reference Books:
1. Grewal, S., Numerical methods of Engineering and Science, Khanna Publishers.
2. Glyn James, Advanced Modern Engineering Mathematics, PearsonEducation,-3rd
Edition.
3. Rudrapratap, Getting Started with MATLAB- A Quick Introduction for Scientists and
Engineers, Oxford Press, 2009.
Course Outcomes: On successful completion of this course the students will be able to
1. Explain various numerical methods used in mathematics.
2. Apply these techniques in solving Chemical Engineering problems.
3. Develop step-wise procedure (Algorithms) for solving chemical engineering models.
4. Write C programs for numerical methods
5. Execute them in laboratory and use C or MATLAB for other problems also.
6. Perform data analysis and regression.
7. Apply these methods in the design of chemical engineering equipment and processes.
21
PETROLEUM TECHNOLOGY
Sub Code:
Credit:
CIE:
CHPE011
3:0:0
50 Marks
Contact Hours: 42
SEE:
50 Marks
Pre-requisites: Nil
Course coordinator: Chemical Engineering Department
Course Objectives: The students will
1. Study about the petroleum industries in the country and abroad and the operations that is
carried out in them.
2. Learn about the classification and compositions of crudes.
3. Study the important products (Gasoline, Diesel, Kerosene and lube oil), properties and
test methods for crudes.
4. Study the various crude processing methods such as reforming, cracking etc.
5. Learn the crude pretreatment methods and operations involved in it.
6. Study about the various impurities present in the crude and method of their treatment to
produce useful products like LPG, LNG, Gasoline, lube etc.
Course Content:
Unit I
Indian Petroleum industry: Prospects & Future. Major companies. World production,
Markets, Offshore and onshore, Oil well technology.
Composition of crude: Classification. Evaluation of petroleum. UOP-k factor. TBP analysis.
EFV analysis. Average boiling point. ASTM curves. Thermal properties of petroleum
fractions.
Product properties and test methods: Gas. Various types of gas and LPG. Reid vapor
pressure analysis. Gasoline and naptha. Octane No. Oxidation stability.
Additives for gasoline. Kerosene. Characterization for flash point or fire point, volatility,
burning qualities etc, Diesel, octane testing, viscosity etc. Grades of diesels e.g. HSD, LDO.
Diesel additives. Lube oils : Types, tests-carbon residue and viscosity index
Unit II
Crude pretreatment: Pumping of crude oils. Dehydration of crude by chemical, gravity,
centrifugal, electrical de-salter and comparision of each. Heating of crude- heater, different
types of pipe still heaters including box type, cylindrical etc. Crude distillation, arrangement
of towers for various types of reflux. Design aspects for atmospheric and vacuum column.
Atmospheric distillation distillation unit: internals and operational.
Unit III
Treatment techniques: Types of impurities present and various desulfurisation processes.
Production and treatment of LPG. LNG technology. Sweetening operations for gases
including merox, ethanolamine, copper chloride, stertford etc. Catalytic de sulphonisation.
Treatment of kerosene, De-aromatisation and merox. Treatment of diesel, naptha:
desulpurisation by hydrogen and catalysts. Treatment of lubes: sulphuric acid, clay treatment,
solvent treatment-phenol, furfural.
Unit IV
Thermal Processes: Thermal cracking reactions- theory of thermal cracking. Properties of
cracked materials and factors influencing the properties of cracked materials. Visbreaking,
dubbs two coil cracking process.
22
23
GREEN TECHNOLOGY
Sub Code:
Credit:
CIE:
CHPE012
3:0:0
50 Marks
Contact Hours: 42
SEE:
50 Marks
Unit IV
Structure of the pollution prevention process,
Unit V
Design for the environment and improvement in manufacturing operations, case studies.
Text Books:
1. Anastas P.T., Warner J.C., Green Chemistry: Theory and Practice. Oxford Science
Publications, Oxford, 1998.
2. Paul L. Bishop, Pollution Prevention: Fundamentals and Practice, McGraw Hill,2000.
Reference Books:
1. Mike Lancaster, Green Chemistry- An Introductory Text, Royal Society of Chemistry
Publishing, 2010
2. Boyle, Godfrey, Bob Everett, Janet Ramage, Energy Systems and Sustainability: Power
for a Sustainable Future, Oxford University Press, 2004.
Course Outcomes: On successful completion of this course the student will be able to
1. Understand environment laws, carbon credits, ISO 14000 series
2. Explain the importance of green technology in sustainable development.
3. Explain tools of green technology and life cycle assessment.
4. Understand pollution prevention planning and environment friendly design
24
CHEMINFORMATICS
Sub Code:
Credit:
CIE:
CHPE013
3:0:0
50 Marks
Contact Hours: 42
SEE:
50 Marks
Pre-requisites: Nil
Course coordinator: Chemical Engineering Department
Course Objectives: Cheminformatics (or Chemoinformatics) is a field of research that
combines methods from computer science and chemistry with the aim of solving chemical
engineering problems efficiently. The course will provide the necessary theoretical
background to solve such problems. The students will learn how to apply the methods in
order to study complex interactions in chemical and bio chemical systems and to discover
new emerging properties arising from the systemic viewpoint.
Course Content:
Unit I
Introduction: Cheminformatics, History and Evolution of cheminformatics, Use of
cheminformatics, Prospects of cheminformatics, Molecular Modeling and Structure
Elucidation.
Unit II
Representation of Molecules and Chemical Reactions, Nomenclature; Different types of
Notations; SMILES Coding; Matrix Representations; Structure of Molfiles and Sdfiles;
Libraries and toolkits; Different electronic effects; Reaction classification, Properties
estimation using ASPEN v8 suite.
Unit III
Database Design & their Management, Database Concepts. Structured Query Language.
Design of Chemical Databases, Data Abstraction; Data Models; Instances & Schemes; E-R
Model - Entity and entity sets; Relations and relationship sets; E-R diagrams; Reducing E-R
Diagrams to tables; Network Data Model: Basic concepts; Hierarchical Data Model: Basic
Concepts; Metadatabases; Indexing and Hashing; Basic concepts; Text Databases;
Introduction to Distributed Database Processing, Data Security. Intefacing programs with
databases; Structure databases; Reaction Databases; Literature Databases; Medline;GenBank;
PIR; CAS Registry; National Cancer Institute (NCI) Database.
Unit IV
Searching Chemical Structure, Full structure search; sub structure search; basic ideas;
similarity search; Three dimensional search methods; Basics of Computation of Physical and
Chemical Data and structure descriptors; Data visualization and Non-linear Mapping.
Unit V
Chemo-informatics Applications, Prediction of Properties of Compounds; Linear Free Energy
Relations; Quantitative Structure-Property Relations; Descriptor Analysis; Model Building;
Modeling Toxicity; Structure-Spectra correlations; Prediction of NMR, IR and Mass spectra;
Computer Assisted Structure elucidations; Computer Assisted Synthesis Design, Introduction
to drug design; Target Identification and Validation; Lead Finding and Optimization;
Analysis of HTS data; Virtual Screening; Design of Combinatorial Libraries; Ligand-Based
25
Course Outcomes: On successful completion of this course the student will be able to
1.
Apply and explain methods, models, and algorithmic ideas covered in the course,
2.
Formulate the above in precise language and notation,
3.
Implement algorithms and data structures from the course,
4.
Describe the implementation and experimental work done in clear and precise
language, and in a structured fashion.
26
Sub Code:
Credit:
CIE:
Pre-requisites: Nil
Course coordinator: Chemical Engineering Department
Course Objectives: The student will
1. Have awareness of different hazards in process industries
2. Learn classification of hazards and their identifications
3. Learn precautions in chemical storage and handling
4. Learn risk analysis techniques and quantify them
5. Learn emergency management plans
Course Content:
Unit I
Plant Hazards: Fire hazards., Chemical hazards, Toxic hazards, Explosion hazards, Electrical
hazards, Mechanical hazards, Radiation hazards, Noise hazards. Control, precautions &
prevention, Safety measures in plant.
Unit II
Fire hazards, Chemical hazards, Toxic hazards, Explosion hazards, Electrical hazards,
Mechanical hazards, Radiation hazards, Noise hazards, Control, precautions & prevention,
Safety measures in plant.
Unit III
Storage & Transportation of chemicals: Characteristics of chemical with special reference to
safe storage & handling of chemicals, Layout of storage, Various modes of transport and
Safety precautions in transportation of different types of chemicals.
Unit IV
Risk Analysis Techniques: Hazard & Operability (HAZOP) studies, Hazard Analysis
(HAZAN), Fault Tree Analysis, Consequence Analysis.
Unit V
Onsite and Offsite emergency management plans. Human Error Analysis. Accident Error
Analysis. Economics of Risk Management.
Text Book:
1.K. V. Raghavan and AA. Khan, Methodologies in Hazard Identification and Risk
Assessment, Manual by CLRI, 1990.
2. V. C. Marshal, Major Chemical Hazards, Ellis Horwood Ltd., Chichester, 1987.
3. Sam Mannan, Lees, Loss Prevention in the Process Industries, Hazard Identification,
Assessment and Control, 4th Edition, Butterworth Heineman, 2012.
Course Outcomes: The student should be able to
1. Classify and identify hazards in chemical industries
2. Take precautions in chemical storage and handling
3. Perform fault tree and event tree risk analysis and quantify them
4. Suggest and make others in the plant about emergency management plans
27
Sub Code:
Credit:
CIE:
Pre-requisites: Nil
Course coordinator: Chemical Engineering Department
Course Objectives: The student will study
1.
Characteristics of measuring instruments
2.
Measurement instruments and working of temperature, thermal conductivity,
pressure, flow rate, liquid level, density and electrical conductivity
3.
Analysis of the data obtained graphically and numerically
4.
Optimization of data using factorial method
Course Content:
Unit I
Measurement quality. Characteristics of instruments. Measurement methods for temperature,
thermal conductivity, and viscosity.
Unit II
Measurement methods for pressure, flow rate, and liquid level.
Unit III
Measurement methods for vapour pressure, density, and electrical conductivity.
Unit IV
Role of experiments in engineering and technology. Data collection and interpretation
requirements Graphical and numerical data processing; Variable-screening techniques.
Unit V
Introduction to design of experiments, Factorial method.
Text Books:
1.
Ray, M.S., Engineering Experimentation: Ideas, Techniques, Presentation, McGraw Hill
Book Co. Inc., New York, 1988.
2.
Eckmen, D. P., Process Instrumentation, CBS Publishers and Distributors, 2006.
Reference Books:
1. Gibbings, J.C., The Systematic Experiment, Cambridge University Press, Cambridge, U.K,
1986.
2. Austin E. Frisbane, Industrial Instrumentation Fundamentals, McGraw Hill Co. Inc, NY,
1983.
3. H.S. Mickely, T.K. Sherwood & C.E. Reed, Applied Mathematics in Chemical Engineering,
3rd Edition, Tata McGraw Hill, 1999.
Sub Code:
Credit:
CIE:
Pre-requisites: Nil
Course coordinator: Chemical Engineering Department
List of experiments:
1. Determination of pH, alkalinity of samples.
2. Determination of turbidity of sample using Nephelo turbidometer.
3. Determination of dissolved, suspended and volatile solids.
4. Optimum coagulant dosage using Jar test.
5. Settleable and suspended particulate matter in air using high volume sampler.
6. Determine of chloride, iodide, nitrate ions in water samples using Ion selective electrode.
7. Determination of BOD.
8. Determination of COD.
9. Dissolved oxygen determination using DO meter.
10. Estimation of Copper in mining leachate
11. MPN count.
12. Determination concentration of Sodium, Potassium, Calcium in the given sample.
13. To treat a given phenol effluent and determine the content of phenol pre and post
treatment.
14. Determination of concentration of COx, SOx, NOx in air sample.
15. Analysis using FTIR
16. Determination of Cyclone separator efficiency.
Note: Minimum 10 experiments are to be conducted.
29
Sub Code:
Credit:
CIE:
30
VI Semester
INTELLECTUAL PROPERTY RIGHTS
Sub Code:
Credit:
CIE:
AL601
2:0:0
50 Marks
Contact Hours: 28
SEE:
50 Marks
Pre-requisites: Nil
Course coordinator: Chemical Engineering Department
Course Objectives: The students will learn
1. IPR, its forms and role.
2. Patents: Indian and Global scenario.
3. Procedure for obtaining patent.
4. Trade marks and laws.
5. Copy Right, its requirements, and infringement.
Course Content:
Unit I
Introduction to IPR: Globalization, Knowledge era, History of IPR.
Different forms of IPR Copy Rights, Trade Marks, Industrial designs, Patents and Trade
secrets; Role of IPR in Research and Development.
Design: Designs that can be registered, Procedures of registration.
Unit II
Patents: patent as an intellectual property, Brief history of patents-Indian and global
scenario, Principles underlying Patent law.
Ideas: Generation and review of ideas, process and Product Patents.
Unit III
Procedure for Obtaining Patent: Patent Contents Patent Drafting: Filing requirements.
Case Studies on Patents: Related to chemical and allied industries
Unit IV
Trade Marks: Nature, Essentials, Protection, Trade Marks (contd.) Service marks and
Laws.
Case Studies on Trade marks: Related to chemical and allied industries.
Unit V
Copy Right: Characteristics and Requirements; Neighboring rights, Ownership;
Infringement of Copy right.
Case Studies on Copy Rights: Related to chemical and allied industries.
31
Text Book:
1. Wadehra, B.L., Law relating to Patents, Trademarks, Copyright, Designs and
Geographical Indications, 2nd Edition, Universal Law publishing Co. Pvt. Ltd., 2002.
Reference Books:
1. Prabudha Ganguli, Intellectual Property Rights, Tata McGraw Hill Publishing Co. Ltd.,
2001.
2. Manish Arora, Guide to Patents Law, 4th Edition, Universal Law publishing Co. Pvt. Ltd.,
2007.
Course Outcomes: On completion of this course, the student will be able to
1. Understand the role of IPR and its importance.
2. Understand Indian and global scenario of patents.
3. Search for patents and know the procedure to obtain it.
4. Understand the nature and protection of trade marks.
5. Understand the requirements and infringement of Copyright.
32
Sub Code:
Credit:
CIE:
34
MASS TRANSFER-II
Sub Code:
Credit:
CIE:
CH602
3:1:0
50 Marks
Contact Hours: 70
SEE:
50 Marks
Text Books:
1. Treybal, R.E., Mass Transfer Operations, 3rd Edition, McGraw Hill, 1981.
2. Ananthraman, Sheriffa Begum, K.M., Mass Transfer Theory and Practice, PHI New
Delhi, 2011.
35
Reference Books:
1. Coulson, J.M., Richardson, J.F. and Sinnott, R.K. , Chemical Engineering Vol I, II, IV
and V, 4th Edition, Pergmen Press, 1998.
2. Badger & Banchero, Introduction to Chemical Engineering, TMH, 6th Reprint, 1998.
3. Foust, A., Principals of Unit Operation, 2nd Edition, John Wiley, 1994.
4. Geankoplis, C. J, Transport Processes and Unit Operation, Prentice Hall(I), 2000.
36
BIOCHEMICAL ENGINEERING
Sub Code:
Credit:
CIE:
CH603
3:0:0
50 Marks
Contact Hours: 42
SEE:
50 Marks
Pre-requisites: Nil
Course coordinator: Chemical Engineering Department
Course Objectives: The students will
1. Study introduction to the application of chemical engineering principles in biochemical
systems.
2. Be enabled to understand the biological systems and kinetics of enzymatic reactions.
3. Learn the kinetics of growth of microorganisms, hence be able to control the process.
4. Be able to design equipments for handing biological processes.
5. Study Operations utilized in the purification of biological products enable them to
recommend, install and easily learn to operate the equipments.
Course Content:
Unit I
Introduction: Bioprocess engineering and technology. Role of a Chemical engineer in
bioprocess industry. An introduction to basic biological sciences. Microbiology: Structure of
cells: Prokaryotes and Eukaryotes. Classification of micro-organisms. Taxonomy, Whitakers
5-kingdom concept. Characteristics and control of microorganisms. Environmental and
Industrial microbiology.
Biochemistry: Chemicals of Life: Lipids, Sugars, Polysaccharides, Amino acids and
proteins, Vitamins, Biopolymers, Nucleic Acids: RNA, DNA and their derivatives (Structure,
Biological function and Importance for life only to be studied).
Unit II
Enzymes and Proteins: Detailed structure of proteins and enzymes: Primary, Secondary,
Tertiary and quaternary. Functions. Production and purification of Enzymes (Methods only).
Nomenclature and Classification of enzymes. Mechanism and Kinetics using various models.
Kinetics of Enzyme action: MichaelisMenten rate equation. Derivation with Equilibrium
and Pseudo- (quasi-) steady state approximations. Experimental determination of rate
parameters: Batch and continuous flow experiments.
Unit III
Enzyme Inhibition: Effect of Inhibitors (Competitive, noncompetitive, uncompetitive,
substrate and product inhibitions), Temperature and pH on the rates enzyme catalyzed
reactions.
Unit IV
Fermentation Technology: Ideal reactors: A review of Batch and Continuous flow reactors
for bio kinetic measurements. Microbiological reactors: Operation and maintenance of
typical aseptic aerobic fermentation processes. Formulation of medium: Sources of nutrients.
Alternate bioreactor configurations. Introduction to sterilization of bioprocess equipment.
Design of batch & continuous sterilization equipment.
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Unit V
Growth Kinetics of Microorganisms: Transient growth kinetics (Different phases of batch
cultivation). Quantification of growth kinetics: Substrate limited growth, Models with growth
inhibitors, Logistic equation, Filamentous cell growth model. Continuous culture: Optimum
Dilution rate, Critical Dilution rate in Ideal Chemostat. Introduction to Fed-batch reactors.
Strategies and Steps involved in product purification.
Text Book:
1. Bailey and Ollis, Biochemical Engineering Fundamentals, 2nd Edition, McGraw Hill,
1976.
2. Shuler, M. L. and Kargi, F., Bioprocess Engineering, 2nd Edition, Prentice Hall, 2002.
Reference Books:
1. Pelczer, Microbiology Concept and Application, 5th Edition, McGraw Hill, 2001 Reprint.
2. Stanbury and Whittaker, Principles of Fermentation Technology, II Edition.
38
Sub Code:
Credit:
CIE:
Unit III
Cryogenic extraction of natural gas liquids (NGL). Minor component (nitrogen, helium,
mercury, and BTEX) recovery or removal. Acid Gas (hydrogen sulfide and carbon dioxide)
removal.
Unit IV
Sweetening and dehydration of condensate and natural gas liquids (NGL).
Sulfur recovers with the Claus process, Tail gas cleanup.
Unit V
Acid gas injection. Liquefied natural gas (LNG), production, storage, transportation, and
regasification.
Text Books:
1. Katz, D. L. and Lee, R.L., Natural Gas Engineering, McGraw Hill, 1990.
Reference Books:
1. Kidnay, A.J., Parnish, W.R., Dekker, Fundamentals of Natural Gas Processing, McGraw
Hill.
2. Mokhatab, S., Handbook of Natural Gas Transmission and Processing.
Course Outcomes: On successful completion of this course the students will be able to
1. Explain the principles of gas compression, handling and transportation.
39
2. Explain Various methods and equipment used for gas handling and transportation are
learnt.
3. Explain Gas treatment processes and impurity removal methods will make the student
employable in these industries.
4. Apply the knowledge of chemical engineering and design to the gas processing and
transportation.
5. Explain about LNG production and processing.
40
41
42
COMPOSITE MATERIALS
Sub Code:
Credit:
CIE:
CHPE023
3:0:0
50 Marks
Contact Hours: 42
SEE:
50 Marks
Unit III
Processing Techniques based on reaction methods: such as Chemical vapour deposition
(CVD), vapour phase epitaxy, plasma-enhanced chemical vapour deposition (PECVD),
chemical vapour infiltration (CVI). Self propagating high temperature synthesis (SHS) for the
preparation of monolithic ceramics, composites, coating, thin films, whiskers and fibres and
semi conducting materials such as Si and Gallium Arsenide.
Unit IV
Synthesis and processing of mixed ceramic oxides with high temperature super conducting
properties
Reinforcement, additives, fillers for polymer composite, master batch & compounding.
Unit V
Polymer composite. Fibre reinforced composites. Stress Strain modulus relationship Nano
composites.
43
44
ADVANCED THERMODYNAMICS
Sub Code:
Credit:
CIE:
CHPE024
3:0:0
50 Marks
Contact Hours: 42
SEE:
50 Marks
Unit III
Thermo chemistry, first Law analysis of reacting systems, Adiabatic Flame temperature,
Entropy change of reacting systems, Second Law analysis of reacting systems, Criterion for
reaction equilibrium composition.
Unit IV
Microstates and Macrostates, Thermodynamic probability, Degeneracy of energy levels,
Maxwell-Boltzman, Fermi-Dirac and Bose-Einstein Statistics, Microscopic Interpretation
of heat and work, Evaluation of entropy, Partition function, Calculation of the
Microscopic properties from partition functions. Collision Theory and Transport
properties.
Unit V
Conjugate Fluxes and Forces, Entropy Production, Onsager's Reciprocity relations,
thermo-electric phenomena and formulations. Thermodynamics of High-Gas flow.
45
Text Books:
1. Kenneth Wark Jr., Advanced Thermodynamics for Engineers, McGraw-Hill Inc., 2001.
2. Sonntag, R.E., and Vann Wylen, G., Introduction to Thermodynamics, Classical and
Statistical, third Edition, John Wiley and Sons, 1991.
References
1. Bejan, A., Advanced Engineering Thermodynamics, John Wiley and Sons, 1998.
2. Holman, J.P., Thermodynamics, Fourth Edition, McGraw-Hill Inc., 1998.
3. Smith, J.M and Van Ness., H.C., Introduction to chemical Engineering
Thermodynamics, Fourth Edition, McGraw-Hill Inc., 1987.
4. Sears, F.W. and Salinger G.I., Thermodynamics, Kinetic Theory and Statistical
Thermodynamics, third Edition, Narosa Publishing House, New Delhi, 1993.
5. De Hoft, R.T. Thermodynamics in Materials Science, McGraw-Hill Inc., 1993.
6. Rao, Y.V.C., Postulational and Statistical thermodynamics, Allied Publisher Limited,
New Delhi, 1994.
46
OPERATIONS RESEARCH
Sub Code:
Credit:
CIE:
CHPE025
3:0:0
50 Marks
Contact Hours: 42
SEE:
50 Marks
Course Outcomes: On successful completion of this course the students will be able to
1. Develop the problems for mathematical analysis.
2. Identify problems and constraints in a problem.
3. Assign activities on priority base and optimize time.
4. Minimize time or cost for transportation.
5. Network activities in a project, identify crucial activities and have control over the
project.
6. Maintain correct inventory and reduce the cost.
7. Poses management techniques, will make students handle projects effectively.
48
Sub Code:
Credit:
CIE:
Reference Books:
1. Joshi, M.V., Process Equipment Design, Macmillan India,1991.
2. Brownell, L.E. and Young, E.H., Process Equipment Design - Vessel Design, John Wiley
and Sons, Inc.1959.
3. Ludwig, E.E., Applied Process Design for Chemical and Petrochemical Plants, Vol. 1 and
2, 3rd Ed., Gulf Publishing Co. 1997.
4. Indian Standards Institution, Code for Unfired Pressure Vessels, IS 2825.
5. Bhattacharya, B.C, Introduction to Chemical Equipment Design, CBS Publications,1985.
6. Perrys Chemical Engineers Handbook.
Course Outcomes: On successful completion of this course the students will be able to
1. Design process and design equipment by choosing appropriate material of construction by
following applicable design codes.
2. Capable of translating the design to fabrication drawings for plant erection.
3. Explain the correct fabrication techniques and testing methods.
4. Possess engineering skills directly applied in design, installation and commissioning of
equipments.
49
Sub Code:
Credit:
CIE:
Batch Reactor
Isothermal plug flow reactor
Mixed flow reactor
Semi batch reactor
Heterogeneous catalytic Reactor
CSTRs in Series
Adiabatic Reactor
Packed bed Reactor
RTD Studies in Tubular Reactor
Effect of temperature on Rate of reaction
Bio Chemical Reaction (Batch)
Enzyme catalyzed reactions in batch reactor
RTD Studies in mixed flow reactor
Sono-chemical reactor
Photochemical reactor
50
CHL602
0:0:2
50 Marks
Contact Hours: 42
SEE:
50 Marks
51