Phase II ESA

Phase II
Environmental Site Assessment

Central Services Facility
202 South Thornton Avenue
Madison, Wisconsin
DFD Project No. 09H2L
Prepared for:
Wisconsin Department of Administration
Division of Facilities Development
PO Box 7866
Madison, WI 53707
September 2013
Phase II Environmental Site Assessment

Central Services Facility
202 South Thornton Avenue
Madison, Wisconsin
This report prepared by:
________________________________
Mitchell C. Banach
Environmental Scientist
________________________________
Neil E. Carney, PE
Project Engineer
This report reviewed by:
________________________________
Dennis L. Johnson, PE
Supervisor Environmental Services
5201 E. Terrace Drive, Suite 200

Madison, WI 53718
608.443.1200 Fax: 608.443.1250
www.AyresAssociates.com
Ayres Associates Project No. 19-0291.10
File: v:\env\final\19029110\09h2l - thornton ave phase ii esa.docx
Contents
Page No.
Executive Summary ................................................................................................................... iii
Phase II ESA Scope ..............................................................................................................iv
Findings ................................................................................................................................. v
General Findings ............................................................................................................... v
Introduction ................................................................................................................................ 1
Site Location and Project Numbers ........................................................................................ 2
Project Contacts .................................................................................................................... 3
Drilling and Laboratory Contractors........................................................................................ 3
Site Background ......................................................................................................................... 4
Phase II ESA Scope ................................................................................................................... 5
Fieldwork .................................................................................................................................... 6
Findings ..................................................................................................................................... 8
Soil Texture ........................................................................................................................... 8
Soil Quality .......................................................................................................................... 10
Headspace Screening ..................................................................................................... 10
VOCs .............................................................................................................................. 10
PAHs............................................................................................................................... 10
Metals ............................................................................................................................. 10
PCBs............................................................................................................................... 11
Groundwater Quality ............................................................................................................ 11
PAHs............................................................................................................................... 11
Metals ............................................................................................................................. 11
PCBs............................................................................................................................... 12
Conclusions .............................................................................................................................. 13
Recommendations ................................................................................................................... 14
Standard of Care ................................................................................................................. 14
List of Appendices
Appendix A 2013 Phase I ESA Sanborn Maps
Appendix B Field Procedures
Appendix C Soil Probe Logs and Abandonment Forms
Appendix D Laboratory Analytical Results
List of Figures
Figure 1 Regional Location Map
Figure 2 Sample Location Map
Figure 3 Regulatory Exceedance Map
List of Tables
Table 1A Volatile Organic Compounds (VOCs) in Soil
Table 1B Polycyclic Aromatic Hydrocarbons (PAHs) in Soil
Table 1C Metals in Soil
Table 1D Polychlorinated Biphenyls (PCBs) in Soil
Table 2 Summary of Groundwater Analytical Results
ii
Executive Summary
The State of Wisconsin Department of Administration (DOA), Division of Facilities
Development (DFD) intends to construct the new State Archive Preservation Facility (SAPF)
(DFD Project No. 09H2L) proposed to be located at 202 S. Thornton Avenue in Madison,
Wisconsin. This 5.10 acre property is the current site of the DOA Central Services Facility.
Prior to construction of the new facility, existing site improvements including buildings and
pavements will be removed, and buried utilities will be abandoned. In order to conduct
environmental due diligence efforts in advance of proposed demolition and construction
activities, the DFD retained Ayres Associates to conduct a Phase I and Phase II
Environmental Site Assessment (ESA) of the facility. The Phase I ESA of the property was
completed in June 2013. This report presents the findings of the Phase II ESA.
Review of historical Sanborn fire insurance maps compiled during the Phase I ESA identified
recognized environmental conditions (RECs) primarily related to the historical operation of
electric motor and machine manufacturing companies, including a machine shop, paint shop,
brass foundry, and loading/unloading activities from adjacent railroad spurs. Additional
information sources also indicated the former presence of polychlorinated biphenyls (PCB)
containing transformers, storage tanks, and historical releases. The Phase I ESA identified
several RECs on the property. Descriptions of RECs as stated in the Phase I ESA are
detailed below:
The current presence of a 10,000-gallon underground storage tank (UST) system,

operational since 1988. Although the UST system has been subject to annual
inspection and is compliant with applicable regulations, regular operation of the
system over time is likely to result in releases from spills, overfills and leaks below
detection thresholds (See Figure 2 Area 4).
Foundry slag observed at the ground surface in the west wing of the courtyard, and
its use as fill material to a depth of 2 feet as indicated by soil probe boring logs from
2007. The slag is believed to have originated from a former brass foundry as
identified by historical fire insurance maps, and may contain heavy metals such as
lead (See Figure 2 Area 2).
The former presence of PCB-containing material in the courtyard cistern that was not
investigated for horizontal or vertical extent. Although PCBs were found to be present
in cistern contents, and impacts in the vicinity were investigated in 2007, the
investigation did not include the analysis of PCBs in soil and groundwater
surrounding the cistern. PCBs in cistern contents were present at concentrations that
exceed Residual Contaminant Levels (RCLs) for the protection of groundwater (See
Table 1D, Figure 2 Area 1).
The former presence of oil dipping rooms, as identified on historical fire insurance
maps. The quantity of oil used is presumed to be significant due to the size of the
rooms depicted, and releases may have occurred from the regular operation of these
tanks or leakage over time (See Figure 2 Area 3).
The former presence of scrap sheds along rail lines adjacent to the north and south
property boundaries as identified by historical fire insurance maps. The regular
loading and unloading of the bins may have resulted in contamination from metal
scrap or dust and residual oils from machining (See Figure 2 Areas 5 and 8).
iii
The former presence of three coal bins located throughout the site, as identified by
historical fire insurance maps. Soil impacts from metals such as arsenic may exist
due to the accumulation of coal dust in these areas (See Figure 2 Areas 1, 6, and
7).
The former presence of a paint shop, as identified on historical fire insurance maps.
There is a reasonable likelihood of subsurface impacts from the operational cleaning
of painting equipment using solvents on the site. Although previous investigations
have discovered low concentrations of chlorinated solvents in the groundwater, no
previous investigations have included soil sampling in this area (See Figure 2 Area
9).
The former presence of an oil house, as identified on historical fire insurance maps
(See Figure 2 Area 10).
The former presence of a gasoline house, as identified on historical fire insurance

maps (See Figure 2 Area 11).
The former presence of PCB transformers on the site as revealed by the EDR Radius
Map Report; former transformer locations were also revealed by a 1956 building
survey drawing by Gisholt Machine Company. Releases may have occurred due to
the deterioration of transformers that were on site, estimated to be from 1956 to 2007,
and PCBs were previously detected on the site during a 2007 investigation of the
courtyard, a known transformer location (See Figure 2 Areas 1 and 12).
The former operation of a machine shop on the site from 1895 to 1970, which is
associated with the regular use of various oils and solvents. Although one of the two
former machine shop areas was previously investigated for potential subsurface
impacts, the report contains no data regarding polycyclic aromatic hydrocarbons
(PAHs), which are commonly present in machine oils and lubricants (See Figure 2
Areas 4 and 13).
The former operation of a railway power house, as identified on historical fire

insurance maps. The power house is likely to have utilized significant quantities of
coal or oil, and although one soil sample was indicated to be previously collected in
this area, there is no information in the report describing the sampling rationale,
procedure or laboratory analysis (See Figure 2 Area 14).
Because of these findings, a Phase II ESA was completed to evaluate soil and groundwater
quality on the subject property.
Phase II ESA Scope

To investigate the areas identified in the Phase I ESA, the following scope of services was
conducted:
Retained a drilling contractor and installed 26 soil probes to a maximum depth of 12

feet (ft) below ground surface (bgs). Selected boreholes were converted to temporary
wells for the purpose of collecting groundwater samples.
Collected soil samples at approximately 2-2.5-foot intervals and screened samples for
the presence of organic compounds using a photoionization detector (PID).
iv
Submitted soil and groundwater samples to a Wisconsin certified laboratory for

analysis for select volatile organic compounds (VOCs), PAHs, Resource
Conservation & Recovery Act (RCRA) metals (arsenic, barium, cadmium, chromium,
mercury, silver and selenium) and PCBs.
Analyzed soils with potentially hazardous concentrations of lead by toxicity

characteristic leaching procedure (TCLP) to address potential disposal
considerations.
Prepared soil probe logs and abandonment forms, tables summarizing laboratory
results, and a site map showing probe locations.
Prepared this Phase II ESA report to document field procedures and findings of the
assessment and to present conclusions and recommendations for the site.
Phase II ESA fieldwork was completed on June 13 and 14, 2013. Field procedures, soil
probe logs, analytical results, and findings relative to the soil quality are described in the
main body of this report.
Findings
This Phase II ESA investigated the potential for soil and groundwater contamination
associated with the RECs identified in the June 2013 Phase I ESA. The following paragraphs
provide a general summary of conclusions derived from field observations and laboratory
analytical results for soil and groundwater samples obtained from the site. The discussion is
broken down into the areas identified as RECs during the Phase I ESA, and also includes
locations where geotechnical borings were previously advanced by Badger State Drilling in
April 2013 and Soil Essentials in May 2013 during site design activities.
General Findings
The majority of the site contains a layer of fill material from 0-3 feet below ground surface
(bgs) which demonstrates dark discoloration and contains detectable levels of PAHs and
metals (arsenic, cadmium, and lead) in exceedance of RCLs listed in the United States
Environmental Protection Agency (USEPA) Regional Screening Level Web-Calculator.
Arsenic concentrations were compared to background threshold value (BTV) of 8 parts per
million, which is endorsed by the Wisconsin Department of Natural Resources (WDNR),
based on data provided in a study published by the United States Geological Survey (USGS)
titled Distribution and Variation of Arsenic in Wisconsin Soils, With Data on Other Trace
Elements (February 2013). Groundwater data indicated Wisconsin Administrative Code NR
140 Enforcement Standard (ES) exceedances for metals across the site.
Area 1, Courtyard (Former Cistern, Central Coal Bin; GP-1 through GP-3)
Probes were advanced to 12 feet bgs. Detectable levels of PCBs (below RCLs) were
detected in soils from 5-7 feet bgs. No PCBs were detected in groundwater. Soil data
indicates RCL exceedances from 0-2 feet for various metals. Groundwater data
indicates levels of arsenic, chromium, and lead above Chapter NR 140, Wis. Admin.
Code ESs. Impacted soils are anticipated from 0-3 feet bgs.
Area 2, Former Brass Foundry (West Wing of Courtyard; GP-4 and GP-5)
Probes were advanced to 12 feet bgs. Soil data indicates RCL exceedances from 0-2
feet for various PAHs and metals. Groundwater data indicates levels of arsenic and
lead above ESs. Impacted soils are anticipated from 0-3 feet bgs.
Area 3, Former Oil Dipping Rooms (GP-6) Probe was advanced to 12 feet bgs.
No VOCs were detected in shallow or deep soils. RCL exceedances were detected
from 1-3 feet for PAHs. No RCL exceedances were detected in soils from 5-7 feet
bgs. Impacted soils are anticipated from 0-3 feet bgs.
Area 4, Current Fuel Tank Systems (GP-7 through GP-9) Probes were advanced
to 12 feet bgs. No VOCs were detected and PAHs concentrations are below RCLs. A
release from the current above ground storage tank (AST) or UST is not indicated
based upon available data.
Area 5, Former North Scrap Shed (GP-10) Probe was advanced to 4 feet bgs.
Soil data indicates RCL exceedances from 1-3 feet bgs for PAHs. No metals
concentrations were indicated to exceed RCLs. Impacted soils are anticipated from 03 feet bgs.
Area 6 Former West Coal Bin (GP-11) Probe was advanced to 4 feet bgs. Soil
data indicates RCL exceedances from 1-3 feet bgs for PAHs. Metals concentrations
in soil were found to exceed RCLs for protection of groundwater. Impacted soils are
anticipated from 0-4 feet bgs.
Area 7 Former East Coal Bin (GP-12) Probe was advanced to 4 feet bgs. Soil
data indicates RCL exceedances from 2-3 feet bgs for PAHs. Metals concentrations
in soil were found to exceed RCLs for protection of groundwater. Impacted soils are
Area 8, South Scrap Shed (GP-13 and GP-14) Probes were advanced to 4 feet
bgs. Soil data indicates RCL exceedances from 1-2 feet bgs for PAHs and metals.
Relatively high levels of lead and cadmium in soils are indicated at this location. Due
to high levels of lead observed at this location, a TCLP analysis was conducted by
the laboratory; results indicated that the soil at this location is not characteristically
hazardous. Impacted soils are anticipated from 0-4 feet bgs.
Area 9, Former Paint Shop (GP-15 and GP-16) Probes were advanced to 12 feet
bgs. No VOCs were detected in soil or groundwater. Soil data indicates BTV
exceedances from 2-4 feet bgs for arsenic. Lead concentrations in soil were found to
exceed RCLs for protection of groundwater from 2-4 feet bgs. Groundwater data
indicates levels of lead above ESs. Impacted soils are anticipated from 0-5 feet bgs.
Area 10, Former Oil House (GP-17) Probe was advanced to 12 feet bgs. No VOCs
detected in shallow or deeper soils. Soil data indicates an RCL exceedance from 2-4
feet bgs for one PAH compound. No compounds were present at detectable
concentrations from 5-7 feet bgs. Impacted soils are anticipated from 0-4 feet bgs.
Area 11, Former Gasoline House (GP-18) Probe was advanced to 12 feet bgs. No
VOCs were detected in shallow (2-4 feet bgs) or deeper (5-7 feet bgs) soils. Soil data
indicates RCL exceedances at both 2-4 feet and 5-7 feet bgs for PAHs and lead.
Groundwater data indicates levels of lead and PAHs above ESs. Impacted soils are
vi
Area 12, Former PCB Transformer Area (GP-19) Probe was advanced to 12 feet
bgs. No detectable PCB concentrations were identified at this area. One VOC
compound (naphthalene) was detected below RCLs. Soil data indicates RCL
exceedances from 2-4 feet for PAHs. Impacted soils are anticipated from 0-6 feet
bgs. Impacts to groundwater have not been determined for this area.
Area 13, Former Machine Shop (GP-20 and GP-21) Probes were advanced to 12
feet bgs. No detectable PAH concentrations were identified at this area from 5-7 feet
bgs. Groundwater data indicates levels above Chapter NR 140, Wis. Admin. Code
Preventative Action Limits (PALs) for PAHs.
Area 14, Former Rail Powerhouse (GP-22) Probe was advanced to 12 feet bgs.
Soil data indicates RCL exceedances from 1-3 feet bgs for PAHs. Lead
concentrations in soil were found to exceed RCLs for protection of groundwater.
Impacted soils are anticipated from 0-4 feet bgs.
Former Geotech Boring #11 (GP-23) Probe was advanced to 12 feet bgs. No
suspected contamination based on soil observation. Fill under the existing concrete
slab appeared clean with no traces of coal or slag. Soil from this location was not
analyzed based on indicators for non-impacted media.
Former Geotech Boring #12 (GP-24) Probe was advanced to 12 feet bgs.
Geoprobe refusal at approximately two feet below grade due to unknown obstruction.
Based on observations of Area 9 to the north, this area is assumed to have impacted
soils from 0-3 feet bgs.
Former Geotech Boring #15 (GP-25) Probe was advanced to 12 feet bgs. Suspect
fill material encountered from approximately 0-2 feet bgs. Soil from this location was
not analyzed based on similar appearance to material from nearby Area 7, for which
soil data indicates RCL exceedances from 2-3 feet bgs for PAHs and metals
concentrations in soil which exceed RCLs for protection of groundwater. Impacted
soils are anticipated from 0-3 feet bgs.
Former Geotech Boring #7 (GP-26) Probe was advanced to 12 feet bgs. Suspect
black fill material was encountered from 1-2 feet bgs in this location. No VOCs or
PAHs were detected in soil from 5-7 feet bgs. Lead concentrations in soil were found
to exceed RCLs for protection of groundwater from 1-2 feet bgs. Groundwater data
indicates levels of lead above ESs. Impacted soils are anticipated from 0-3 feet bgs.
Recommendations
Because several metals and PAH compounds above regulatory standards were indicated at
the site and have not been documented to have been previously investigated, we
recommend that the site owner submit this report to the WDNR for review prior to beginning
construction at the property.
Development plans for the new SAPF are currently being prepared. DFD has indicated that
impacted soils will remain on site, during and following construction, and will be managed
long-term through construction of an engineered cap. A cap maintenance plan will be
vii
developed and implemented at the site. Details of the cap maintenance plan should be
submitted to the WDNR for review and approval prior to construction of the new facility.
DFD will conduct building demolition and utility removal activities in the fall/winter of 2013 to
prepare the site for new construction. Because these activities will likely expose areas of
impacted soils, we recommend that DFD develop separate Soils Management Plans for the
demolition phase and construction phase of the project to appropriately manage impacted
soils identified in the Phase II ESA.
viii
Introduction
The State of Wisconsin Department of Administration (DOA), Division of Facilities
Development (DFD) intends to construct the new State Archive Preservation Facility (SAPF)
(DFD Project No. 09H2L) proposed to be located at 202 S. Thornton Avenue in Madison,
Wisconsin. This 5.10-acre property is the current site of the DOA Central Services Facility.
Prior to construction of the new facility, existing site improvements including buildings and
pavements will be removed, and buried utilities will be abandoned. In order to conduct
environmental due diligence efforts in advance of proposed demolition and construction
activities, the DFD retained Ayres Associates to conduct a Phase I and Phase II
Environmental Site Assessment (ESA) of the facility. The Phase I ESA of the property was
completed in June 2013. This report presents the findings of the Phase II ESA.
Review of historical Sanborn fire insurance maps compiled during the Phase I ESA identified
recognized environmental conditions (RECs) primarily related to the historical operation of
electric motor and machine manufacturing companies, including a machine shop, paint shop,
brass foundry, and loading/unloading activities from adjacent railroad spurs. Additional
information sources also indicated the former presence of polychlorinated biphenyl (PCB)
containing transformers, storage tanks and historical releases. Descriptions of RECs as
stated in the Phase I ESA are detailed below:
The current presence of a 10,000-gallon underground storage tank (UST) system in

use since 1988. Although the UST system has been subject to annual inspection and
is compliant with applicable regulations, regular operation of the system over time is
likely to result in releases from spills, overfills and leaks below detection thresholds
The current presence of foundry slag observed at the ground surface in the west wing
of the courtyard and use as fill material to a depth of 2 feet as indicated by soil probe
boring logs from 2007. The slag believed to have originated from a former brass
foundry as identified by historical fire insurance maps, and is likely to contain heavy
metals such as lead (Pb) (See Figure 2 Area 2).
The former presence of PCB-containing material in the courtyard cistern that was not
thoroughly investigated. Although PCBs were found to be present in cistern contents,
and impacts in the vicinity were investigated in 2007, the investigation did not include
the analysis of PCBs in soil and groundwater surrounding the cistern. PCBs in cistern
contents were present at concentrations that exceed Residual Contaminant Levels for
the protection of groundwater (See Figure 2 Area 1).
The former presence of oil dipping rooms, as identified on historical fire insurance
maps. The quantity of oil used is presumed to be significant due to the size of the
rooms depicted, and releases likely result from the regular operation of these tanks or
leakage over time (See Figure 2 Area 3).
The former presence of scrap sheds along rail lines adjacent to the north and south
property boundaries as identified by historical fire insurance maps. The regular
loading and unloading of the bins is likely to result in contamination from metal scrap
or dust and residual oils from machining (See Figure 2 Areas 5 and 8).
The former presence of three coal bins located throughout the site, as identified by
historical fire insurance maps. Soil impacts from metals such as arsenic are likely to
exist due to the accumulation of coal dust in these areas (See Figure 2 Areas 1, 6,
and 7).
The former presence of a paint shop, as identified on historical fire insurance maps.
There is a reasonable likelihood of subsurface impacts from the operational cleaning
of painting equipment using solvents on the site. Although previous investigations
have discovered low concentrations of chlorinated solvents in the groundwater, no
previous investigations have included soil sampling in this area (See Figure 2 Area
9).
The former presence of an oil house, as identified on historical fire insurance maps
The former presence of a gasoline house, as identified on historical fire insurance

maps (See Figure 2 Area 11).
The former presence of PCB transformers on the site as revealed by the EDR Radius
Map Report; former transformer locations were also revealed by a 1956 building
survey drawing by Gisholt Machine Company. Releases may have occurred due to
the deterioration of transformers that were on site from at least 1956 to 2007, and
PCBs were previously detected on the site during a 2007 investigation of the
courtyard, a known transformer location (See Figure 2 Areas 1 and 12).
The former operation of a machine shop on the site from 1895 to 1970, which is
associated with the regular use of various oils and solvents. Although one of the two
former machine shop areas was previously investigated for potential subsurface
impacts, the report contains no data regarding polycyclic aromatic hydrocarbons
(PAHs), which are commonly present in machine oils and lubricants (See Figure 2
Areas 4 and 13).
The former operation of a railway power house, as identified on historical fire

insurance maps. The power house is likely to have utilized significant quantities of
coal or oil, and although one soil sample was indicated to be previously collected in
this area, there is no information in the report describing the sampling rationale,
procedure or laboratory analysis (See Figure 2 Area 14).
Because of these findings, a Phase II ESA was completed to evaluate soil and groundwater
quality on the subject property.
This report presents the results of the Phase II ESA. The report includes a discussion of site
background, field procedures, findings, and recommendations as well as site drawings, soil
probe logs and abandonment forms, laboratory reports and tables that summarize analytical
results.
Site Location and Project Numbers

The subject property is located in the Northwest 1/4 of the Northwest 1/4 of Section 7,
Township 7 North, Range 10 East, in the City of Madison, Dane County, Wisconsin, and
measures approximately 5.10 acres. Figure 1 shows the regional location of the property and
Figure 2 is an aerial photograph that shows the current layout of subject property.
2
Project Contacts
The project contacts for this site are as follows:
Client/Property Owner:
Wisconsin Department of Administration

Division of Facilities Development
PO Box 7866
Madison, Wisconsin 53707
Bill Napier, PE
bill.napier@wisconsin.gov
Consultant:
Ayres Associates
5201 E. Terrace Drive, Suite 200
Madison, Wisconsin 53718
Neil E. Carney, PE
carneyn@ayresassociates.com
608.443.1298
Drilling and Laboratory Contractors

Pace Analytical, Green Bay, Wisconsin, provided analytical services. This laboratory is
certified by the Wisconsin Department of Natural Resources (Certification No. 405132750).
Horizon Construction and Exploration, of Grafton, Wisconsin, provided drilling services.
Site Background
The subject property is an approximately 5.10-acre lot located at 202 South Thornton
Avenue, Madison, Wisconsin, that includes an approximately 147,700-square-foot building
complex constructed between 1895 and 1942.
The earliest known developed use of the property was as Northern Electrical Manufacturing
Company, established in 1895. The company specialized in the design and manufacturing of
electrical motors, and had its own brass foundry. Site features also included a machine shop,
punch press room, dipping rooms, winding department, tool room, paint shop, oil house, and
gasoline house. Two scrap houses were also located along the railroads to the north and the
south. Three rail spurs entered the property on the north and south sides to provide transport
of supplies and finished goods. By 1942, the property had become Gisholt Machine
Company, after the founder of Northern Electrical Manufacturing Company, Conrad
Conradson, had passed away in 1940. Conradson was the former Vice President of Gisholt
prior to founding Northern Electrical and continued to patent machine tool designs while
running Northern Electrical.
Gisholt Machine Company used the site for the manufacturing of machine tools, such as
lathes and balancing machines, and employed approximately 1,200 people. Gisholt
expanded the facilities with new construction on the eastern half of the property. A building
survey map produced in 1954 also indicates that the east half of the Gisholt complex was
occupied by Smith White Truck Sales and Nagle Hart Company, and used the building for
tractor repair and storage. Gisholt was later purchased by Giddings & Lewis Machine Tool in
1966, and was shut down in 1970 due to economic downturn. The property is presumed to
have been vacant for approximately two years before being sold to the State of Wisconsin in
1972 for its current use.
The property is currently known as the Central Services Building, operated by the State of
Wisconsin Department of Administration. Several entities occupy the property including
Information Technology Services, State Agency Services, Transportation Services and
University of Wisconsin Tandem Press, and primary operations consist of vehicle fleet
maintenance, printing and mailing services, art studios and administrative offices.
Demolition of the existing buildings are scheduled to occur during 2014, with construction of
a new, State-owned, archival storage facility on the subject property from 2014-2016.
Phase II ESA Scope

To investigate the areas with RECs identified in the previous environmental studies, Ayres
Associates conducted the following scope of services:
Retained a drilling contractor and installed 26 soil probes to a maximum depth of 12

feet (ft) below ground surface (bgs). Selected boreholes were converted to temporary
wells for the purpose of collecting groundwater samples.
Collected soil samples at approximately 2-2.5-foot intervals and screened samples for
the presence of organic compounds using a photoionization detector (PID).
Submitted soil and groundwater samples to a Wisconsin certified laboratory for

analysis for select volatile organic compounds (VOCs), PAHs, Resource
Conservation & Recovery Act (RCRA) metals (arsenic, barium, cadmium, chromium,
mercury, silver and selenium) and PCBs.
Analyzed soils with potentially hazardous concentrations of lead by toxicity

characteristic leaching procedure (TCLP) to address potential disposal
considerations.
Prepared soil probe logs and abandonment forms, tables summarizing laboratory
results, and a site map showing probe locations.
Prepared this Phase II ESA report to document field procedures and findings of the
assessment and to present conclusions and recommendations for the site.
Fieldwork
Ayres Associates observed the installation of 26 soil probes (GP-1 through GP-26) on
June 13 and 14, 2013. Horizon Construction and Exploration of Grafton, Wisconsin,
performed the soil probing using a direct push Geoprobe machine. Weather conditions were
dry and sunny with temperatures up to 89 degrees Fahrenheit. Field procedures used to
obtain soil and groundwater samples are summarized in Appendix B.
The 26 soil probes were installed to a depth of 4 to 12 feet below ground surface (bgs). Soil
samples were collected at continuous intervals in each probe starting at the surface to the
terminus. Soils were classified, field screened, and collected for laboratory analysis. Soil
samples were screened in the field for the presence of organic vapors using a calibrated PID.
Soil probe logs with soil classification and PID readings and abandonment forms are in
Appendix C.
The soil probes and temporary monitoring wells were installed at selected locations to
address RECs identified in the Phase 1 ESA. The locations, sampling rationale, and
quantities are summarized in the following table:
Location
Area 1
Area 2
Area 3
Area 4
Area 5
Area 6
Description
Former Cistern
Former Brass Foundry
Sampling Rationale
PCBs, Pb, and Cr in former cistern during

previous investigations were greater than
Residual Contaminant Levels (RCLs) for
direct contact and protection of
groundwater. No samples were previously
collected outside of cistern to determine
potential horizontal or vertical extent.
Analysis included: PCBs, PAHs, RCRA
metals.
Brass foundry slag not previously
investigated. Analysis included: PCBs,
PAHs, RCRA metals.
Former Oil Dipping

Rooms
Not previously investigated. Analysis

included: VOCs and PAHs. Temporary
MW was installed due to visual indicators
for impacted soil.
Existing 10,000-gal
Gasoline UST, Former
Machine Shop

included: VOCs and PAHs.
Former North Scrap

Shed

included: PAHs and RCRA metals.
Former West Coal Bin

No. of
Bores
Sample
Quantities
(Depth)
Soil
GW
(12 feet)
2
(12 feet)
1
(12 feet)
3
(12 feet)
1
(4 feet)
1
(4 feet)
Location
Description
Sampling Rationale
No. of
Bores
(Depth)
Area 7
Area 8
Area 9
Area 10
Area 11
Area 12
Area 13
Area 14
Former East Coal Bin

(now in warehouse)

Former South Scrap

Shed

Former Paint Shop

included: VOCs and RCRA metals.
Former Oil House
Former Gasoline House

included: VOCs and PAHs.
included: Pb, VOCs and PAHs. Temporary
MW was installed due to visual indicators
for impacted soil.
Former PCB
Transformer Area

included: VOCs, PAHs, and PCBs.
Temporary MW was installed due to visual
indicators for impacted soil.
Former Machine Shop
Previously investigated by Ivertech in

2006, but no data was collected for PAHs
from hydraulic and lubricating oil. Analysis
included: PAHs.
Former Railway Power

House
No information available regarding

historical sampling events for impacts from
coal and oil. Historical activity at the site
included the use of coal and oil. Analysis
Former Geotechnical
Borings
No environmental screening data collected

during 2013 geotechnical investigation for
mechanical system construction. Three
additional borings were conducted to
supplement data from Areas 1 to 14 to
match previous geotechnical investigation.
Analysis included: VOCs, PAHs, and
RCRA metals.
Sample
Quantities
1
(4 feet)
2
(4 feet)
2
(12 feet)
1
(12 feet)
1
(12 feet)
1
(12 feet)
2
(12 feet)
1
(12 feet)
3
(12 feet)
Soil probe locations are shown on Figures 2 and 3.

Soil samples were collected for laboratory analysis from every probe, with the exception of
GP-24 which experienced refusal at 0.5 ft bgs due to a subsurface obstruction. Sample depth
was determined by observation of likely contaminated soil (staining, odor, slag, etc.) and
depth to groundwater (approximately 6 to 7 feet bgs). Laboratory reports and the chain-ofcustody forms are in Appendix D. Laboratory results for the soil samples are summarized in
Table 1.
Findings
Soil Texture
Soils were classified using the United Soil Classification System (USCS) and classifications
are listed on the boring logs in Appendix C. A description of soil textures by area is provided
in the following table:
Area
1
Description
Former Cistern
Probe #
GP-1 through
GP-3
General Soil Description

Black sandy fill with coal and slag from 0-2
ft bgs. Medium brown silty clay or sandy
clay from 2-6 ft bgs, and clayey sand and
gravel from 6-12 ft bgs. Groundwater
encountered at approximately 6 ft bgs.
Former Brass
Foundry
GP-4 and GP-5
Sand and slag fill from 0-2 ft bgs. Medium

brown clayey sand from 2-4 ft bgs, and
clayey sand and gravel from 4 to 12 ft bgs.
Groundwater encountered at approximately
6 ft bgs.
Former Oil
Dipping Rooms
GP-6
Asphalt and gravel fill from 0-1.5 ft bgs,

black fill from 1.5-2 ft bgs, medium brown
silty clay from 2-8 ft bgs, and sand and
gravel from 8-12 ft bgs. Groundwater
Existing
10,000-gal
Gasoline UST,
Former
Machine Shop
GP-7 through
GP-9
Asphalt and gravel fill from 0-2 ft bgs, pea

gravel from 2-11 ft bgs and medium brown
sand or clayey sand and gravel from 11-12
ft bgs around UST. Medium brown silty clay
from 3.5-4.5 ft bgs, and dark brown silty
clay from 4.5-5 ft bgs near pump island.
7.5 ft bgs.
Former North
Scrap Shed
GP-10
Medium brown silty clay from 0-1.5 ft bgs,

dark brown sandy fill from 1.5-2.5 ft bgs
and medium brown sand and gravel from
2.5-4 ft bgs.
Former West
Coal Bin
GP-11
Asphalt and gravel fill from 0-1 ft bgs, silty

clay with coal from 1-1.5 ft, gravel fill from
1.5-3.5 ft, and sand and gravel from 3.5-4 ft
bgs.
Former East
Coal Bin (now
in warehouse)
GP-12
Concrete and clayey sand or gravel fill from

0-2 ft bgs, black fill with coal from 2-3 ft,
medium brown clayey silt from 3-3.5 ft and
medium brown sand from 3.-5-4 ft bgs.
Former South
Scrap Shed
GP-13 and GP14
Dark brown fill and slag from 0-2 ft bgs with

medium brown sand and gravel from 2-4 ft
bgs.
Former Paint
Shop
GP-15 and GP16
Concrete and sand fill from 0-2 ft bgs, black

fill and coal from 2-3 ft, medium brown
Area
Description
Probe #

sandy clay from 3-6 ft, and sand and gravel
from 6-12 ft bgs. Groundwater encountered
at approximately 7 ft bgs.
10
Former Oil
House
GP-17
Asphalt and gravel fill from 0-2 ft bgs,

medium brown clayey sand with trace coal
from 2-6 ft, and medium brown sand from
6-12 ft bgs. Groundwater encountered at
approximately 7 ft bgs.
11
Former
Gasoline
House
GP-18
Asphalt and gravel fill from 0-2 ft bgs, black

sandy fill with coal from 2-6 ft bgs, and
medium brown clayey sand and gravel
from 6-9 ft bgs. Groundwater encountered
at approximately 6 ft bgs.
12
Former PCB
Transformer
Area
GP-19
Gravel fill from 0-1 ft bgs, black gravel fill

from 1-3 ft, medium brown clayey silt from
3-4.5 ft, sand and gravel from 4.5-6.5 ft,
sandy clay from 6.5-9 ft, peat from 9-10 ft,
medium brown sand from 10-11.5 ft and
peat from 11.5-12 ft bgs. Groundwater
13
Former
Machine Shop
GP-20 and GP21
GP-20: Concrete and medium brown silty

sand from 0-2.5 ft bgs, silty clay from 2.5-6
ft, and silty sand and gravel from 6-12 ft
bgs. Groundwater encountered at
GP-21: Concrete and medium brown sand
and gravel from 0-6 ft bgs. Silty sand and
gravel from 6-12 ft bgs.
14
Former
Railway Power
House
GP-22
Asphalt and black fill from 0-2.5 ft bgs,

medium brown silty clay from 2.5-4 ft,
reddish-brown sand from 4-5.5 ft, and
medium brown sand from 5.5-12 ft bgs.
6.5 ft bgs.
Former Geotech
Boring #11
Former
Geotechnical
Borings
GP-23
Concrete and sand fill from 0-2.5 ft bgs,

medium brown silty clay from 2.5-7 ft bgs,
and silty sand and gravel from 7-12 ft bgs.
Groundwater was encountered at
approximately 7.5 ft bgs.
Former Geotech
Boring #12
Former
Geotechnical
Borings
GP-24
No soil was sampled. The boring could not

be completed due to an obstruction in the
borehole.
Former Geotech
Boring #15
Former
Geotechnical
Borings
GP-25
Concrete and sand and gravel fill from 0-2

ft bgs, black fill from 2-3 ft, medium brown
sand from 3-6 ft and silty sand and gravel
from 6-12 ft bgs. Groundwater was
Area
Former Geotech
Boring #7
Description
Former
Geotechnical
Borings
Probe #
GP-26

Asphalt and gravel fill from 0-1.5 ft bgs,
black fill from 1.5-2 ft, medium brown silty
clay from 2-3 ft, reddish-brown sand from
3-7 ft and medium brown sand from 7-12 ft
bgs. Groundwater was encountered at
Soil Quality
Headspace Screening
PID readings were generally low (<10 instrument units (i.u.s.)) in soil probes, with the
exception of three probes. Elevated PID readings were recorded in GP-2 (60 i.u.s.) at 10-12
feet bgs in a layer of stained soil, GP-5 (62 i.u.s.) at 2-4 feet bgs, and GP-26 (38 i.u.s.) at
7.5-10 feet bgs. GP-2 was the only boring with observable soil staining and/or odor.
VOCs
With the exception of naphthalene in shallow soil (2-4 feet bgs) at GP-19, no VOCs were
detected in soil on the site. The naphthalene concentration was below the compound RCL. .
Table 1A provides a summary of VOCs analyzed in soil.
PAHs
Elevated concentrations of PAHs over residual contaminant levels (RCLs) from the USEPA
Regional Screening Level Calculator proposed for Chapter NR 720, Wisconsin
Administrative Code, were observed in 12 of 21 probe locations (GP-4, GP-5, GP-6, GP-10,
GP-11, GP-12, GP-13, GP-14, GP-17, GP-18, GP-19, and GP-22). PAHs were primarily
detected in shallow fill material on the site, from 0-4 feet bgs. Elevated levels of PAHs in
deeper soils (typically 5-7 feet bgs) were detected at GP-18. All locations with RCL
exceedances included exceedances for direct contact in a non-industrial setting, and 10 of
the locations exceeded RCLs for protection of groundwater (GP-5, GP-6, GP-10, GP-12, GP13, GP-14, GP-18, GP-19, and GP-22). PAH compounds in exceedance of direct contact
RCLs include benzo(a)anthracene, benzo(a)pyrene, benzo(b)fluoranthene,
benzo(k)fluoranthene, dibenz(a,h)anthracene and indeno(1,2,3-cd)pyrene. PAH compounds
in exceedance of protection of groundwater RCLs include benzo(a)pyrene,
benzo(b)fluoranthene, chrysene and naphthalene. Table 1B provides a summary of PAHs
analyzed in soil.
Metals
Several metals, including arsenic, cadmium, lead, mercury, selenium and silver were
detected in soil at levels exceeding RCLs. Elevated levels of metals were detected in 13 of
15 boring locations in shallow fill material from 0-4 feet bgs, with the exception of GP-18,
where lead in soil from 5-7 feet was found to exceed the RCL for protection of groundwater.
Elevated arsenic levels exceeding the Wisconsin background threshold value (BTV) were
observed at 6 of 15 boring locations (GP-1, GP-3, GP-5, GP-13, GP-14 and GP-16). A recent
study by the United States Geological Survey (USGS), Scientific Investigations Report
2011-5202 (pubs.usgs.gov/sir/2011/5202) researched naturally occurring arsenic
10
concentrations in surface soils in Wisconsin. Based on the findings of this study, the WDNR
Remediation and Redevelopment Program concluded that the data set in this report is of
sufficient scope and quality to establish a statewide soil arsenic BTV of 8 mg/kg.
Cadmium was found to exceed RCLs for protection of groundwater at GP-1, GP-11, GP-13,
and GP-14.
Lead was found to exceed RCLs for protection of groundwater at GP-1, GP-11, GP-12, GP13, GP-14, GP-15, GP-16, GP-18, GP-22, and GP-26, with exceedances for direct contact at
GP-13 and GP-14. Due to significantly higher concentrations of lead at GP-13 and GP-14
(404 mg/kg and 1190 mg/kg, respectively), soil samples from 1-2 feet bgs were analyzed
using the toxicity characteristic leaching procedure (TCLP) to determine if the soil may be
classified as characteristically hazardous. Neither sample indicated concentrations meeting
the TCLP lead threshold to be classified as characteristically hazardous. Slightly deeper soil
at these locations (2-4 feet bgs) was not found to contain metal concentrations over RCLs.
Selenium and mercury levels were found to exceed RCLs for protection of groundwater in
shallow soil at GP-5, and silver was found to exceed the RCL for the protection of
groundwater in shallow soil at GP-16.
Table 1C includes a summary of metals and TCLP analysis results in soil.
PCBs
No PCBs were detected in soil on the site, with the exception of GP-2 from 5-7 feet bgs.
Total PCBs were found to exceed the RCL for protection of groundwater. Table 1B includes
a summary of PCBs analyzed in soil.
A map depicting areas of regulatory exceedances in soil and groundwater is provided as
Figure 3.
Groundwater Quality
PAHs
PAHs were detected at levels of regulatory significance [above a Preventative Action Limit
(PAL) or Enforcement Standard (ES) in Ch. NR 140] in 6 of 10 temporary wells. The only
location which exceeded an NR 140 ES was GP-18, with ES exceedances for
benzo(a)pyrene, benzo(b)fluoranthene and chrysene. NR 140 PAL exceedances on the site
included benzo(a)pyrene, benzo(b)fluoranthene and chrysene in GP-1, GP-3, GP-20 and
GP-25. Benzo(b)fluoranthene and chrysene were above the PAL in GP-21. Table 2 includes
a summary of groundwater analytical results.
Metals
Arsenic, barium, cadmium, chromium, lead and mercury were detected at levels of regulatory
significance in 6 of 7 temporary wells sampled for lead or RCRA metals. Arsenic was above
the PAL in GP-2 and above the ES in GP-3 and GP-4. Barium was above the PAL in GP-3.
11
Cadmium was above the PAL in GP-3 and GP-4. Chromium was above the ES in GP-3 and
the PAL in GP-4. Lead was above the ES in GP-3, GP-4, GP-16, GP-18 and GP-26. Mercury
was above the PAL in GP-3, but was not detected in other temporary wells.
PCBs
No PCBs were detected in groundwater from any of the four temporary wells analyzed.
12
Conclusions
This Phase II ESA investigated the potential for soil contamination associated with RECs
primarily related to the historical operation of electric motor and machine manufacturing
companies, including a machine shop, paint shop, brass foundry, and loading/unloading
activities from adjacent railroad spurs. We conclude the following:
The majority of the site contains a layer of fill material on average from 0-3 feet bgs
which demonstrates dark discoloration and contains detectable levels of PAHs and
metals (arsenic, cadmium, and lead) in exceedance of RCLs listed in the USEPA
Regional Screening Level Web-Calculator. Arsenic concentrations were compared to
a BTV of 8 parts per million, which is endorsed by the WDNR based on data provided
in a study published by the USGS titled Distribution and Variation of Arsenic in
Wisconsin Soils, With Data on Other Trace Elements (February 2013).
An undefined area of groundwater across the site appears to be impacted by lead.

Other metals compounds were detected at levels exceeding the NR 140 ES in the
courtyard area.
The highest detected levels of lead were identified in Area 8, Former South Scrap
Shed. Based on TCLP testing, the soil has been determined to be non-hazardous.
Elevated levels of PAHs are present in Area 12 Former PCB Transformer. Shallow
soils (2-4 feet bgs) at this location display higher PAH concentrations than other
areas of fill around the site, and several PAH compounds exceed RCLs for protection
of groundwater.
Although PCBs were detected in one soil boring in the courtyard, there no
groundwater impacts from PCBs were detected in the area.
13
Recommendations
Because several metals and PAH compounds above regulatory standards were indicated at
the site and have not been documented to have been previously investigated, we
recommend that the site owner submit this report to the WDNR for review prior to beginning
construction at the property.
Development plans for the new SAPF are currently being prepared. DFD has indicated that
impacted soils will remain on site, during and following construction, and will be managed
long-term through construction of an engineered cap. A cap maintenance plan will be
developed and implemented at the site. Details of the cap maintenance plan should be
submitted to the WDNR for review and approval prior to construction of the new facility.
DFD will conduct building demolition and utility removal activities in the fall/winter of 2013 to
prepare the site for new construction. Because these activities will likely expose areas of
impacted soils, we recommend that DFD develop separate Soils Management Plans for the
demolition phase and construction phase of the project to appropriately manage impacted
soils identified in the Phase II ESA.
Standard of Care
This Phase II ESA investigation report is based on data obtained by Ayres Associates and
other contractors associated with the property through placement of soil probes, temporary
wells and collection and analysis of soil and groundwater samples. Soil qualities reported
apply only to the specific locations and times at which the work was performed.
Conclusions and recommendations made represents our professional engineering judgment
in interpreting these data, as well as data obtained from reports prepared by others relative
to soil conditions in the study area. Data, computations, and correspondence supporting the
information presented in this report are kept on file by Ayres Associates.
14
Figures
Approximate Site Location
Source: USGS Quadrangle 7.5

Minute Series, Madison East, 1983
1 = 2000
Figure 1 Site Location Map

202 S. Thornton Ave.
Madison, Wisconsin
19-0291.20
RAILROAD
5
GP-7
GP-8
12
S.DI
CKI
NSON ST.
GP-9
4
GP-19
GP-15
11
GP-16
GP-17
9
GP-11
GP-18
10
GP-6
GP-1
GP-23
GP-26
GP-12
1
GP-2
GP-3
TH
KE PA
I
VER B
I
R
E
R
YAHA
GP-10
GP-4
GP-5
GP-25
2
GP-20
13
GP-21
GP-22
GP-13
GP-14
14
LEGEND
V:
\ENV\CAD\W isconsin DOA\SITE SLM .
dgn
W:
\Bentley_V8i\W orkSpace\Projects\Engineering_Services\pltcfg\ES_text_sub.
tbl
W:
\Bentley_V8i\W orkSpace\Standards\pltcfg\Ayres_pdf.
pltcfg
7/19/2013
CAPITAL CITY TRAIL
N
O
GP-11
GEOPROBE LOCATION (JUNE 13-14, 2013)
GP-2
GEOPROBE/ TEMP WELL LOCATION (JUNE 13-14, 2013)
BOOK NO.
DR.BY
JOB NO.
SCALE
JULY 2013
202 S. THORNTON AVENUE
19-0291.20
M. BANACH
DATE
AS SHOWN
NO.
DATE
REVISION
MADISON, WISCONSIN
60
RECOGNIZED ENVIRONMENTAL
CONDITION LOCATION
DRAWING NO.
PHASE II ENVIRONMENTAL SITE ASSESSMENT
T. SHUPERT
CHK.BY
R
T
H
SAMPLE LOCATION MAP

ASSOCIATES
Eau Claire, Wisconsin
RAILROAD
GP-8
GP-7
S.DI
CKI
NSON ST.
4
GP-19
GP-9
GP-16
11
GP-17
GP-15
GP-11
GP-18
10
GP-6
GP-1
GP-23
GP-26
GP-12
3
GP-24
1
GP-2
GP-3
TH
KE PA
I
VER B
I
R
E
R
YAHA
GP-10
GP-4
GP-5
GP-25
2
GP-20
13
GP-21
GP-22
GP-13
14
GP-14
N
O
LEGEND
R
T
H
GP-11
GEOPROBE LOCATION (JUNE 13-14, 2013)
60
GP-2
V:
\ENV\CAD\W isconsin DOA\Regulatory Exceedance.
dgn
W:
\Bentley_V8i\W orkSpace\Projects\Engineering_Services\pltcfg\ES_text_sub.
tbl
W:
\Bentley_V8i\W orkSpace\Standards\pltcfg\Ayres_pdf.
pltcfg
7/19/2013
CAPITAL CITY TRAIL
GEOPROBE/ TEMP WELL LOCATION (JUNE 13-14, 2013)

NO RESIDUAL CONTAMINANT LEVEL EXCEEDANCE IN SOIL
NO ENFORCEMENT STANDARD EXCEEDANCE IN GROUNDWATER
PROTECTION OF GROUNDWATER RESIDUAL CONTAMINANT LEVEL EXCEEDANCE
DIRECT CONTACT RESIDUAL CONTAMINANT LEVEL EXCEEDANCE
ENFORCEMENT STANDARD EXCEEDANCE IN GROUNDWATER
BOOK NO.
DR.BY
JOB NO.
SCALE
JULY 2013
202 S. THORNTON AVENUE
19-0291.20
M. BANACH
DATE
DRAWING NO.
T. SHUPERT
CHK.BY
AS SHOWN
NO.
DATE
REVISION
MADISON, WISCONSIN
REGULATORY EXCEEDANCE MAP

ASSOCIATES
Eau Claire, Wisconsin
Tables
Table 1A
VOLATILE ORGANIC COMPUNDS (VOCs) IN SOIL
202 SOUTH THORNTON AVENUE, MADISON, WI
Parameter
Units
DC
GW
GP-6(D) GP-6(S)
Sample Date 6/14/13

Sample Depth
5-7
GP-7
GP-8
GP-9
GP-15
GP-16
GP-19
GP-26
6/14/13
6/14/13
6/14/13
6/14/13
6/13/13
6/13/13
GP-17(D) GP-17(S)
6/13/13
6/13/13
GP-18(D) GP-18(S)
6/13/13
6/13/13
6/13/13
6/14/13
1-3
10-12
6-8
4-5
2-4
2-4
5-7
2-4
5-7
2-4
2-4
5-7
Method EPA 8260

1,1,1,2-Tetrachloroethane
mg/kg
2.59
0.0533
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
1,1,1-Trichloroethane
mg/kg
640
0.1402
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
mg/kg
0.753
0.0002
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
mg/kg
1.42
0.0032
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
1,1-Dichloroethane
mg/kg
4.72
0.4836
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
1,1-Dichloroethene
mg/kg
342
0.005
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
1,1-Dichloropropene
mg/kg
NA
NA
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
1,2,3-Trichlorobenzene
mg/kg
243
NA
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
1,2,3-Trichloropropane
mg/kg
0.005
NA
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
mg/kg
22.1
0.408
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
1,2,4-Trimethylbenzene
mg/kg
89.8
1.3793
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
1,2-Dibromo-3-chloropropane
mg/kg
0.008
0.0002
<0.0498
<0.0498
<0.0498
<0.0498
<0.0498
<0.0498
<0.0498
<0.0498
<0.0498
<0.0498
<0.0498
<0.0498
<0.0498
1,2-Dibromoethane (EDB)
mg/kg
0.047
0.0000282
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
1,2-Dichlorobenzene
mg/kg
193
1.168
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
1,2-Dichloroethane
mg/kg
0.608
0.0028
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
1,2-Dichloropropane
mg/kg
1.33
0.0033
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
mg/kg
182
1.3793
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
1,3-Dichlorobenzene
mg/kg
297
1.1522
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
1,3-Dichloropropane
mg/kg
1490
NA
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
1,4-Dichlorobenzene
mg/kg
3.48
0.144
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
2,2-Dichloropropane
mg/kg
527
NA
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
2-Chlorotoluene
mg/kg
907
NA
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
4-Chlorotoluene
mg/kg
253
NA
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
Benzene
mg/kg
1.49
0.0051
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
Bromobenzene
mg/kg
354
NA
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
Bromochloromethane
mg/kg
232
NA
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
Bromodichloromethane
mg/kg
0.39
NA
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
Bromoform
mg/kg
61.6
0.0023
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
Bromomethane
mg/kg
10.3
0.0051
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
Carbon tetrachloride
mg/kg
0.854
0.0039
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
Chlorobenzene
mg/kg
392
NA
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
Chloroethane
mg/kg
NA
0.2266
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
Chloroform
mg/kg
0.423
0.0033
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
Chloromethane
mg/kg
171
0.0155
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
Dibromochloromethane
mg/kg
0.933
0.032
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
Dibromomethane
mg/kg
35
NA
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
Dichlorodifluoromethane
mg/kg
135
3.0825
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
Diisopropyl ether
mg/kg
2260
NA
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
Ethylbenzene
mg/kg
7.47
1.57
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
Hexachloro-1,3-butadiene
mg/kg
6.23
NA
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
Isopropylbenzene (Cumene)
mg/kg
268
NA
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
Methyl-tert-butyl ether
mg/kg
59.4
0.027
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
Methylene Chloride
mg/kg
60.7
0.0026
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
Naphthalene
mg/kg
5.15
0.6587
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
0.0649 J
<0.0250
Styrene
mg/kg
867
0.22
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
Tetrachloroethene
mg/kg
30.7
0.0045
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
Toluene
mg/kg
818
1.1072
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
Trichloroethene
mg/kg
0.644
0.0036
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
Trichlorofluoromethane
mg/kg
1120
NA
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
Vinyl chloride
mg/kg
0.067
0.0001
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
cis-1,2-Dichloroethene
mg/kg
156
0.0412
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
cis-1,3-Dichloropropene
mg/kg
1220
NA
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
m&p-Xylene
mg/kg
388/390
3.94
<0.0500
<0.0500
<0.0500
<0.0500
<0.0500
<0.0500
<0.0500
<0.0500
<0.0500
<0.0500
<0.0500
<0.0500
<0.0500
n-Butylbenzene
mg/kg
108
NA
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
n-Propylbenzene
mg/kg
NA
NA
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
o-Xylene
mg/kg
434
3.94
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
p-Isopropyltoluene
mg/kg
162
NA
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
sec-Butylbenzene
mg/kg
145
NA
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
tert-Butylbenzene
mg/kg
183
NA
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
trans-1,2-Dichloroethene
mg/kg
211
0.0588
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
trans-1,3-Dichloropropene
mg/kg
1570
0.0003
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
<0.0250
NA = Not Applicable
Bold exceeds WDNR RR Spreadsheet values for Direct Contact (non-industrial) (DC), adopted from USEPA Regional Screening Level Calculator proposed for WI NR 720
Italic exceeds WDNR RR Spreadsheet values for Protection of Groundwater (GW), adopted from USEPA Regional Screening Level Calculator proposed for WI NR 720
Table 1B
POLYCLYCLIC AROMATIC HYDROCARBONS (PAHs) IN SOIL
Parameter
Units
DC
GW
GP-1
GP-2(D)
GP-2
GP-3
GP-4
GP-5
GP-6(D)
GP-6(S)
GP-7
GP-8
GP-9
GP-10
GP-11
GP-12
GP-13
GP-14
GP-17(D)
GP-17(S)
GP-18(D)
GP-18(S)
GP-19
GP-20
GP-21
GP-22
GP-26
Sample Date
6/14/13
6/14/13
6/14/13
6/14/13
6/14/13
6/14/13
6/14/13
6/14/13
6/14/13
6/14/13
6/14/13
6/14/13
6/14/13
6/14/13
6/14/13
6/14/13
6/13/13
6/13/13
6/13/13
6/13/13
6/13/13
6/13/13
6/13/13
6/14/13
6/14/13
Sample Depth
0-2
10-12
0-2
5-7
0-2
1-2
5-7
1-3
10-12
6-8
4-5
1-3
1-2
2-3
1-2
1-2
5-7
2-4
5-7
2-4
2-4
5-6
5-6
1-3
5-7
<0.0033
Method EPA 8270 by SIM

1-Methylnaphthalene
mg/kg
15.6
NA
<0.0035
<0.0033
<0.0034
<0.0034
0.0365
0.120
<0.0036
0.0093 J
<0.0034
<0.0036
<0.0035
0.0110 J
0.0092 J
0.144
0.414 J
0.169 J
<0.0034
<0.0034
0.0486
0.0747
0.882 J
<0.0034
<0.0032
0.0895
2-Methylnaphthalene
mg/kg
229
NA
<0.0098
<0.0093
<0.0097
<0.0097
0.0389
0.131
<0.0102
<0.0200
<0.0096
<0.0102
<0.0100
<0.0099
<0.0111
0.183
<0.393
<0.382
<0.0095
<0.0097
0.0560
0.0795
0.502 J
<0.0096
<0.0091
0.137
<0.0093
Acenaphthene
mg/kg
3440
NA
<0.0098
<0.0093
<0.0097
<0.0097
<0.0102
0.232
<0.0102
<0.0200
<0.0096
<0.0102
<0.0100
0.0206
<0.0111
<0.0095
0.393 J
0.798
<0.0095
<0.0097
0.0250
0.0173 J
1.02
<0.0096
<0.0091
<0.0091
<0.0093
Acenaphthylene
mg/kg
NA
NA
<0.0098
<0.0093
<0.0097
<0.0097
<0.0102
<0.0593
<0.0102
0.141
<0.0096
<0.0102
<0.0100
0.0162 J
<0.0111
0.0180 J
0.588 J
<0.382
<0.0095
<0.0097
<0.0107
0.0237
<0.481
<0.0096
<0.0091
0.0292
<0.0093
Anthracene
mg/kg
17,200
196.7442
<0.0098
<0.0093
<0.0097
<0.0097
0.0173 J
0.693
<0.0102
0.0806
<0.0096
<0.0102
<0.0100
0.102
0.0185 J
0.0401
1.71
2.34
<0.0095
0.0110 J
0.0844
0.0691
3.49
<0.0096
<0.0091
0.0248
<0.0093
Benzo(a)anthracene
mg/kg
0.148
NA
<0.0098
<0.0093
<0.0097
<0.0097
0.0339
0.915
<0.0102
0.237
<0.0096
<0.0102
<0.0100
0.285
0.0893
0.0962
3.61
3.16
<0.0095
0.0250
0.136
0.176
6.24
<0.0096
<0.0091
0.125
<0.0093
Benzo(a)pyrene
mg/kg
0.015
0.47
<0.0035
<0.0033
<0.0035
<0.0034
0.0366
0.858
0.0100 J
0.252
<0.0034
<0.0036
<0.0036
0.384
0.132
0.0624
3.58
3.29
<0.0034
0.0251
0.133
0.188
6.06
<0.0034
<0.0032
0.184
<0.0033
Benzo(b)fluoranthene
mg/kg
0.148
0.48
<0.0098
<0.0093
<0.0097
<0.0097
0.0491
1.12
0.0116 J
0.285
<0.0096
<0.0102
<0.0100
0.470
0.133
0.0914
4.71
4.29
<0.0095
0.0363
0.149
0.153
7.46
<0.0096
<0.0091
0.257
<0.0093
Benzo(g,h,i)perylene
mg/kg
NA
NA
<0.0098
<0.0093
<0.0097
<0.0097
0.0313
0.560
<0.0102
0.247
<0.0096
<0.0102
<0.0100
0.283
0.102
0.0524
2.29
2.18
<0.0095
0.0153 J
0.0751
0.118
3.75
<0.0096
<0.0091
0.134
<0.0093
Benzo(k)fluoranthene
mg/kg
1.48
NA
<0.0035
<0.0033
<0.0034
<0.0034
0.0271
0.585
0.0092 J
0.153
<0.0034
0.0044 J
<0.0035
0.328
0.0895
0.0690
2.12
2.34
<0.0034
0.0149 J
0.109
0.176
3.88
<0.0034
<0.0032
0.186
<0.0033
Chrysene
mg/kg
14.8
0.1451
<0.0098
<0.0093
<0.0097
<0.0097
0.0657
1.18
0.0128 J
0.314
<0.0096
<0.0102
<0.0100
0.392
0.132
0.239
4.93
4.73
<0.0095
0.0364
0.181
0.237
8.09
<0.0096
<0.0091
0.228
<0.0093
Dibenz(a,h)anthracene
mg/kg
0.015
NA
<0.0098
<0.0093
<0.0097
<0.0097
0.0123 J
0.165
<0.0102
0.0741
<0.0096
<0.0102
<0.0100
0.103
0.0241
0.0289
0.827
0.565 J
<0.0095
<0.0097
0.0296
0.0449
1.37
<0.0096
<0.0091
0.0525
<0.0093
Fluoranthene
mg/kg
2290
88.8179
<0.0098
<0.0093
<0.0097
<0.0097
0.0490
2.52
0.0136 J
0.383
<0.0096
<0.0102
<0.0100
0.510
0.194
0.0997
9.87
10.6
<0.0095
0.0609
0.316
0.369
16.7
<0.0096
<0.0091
0.171
<0.0093
Fluorene
mg/kg
2290
14.8148
<0.0098
<0.0093
<0.0097
<0.0097
<0.0102
0.268
<0.0102
<0.0200
<0.0096
<0.0102
<0.0100
0.0208
<0.0111
<0.0095
1.02
0.860
<0.0095
<0.0097
0.0250
0.0149 J
1.25
<0.0096
<0.0091
<0.0091
<0.0093
Indeno(1,2,3-cd)pyrene
mg/kg
0.148
NA
<0.0098
<0.0093
<0.0097
<0.0097
0.0230
0.487
<0.0102
0.174
<0.0096
<0.0102
<0.0100
0.252
0.0819
0.0304
2.01
1.92
<0.0095
0.0141 J
0.0676
0.101
3.46
<0.0096
<0.0091
0.112
<0.0093
Naphthalene
mg/kg
5.15
0.6587
<0.0098
<0.0093
<0.0097
<0.0097
0.0197 J
0.593
<0.0102
<0.0200
<0.0096
<0.0102
<0.0100
0.0114 J
0.0214 J
0.0932
<0.393
1.01
<0.0095
<0.0097
0.0438
0.0448
1.62
<0.0096
<0.0091
0.248
<0.0093
Phenanthrene
mg/kg
NA
NA
<0.0098
<0.0093
<0.0097
<0.0097
0.0780
2.38
<0.0102
0.212
<0.0096
<0.0102
<0.0100
0.313
0.140
0.280
9.47
9.56
<0.0095
0.0381
0.367
0.335
18.1
<0.0096
<0.0091
0.136
<0.0093
Pyrene
mg/kg
1720
54.4725
<0.0098
<0.0093
<0.0097
<0.0097
0.0531
1.99
0.0136 J
0.596
<0.0096
<0.0102
<0.0100
0.449
0.200
0.112
7.70
7.80
<0.0095
0.0482
0.271
0.391
14.2
<0.0096
<0.0091
0.179
<0.0093
NA = Not Applicable
mg/L & mg/kg = PPM
Table 1C
METALS IN SOIL
Parameter
Units
DC
GW
TCLP
GP-1
GP-2
GP-3
GP-4
GP-5
GP-10
GP-11
GP-12
GP-13
GP-14
GP-15
GP-16
GP-18(D) GP-18(S)
Sample Date 6/14/13 6/14/13 6/14/13 6/14/13 6/14/13 6/14/13 6/14/13 6/14/13 6/14/13 6/14/13 6/14/13 6/14/13 6/14/13 6/13/13 6/13/13 6/13/13
Sample Depth
0-2
0-2
1-2
0-2
1-2
2-4
1-3
1-2
2-3
1-2
2-4
1-2
2-4
2-4
2-4
4-6
6/13/13
6/13/13
5-7
2-4
GP-22
GP-26
6/14/13 6/14/13
1-3
1-2
Method EPA 6010

Arsenic
mg/kg
0.39 (8*)
0.584 (8*)
NA
50.6
6.4
8.6
5.6
24.5
5.00
2.6
4.9
4.7
19.0
2.1
15.4
2.0 J
7.3
14.2
3.2
5.8
7.1
Barium
mg/kg
15,300
164.8
NA
96.6
72.1
68.7
54.7
24.3
14.6
101
124
85.8
134
72.4
65.3
45.4
60.8
Cadmium
mg/kg
70.2
0.752
NA
1.8
0.19 J
0.41 J
0.39 J
0.68
0.23 J
0.78
0.32 J
3.1
2.1
0.72
2.9
0.61
0.37 J
Chromium
mg/kg
100,000
360,000
NA
23.4
17.9
13.5
13.6
15.4
5.8
14.3
12.1
30.9
13.8
19.8
9.6
14.7
13.4
Lead
mg/kg
400
27
NA
310
8.9
25.6
11.7
21.2
6.9
69.9
200
404
2.5
1190
3.6
66.4
99.9
99.8
152
82.7
186
Selenium
mg/kg
391
0.52
NA
<0.68
<0.58
<0.61
<0.67
1.8 J
<0.64
<0.68
<0.67
<0.66
<0.61
<0.67
<0.66
<0.55
<0.62
Silver
mg/kg
391
0.8497
NA
0.30 J
<0.21
<0.22
<0.24
0.32 J
<0.23
<0.25
<0.24
0.47 J
0.43 J
<0.24
1.2
<0.20
<0.22
3.13
0.208
NA
0.11
0.039
0.012
0.023
0.45
0.024
0.10
0.021
0.10
0.068
0.033
0.10
0.070
0.036
0.088
0.34
Method EPA 7471

Mercury
mg/kg
Method EPA 1311 - Toxicity Characteristic Leaching Procedure

Lead
mg/L
NA
NA
* WDNR utilizes Background Threshold Value of 8ppm based on 2012 USGS Report.
- not analyzed
NA - not applicable
TCLP - toxicity characteristic leaching procedure; regulatory standards from WI NR 661, Table 2
Table 1D
POLYCHLORINATED BIPHENYLS (PCBs) IN SOIL
Parameter
Units
DC
GW
GP-1
Sample Date 6/14/13

Sample Depth
5-7
GP-2
GP-3
GP-4
GP-5
GP-19
6/14/13
6/14/13
6/14/13
6/14/13
6/14/13
6/13/13
0-2
5-7
5-7
5-7
1-2
1-3
Method EPA 8082

PCB, Total
mg/kg
0.222
0.0094
<0.0294 <0.0343
0.125
<0.0290 <0.0305 <0.0356 <0.0289
PCB-1016 (Aroclor 1016)
mg/kg
3.93
NA
<0.0294 <0.0343
<0.0291
<0.0290 <0.0305 <0.0356 <0.0289
mg/kg
0.159
NA
<0.0294 <0.0343
<0.0291
<0.0290 <0.0305 <0.0356 <0.0289
mg/kg
0.159
NA
<0.0294 <0.0343
<0.0291
<0.0290 <0.0305 <0.0356 <0.0289
mg/kg
0.222
NA
<0.0294 <0.0343
<0.0291
<0.0290 <0.0305 <0.0356 <0.0289
mg/kg
0.222
NA
<0.0294 <0.0343
<0.0291
<0.0290 <0.0305 <0.0356 <0.0289
mg/kg
0.222
NA
<0.0294 <0.0343
0.0834
<0.0290 <0.0305 <0.0356 <0.0289
mg/kg
0.222
NA
<0.0294 <0.0343
0.0417 J <0.0290 <0.0305 <0.0356 <0.0289
Bold exceeds WDNR RR Spreadsheet values for Direct Contact (non-industrial) (DC), adopted from USEPA Regional Screening
Level Calculator proposed for WI NR 720
Italic exceeds WDNR RR Spreadsheet values for Protection of Groundwater (GW), adopted from USEPA Regional Screening Level
Calculator proposed for WI NR 720
NA - not applicable
Table 2
SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
PHASE II ENVIRONMETNAL SITE ASSESSMENT
202 SOUTH THORNTON AVENUE, MADISON, WISCONSIN
Parameter
Units
WI NR 140 GW Quality
Preventive Action Limits
WI NR 140 GW Quality
Enforcement Standards
Sample Date
GP-1
6/14/13
GP-20
GP-21
GP-23
GP-25
GP-26
6/14/13 6/14/13 6/14/13 6/14/13 6/14/13 6/14/13 6/14/13
GP-2
GP-3
GP-4
GP-6
GP-16
GP-18
6/14/13
6/14/13
6/14/13
6/14/13
Method EPA 6010

Arsenic, Dissolved
ug/L
10
Barium, Dissolved
ug/L
400
2000
<4.2
62.5
5.0
61.8
Cadmium, Dissolved
ug/L
.5
Chromium, Dissolved
ug/L
10
Lead, Dissolved
ug/L
Selenium, Dissolved
Silver, Dissolved
69.7
11.2
160
<0.48
2.9 J
<0.48
100
<1.4
4.6
1.2
184
36.5
1.5
15
<2.7
<2.7
81.0
35.5
45.4
38.4
<5.2
15.1
6.7 J
ug/L
10
50
<5.2
<5.2
ug/L
10
50
<1.7
<1.7
<1.7
3.0 J
ug/L
.2
<0.10
<0.10
0.34
<0.10
PCB, Total
ug/L
.003
.03
ug/L
N/A
N/A
<0.29
<0.28
<0.27
<0.31
<0.29
<0.28
<0.27
<0.31
ug/L
N/A
N/A
<0.29
<0.28
<0.27
<0.31
ug/L
ug/L
N/A
N/A
<0.29
<0.28
<0.27
<0.31
N/A
N/A
<0.29
<0.28
<0.27
<0.31
ug/L
N/A
N/A
<0.29
<0.28
<0.27
<0.31
ug/L
N/A
N/A
<0.29
<0.28
<0.27
<0.31
ug/L
N/A
N/A
<0.29
<0.28
<0.27
<0.31
596
Method EPA 7470

Mercury, Dissolved
Method EPA 8082
Method EPA 8270 by HVI

1-Methylnaphthalene
ug/L
N/A
N/A
0.011 J
0.015 J
0.0093 J
0.015 J
0.050
0.061 J
0.012 J
0.021 J
0.015 J
0.036 J
2-Methylnaphthalene
ug/L
N/A
N/A
0.015 J
0.021 J
0.014 J
0.029 J
0.025 J
0.068 J
0.020 J
0.036 J
0.032 J
0.051
Acenaphthene
ug/L
N/A
N/A
0.0095 J
0.0060 J
0.10 J
N/A
N/A
<0.0035
0.25 J
Anthracene
ug/L
600
3000
<0.0038
0.016 J
0.0049 J 0.0041 J <0.0039 0.027 J

<0.0035 0.0042 J <0.0035 0.0082 J
ug/L
<0.0042
0.0051 J
<0.0038
Acenaphthylene
<0.0039
0.0037 J
<0.0052
<0.0048
1.0
0.012 J
0.022 J
0.0051 J
0.032 J
0.025 J
0.032 J
0.0082 J
0.044 J
<0.0049
<0.0038
0.011 J
Benzo(a)anthracene
ug/L
N/A
N/A
0.029 J
<0.0048
0.034 J
<0.0051
<0.0047
1.6
Benzo(a)pyrene
ug/L
.02
.2
0.027
<0.0050
0.031
<0.0053
<0.0049
1.3
0.022
0.010 J
0.0057 J
0.040
ug/L
.02
.2
<0.0068
<0.0067
N/A
N/A
<0.0081
<0.0087
<0.0080
0.98
0.71
0.038
0.020 J
0.048
0.026 J
<0.0068
ug/L
0.032
0.023 J
<0.0073
0.026
0.020 J
0.043
0.027 J
ug/L
N/A
N/A
0.022 J
<0.010
0.031 J
<0.011
<0.010
1.1
0.034 J
ug/L
.02
.2
<0.0062
0.041
<0.0067
<0.0062
ug/L
N/A
N/A
<0.0055
ug/L
80
400
0.077
3.0
0.13
Fluorene
ug/L
80
400
<0.0052
0.0096 J 0.0056 J
<0.0059 <0.0054
0.0065 J 0.0082 J
0.054
0.012 J
Fluoranthene
<0.0059
0.079
1.5
0.23 J
0.035
0.0078 J
0.037 J
<0.010
0.013 J
0.048
0.066
0.0083 J 0.0093 J <0.0055
0.065
0.19
0.017 J
0.040 J
Chrysene
0.0054 J
<0.0042
0.0047 J
0.37 J
0.0071 J
0.013 J
0.0043 J
0.027 J
ug/L
N/A
N/A
0.016 J
0.018 J
0.018 J
0.021 J
100
0.049 J
0.049
0.095 J
0.041 J
0.038 J
<0.0059
0.050
0.023 J
10
<0.0058
0.024 J
0.64
ug/L
<0.0063
0.095
Naphthalene
<0.0059
0.072
0.16
0.013 J
0.062
0.0095 J
0.018 J
2.9
0.073
0.15
0.024 J
0.18
<0.0053
0.081
0.0081 J 0.0094 J
2.8
0.062
0.18
0.019 J
0.13
Phenanthrene
ug/L
N/A
N/A
0.069
Pyrene
ug/L
50
250
0.074
N/A = Not Applicable

ug/L & ug/kg = PPB
- not analyzed
Bold values exceed NR 140 ES
Italic values exceed NR 140 PAL
<0.0081
Appendix A
Phase I ESA Sanborn Maps
State Preservation Storage Facility

202 S Thornton
Madison, WI 53703
Inquiry Number: 3613445.3
May 22, 2013
Certified Sanborn Map Report
Certified Sanborn Map Report

Site Name:
State Preservation Storage
202 S Thornton
Madison, WI 53703
Client Name:
Ayres Associates
1802 Pankratz Street
Madison, WI 53704
EDR Inquiry # 3613445.3
Contact: Tom Gaieck
5/22/13
The complete Sanborn Library collection has been searched by EDR, and fire insurance maps covering the target
property location provided by Ayres Associates were identified for the years listed below. The certified Sanborn Library
search results in this report can be authenticated by visiting www.edrnet.com/sanborn and entering the certification
number. Only Environmental Data Resources Inc. (EDR) is authorized to grant rights for commercial reproduction of
maps by Sanborn Library LLC, the copyright holder for the collection.
Certified Sanborn Results:

Site Name:
Address:
City, State, Zip:
Cross Street:
P.O. #
Project:
Certification #

202 S Thornton
Madison, WI 53703
NA
8.19
018D-4119-911F
Maps Provided:
Sanborn Library search results

Certification # 018D-4119-911F
The Sanborn Library includes more than 1.2 million

Sanborn fire insurance maps, which track historical
property usage in approximately 12,000 American
cities and towns. Collections searched:
1986
1950
1942
1908
Library of Congress
1902
University Publications of America
1898
EDR Private Collection

The Sanborn Library LLC Since 1866
Limited Permission To Make Copies

Ayres Associates (the client) is permitted to make up to THREE photocopies of this Sanborn Map transmittal and each fire insurance map
accompanying this report solely for the limited use of its customer. No one other than the client is authorized to make copies. Upon request made
directly to an EDR Account Executive, the client may be permitted to make a limited number of additional photocopies. This permission is
conditioned upon compliance by the client, its customer and their agents with EDR's copyright policy; a copy of which is available upon request.
Disclaimer - Copyright and Trademark notice

This Report contains certain information obtained from a variety of public and other sources reasonably available to Environmental Data Resources, Inc. It cannot be
concluded from this Report that coverage information for the target and surrounding properties does not exist from other sources. NO WARRANTY EXPRESSED OR
IMPLIED, IS MADE WHATSOEVER IN CONNECTION WITH THIS REPORT. ENVIRONMENTAL DATA RESOURCES, INC. SPECIFICALLY DISCLAIMS THE
MAKING OF ANY SUCH WARRANTIES, INCLUDING WITHOUT LIMITATION, MERCHANTABILITY OR FITNESS FOR A PARTICULAR USE OR PURPOSE. ALL
RISK IS ASSUMED BY THE USER. IN NO EVENT SHALL ENVIRONMENTAL DATA RESOURCES, INC. BE LIABLE TO ANYONE, WHETHER ARISING OUT OF
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INCIDENTAL CONSEQUENTIAL, OR EXEMPLARY DAMAGES. ANY LIABILITY ON THE PART OF ENVIRONMENTAL DATA RESOURCES, INC. IS STRICTLY
LIMITED TO A REFUND OF THE AMOUNT PAID FOR THIS REPORT. Purchaser accepts this Report "AS IS". Any analyses, estimates, ratings, environmental risk
levels or risk codes provided in this Report are provided for illustrative purposes only, and are not intended to provide, nor should they be interpreted as providing
any facts regarding, or prediction or forecast of, any environmental risk for any property. Only a Phase I Environmental Site Assessment performed by an
environmental professional can provide information regarding the environmental risk for any property. Additionally, the information provided in this Report is not to be
construed as legal advice.
Copyright 2013 by Environmental Data Resources, Inc. All rights reserved. Reproduction in any media or format, in whole or in part, of any report or map of
Environmental Data Resources, Inc., or its affiliates, is prohibited without prior written permission.
EDR and its logos (including Sanborn and Sanborn Map) are trademarks of Environmental Data Resources, Inc. or its affiliates. All other trademarks used herein are
the property of their respective owners.
3613445 - 3
page 2
Sanborn Sheet Thumbnails

This Certified Sanborn Map Report is based upon the following Sanborn
Fire Insurance map sheets.
1986 Source Sheets
Volume 1, Sheet 79
Volume 1, Sheet 81
1950 Source Sheets
Volume 1, Sheet 79
Volume 1, Sheet 81
1942 Source Sheets
Volume 1, Sheet 79
Volume 1, Sheet 81
1908 Source Sheets
Volume 1, Sheet 3
Volume 1, Sheet 4
3613445 - 3
page 3
1902 Source Sheets
Volume 1, Sheet 17
Volume 1, Sheet 19
1898 Source Sheets
Volume 1, Sheet 27
3613445 - 3
page 4
018D-4119-911F
1986 Certified Sanborn Map
Site Name:
Address:

202 S Thornton
City, ST, ZIP:
Madison WI 53703
Client:
Ayres Associates
EDR Inquiry:
Order Date:
Certification #
3613445.3
5/22/2013 1:03:00 PM
018D-4119-911F
Copyright:
This Certified Sanborn Map combines the following sheets.

Outlined areas indicate map sheets within the collection.
0 Feet
150
1986
300
600
Volume 1, Sheet 79
Volume 1, Sheet 81
3613445 - 3
page 5
018D-4119-911F
Site Name:
Address:

202 S Thornton
City, ST, ZIP:
Madison WI 53703
Client:
Ayres Associates
EDR Inquiry:
Order Date:
Certification #
3613445.3
5/22/2013 1:03:00 PM
018D-4119-911F
Copyright:

0 Feet
150
1950
300
600
Volume 1, Sheet 79
Volume 1, Sheet 81
3613445 - 3
page 6
018D-4119-911F
Site Name:
Address:

202 S Thornton
City, ST, ZIP:
Madison WI 53703
Client:
Ayres Associates
EDR Inquiry:
Order Date:
Certification #
3613445.3
5/22/2013 1:03:00 PM
018D-4119-911F
Copyright:

0 Feet
150
1942
300
600
Volume 1, Sheet 79
Volume 1, Sheet 81
3613445 - 3
page 7

Site Name:
Address:

202 S Thornton
City, ST, ZIP:
Madison WI 53703
Client:
Ayres Associates
EDR Inquiry:
Order Date:
Certification #
3613445.3
5/22/2013 1:03:00 PM
018D-4119-911F
Copyright:
1908
018D-4119-911F

0 Feet
150
300
600
Volume 1, Sheet 3
Volume 1, Sheet 4
3613445 - 3
page 8

Site Name:
Address:

202 S Thornton
City, ST, ZIP:
Madison WI 53703
Client:
Ayres Associates
EDR Inquiry:
Order Date:
Certification #
3613445.3
5/22/2013 1:03:00 PM
018D-4119-911F
Copyright:
1902
018D-4119-911F

0 Feet
150
300
600
Volume 1, Sheet 17
Volume 1, Sheet 19
3613445 - 3
page 9
018D-4119-911F
Site Name:
Address:

202 S Thornton
City, ST, ZIP:
Madison WI 53703
Client:
Ayres Associates
EDR Inquiry:
Order Date:
Certification #
3613445.3
5/22/2013 1:03:00 PM
018D-4119-911F
Copyright:

0 Feet
150
1898
300
600
Volume 1, Sheet 27
3613445 - 3
page 10
Appendix B
Field Procedures
Field Procedures
This appendix describes field work procedures for this project. Where applicable, these
procedures are performed in accordance with Wisconsin Department of Natural Resources
(WDNR), Wisconsin Administrative Code requirements, American Society for Testing and
Materials (ASTM) standards, or accepted engineering or geologic standards.
Soil Probe Installation

Soil probes are installed by the contractor, in accordance the procedures described in
Wisconsin Administrative Code, Chapter NR 141. Soil probe sampling consists of installing a
hydraulically-driven steel 2-inch-diameter rod. The steel sampling device at the end of the rods
is 5 feet long and is assembled with a disposable plastic liner for sample collection. Samples are
collected continuously using the following method:
When the rod is positioned at the top of the desired sampling interval, the piston stop pin
is removed, and the sampler is driven the desired sample interval to encase the soil
sample in the plastic liner. The rods are then retracted from the hole and brought to the
surface. The plastic liner is removed from the sample rod that contains the undisturbed
soil sample. The liner is split open with a clean utility knife and the soil is classified and
then transferred to laboratory and field screening containers as described in the soil
sample collection section in this appendix.
An Ayres Associates representative is present during the field work to establish soil probe
locations, determine soil sample intervals, classify soils using the Unified Soil Classification
System (USCS), log soil probes, and collect and screen soil samples. Soil classification
information is recorded on the soil boring logs (WDNR Form 4400-122), and copies are included
in the site investigation report.
Sampling equipment is decontaminated as described under decontamination in this appendix.
All probe equipment is steam cleaned before reuse. Plastic liners are disposable, and are not
reused.
When the sampling is completed, soil probe holes are filled with bentonite and the surface
material restored. Soil probe abandonment details are described on WDNR Form 3300-5W, and
copies are included in the site investigation report. Soil cuttings generated during drilling are
containerized in 5-gallon buckets on site and are labeled with the date and the soils origin.
Because of the small quantity, these cuttings are typically disposed of in a dumpster.
Soil Sample Collection

Ayres Associates personnel retrieve soil samples from the sampling equipment using a clean
wooden spatula or a clean 20- to 30-milliliter polyethylene syringe, and avoid collecting slough
materials.
At each sampling point, we will collect samples for potential laboratory analysis. Soil collection
methods used are in accordance with WDNR's Leaking Underground Storage Tank and
Petroleum Analytical and Quality Assurance Guidance, July 1993, PUBL SW-130 93.
During collection of laboratory grade samples, we place the required amount of soil in the
laboratory provided container. We then place the selected laboratory samples on ice in a cooler
immediately after collection, and keep samples cool until analysis by the laboratory.
The specific collection method, including the size and type of containers used, are dependent
on the type of analysis to be conducted:
Percent solids (moisture analysis) and RCRA metals - Fill a 125-milliliter plastic jar with
soil.
VOCs Place 10 cubic centimeters of soil in pre-weighed VOA vial with methanol
preservative.
PAHs and PCBs Fill 4-ounce amber jar.
Ayres Associates initiates a chain-of-custody log, WDNR Form 4400-151 or equivalent, when
the samples are collected. We record the project name and number, sampler's name(s), sample
location and depth, sample number, date and time of collection, type of sample, method of
sample collection, number of containers, type of preservation, type of chemical analyses to be
performed, field screening results (soils only), and additional remarks about the sample if
needed on the chain-of-custody log. The individual(s) handling the samples signs and dates the
log. Shipment arrangements are made so the samples arrive within the appropriate shipping
time allowed by WDNR guidance.
Soil Laboratory Analysis

Samples are analyzed by a laboratory certified by the WDNR. Analytical methods used are as
follows:
PARAMETER
METHOD
MDL
VOCs
EPA Method 8260
25 g/kg
PAHs
EPA Method 8270
0.15-1.2 mg/kg
RCRA Metals
EPA Method 6010/7410
0.1 mg/kg
PCBs
EPA Method 8082
34.3 mg/kg
Percent Moisture
ASTM-D2974-87
0.10 mg/kg
Headspace Screening (PID)

Headspace screening samples are qualitatively screened for organic vapors using a photo
ionization detector (PID) equipped with a 10.6 eV lamp. Before we use the PID, it is calibrated
using 100 ppm isobutylene gas.
After allowing the soil sample to equilibrate in accordance with WDNR guidance, we screen the
total organic vapors in the jar by piercing the lid and then immediately inserting the PID probe.
Meter responses are recorded as instrument units (i.u.s) isobutylene gas equivalents. The
highest meter response is recorded in the field notes and/or on the soil boring logs. The PID
responses are a relative indication of total ionizable volatile organic compounds present in the
atmosphere surrounding the sample and do not necessarily represent the concentration of any
specific compound.
Groundwater Sample Collection from Soil Probes

Ayres Associates personnel conduct ground water sampling in accordance with the procedures
described in the Groundwater Sampling Field Manual (PUBL-DG-038 96) and the Groundwater
Sampling Desk Reference (PUBL-DG-037 96).
Following soil probe installation, a screened 1 PVC well casing is driven to the water table. A
1/8-inch-diameter disposable high density polyethylene hose is inserted into the well and
connected to a peristaltic pump to collect water samples directly into containers. Alternatively, a
disposable plastic bailer may be used to collect water. We continue this process until enough
volume is retrieved to fill all sample containers.
Samples are collected for analysis of the following parameters:
RCRA MetalsCollect 250 milliliters in a disposable plastic container and store on ice.
Filter sample through a 0.45-micron disposable filter within 2 hours of collection. Pour
the filtrate into a polyethylene jar and preserve the sample with nitric acid. Store sample
in an ice slurry.
Polynuclear aromatic hydrocarbons (PAH) and PCBsFill a 1-liter amber jar that has a
cap (no septum). No preservative is added to this sample.
We place the samples on ice in a cooler; enclose a completed WDNR chain-of-custody record,
Form 4400-151 or equivalent; and ship the cooler to the laboratory so it arrives within the
shipping time allowed by WDNR.
Groundwater Laboratory Analysis

Samples are analyzed by a laboratory certified by the WDNR. Analytical methods used are as
follows:
PARAMETER
METHOD
LOD
LOQ
PAHs
EPA Method 8270
0.0039-0.010 g/L
0.045 g/L
RCRA Metals
EPA Method 6010/7410
0.1-5.2 g/L
0.2-20 g/L
PCBs
EPA Method 8082
0.29 g/L
0.58 g/L
Appendix C
Phase II ESA
Soil Probe Logs and Abandonment Forms
Appendix D
Laboratory Analytical Results Soil
#=CL#
Pace Analytical Services, Inc.

1241 Bellevue Street - Suite 9
Green Bay, WI 54302
(920)469-2436
LIMS USE: FR - MITCHELL BANACH

LIMS OBJECT ID: 4079685
June 19, 2013
Mitchell Banach
Ayres & Associates, Inc.
3433 Oakwood Hills Parkway
Eau Claire, WI 547017698
RE: Project: 19-0291.20 DEPT OF ADMIN.

Pace Project No.: 4079685
Dear Mitchell Banach:
Enclosed are the analytical results for sample(s) received by the laboratory on June 15, 2013. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Steven Mleczko
steve.mleczko@pacelabs.com
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 60
#=CP#

Green Bay, WI 54302
(920)469-2436
CERTIFICATIONS
Project:
19-0291.20 DEPT OF ADMIN.
Pace Project No.:
4079685
Green Bay Certification IDs

1241 Bellevue Street, Green Bay, WI 54302
Florida/NELAP Certification #: E87948
Illinois Certification #: 200050
Kentucky Certification #: 82
Louisiana Certification #: 04168
Minnesota Certification #: 055-999-334
New York Certification #: 11888

North Dakota Certification #: R-150
South Carolina Certification #: 83006001
US Dept of Agriculture #: S-76505
Wisconsin Certification #: 405132750

Page 2 of 60
#=SS#

Green Bay, WI 54302
(920)469-2436
SAMPLE SUMMARY
Project:
Pace Project No.:
4079685
Lab ID
Sample ID
Matrix
Date Collected
Date Received
4079685001
GP-12
Solid
06/14/13 00:00
06/15/13 09:45
4079685002
GP-15
Solid
06/13/13 00:00
06/15/13 09:45
4079685003
GP-16
Solid
06/13/13 00:00
06/15/13 09:45
4079685004
GP-17(S)
Solid
06/13/13 00:00
06/15/13 09:45
4079685005
GP-17(D)
Solid
06/13/13 00:00
06/15/13 09:45
4079685006
GP-18(S)
Solid
06/13/13 00:00
06/15/13 09:45
4079685007
GP-18(D)
Solid
06/13/13 00:00
06/15/13 09:45
4079685008
GP-19
Solid
06/13/13 00:00
06/15/13 09:45
4079685009
GP-20
Solid
06/13/13 00:00
06/15/13 09:45
4079685010
GP-20
Water
06/13/13 00:00
06/15/13 09:45
4079685011
GP-21
Solid
06/13/13 00:00
06/15/13 09:45
4079685012
GP-21
Water
06/13/13 00:00
06/15/13 09:45
4079685013
GP-23
Solid
06/13/13 00:00
06/15/13 09:45
4079685014
GP-23
Water
06/13/13 00:00
06/15/13 09:45
4079685015
GP-25
Solid
06/14/13 00:00
06/15/13 09:45
4079685016
GP-25
Water
06/14/13 00:00
06/15/13 09:45
4079685017
TRIP BLANK
Water
06/13/13 00:00
06/15/13 09:45

Page 3 of 60
#=SA#

Green Bay, WI 54302
(920)469-2436
SAMPLE ANALYTE COUNT

Project:
Pace Project No.:
4079685
Lab ID
Sample ID
4079685001
GP-12
4079685002
4079685003
4079685004
4079685005
4079685006
4079685007
4079685008
GP-15
GP-16
GP-17(S)
GP-17(D)
GP-18(S)
GP-18(D)
GP-19
Method
Analysts
EPA 6010
DLB
Analytes
Reported
Laboratory
PASI-G
EPA 7471
CMS
PASI-G
EPA 8270 by SIM
ARO
20
PASI-G
ASTM D2974-87
SKW
PASI-G
EPA 6010
DLB
PASI-G
EPA 7471
CMS
PASI-G
EPA 8260
SMT
64
PASI-G
ASTM D2974-87
SKW
PASI-G
EPA 6010
DLB
PASI-G
EPA 7471
CMS
PASI-G
EPA 8260
SMT
64
PASI-G
ASTM D2974-87
SKW
PASI-G
EPA 8270 by SIM
ARO
20
PASI-G
EPA 8260
SMT
64
PASI-G
ASTM D2974-87
SKW
PASI-G
EPA 8270 by SIM
ARO
20
PASI-G
EPA 8260
SMT
64
PASI-G
ASTM D2974-87
SKW
PASI-G
EPA 6010
DLB
PASI-G
EPA 8270 by SIM
ARO
20
PASI-G
EPA 8260
SMT
64
PASI-G
ASTM D2974-87
SKW
PASI-G
EPA 6010
DLB
PASI-G
EPA 8270 by SIM
ARO
20
PASI-G
EPA 8260
SMT
64
PASI-G
ASTM D2974-87
SKW
PASI-G
EPA 8082
BLM
10
PASI-G
EPA 8270 by SIM
ARO
20
PASI-G
EPA 8260
SMT
64
PASI-G
ASTM D2974-87
SKW
PASI-G
4079685009
GP-20
EPA 8270 by SIM
ARO
20
PASI-G
ASTM D2974-87
SKW
PASI-G
4079685010
GP-20
EPA 8270 by HVI
RJN
20
PASI-G
4079685011
GP-21
EPA 8270 by SIM
ARO
20
PASI-G
ASTM D2974-87
SKW
PASI-G
4079685012
GP-21
EPA 8270 by HVI
RJN
20
PASI-G
4079685013
GP-23
ASTM D2974-87
SKW
PASI-G

Page 4 of 60
#=SA#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079685
Lab ID
Sample ID
4079685015
GP-25
4079685017
TRIP BLANK
Analytes
Reported
Method
Analysts
Laboratory
ASTM D2974-87
SKW
PASI-G
EPA 8260
HNW
64
PASI-G

Page 5 of 60
#=HO#

Green Bay, WI 54302
(920)469-2436
HITS ONLY
Project:
Pace Project No.:
4079685
Lab Sample ID
Client Sample ID
Method
Parameters
Result
4079685001
GP-12
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 7471
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
ASTM D2974-87
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Percent Moisture
4079685002
GP-15
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 7471
ASTM D2974-87
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Percent Moisture
4079685003
GP-16
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 7471
ASTM D2974-87
Arsenic
Barium
Cadmium
Chromium
Lead
Silver
Mercury
Percent Moisture
4079685004
GP-17(S)
EPA 8270 by SIM

EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Units
Report Limit
Analyzed
4.7
124
0.32J
12.1
200
0.021
<9.5
18.0J
40.1
96.2
62.4
91.4
52.4
69.0
239
28.9
99.7
30.4
144
183
93.2
280
112
12.1
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
2.3
0.57
0.57
0.57
1.1
0.0067
19.0
19.0
19.0
19.0
19.0
19.0
19.0
19.0
19.0
19.0
19.0
19.0
19.0
19.0
19.0
19.0
19.0
0.10
06/18/13 13:39
06/18/13 13:39
06/18/13 13:39
06/18/13 13:39
06/18/13 13:39
06/18/13 07:58
06/18/13 17:42
06/18/13 17:42
06/18/13 17:42
06/18/13 17:42
06/18/13 17:42
06/18/13 17:42
06/18/13 17:42
06/18/13 17:42
06/18/13 17:42
06/18/13 17:42
06/18/13 17:42
06/18/13 17:42
06/18/13 17:42
06/18/13 17:42
06/18/13 17:42
06/18/13 17:42
06/18/13 17:42
06/17/13 13:02
7.3
72.4
0.72
19.8
66.4
0.033
18.1
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
%
2.3
0.56
0.56
0.56
1.1
0.0078
0.10
06/18/13 13:49
06/18/13 13:49
06/18/13 13:49
06/18/13 13:49
06/18/13 13:49
06/18/13 08:00
06/17/13 16:52
14.2
65.3
2.9
9.6
99.9
1.2
0.10
12.0
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
%
11.1
0.56
2.8
0.56
5.6
1.1
0.0074
0.10
06/19/13 09:15
06/18/13 13:51
06/19/13 09:15
06/18/13 13:51
06/19/13 09:15
06/18/13 13:51
06/18/13 08:02
06/17/13 16:52
11.0J
25.0
25.1
36.3
ug/kg
ug/kg
ug/kg
ug/kg
19.3
19.3
19.3
19.3
06/18/13 18:34
06/18/13 18:34
06/18/13 18:34
06/18/13 18:34
Qualifiers
M0
M0

Page 6 of 60
#=HO#

Green Bay, WI 54302
(920)469-2436
HITS ONLY
Project:
Pace Project No.:
4079685
Lab Sample ID
Client Sample ID
Method
Parameters
Result
4079685004
GP-17(S)
EPA 8270 by SIM

EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
ASTM D2974-87
Chrysene
Fluoranthene
Phenanthrene
Pyrene
Percent Moisture
4079685005
GP-17(D)
ASTM D2974-87
Percent Moisture
4079685006
GP-18(S)
EPA 6010
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
ASTM D2974-87
Lead
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Percent Moisture
15.3J
14.9J
36.4
60.9
14.1J
38.1
48.2
13.7
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
12.6 %
4079685007
GP-18(D)
EPA 6010
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
Lead
Acenaphthene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
Report Limit
Analyzed
19.3
19.3
19.3
19.3
19.3
19.3
19.3
0.10
06/18/13 18:34
06/18/13 18:34
06/18/13 18:34
06/18/13 18:34
06/18/13 18:34
06/18/13 18:34
06/18/13 18:34
06/17/13 13:02
0.10
06/17/13 13:02
152
17.3J
23.7
69.1
176
188
153
118
176
237
44.9
369
14.9J
101
74.7
79.5
44.8
335
391
14.4
mg/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
1.1
19.5
19.5
19.5
19.5
19.5
19.5
19.5
19.5
19.5
19.5
19.5
19.5
19.5
19.5
19.5
19.5
19.5
19.5
0.10
06/18/13 13:54
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
06/17/13 13:03
99.8
25.0
84.4
136
133
149
75.1
109
181
29.6
316
25.0
67.6
48.6
mg/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1.1
21.5
21.5
21.5
21.5
21.5
21.5
21.5
21.5
21.5
21.5
21.5
21.5
21.5
06/18/13 13:56
06/18/13 17:59
06/18/13 17:59
06/18/13 17:59
06/18/13 17:59
06/18/13 17:59
06/18/13 17:59
06/18/13 17:59
06/18/13 17:59
06/18/13 17:59
06/18/13 17:59
06/18/13 17:59
06/18/13 17:59
06/18/13 17:59
Qualifiers

Page 7 of 60
#=HO#

Green Bay, WI 54302
(920)469-2436
HITS ONLY
Project:
Pace Project No.:
4079685
Lab Sample ID
Client Sample ID
Method
Parameters
Result
4079685007
GP-18(D)
EPA 8270 by SIM

EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
ASTM D2974-87
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Percent Moisture
4079685008
GP-19
EPA 8270 by SIM

EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8260
ASTM D2974-87
Acenaphthene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Naphthalene
Percent Moisture
4079685009
GP-20
ASTM D2974-87
Percent Moisture
Units
GP-20
EPA 8270 by HVI

EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
Acenaphthene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Analyzed
56.0
43.8
367
271
22.4
ug/kg
ug/kg
ug/kg
ug/kg
%
21.5
21.5
21.5
21.5
0.10
06/18/13 17:59
06/18/13 17:59
06/18/13 17:59
06/18/13 17:59
06/17/13 13:03
1020
3490
6240
6060
7460
3750
3880
8090
1370
16700
1250
3460
882J
502J
1620
18100
14200
64.9J
13.4
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
962
962
962
962
962
962
962
962
962
962
962
962
962
962
962
962
962
69.3
0.10
06/19/13 09:00
06/19/13 09:00
06/19/13 09:00
06/19/13 09:00
06/19/13 09:00
06/19/13 09:00
06/19/13 09:00
06/19/13 09:00
06/19/13 09:00
06/19/13 09:00
06/19/13 09:00
06/19/13 09:00
06/19/13 09:00
06/19/13 09:00
06/19/13 09:00
06/19/13 09:00
06/19/13 09:00
06/17/13 16:04
06/17/13 13:03
0.10
06/17/13 13:03
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
06/19/13 08:21
06/19/13 08:21
06/19/13 08:21
06/19/13 08:21
06/19/13 08:21
06/19/13 08:21
06/19/13 08:21
06/19/13 08:21
06/19/13 08:21
06/19/13 08:21
06/19/13 08:21
06/19/13 08:21
06/19/13 08:21
06/19/13 08:21
06/19/13 08:21
06/19/13 08:21
06/19/13 08:21
13.1 %
4079685010
Report Limit
0.0049J
0.012J
0.025J
0.022J
0.038J
0.020J
0.034J
0.048
0.0083J
0.065
0.0071J
0.018J
0.012J
0.020J
0.041J
0.073
0.062
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Qualifiers

Page 8 of 60
#=HO#

Green Bay, WI 54302
(920)469-2436
HITS ONLY
Project:
Pace Project No.:
4079685
Lab Sample ID
Client Sample ID
Method
Parameters
Result
4079685011
GP-21
ASTM D2974-87
Percent Moisture
4079685012
GP-21
EPA 8270 by HVI

EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
4079685013
GP-23
8.1 %
ASTM D2974-87
Percent Moisture
4079685014
GP-23
EPA 8270 by HVI

EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
4079685015
GP-25
ASTM D2974-87
Percent Moisture
Units
0.0041J
0.0042J
0.022J
0.032J
0.010J
0.048
0.026J
0.037J
0.066
0.0093J
0.19
0.013J
0.021J
0.021J
0.036J
0.038J
0.15
0.18
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
14.3 %
0.0051J
0.0082J
0.0057J
0.013J
0.017J
0.0043J
0.015J
0.032J
0.050
0.024J
0.019J
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
13.4 %
4079685016
GP-25
EPA 8270 by HVI

EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
0.027J
0.0082J
0.032J
0.044J
0.040J
0.043J
0.027J
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Report Limit
Analyzed
0.10
06/17/13 13:03
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
0.10
06/17/13 13:03
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
06/19/13 08:57
06/19/13 08:57
06/19/13 08:57
06/19/13 08:57
06/19/13 08:57
06/19/13 08:57
06/19/13 08:57
06/19/13 08:57
06/19/13 08:57
06/19/13 08:57
06/19/13 08:57
0.10
06/17/13 13:03
0.049
0.049
0.049
0.049
0.049
0.049
0.049
06/19/13 09:15
06/19/13 09:15
06/19/13 09:15
06/19/13 09:15
06/19/13 09:15
06/19/13 09:15
06/19/13 09:15
Qualifiers

Page 9 of 60
#=HO#

Green Bay, WI 54302
(920)469-2436
HITS ONLY
Project:
Pace Project No.:
4079685
Lab Sample ID
Client Sample ID
Method
Parameters
Result
4079685016
GP-25
EPA 8270 by HVI

EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
0.040J
0.054
0.012J
0.13
0.027J
0.023J
0.036J
0.051
0.16
0.18
0.13
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Report Limit
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
Analyzed
Qualifiers
06/19/13 09:15
06/19/13 09:15
06/19/13 09:15
06/19/13 09:15
06/19/13 09:15
06/19/13 09:15
06/19/13 09:15
06/19/13 09:15
06/19/13 09:15
06/19/13 09:15
06/19/13 09:15

Page 10 of 60
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079685
Sample: GP-12
Lab ID: 4079685001
Collected: 06/14/13 00:00
Received: 06/15/13 09:45
Matrix: Solid
Results reported on a "dry-weight" basis

Parameters
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7471 Mercury
Mercury
8270 MSSV PAH by SIM
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Percent Moisture
Percent Moisture
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 6010 Preparation Method: EPA 3050

4.7
124
0.32J
12.1
200
<0.67
<0.24
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
2.3
0.57
0.57
0.57
1.1
2.3
1.1
0.61
0.099
0.058
0.14
0.33
0.67
0.24
1
1
1
1
1
1
1
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/18/13 13:39
06/18/13 13:39
06/18/13 13:39
06/18/13 13:39
06/18/13 13:39
06/18/13 13:39
06/18/13 13:39
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4
M0
M0

0.021 mg/kg
0.0067
0.0033
06/17/13 16:14 06/18/13 07:58 7439-97-6
Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3546

<9.5
18.0J
40.1
96.2
62.4
91.4
52.4
69.0
239
28.9
99.7
<9.5
30.4
144
183
93.2
280
112
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
57 %
59 %
19.0
19.0
19.0
19.0
19.0
19.0
19.0
19.0
19.0
19.0
19.0
19.0
19.0
19.0
19.0
19.0
19.0
19.0
9.5
9.5
9.5
9.5
3.4
9.5
9.5
3.3
9.5
9.5
9.5
9.5
9.5
3.4
9.5
9.5
9.5
9.5
40-130
40-130
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 17:42
06/18/13 17:42
06/18/13 17:42
06/18/13 17:42
06/18/13 17:42
06/18/13 17:42
06/18/13 17:42
06/18/13 17:42
06/18/13 17:42
06/18/13 17:42
06/18/13 17:42
06/18/13 17:42
06/18/13 17:42
06/18/13 17:42
06/18/13 17:42
06/18/13 17:42
06/18/13 17:42
06/18/13 17:42
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0
1
1
06/18/13 06:50 06/18/13 17:42 321-60-8

06/18/13 06:50 06/18/13 17:42 1718-51-0
Analytical Method: ASTM D2974-87

12.1 %
0.10
0.10
06/17/13 13:02

Date: 06/19/2013 03:55 PM
Page 11 of 60
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079685
Sample: GP-15
Lab ID: 4079685002
Collected: 06/13/13 00:00
Received: 06/15/13 09:45
Matrix: Solid

Parameters
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7471 Mercury
Mercury
8260 MSV Med Level Normal List
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

7.3
72.4
0.72
19.8
66.4
<0.67
<0.24
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
2.3
0.56
0.56
0.56
1.1
2.3
1.1
0.61
0.098
0.057
0.14
0.33
0.67
0.24
1
1
1
1
1
1
1
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/18/13 13:49
06/18/13 13:49
06/18/13 13:49
06/18/13 13:49
06/18/13 13:49
06/18/13 13:49
06/18/13 13:49
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4

0.033 mg/kg
0.0078
0.0039
06/17/13 16:14 06/18/13 08:00 7439-97-6
Analytical Method: EPA 8260 Preparation Method: EPA 5035/5030B

<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<49.8
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
250
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
49.8
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W

Date: 06/19/2013 03:55 PM
Page 12 of 60
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079685
Sample: GP-15
Lab ID: 4079685002
Collected: 06/13/13 00:00
Received: 06/15/13 09:45
Matrix: Solid

Parameters
Diisopropyl ether
Ethylbenzene
p-Isopropyltoluene
Methylene Chloride
Naphthalene
n-Propylbenzene
Styrene
Tetrachloroethene
Toluene
Trichloroethene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Dibromofluoromethane (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Percent Moisture
Percent Moisture
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
06/17/13 13:47
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
1634-04-4
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
179601-23-1
95-47-6
Qual

<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<50.0
<25.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
113 %
115 %
100 %
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
120
60.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
57-130
54-133
49-130
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
1
1
1
06/17/13 12:54 06/17/13 13:47 1868-53-7

06/17/13 12:54 06/17/13 13:47 2037-26-5
06/17/13 12:54 06/17/13 13:47 460-00-4
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W

18.1 %
0.10
0.10
06/17/13 16:52

Date: 06/19/2013 03:55 PM
Page 13 of 60
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079685
Sample: GP-16
Lab ID: 4079685003
Collected: 06/13/13 00:00
Received: 06/15/13 09:45
Matrix: Solid

Parameters
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7471 Mercury
Mercury
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

14.2
65.3
2.9
9.6
99.9
<0.66
1.2
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
11.1
0.56
2.8
0.56
5.6
2.2
1.1
3.0
0.096
0.28
0.14
1.6
0.66
0.24
5
1
5
1
5
1
1
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/19/13 09:15
06/18/13 13:51
06/19/13 09:15
06/18/13 13:51
06/19/13 09:15
06/18/13 13:51
06/18/13 13:51
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4

0.10 mg/kg
0.0074
0.0037
06/17/13 16:14 06/18/13 08:02 7439-97-6

<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<49.8
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
250
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
49.8
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W

Date: 06/19/2013 03:55 PM
Page 14 of 60
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079685
Sample: GP-16
Lab ID: 4079685003
Collected: 06/13/13 00:00
Received: 06/15/13 09:45
Matrix: Solid

Parameters
Diisopropyl ether
Ethylbenzene
p-Isopropyltoluene
Methylene Chloride
Naphthalene
n-Propylbenzene
Styrene
Tetrachloroethene
Toluene
Trichloroethene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Percent Moisture
Percent Moisture
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
06/17/13 14:10
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
1634-04-4
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
179601-23-1
95-47-6
Qual

<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<50.0
<25.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
119 %
118 %
103 %
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
120
60.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
57-130
54-133
49-130
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
1
1
1
06/17/13 12:54 06/17/13 14:10 1868-53-7

06/17/13 12:54 06/17/13 14:10 2037-26-5
06/17/13 12:54 06/17/13 14:10 460-00-4
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W

12.0 %
0.10
0.10
06/17/13 16:52

Date: 06/19/2013 03:55 PM
Page 15 of 60
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079685
Sample: GP-17(S)
Lab ID: 4079685004
Collected: 06/13/13 00:00
Received: 06/15/13 09:45
Matrix: Solid

Parameters
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Terphenyl-d14 (S)
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

<9.7
<9.7
11.0J
25.0
25.1
36.3
15.3J
14.9J
36.4
<9.7
60.9
<9.7
14.1J
<3.4
<9.7
<9.7
38.1
48.2
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
67 %
77 %
19.3
19.3
19.3
19.3
19.3
19.3
19.3
19.3
19.3
19.3
19.3
19.3
19.3
19.3
19.3
19.3
19.3
19.3
9.7
9.7
9.7
9.7
3.4
9.7
9.7
3.4
9.7
9.7
9.7
9.7
9.7
3.4
9.7
9.7
9.7
9.7
40-130
40-130
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 18:34
06/18/13 18:34
06/18/13 18:34
06/18/13 18:34
06/18/13 18:34
06/18/13 18:34
06/18/13 18:34
06/18/13 18:34
06/18/13 18:34
06/18/13 18:34
06/18/13 18:34
06/18/13 18:34
06/18/13 18:34
06/18/13 18:34
06/18/13 18:34
06/18/13 18:34
06/18/13 18:34
06/18/13 18:34
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0
1
1
06/18/13 06:50 06/18/13 18:34 321-60-8

06/18/13 06:50 06/18/13 18:34 1718-51-0

<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<49.8
<25.0
<25.0
<25.0
<25.0
<25.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
250
60.0
60.0
60.0
60.0
60.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
49.8
25.0
25.0
25.0
25.0
25.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W

Date: 06/19/2013 03:55 PM
Page 16 of 60
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079685
Sample: GP-17(S)
Lab ID: 4079685004
Collected: 06/13/13 00:00
Received: 06/15/13 09:45
Matrix: Solid

Parameters
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
p-Isopropyltoluene
Methylene Chloride
Naphthalene
n-Propylbenzene
Styrene
Tetrachloroethene
Toluene
Trichloroethene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
06/17/13 14:32
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
1634-04-4
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
179601-23-1
95-47-6
Qual

<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<50.0
<25.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
116 %
119 %
100 %
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
120
60.0
57-130
54-133
49-130
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
1
1
1
06/17/13 12:54 06/17/13 14:32 1868-53-7

06/17/13 12:54 06/17/13 14:32 2037-26-5
06/17/13 12:54 06/17/13 14:32 460-00-4
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W

Date: 06/19/2013 03:55 PM
Page 17 of 60
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079685
Sample: GP-17(S)
Lab ID: 4079685004
Collected: 06/13/13 00:00
Received: 06/15/13 09:45
Matrix: Solid

Parameters
Percent Moisture
Percent Moisture
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

13.7 %
0.10
0.10
06/17/13 13:02

Date: 06/19/2013 03:55 PM
Page 18 of 60
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079685
Sample: GP-17(D)
Lab ID: 4079685005
Collected: 06/13/13 00:00
Received: 06/15/13 09:45
Matrix: Solid

Parameters
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Terphenyl-d14 (S)
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

<9.5
<9.5
<9.5
<9.5
<3.4
<9.5
<9.5
<3.4
<9.5
<9.5
<9.5
<9.5
<9.5
<3.4
<9.5
<9.5
<9.5
<9.5
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
61 %
69 %
19.1
19.1
19.1
19.1
19.1
19.1
19.1
19.1
19.1
19.1
19.1
19.1
19.1
19.1
19.1
19.1
19.1
19.1
9.5
9.5
9.5
9.5
3.4
9.5
9.5
3.4
9.5
9.5
9.5
9.5
9.5
3.4
9.5
9.5
9.5
9.5
40-130
40-130
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 16:50
06/18/13 16:50
06/18/13 16:50
06/18/13 16:50
06/18/13 16:50
06/18/13 16:50
06/18/13 16:50
06/18/13 16:50
06/18/13 16:50
06/18/13 16:50
06/18/13 16:50
06/18/13 16:50
06/18/13 16:50
06/18/13 16:50
06/18/13 16:50
06/18/13 16:50
06/18/13 16:50
06/18/13 16:50
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0
1
1
06/18/13 06:50 06/18/13 16:50 321-60-8

06/18/13 06:50 06/18/13 16:50 1718-51-0

<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<49.8
<25.0
<25.0
<25.0
<25.0
<25.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
250
60.0
60.0
60.0
60.0
60.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
49.8
25.0
25.0
25.0
25.0
25.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W

Date: 06/19/2013 03:55 PM
Page 19 of 60
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079685
Sample: GP-17(D)
Lab ID: 4079685005
Collected: 06/13/13 00:00
Received: 06/15/13 09:45
Matrix: Solid

Parameters
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
p-Isopropyltoluene
Methylene Chloride
Naphthalene
n-Propylbenzene
Styrene
Tetrachloroethene
Toluene
Trichloroethene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
06/17/13 14:55
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
1634-04-4
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
179601-23-1
95-47-6
Qual

<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<50.0
<25.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
113 %
112 %
98 %
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
120
60.0
57-130
54-133
49-130
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
1
1
1
06/17/13 12:54 06/17/13 14:55 1868-53-7

06/17/13 12:54 06/17/13 14:55 2037-26-5
06/17/13 12:54 06/17/13 14:55 460-00-4
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W

Date: 06/19/2013 03:55 PM
Page 20 of 60
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079685
Sample: GP-17(D)
Lab ID: 4079685005
Collected: 06/13/13 00:00
Received: 06/15/13 09:45
Matrix: Solid

Parameters
Percent Moisture
Percent Moisture
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

12.6 %
0.10
0.10
06/17/13 13:02

Date: 06/19/2013 03:55 PM
Page 21 of 60
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079685
Sample: GP-18(S)
Lab ID: 4079685006
Collected: 06/13/13 00:00
Received: 06/15/13 09:45
Matrix: Solid

Parameters
6010 MET ICP
Lead
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Terphenyl-d14 (S)
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

152 mg/kg
1.1
0.31
06/17/13 10:05 06/18/13 13:54 7439-92-1

17.3J
23.7
69.1
176
188
153
118
176
237
44.9
369
14.9J
101
74.7
79.5
44.8
335
391
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
64 %
63 %
19.5
19.5
19.5
19.5
19.5
19.5
19.5
19.5
19.5
19.5
19.5
19.5
19.5
19.5
19.5
19.5
19.5
19.5
9.7
9.7
9.7
9.7
3.5
9.7
9.7
3.4
9.7
9.7
9.7
9.7
9.7
3.4
9.7
9.7
9.7
9.7
40-130
40-130
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
06/18/13 17:07
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0
1
1
06/18/13 06:50 06/18/13 17:07 321-60-8

06/18/13 06:50 06/18/13 17:07 1718-51-0

<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<49.8
<25.0
<25.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
250
60.0
60.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
49.8
25.0
25.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W

Date: 06/19/2013 03:55 PM
Page 22 of 60
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079685
Sample: GP-18(S)
Lab ID: 4079685006
Collected: 06/13/13 00:00
Received: 06/15/13 09:45
Matrix: Solid

Parameters
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
p-Isopropyltoluene
Methylene Chloride
Naphthalene
n-Propylbenzene
Styrene
Tetrachloroethene
Toluene
Trichloroethene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
06/17/13 15:18
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
1634-04-4
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
179601-23-1
95-47-6
Qual

<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<50.0
<25.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
121 %
119 %
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
120
60.0
57-130
54-133
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
1
1
06/17/13 12:54 06/17/13 15:18 1868-53-7

06/17/13 12:54 06/17/13 15:18 2037-26-5
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W

Date: 06/19/2013 03:55 PM
Page 23 of 60
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079685
Sample: GP-18(S)
Lab ID: 4079685006
Collected: 06/13/13 00:00
Received: 06/15/13 09:45
Matrix: Solid

Parameters
Surrogates
Percent Moisture
Percent Moisture
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

106 %
49-130
06/17/13 12:54 06/17/13 15:18 460-00-4

14.4 %
0.10
0.10
06/17/13 13:03

Date: 06/19/2013 03:55 PM
Page 24 of 60
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079685
Sample: GP-18(D)
Lab ID: 4079685007
Collected: 06/13/13 00:00
Received: 06/15/13 09:45
Matrix: Solid

Parameters
6010 MET ICP
Lead
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Terphenyl-d14 (S)
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

99.8 mg/kg
1.1
0.32
06/17/13 10:05 06/18/13 13:56 7439-92-1

25.0
<10.7
84.4
136
133
149
75.1
109
181
29.6
316
25.0
67.6
48.6
56.0
43.8
367
271
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
79 %
75 %
21.5
21.5
21.5
21.5
21.5
21.5
21.5
21.5
21.5
21.5
21.5
21.5
21.5
21.5
21.5
21.5
21.5
21.5
10.7
10.7
10.7
10.7
3.8
10.7
10.7
3.8
10.7
10.7
10.7
10.7
10.7
3.8
10.7
10.7
10.7
10.7
40-130
40-130
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 17:59
06/18/13 17:59
06/18/13 17:59
06/18/13 17:59
06/18/13 17:59
06/18/13 17:59
06/18/13 17:59
06/18/13 17:59
06/18/13 17:59
06/18/13 17:59
06/18/13 17:59
06/18/13 17:59
06/18/13 17:59
06/18/13 17:59
06/18/13 17:59
06/18/13 17:59
06/18/13 17:59
06/18/13 17:59
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0
1
1
06/18/13 06:50 06/18/13 17:59 321-60-8

06/18/13 06:50 06/18/13 17:59 1718-51-0

<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<49.8
<25.0
<25.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
250
60.0
60.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
49.8
25.0
25.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W

Date: 06/19/2013 03:55 PM
Page 25 of 60
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079685
Sample: GP-18(D)
Lab ID: 4079685007
Collected: 06/13/13 00:00
Received: 06/15/13 09:45
Matrix: Solid

Parameters
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
p-Isopropyltoluene
Methylene Chloride
Naphthalene
n-Propylbenzene
Styrene
Tetrachloroethene
Toluene
Trichloroethene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
06/17/13 15:41
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
1634-04-4
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
179601-23-1
95-47-6
Qual

<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<50.0
<25.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
118 %
117 %
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
120
60.0
57-130
54-133
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
1
1
06/17/13 12:54 06/17/13 15:41 1868-53-7

06/17/13 12:54 06/17/13 15:41 2037-26-5
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W

Date: 06/19/2013 03:55 PM
Page 26 of 60
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079685
Sample: GP-18(D)
Lab ID: 4079685007
Collected: 06/13/13 00:00
Received: 06/15/13 09:45
Matrix: Solid

Parameters
Surrogates
Percent Moisture
Percent Moisture
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

102 %
49-130
06/17/13 12:54 06/17/13 15:41 460-00-4

22.4 %
0.10
0.10
06/17/13 13:03

Date: 06/19/2013 03:55 PM
Page 27 of 60
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079685
Sample: GP-19
Lab ID: 4079685008
Collected: 06/13/13 00:00
Received: 06/15/13 09:45
Matrix: Solid

Parameters
8082 GCS PCB
PCB, Total
Surrogates
Tetrachloro-m-xylene (S)
Decachlorobiphenyl (S)
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Terphenyl-d14 (S)
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

<28.9
<28.9
<28.9
<28.9
<28.9
<28.9
<28.9
<28.9
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
89 %
97 %
57.7
57.7
57.7
57.7
57.7
57.7
57.7
57.7
28.9
28.9
28.9
28.9
28.9
28.9
28.9
28.9
40-130
48-130
1
1
1
1
1
1
1
1
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/19/13 11:33
06/19/13 11:33
06/19/13 11:33
06/19/13 11:33
06/19/13 11:33
06/19/13 11:33
06/19/13 11:33
06/19/13 11:33
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
1336-36-3
1
1
06/18/13 12:30 06/19/13 11:33 877-09-8

06/18/13 12:30 06/19/13 11:33 2051-24-3

1020
<481
3490
6240
6060
7460
3750
3880
8090
1370
16700
1250
3460
882J
502J
1620
18100
14200
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
64 %
65 %
962
962
962
962
962
962
962
962
962
962
962
962
962
962
962
962
962
962
481
481
481
481
171
481
481
170
481
481
481
481
481
170
481
481
481
481
40-130
40-130
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/19/13 09:00
06/19/13 09:00
06/19/13 09:00
06/19/13 09:00
06/19/13 09:00
06/19/13 09:00
06/19/13 09:00
06/19/13 09:00
06/19/13 09:00
06/19/13 09:00
06/19/13 09:00
06/19/13 09:00
06/19/13 09:00
06/19/13 09:00
06/19/13 09:00
06/19/13 09:00
06/19/13 09:00
06/19/13 09:00
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0
50
50
06/18/13 06:50 06/19/13 09:00 321-60-8

06/18/13 06:50 06/19/13 09:00 1718-51-0

<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
1
1
1
1
1
1
1
1
1
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
W
W
W
W
W
W
W
W
W

Date: 06/19/2013 03:55 PM
Page 28 of 60
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079685
Sample: GP-19
Lab ID: 4079685008
Collected: 06/13/13 00:00
Received: 06/15/13 09:45
Matrix: Solid

Parameters
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
p-Isopropyltoluene
Methylene Chloride
Naphthalene
n-Propylbenzene
Styrene
Tetrachloroethene
Toluene
Trichloroethene
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<49.8
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
64.9J
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
60.0
60.0
60.0
60.0
60.0
60.0
60.0
250
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
69.3
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
49.8
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
28.9
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
1634-04-4
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W

Date: 06/19/2013 03:55 PM
Page 29 of 60
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079685
Sample: GP-19
Lab ID: 4079685008
Collected: 06/13/13 00:00
Received: 06/15/13 09:45
Matrix: Solid

Parameters
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Percent Moisture
Percent Moisture
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
06/17/13 16:04
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
179601-23-1
95-47-6
Qual

<25.0
<25.0
<25.0
<25.0
<25.0
<50.0
<25.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
120 %
121 %
106 %
60.0
60.0
60.0
60.0
60.0
120
60.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
57-130
54-133
49-130
1
1
1
1
1
1
1
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
06/17/13 12:54
1
1
1
06/17/13 12:54 06/17/13 16:04 1868-53-7

06/17/13 12:54 06/17/13 16:04 2037-26-5
06/17/13 12:54 06/17/13 16:04 460-00-4
W
W
W
W
W
W
W

13.4 %
0.10
0.10
06/17/13 13:03

Date: 06/19/2013 03:55 PM
Page 30 of 60
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079685
Sample: GP-20
Lab ID: 4079685009
Collected: 06/13/13 00:00
Received: 06/15/13 09:45
Matrix: Solid

Parameters
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Terphenyl-d14 (S)
Percent Moisture
Percent Moisture
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

<9.6
<9.6
<9.6
<9.6
<3.4
<9.6
<9.6
<3.4
<9.6
<9.6
<9.6
<9.6
<9.6
<3.4
<9.6
<9.6
<9.6
<9.6
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
64 %
72 %
19.2
19.2
19.2
19.2
19.2
19.2
19.2
19.2
19.2
19.2
19.2
19.2
19.2
19.2
19.2
19.2
19.2
19.2
9.6
9.6
9.6
9.6
3.4
9.6
9.6
3.4
9.6
9.6
9.6
9.6
9.6
3.4
9.6
9.6
9.6
9.6
40-130
40-130
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 14:12
06/18/13 14:12
06/18/13 14:12
06/18/13 14:12
06/18/13 14:12
06/18/13 14:12
06/18/13 14:12
06/18/13 14:12
06/18/13 14:12
06/18/13 14:12
06/18/13 14:12
06/18/13 14:12
06/18/13 14:12
06/18/13 14:12
06/18/13 14:12
06/18/13 14:12
06/18/13 14:12
06/18/13 14:12
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0
1
1
06/18/13 06:50 06/18/13 14:12 321-60-8

06/18/13 06:50 06/18/13 14:12 1718-51-0

13.1 %
0.10
0.10
06/17/13 13:03

Date: 06/19/2013 03:55 PM
Page 31 of 60
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079685
Sample: GP-20
Parameters
Lab ID: 4079685010

Results
Units
Collected: 06/13/13 00:00

LOQ
LOD
Received: 06/15/13 09:45
DF
Prepared
8270 MSSV PAH by HVI
Analytical Method: EPA 8270 by HVI Preparation Method: EPA 3510
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Terphenyl-d14 (S)
0.0049J
<0.0035
0.012J
0.025J
0.022J
0.038J
0.020J
0.034J
0.048
0.0083J
0.065
0.0071J
0.018J
0.012J
0.020J
0.041J
0.073
0.062
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
65 %
106 %
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
39-130
73-155
0.0038
0.0035
0.0048
0.0047
0.0049
0.0067
0.0080
0.010
0.0062
0.0054
0.0052
0.0038
0.0058
0.0036
0.0061
0.0033
0.0038
0.0053
Matrix: Water
Analyzed
06/19/13 08:21
06/19/13 08:21
06/19/13 08:21
06/19/13 08:21
06/19/13 08:21
06/19/13 08:21
06/19/13 08:21
06/19/13 08:21
06/19/13 08:21
06/19/13 08:21
06/19/13 08:21
06/19/13 08:21
06/19/13 08:21
06/19/13 08:21
06/19/13 08:21
06/19/13 08:21
06/19/13 08:21
06/19/13 08:21
CAS No.
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
1
1
06/18/13 07:44 06/19/13 08:21 321-60-8

06/18/13 07:44 06/19/13 08:21 1718-51-0
Qual
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0

Date: 06/19/2013 03:55 PM
Page 32 of 60
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079685
Sample: GP-21
Lab ID: 4079685011
Collected: 06/13/13 00:00
Received: 06/15/13 09:45
Matrix: Solid

Parameters
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Terphenyl-d14 (S)
Percent Moisture
Percent Moisture
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

<9.1
<9.1
<9.1
<9.1
<3.2
<9.1
<9.1
<3.2
<9.1
<9.1
<9.1
<9.1
<9.1
<3.2
<9.1
<9.1
<9.1
<9.1
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
59 %
62 %
18.1
18.1
18.1
18.1
18.1
18.1
18.1
18.1
18.1
18.1
18.1
18.1
18.1
18.1
18.1
18.1
18.1
18.1
9.1
9.1
9.1
9.1
3.2
9.1
9.1
3.2
9.1
9.1
9.1
9.1
9.1
3.2
9.1
9.1
9.1
9.1
40-130
40-130
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 15:38
06/18/13 15:38
06/18/13 15:38
06/18/13 15:38
06/18/13 15:38
06/18/13 15:38
06/18/13 15:38
06/18/13 15:38
06/18/13 15:38
06/18/13 15:38
06/18/13 15:38
06/18/13 15:38
06/18/13 15:38
06/18/13 15:38
06/18/13 15:38
06/18/13 15:38
06/18/13 15:38
06/18/13 15:38
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0
1
1
06/18/13 06:50 06/18/13 15:38 321-60-8

06/18/13 06:50 06/18/13 15:38 1718-51-0

8.1 %
0.10
0.10
06/17/13 13:03

Date: 06/19/2013 03:55 PM
Page 33 of 60
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079685
Sample: GP-21
Parameters
Lab ID: 4079685012

Results
Units
Collected: 06/13/13 00:00

LOQ
LOD
Received: 06/15/13 09:45
DF
Prepared
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Terphenyl-d14 (S)
0.0041J
0.0042J
0.022J
0.032J
0.010J
0.048
0.026J
0.037J
0.066
0.0093J
0.19
0.013J
0.021J
0.021J
0.036J
0.038J
0.15
0.18
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
66 %
108 %
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
39-130
73-155
0.0039
0.0035
0.0049
0.0048
0.0050
0.0068
0.0081
0.010
0.0062
0.0055
0.0052
0.0039
0.0059
0.0036
0.0061
0.0033
0.0039
0.0053
Matrix: Water
Analyzed
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
06/19/13 08:39
CAS No.
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
1
1
06/18/13 07:44 06/19/13 08:39 321-60-8

06/18/13 07:44 06/19/13 08:39 1718-51-0
Qual
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0

Date: 06/19/2013 03:55 PM
Page 34 of 60
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079685
Sample: GP-23
Lab ID: 4079685013
Collected: 06/13/13 00:00
Received: 06/15/13 09:45
Matrix: Solid

Parameters
Percent Moisture
Percent Moisture
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

14.3 %
0.10
0.10
06/17/13 13:03

Date: 06/19/2013 03:55 PM
Page 35 of 60
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079685
Sample: GP-23
Parameters
Lab ID: 4079685014

Results
Units
Collected: 06/13/13 00:00

LOQ
LOD
Received: 06/15/13 09:45
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Terphenyl-d14 (S)
<0.0039
<0.0035
0.0051J
0.0082J
0.0057J
<0.0068
<0.0081
<0.010
0.013J
<0.0055
0.017J
0.0043J
<0.0059
0.015J
0.032J
0.050
0.024J
0.019J
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
65 %
101 %
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
39-130
73-155
0.0039
0.0035
0.0049
0.0048
0.0050
0.0068
0.0081
0.010
0.0062
0.0055
0.0052
0.0039
0.0059
0.0036
0.0061
0.0033
0.0039
0.0053
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/19/13 08:57
06/19/13 08:57
06/19/13 08:57
06/19/13 08:57
06/19/13 08:57
06/19/13 08:57
06/19/13 08:57
06/19/13 08:57
06/19/13 08:57
06/19/13 08:57
06/19/13 08:57
06/19/13 08:57
06/19/13 08:57
06/19/13 08:57
06/19/13 08:57
06/19/13 08:57
06/19/13 08:57
06/19/13 08:57
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0
1
1
06/18/13 07:44 06/19/13 08:57 321-60-8

06/18/13 07:44 06/19/13 08:57 1718-51-0

Date: 06/19/2013 03:55 PM
Page 36 of 60
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079685
Sample: GP-25
Lab ID: 4079685015
Collected: 06/14/13 00:00
Received: 06/15/13 09:45
Matrix: Solid

Parameters
Percent Moisture
Percent Moisture
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

13.4 %
0.10
0.10
06/17/13 13:03

Date: 06/19/2013 03:55 PM
Page 37 of 60
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079685
Sample: GP-25
Parameters
Lab ID: 4079685016

Results
Units
Collected: 06/14/13 00:00

LOQ
LOD
Received: 06/15/13 09:45
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Terphenyl-d14 (S)
0.027J
0.0082J
0.032J
0.044J
0.040J
0.043J
0.027J
0.040J
0.054
0.012J
0.13
0.027J
0.023J
0.036J
0.051
0.16
0.18
0.13
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
71 %
101 %
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
39-130
73-155
0.0042
0.0038
0.0052
0.0051
0.0053
0.0073
0.0087
0.011
0.0067
0.0059
0.0056
0.0042
0.0063
0.0039
0.0066
0.0036
0.0042
0.0057
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/19/13 09:15
06/19/13 09:15
06/19/13 09:15
06/19/13 09:15
06/19/13 09:15
06/19/13 09:15
06/19/13 09:15
06/19/13 09:15
06/19/13 09:15
06/19/13 09:15
06/19/13 09:15
06/19/13 09:15
06/19/13 09:15
06/19/13 09:15
06/19/13 09:15
06/19/13 09:15
06/19/13 09:15
06/19/13 09:15
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0
1
1
06/18/13 07:44 06/19/13 09:15 321-60-8

06/18/13 07:44 06/19/13 09:15 1718-51-0

Date: 06/19/2013 03:55 PM
Page 38 of 60
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079685
Sample: TRIP BLANK

Parameters
8260 MSV
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
p-Isopropyltoluene
Methylene Chloride
Naphthalene
n-Propylbenzene
Styrene
Lab ID: 4079685017

Results
Units
Collected: 06/13/13 00:00

LOQ
LOD
Received: 06/15/13 09:45
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260

<0.50
<0.48
<0.49
<0.45
<0.23
<0.43
<0.40
<0.60
<0.42
<0.37
<0.36
<0.44
<0.69
<0.39
<0.48
<0.48
<1.5
<1.9
<0.38
<0.48
<0.44
<0.45
<0.43
<0.40
<0.28
<0.48
<0.43
<0.42
<0.37
<0.50
<0.46
<0.37
<0.51
<0.29
<0.26
<0.50
<0.50
<1.3
<0.34
<0.40
<0.36
<0.49
<2.5
<0.50
<0.35
<0.45
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
1.0
1.0
1.0
1.0
1.0
5.0
1.0
5.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
5.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
0.50
0.48
0.49
0.45
0.23
0.43
0.40
0.60
0.42
0.37
0.36
0.44
0.69
0.39
0.48
0.48
1.5
1.9
0.38
0.48
0.44
0.45
0.43
0.40
0.28
0.48
0.43
0.42
0.37
0.50
0.46
0.37
0.51
0.29
0.26
0.50
0.50
1.3
0.34
0.40
0.36
0.49
2.5
0.50
0.35
0.45
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
1634-04-4
91-20-3
103-65-1
100-42-5
630-20-6

Date: 06/19/2013 03:55 PM
Page 39 of 60
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079685
Sample: TRIP BLANK

Parameters
8260 MSV
Tetrachloroethene
Toluene
Trichloroethene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Lab ID: 4079685017

Results
Units
Collected: 06/13/13 00:00

LOQ
LOD
Received: 06/15/13 09:45
DF
Prepared
Matrix: Water
Analyzed
CAS No.
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
06/17/13 23:50
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
179601-23-1
95-47-6
1
1
1
06/17/13 23:50 460-00-4

06/17/13 23:50 1868-53-7
06/17/13 23:50 2037-26-5
Qual
Analytical Method: EPA 8260

<0.38
<0.47
<0.44
<0.77
<2.5
<0.44
<0.39
<0.43
<0.48
<0.47
<0.57
<2.5
<0.18
<0.82
<0.50
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
90 %
94 %
101 %
1.0
1.0
1.0
5.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
5.0
1.0
2.0
1.0
43-137
70-130
55-137
0.38
0.47
0.44
0.77
2.5
0.44
0.39
0.43
0.48
0.47
0.57
2.5
0.18
0.82
0.50

Date: 06/19/2013 03:55 PM
Page 40 of 60
#=QC#

Green Bay, WI 54302
(920)469-2436
QUALITY CONTROL DATA

Project:
Pace Project No.:
4079685
QC Batch:
MERP/3700
Analysis Method:
EPA 7471
QC Batch Method:
EPA 7471
Analysis Description:
7471 Mercury
Associated Lab Samples:

METHOD BLANK:
4079685001, 4079685002, 4079685003
809241

Parameter
Matrix: Solid
4079685001, 4079685002, 4079685003
Blank
Units
Result
Mercury
mg/kg
LABORATORY CONTROL SAMPLE:
809242
Parameter
Mercury
<0.0033
Spike
Conc.
Units
mg/kg
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
Parameter
Mercury
0.0067
LCS
Result
.17
0.042
Analyzed
Qualifiers
06/18/13 07:48
LCS
% Rec
0.15
809243
10231800001
Units
Result
mg/kg
Reporting
Limit
% Rec
Limits
92
Qualifiers
85-115
809244
MS
Spike
Conc.
MSD
Spike
Conc.
.2
MS
Result
.2
0.22
MSD
Result
MS
% Rec
0.21
91
MSD
% Rec
84
% Rec
Limits
85-115
Max
RPD RPD
5
Qual
20 M0

Date: 06/19/2013 03:55 PM
Page 41 of 60
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079685
QC Batch:
MPRP/8637
Analysis Method:
EPA 6010
QC Batch Method:
EPA 3050
6010 MET

METHOD BLANK:
4079685001, 4079685002, 4079685003, 4079685006, 4079685007
809183

Parameter
Matrix: Solid
4079685001, 4079685002, 4079685003, 4079685006, 4079685007
Blank
Reporting
Analyzed
Units
Result
Limit
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
809184
Parameter
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
<0.54
<0.087
<0.051
<0.13
<0.29
<0.59
<0.21
Spike
Conc.
Units
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Parameter
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Units
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
2.0
0.50
0.50
0.50
1.0
2.0
1.0
LCS
Result
50
50
50
50
50
50
25
809185
4079685001
Result
4.7
124
0.32J
12.1
200
<0.67
<0.24
06/18/13 13:34
06/18/13 13:34
06/18/13 13:34
06/18/13 13:34
06/18/13 13:34
06/18/13 13:34
06/18/13 13:34
LCS
% Rec
48.4
50.4
48.2
49.5
49.0
47.3
23.7
Qualifiers
% Rec
Limits
97
101
96
99
98
95
95
Qualifiers
80-120
80-120
80-120
80-120
80-120
80-120
80-120
809186
MS
Spike
Conc.
56.4
56.4
56.4
56.4
56.4
56.4
28.2
MSD
Spike
Conc.
56.4
56.4
56.4
56.4
56.4
56.4
28.2
MS
Result
56.6
198
53.3
67.8
188
51.8
26.4
MSD
Result
MS
% Rec
57.7
210
53.5
68.0
215
52.0
26.8
92
131
94
99
-22
92
93
MSD
% Rec
94
153
94
99
26
92
95
% Rec
Limits
75-125
75-125
75-125
75-125
75-125
75-125
75-125
Max
RPD RPD
2
6
0
0
13
0
2
Qual
20
20 M0
20
20
20 M0
20
20

Date: 06/19/2013 03:55 PM
Page 42 of 60
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079685
QC Batch:
MSV/20114
Analysis Method:
EPA 8260
QC Batch Method:
EPA 5035/5030B

METHOD BLANK:
4079685002, 4079685003, 4079685004, 4079685005, 4079685006, 4079685007, 4079685008
809326

Parameter
Matrix: Solid
4079685002, 4079685003, 4079685004, 4079685005, 4079685006, 4079685007, 4079685008
Blank
Reporting
Analyzed
Units
Result
Limit
Qualifiers
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Chlorotoluene
4-Chlorotoluene
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromomethane
Diisopropyl ether
Ethylbenzene
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<49.8
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
250
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52

Date: 06/19/2013 03:55 PM
Page 43 of 60
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079685
METHOD BLANK:
809326

Parameter
Matrix: Solid
4079685002, 4079685003, 4079685004, 4079685005, 4079685006, 4079685007, 4079685008
Blank
Reporting
Analyzed
Units
Result
Limit
Qualifiers
m&p-Xylene
Methylene Chloride
n-Butylbenzene
n-Propylbenzene
Naphthalene
o-Xylene
p-Isopropyltoluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
Trichloroethene
Vinyl chloride
Toluene-d8 (S)
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
LABORATORY CONTROL SAMPLE & LCSD:

Parameter
1,1-Dichloroethane
1,1-Dichloroethene
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzene
Bromoform
Bromomethane
Chlorobenzene
Chloroethane
<50.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
90
100
100
809327
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
120
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
49-130
57-130
54-133
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
06/17/13 11:52
809328
Spike
Conc.
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
LCS
Result
2590
2770
2570
2390
2350
2440
2650
2580
2540
2670
2710
2550
2510
2560
2840
2820
2230
2600
2550
2100
LCSD
Result
2600
2770
2550
2460
2360
2570
2670
2540
2600
2640
2620
2580
2620
2620
2830
2840
2290
2630
2590
2340
LCS LCSD
% Rec % Rec
103
111
103
96
94
98
106
103
102
107
108
102
100
102
113
113
89
104
102
84
104
111
102
98
94
103
107
102
104
105
105
103
105
105
113
114
91
105
103
93
% Rec
Limits
70-130
70-130
70-130
70-130
64-130
68-130
50-150
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
63-130
41-142
70-130
70-130
57-130
Max
RPD
RPD
1
0
1
3
0
5
1
1
2
1
3
1
5
2
0
1
2
1
1
10
Qualifiers
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20

Date: 06/19/2013 03:55 PM
Page 44 of 60
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079685

Parameter
Chloroform
Chloromethane
Ethylbenzene
m&p-Xylene
Methylene Chloride
o-Xylene
Styrene
Tetrachloroethene
Toluene
Trichloroethene
Vinyl chloride
Toluene-d8 (S)
809327
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
809328
Spike
Conc.
2500
2500
2500
2500
2500
2500
2500
2500
5000
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
LCS
Result
2400
2520
2270
2680
2700
2250
2740
2680
5480
2260
2350
2780
2490
2350
2630
2310
2870
2620
2290
2690
LCSD
Result
2440
2540
2230
2650
2780
2170
2720
2710
5550
2290
2390
2740
2460
2430
2660
2350
2870
2650
2300
2660
LCS LCSD
% Rec % Rec
96
101
91
107
108
90
109
107
110
91
94
111
100
94
105
92
115
105
91
108
107
101
105
97
102
89
106
111
87
109
108
111
91
96
109
98
97
106
94
115
106
92
107
109
102
106
% Rec
Limits
70-130
57-130
70-130
70-130
70-130
31-150
65-137
70-130
64-139
69-130
70-130
63-135
69-130
70-130
70-130
70-130
70-130
70-130
50-150
57-130
49-130
57-130
54-133
Max
RPD
RPD
1
1
2
1
3
4
0
1
1
1
2
2
2
3
1
2
0
1
1
1
Qualifiers
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20

Date: 06/19/2013 03:55 PM
Page 45 of 60
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079685
QC Batch:
MSV/20103
Analysis Method:
EPA 8260
QC Batch Method:
EPA 8260
8260 MSV

METHOD BLANK:
4079685017
809255
Matrix: Water
4079685017
Parameter
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Chlorotoluene
4-Chlorotoluene
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromomethane
Diisopropyl ether
Ethylbenzene
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Blank
Result
<0.45
<0.44
<0.38
<0.39
<0.28
<0.43
<0.51
<0.77
<0.47
<2.5
<0.57
<1.5
<0.38
<0.44
<0.48
<0.50
<2.5
<0.45
<0.46
<0.43
<0.37
<0.48
<0.48
<0.50
<0.48
<0.49
<0.45
<0.23
<0.43
<0.37
<0.36
<0.44
<0.69
<0.39
<0.42
<0.29
<1.9
<0.48
<0.40
<0.50
<0.50
<1.3
<0.34
Reporting
Limit
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
5.0
5.0
5.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
5.0
1.0
Analyzed
Qualifiers
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08

Date: 06/19/2013 03:55 PM
Page 46 of 60
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079685
METHOD BLANK:
809255
Matrix: Water
4079685017
Parameter
m&p-Xylene
Methylene Chloride
n-Butylbenzene
n-Propylbenzene
Naphthalene
o-Xylene
p-Isopropyltoluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
Trichloroethene
Vinyl chloride
Toluene-d8 (S)
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%

Parameter
1,1-Dichloroethane
1,1-Dichloroethene
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzene
Bromoform
Bromomethane
Chlorobenzene
Chloroethane
Blank
Result
Units
<0.82
<0.49
<0.36
<0.40
<0.50
<2.5
<0.50
<0.40
<0.60
<0.35
<0.42
<0.47
<0.44
<0.37
<0.26
<0.43
<0.48
<0.18
89
94
102
2.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
43-137
70-130
55-137
809256
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Reporting
Limit
Analyzed
Qualifiers
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
06/17/13 18:08
809257
Spike
Conc.
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
LCS
Result
46.2
49.1
52.2
50.9
53.4
46.4
39.7
49.9
51.4
48.7
50.2
49.1
50.9
50.6
48.2
42.6
30.5
46.7
53.0
52.2
LCSD
Result
46.9
50.4
51.8
51.6
53.3
47.8
38.3
50.9
52.0
47.9
52.7
50.3
51.8
50.4
48.7
44.2
35.2
48.8
54.1
53.6
LCS LCSD
% Rec % Rec
92
98
104
102
107
93
79
100
103
97
100
98
102
101
96
85
61
93
106
104
94
101
104
103
107
96
77
102
104
96
105
101
104
101
97
88
70
98
108
107
% Rec
Limits
70-136
70-130
70-130
70-146
70-130
70-130
46-150
70-130
70-130
70-144
70-136
70-130
70-130
70-137
70-133
59-130
41-148
70-154
70-130
70-139
Max
RPD
RPD
2
2
1
1
0
3
4
2
1
1
5
2
2
0
1
4
14
4
2
3
Qualifiers
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20

Date: 06/19/2013 03:55 PM
Page 47 of 60
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079685

Parameter
809256
Units
Chloroform
Chloromethane
Ethylbenzene
m&p-Xylene
Methylene Chloride
o-Xylene
Styrene
Tetrachloroethene
Toluene
Trichloroethene
Vinyl chloride
Toluene-d8 (S)
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
Parameter
1,1-Dichloroethane
1,1-Dichloroethene
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzene
Bromoform
Bromomethane
Chlorobenzene
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
809257
Spike
Conc.
50
50
50
50
50
50
50
50
100
50
50
50
50
50
50
50
50
50
50
50
LCS
Result
50.5
47.0
50.2
42.0
46.1
57.2
52.1
51.6
107
42.4
52.1
53.1
52.3
51.6
53.2
50.0
44.3
53.5
63.0
53.6
809376
4079576008
Result
<0.44
<0.38
<0.39
<0.28
<0.43
<2.5
<1.5
<0.38
<0.44
<0.48
<0.50
<0.45
<0.43
<0.50
<0.45
<0.23
<0.43
<0.37
<0.36
LCSD
Result
50.9
48.9
49.9
42.7
46.5
57.6
53.0
52.5
108
41.8
52.0
54.3
52.9
52.4
53.6
50.1
44.2
54.3
62.8
54.2
LCS LCSD
% Rec % Rec
101
94
100
84
92
114
104
103
107
85
104
106
105
103
106
100
89
107
126
107
97
99
101
% Rec
Limits
102
98
100
85
93
115
106
105
108
84
104
109
106
105
107
100
88
109
126
108
96
98
102
Max
RPD
RPD
70-130
45-154
70-130
70-136
70-130
20-157
70-130
70-130
70-130
59-141
70-130
70-130
70-130
70-130
70-130
70-130
55-135
70-130
50-150
61-143
43-137
70-130
55-137
1
4
1
1
1
1
2
2
2
2
0
2
1
1
1
0
0
1
0
1
Qualifiers
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
809377
MS
Spike
Conc.
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
MSD
Spike
Conc.
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
MS
Result
46.5
48.2
50.9
50.5
52.5
46.9
37.8
50.0
51.4
47.1
51.3
49.1
51.1
50.3
47.8
43.4
35.0
47.8
52.7
MSD
Result
MS
% Rec
47.4
50.9
53.8
52.2
54.2
48.3
41.4
51.9
52.7
49.0
53.2
50.9
52.1
51.7
49.7
45.1
36.5
50.1
53.7
93
96
102
101
105
92
76
100
102
94
103
98
102
101
96
87
70
96
105
MSD
% Rec
95
102
108
104
108
95
83
104
105
98
106
101
104
103
99
90
73
100
107
% Rec
Limits
70-136
70-130
70-130
70-146
70-130
70-130
46-150
70-130
70-130
70-146
70-136
70-130
70-130
70-137
70-133
57-130
41-148
70-154
70-130
Max
RPD RPD
2
6
6
3
3
3
9
4
3
4
4
4
2
3
4
4
4
5
2
Qual
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20

Date: 06/19/2013 03:55 PM
Page 48 of 60
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079685
Parameter
Chloroethane
Chloroform
Chloromethane
Ethylbenzene
m&p-Xylene
Methylene Chloride
o-Xylene
Styrene
Tetrachloroethene
Toluene
Trichloroethene
Vinyl chloride
Toluene-d8 (S)
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
809376
4079576008
Result
<0.44
<0.69
<0.39
<0.42
<0.29
<1.9
<0.40
<0.50
<0.34
<0.49
<0.36
<0.35
<0.47
<0.44
<0.37
<0.26
<0.43
<0.48
<0.18
809377
MS
Spike
Conc.
50
50
50
50
50
50
50
50
50
100
50
50
50
50
50
50
50
50
50
50
50
MSD
Spike
Conc.
50
50
50
50
50
50
50
50
50
100
50
50
50
50
50
50
50
50
50
50
50
MS
Result
52.1
50.1
47.8
49.9
42.1
46.0
54.9
51.7
51.3
106
41.5
51.4
52.6
51.7
51.1
52.9
49.3
44.6
52.9
61.5
53.0
MSD
Result
MS
% Rec
53.7
52.0
50.3
51.7
44.0
47.7
56.7
52.6
52.2
109
44.1
52.7
53.9
52.8
52.8
53.8
51.8
46.0
54.0
62.8
54.7
104
100
96
100
84
92
110
103
102
106
83
103
105
103
102
105
99
89
106
123
106
96
99
102
MSD
% Rec
107
104
101
103
88
95
113
105
104
109
88
105
108
106
106
107
104
92
108
126
109
95
99
101
% Rec
Limits
70-140
70-130
45-154
70-130
70-136
70-130
10-157
70-130
70-130
70-130
59-141
70-130
70-130
35-164
70-130
70-130
70-130
55-137
70-130
50-150
59-144
43-137
70-130
55-137
Max
RPD RPD
3
4
5
4
4
4
3
2
2
3
6
3
3
2
3
2
5
3
2
2
3
Qual
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20

Date: 06/19/2013 03:55 PM
Page 49 of 60
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079685
QC Batch:
OEXT/18642
Analysis Method:
EPA 8082
QC Batch Method:
EPA 3541
8082 GCS PCB

METHOD BLANK:
4079685008
809863
Matrix: Solid
4079685008
Parameter
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
809864
Parameter

Spike
Conc.
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
50.0
50.0
50.0
50.0
50.0
50.0
50.0
48-130
40-130
LCS
Result
809865
<29.4
<29.4
<29.4
<29.4
<29.4
<29.4
<29.4
Analyzed
Qualifiers
06/19/13 10:06
06/19/13 10:06
06/19/13 10:06
06/19/13 10:06
06/19/13 10:06
06/19/13 10:06
06/19/13 10:06
06/19/13 10:06
06/19/13 10:06
LCS
% Rec
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
507
500
4079703001
Units
Result
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
Reporting
Limit
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
97
79
Parameter
Blank
Result
Units
% Rec
Limits
101
102
84
Qualifiers
70-130
48-130
40-130
809866
MS
Spike
Conc.
588
MSD
Spike
Conc.
588
MS
Result
<29.4
<29.4
<29.4
<29.4
<29.4
<29.4
594
MSD
Result
MS
% Rec
<29.4
<29.4
<29.4
<29.4
<29.4
<29.4
602
101
98
83
MSD
% Rec
102
101
89
% Rec
Limits
40-149
48-130
40-130
Max
RPD RPD
Qual
31
31
31
31
31
31
31

Date: 06/19/2013 03:55 PM
Page 50 of 60
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079685
QC Batch:
OEXT/18628
Analysis Method:
EPA 8270 by SIM
QC Batch Method:
EPA 3546
8270/3546 MSSV PAH by SIM

METHOD BLANK:
4079685001, 4079685004, 4079685005, 4079685006, 4079685007, 4079685008, 4079685009, 4079685011
809525

Parameter
Matrix: Solid
4079685001, 4079685004, 4079685005, 4079685006, 4079685007, 4079685008, 4079685009, 4079685011
Blank
Reporting
Analyzed
Units
Result
Limit
Qualifiers
1-Methylnaphthalene
2-Methylnaphthalene
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
Naphthalene
Phenanthrene
Pyrene
Terphenyl-d14 (S)
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
809526
Parameter
1-Methylnaphthalene
2-Methylnaphthalene
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
Naphthalene
Phenanthrene
<2.9
<8.3
<8.3
<8.3
<8.3
<8.3
<3.0
<8.3
<8.3
<2.9
<8.3
<8.3
<8.3
<8.3
<8.3
<8.3
<8.3
<8.3
61
70
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Spike
Conc.
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
40-130
40-130
LCS
Result
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
% Rec
Limits
LCS
% Rec
223
205
253
248
265
200
228
223
234
230
262
243
218
248
236
194
213
67
61
76
74
80
60
68
67
70
69
78
73
65
74
71
58
64
Qualifiers
47-130
48-130
55-130
55-130
66-130
55-130
56-130
53-130
51-130
52-130
58-130
55-130
62-130
58-130
54-130
41-130
60-130

Date: 06/19/2013 03:55 PM
Page 51 of 60
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079685
809526
Parameter
Pyrene
Terphenyl-d14 (S)
ug/kg
%
%
Parameter
1-Methylnaphthalene
2-Methylnaphthalene
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
Naphthalene
Phenanthrene
Pyrene
Terphenyl-d14 (S)
Spike
Conc.
Units
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
333
220
809527
4079703008
Result
<3.4
<9.6
<9.6
<9.6
<9.6
<9.6
<3.4
<9.6
<9.6
<3.4
<9.6
<9.6
<9.6
<9.6
<9.6
<9.6
<9.6
<9.6
LCS
% Rec
LCS
Result
% Rec
Limits
66
71
76
Qualifiers
51-130
40-130
40-130
809528
MS
Spike
Conc.
384
384
384
384
384
384
384
384
384
384
384
384
384
384
384
384
384
384
MSD
Spike
Conc.
384
384
384
384
384
384
384
384
384
384
384
384
384
384
384
384
384
384
MS
Result
228
217
261
260
271
186
236
187
225
259
270
235
219
249
231
216
222
214
MSD
Result
MS
% Rec
215
222
263
252
258
153
194
150
195
239
237
198
195
191
202
227
199
187
59
57
68
68
71
48
61
49
58
67
70
61
57
65
60
56
58
56
67
65
MSD
% Rec
56
58
68
66
67
40
50
39
51
62
62
52
51
50
53
59
52
49
62
54
% Rec
Limits
42-130
34-130
31-130
32-130
39-131
29-130
35-130
21-142
12-134
35-130
37-130
23-130
29-137
32-130
17-134
24-130
27-135
24-130
40-130
40-130
Max
RPD RPD
6
2
1
3
5
20
19
22
14
8
13
17
11
27
13
5
11
13
Qual
32
35
35
25
38
30
33
44
33
37
38
27
50
32
28
40
46
49

Date: 06/19/2013 03:55 PM
Page 52 of 60
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079685
QC Batch:
OEXT/18634
Analysis Method:
EPA 8270 by HVI
QC Batch Method:
EPA 3510
8270 Water PAH by HVI

METHOD BLANK:
4079685010, 4079685012, 4079685014, 4079685016
809563

Parameter
1-Methylnaphthalene
2-Methylnaphthalene
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
Naphthalene
Phenanthrene
Pyrene
Terphenyl-d14 (S)
Matrix: Water
4079685010, 4079685012, 4079685014, 4079685016
Blank
Reporting
Units
Result
Limit
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%

Parameter
1-Methylnaphthalene
2-Methylnaphthalene
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
Naphthalene
Phenanthrene
<0.0040
<0.0068
<0.0043
<0.0039
<0.0054
<0.0053
<0.0055
<0.0075
<0.0090
<0.012
<0.0069
<0.0061
<0.0058
<0.0043
<0.0065
<0.0037
<0.0043
<0.0059
69
116
809564
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
39-130
73-155
Analyzed
Qualifiers
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
809565
LCS
Result
Spike
Conc.
.2
.2
.2
.2
.2
.2
.2
.2
.2
.2
.2
.2
.2
.2
.2
.2
.2
0.11
0.11
0.15
0.15
0.17
0.21
0.19
0.20
0.19
0.21
0.21
0.19
0.19
0.15
0.19
0.14
0.17
LCSD
Result
0.11
0.11
0.15
0.15
0.18
0.20
0.19
0.20
0.19
0.21
0.21
0.19
0.19
0.15
0.19
0.12
0.17
LCS LCSD
% Rec % Rec
54
54
75
75
87
103
93
99
94
107
104
93
95
76
93
69
87
54
53
74
73
89
101
95
100
94
106
106
93
93
77
93
61
86
% Rec
Limits
23-130
22-130
31-130
31-130
26-130
47-130
41-130
37-130
37-130
51-130
50-130
34-130
49-130
30-130
36-130
24-130
39-130
Max
RPD
RPD
1
1
1
2
2
2
3
2
0
1
2
0
2
1
1
11
0
Qualifiers
49
50
34
37
35
27
28
27
29
26
26
30
26
34
29
40
30

Date: 06/19/2013 03:55 PM
Page 53 of 60
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079685

Parameter
Pyrene
Terphenyl-d14 (S)
809564
Units
ug/L
%
%
809565
Spike
Conc.
LCS
Result
.2
0.22
LCSD
Result
0.21
LCS LCSD
% Rec % Rec
108
68
101
106
66
101
% Rec
Limits
47-130
39-130
73-155
Max
RPD
RPD
2
Qualifiers
25

Date: 06/19/2013 03:55 PM
Page 54 of 60
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079685
QC Batch:
PMST/8578
Analysis Method:
ASTM D2974-87
QC Batch Method:
ASTM D2974-87
Dry Weight/Percent Moisture

SAMPLE DUPLICATE:
4079685001, 4079685004, 4079685005, 4079685006, 4079685007, 4079685008, 4079685009, 4079685011,

4079685013, 4079685015
809329
Parameter
Percent Moisture
Units
%
4079693002
Result
17.6
Dup
Result
Max
RPD
RPD
18.2
Qualifiers
10

Date: 06/19/2013 03:55 PM
Page 55 of 60
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079685
QC Batch:
PMST/8583
Analysis Method:
ASTM D2974-87
QC Batch Method:
ASTM D2974-87

SAMPLE DUPLICATE:
4079685002, 4079685003
809467
Parameter
Percent Moisture
Units
%
4079685002
Result
18.1
Dup
Result
Max
RPD
RPD
18.0
Qualifiers
10

Date: 06/19/2013 03:55 PM
Page 56 of 60
#=QL#

Green Bay, WI 54302
(920)469-2436
QUALIFIERS
Project:
Pace Project No.:
4079685
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-G
Pace Analytical Services - Green Bay
BATCH QUALIFIERS
Batch: MSV/20115
[M5]
A matrix spike/matrix spike duplicate was not performed for this batch due to insufficient sample volume.
Batch: MSSV/5759
Benzo(b)fluoranthene and benzo(k)fluoranthene were in the check standard but did not meet the resolution criteria in
[IP]
SW846 Method 8270C. Whereas sample results included are reported as individual isomers, the lab and the customer
must recognize them as an isomeric pair.
Batch: MSSV/5762
[M5]
ANALYTE QUALIFIERS
M0
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
Non-detect results are reported on a wet weight basis.

Date: 06/19/2013 03:55 PM
Page 57 of 60
#=CR#

Green Bay, WI 54302
(920)469-2436
QUALITY CONTROL DATA CROSS REFERENCE TABLE

Project:
Pace Project No.:
4079685
Analytical Method
Analytical
Batch
Lab ID
Sample ID
QC Batch Method
QC Batch
4079685008
GP-19
EPA 3541
OEXT/18642 EPA 8082
GCSV/9725
4079685001
4079685002
4079685003
4079685006
4079685007
GP-12
GP-15
GP-16
GP-18(S)
GP-18(D)
EPA 3050
EPA 3050
EPA 3050
EPA 3050
EPA 3050
MPRP/8637
MPRP/8637
MPRP/8637
MPRP/8637
MPRP/8637
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
ICP/7673
ICP/7673
ICP/7673
ICP/7673
ICP/7673
4079685001
4079685002
4079685003
GP-12
GP-15
GP-16
EPA 7471
EPA 7471
EPA 7471
MERP/3700
MERP/3700
MERP/3700
EPA 7471
EPA 7471
EPA 7471
MERC/4611
MERC/4611
MERC/4611
4079685001
4079685004
4079685005
4079685006
4079685007
4079685008
4079685009
4079685011
GP-12
GP-17(S)
GP-17(D)
GP-18(S)
GP-18(D)
GP-19
GP-20
GP-21
EPA 3546
EPA 3546
EPA 3546
EPA 3546
EPA 3546
EPA 3546
EPA 3546
EPA 3546
OEXT/18628
OEXT/18628
OEXT/18628
OEXT/18628
OEXT/18628
OEXT/18628
OEXT/18628
OEXT/18628
EPA 8270 by SIM

EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
MSSV/5759
MSSV/5759
MSSV/5759
MSSV/5759
MSSV/5759
MSSV/5759
MSSV/5759
MSSV/5759
4079685010
4079685012
GP-20
GP-21
EPA 3510
EPA 3510
OEXT/18634 EPA 8270 by HVI

OEXT/18634 EPA 8270 by HVI
MSSV/5762
MSSV/5762
4079685002
4079685003
4079685004
4079685005
4079685006
4079685007
4079685008
GP-15
GP-16
GP-17(S)
GP-17(D)
GP-18(S)
GP-18(D)
GP-19
EPA 5035/5030B
EPA 5035/5030B
EPA 5035/5030B
EPA 5035/5030B
EPA 5035/5030B
EPA 5035/5030B
EPA 5035/5030B
MSV/20114
MSV/20114
MSV/20114
MSV/20114
MSV/20114
MSV/20114
MSV/20114
MSV/20115
MSV/20115
MSV/20115
MSV/20115
MSV/20115
MSV/20115
MSV/20115
4079685017
TRIP BLANK
EPA 8260
MSV/20103
4079685001
GP-12
ASTM D2974-87
PMST/8578
4079685002
4079685003
GP-15
GP-16
ASTM D2974-87
ASTM D2974-87
PMST/8583
PMST/8583
4079685004
4079685005
4079685006
4079685007
4079685008
4079685009
4079685011
4079685013
4079685015
GP-17(S)
GP-17(D)
GP-18(S)
GP-18(D)
GP-19
GP-20
GP-21
GP-23
GP-25
ASTM D2974-87
ASTM D2974-87
ASTM D2974-87
ASTM D2974-87
ASTM D2974-87
ASTM D2974-87
ASTM D2974-87
ASTM D2974-87
ASTM D2974-87
PMST/8578
PMST/8578
PMST/8578
PMST/8578
PMST/8578
PMST/8578
PMST/8578
PMST/8578
PMST/8578
EPA 8260
EPA 8260
EPA 8260
EPA 8260
EPA 8260
EPA 8260
EPA 8260

Date: 06/19/2013 03:55 PM
Page 58 of 60
Page 59 of 60
Page 60 of 60
#=CL#

Green Bay, WI 54302
(920)469-2436

June 26, 2013
Mitchell Banach

Sincerely,
Steven Mleczko
Project Manager
Enclosures

Page 1 of 11
#=CP#

Green Bay, WI 54302
(920)469-2436
CERTIFICATIONS
Project:
Pace Project No.:
4079686



Page 2 of 11
#=SS#

Green Bay, WI 54302
(920)469-2436
SAMPLE SUMMARY
Project:
Pace Project No.:
4079686
Lab ID
Sample ID
Matrix
Date Collected
Date Received
4079686001
GP-15
Water
06/14/13 00:00
06/15/13 09:45
4079686002
GP-16
Water
06/14/13 00:00
06/15/13 09:45

Page 3 of 11
#=SA#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079686
Lab ID
Sample ID
4079686002
GP-16
Method
Analysts
EPA 6010
DLB
Analytes
Reported
1
Laboratory
PASI-G

Page 4 of 11
#=HO#

Green Bay, WI 54302
(920)469-2436
HITS ONLY
Project:
Pace Project No.:
4079686
Lab Sample ID
Client Sample ID
Method
Parameters
4079686002
GP-16
EPA 6010
Lead, Dissolved
Result
Units
35.5 ug/L
Report Limit
7.5
Analyzed
Qualifiers
06/25/13 16:00

Page 5 of 11
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079686
Sample: GP-16
Parameters
6010 MET ICP, Dissolved
Lead, Dissolved
Lab ID: 4079686002

Results
Units
Collected: 06/14/13 00:00

LOQ
LOD
Received: 06/15/13 09:45
DF
Prepared
Analyzed
Matrix: Water
CAS No.
Qual

35.5 ug/L
7.5
2.7
06/24/13 15:50 06/25/13 16:00 7439-92-1

Date: 06/26/2013 01:09 PM
Page 6 of 11
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079686
QC Batch:
MPRP/8681
Analysis Method:
EPA 6010
QC Batch Method:
EPA 3010
6010 MET Dissolved

METHOD BLANK:
4079686002
813229
Matrix: Water
4079686002
Parameter
Lead, Dissolved
ug/L
813230
Parameter
Lead, Dissolved
Spike
Conc.
ug/L
Units
ug/L
Reporting
Limit
<2.7
Units
Lead, Dissolved
Parameter
Blank
Result
Units
7.5
LCS
Result
500
4079686002
Result
35.5
Qualifiers
06/25/13 15:56
LCS
% Rec
477
813231
Analyzed
% Rec
Limits
95
Qualifiers
80-120
813232
MS
Spike
Conc.
500
MSD
Spike
Conc.
500
MS
Result
496
MSD
Result
MS
% Rec
505
92
MSD
% Rec
94
% Rec
Limits
75-125
Max
RPD RPD
2
Qual
20

Date: 06/26/2013 01:09 PM
Page 7 of 11
#=QL#

Green Bay, WI 54302
(920)469-2436
QUALIFIERS
Project:
Pace Project No.:
4079686
DEFINITIONS
S - Surrogate
LABORATORIES
PASI-G

Date: 06/26/2013 01:09 PM
Page 8 of 11
#=CR#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079686
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
4079686002
GP-16
EPA 3010
MPRP/8681
EPA 6010
ICP/7703

Date: 06/26/2013 01:09 PM
Page 9 of 11
Page 10 of 11
Page 11 of 11
#=CL#

Green Bay, WI 54302
(920)469-2436

June 19, 2013
Mitchell Banach

Sincerely,
Steven Mleczko
Project Manager
Enclosures

Page 1 of 63
#=CP#

Green Bay, WI 54302
(920)469-2436
CERTIFICATIONS
Project:
Pace Project No.:
4079703



Page 2 of 63
#=SS#

Green Bay, WI 54302
(920)469-2436
SAMPLE SUMMARY
Project:
Pace Project No.:
4079703
Lab ID
Sample ID
Matrix
Date Collected
Date Received
4079703001
GP-1
Solid
06/14/13 00:00
06/15/13 12:01
4079703002
GP-2
Solid
06/14/13 00:00
06/15/13 12:01
4079703003
GP-3
Solid
06/14/13 00:00
06/15/13 12:01
4079703004
GP-4
Solid
06/14/13 00:00
06/15/13 12:01
4079703005
GP-5
Solid
06/14/13 00:00
06/15/13 12:01
4079703006
GP-6(S)
Solid
06/14/13 00:00
06/15/13 12:01
4079703007
GP-6(D)
Solid
06/14/13 00:00
06/15/13 12:01
4079703008
GP-7
Solid
06/14/13 00:00
06/15/13 12:01
4079703009
GP-8
Solid
06/14/13 00:00
06/15/13 12:01
4079703010
GP-9
Solid
06/14/13 00:00
06/15/13 12:01
4079703011
GP-10
Solid
06/14/13 00:00
06/15/13 12:01
4079703012
GP-11
Solid
06/14/13 00:00
06/15/13 12:01
4079703013
GP-13
Solid
06/14/13 00:00
06/15/13 12:01
4079703014
GP-14
Solid
06/14/13 00:00
06/15/13 12:01
4079703015
GP-22
Solid
06/14/13 00:00
06/15/13 12:01
4079703016
GP-26
Solid
06/14/13 00:00
06/15/13 12:01
4079703017
GP-2(D)
Solid
06/14/13 00:00
06/15/13 12:01

Page 3 of 63
#=SA#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079703
Lab ID
Sample ID
4079703001
GP-1
4079703002
4079703003
4079703004
4079703005
4079703006
4079703007
4079703008
4079703009
GP-2
GP-3
GP-4
GP-5
GP-6(S)
GP-6(D)
GP-7
GP-8
Analytes
Reported
Method
Analysts
Laboratory
EPA 8082
BLM
10
PASI-G
EPA 6010
DLB
PASI-G
EPA 7471
CMS
PASI-G
EPA 8270 by SIM
ARO
20
PASI-G
ASTM D2974-87
SKW
PASI-G
EPA 8082
BLM
10
PASI-G
EPA 6010
DLB
PASI-G
EPA 7471
CMS
PASI-G
EPA 8270 by SIM
ARO
20
PASI-G
ASTM D2974-87
SKW
PASI-G
EPA 8082
BLM
10
PASI-G
EPA 6010
DLB
PASI-G
EPA 7471
CMS
PASI-G
EPA 8270 by SIM
ARO
20
PASI-G
ASTM D2974-87
SKW
PASI-G
EPA 8082
BLM
10
PASI-G
EPA 6010
DLB
PASI-G
EPA 7471
CMS
PASI-G
EPA 8270 by SIM
ARO
20
PASI-G
ASTM D2974-87
SKW
PASI-G
EPA 8082
BLM
10
PASI-G
EPA 6010
DLB
PASI-G
EPA 7471
CMS
PASI-G
EPA 8270 by SIM
ARO
20
PASI-G
ASTM D2974-87
SKW
PASI-G
EPA 8270 by SIM
ARO
20
PASI-G
EPA 8260
SMT
64
PASI-G
ASTM D2974-87
SKW
PASI-G
EPA 8270 by SIM
ARO
20
PASI-G
EPA 8260
SMT
64
PASI-G
ASTM D2974-87
SKW
PASI-G
EPA 8270 by SIM
ARO
20
PASI-G
EPA 8260
SMT
64
PASI-G
ASTM D2974-87
SKW
PASI-G
EPA 8270 by SIM
ARO
20
PASI-G
EPA 8260
SMT
64
PASI-G
ASTM D2974-87
SKW
PASI-G

Page 4 of 63
#=SA#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079703
Lab ID
Sample ID
4079703010
GP-9
4079703011
4079703012
4079703013
4079703014
4079703015
4079703016
4079703017
GP-10
GP-11
GP-13
GP-14
GP-22
GP-26
GP-2(D)
Analytes
Reported
Method
Analysts
EPA 8270 by SIM
ARO
20
Laboratory
PASI-G
EPA 8260
SMT
64
PASI-G
ASTM D2974-87
SKW
PASI-G
EPA 6010
DLB
PASI-G
EPA 7471
CMS
PASI-G
EPA 8270 by SIM
ARO
20
PASI-G
ASTM D2974-87
SKW
PASI-G
EPA 6010
DLB
PASI-G
EPA 7471
CMS
PASI-G
EPA 8270 by SIM
ARO
20
PASI-G
ASTM D2974-87
SKW
PASI-G
EPA 6010
DLB
PASI-G
EPA 7471
CMS
PASI-G
EPA 8270 by SIM
ARO
20
PASI-G
ASTM D2974-87
SKW
PASI-G
EPA 6010
DLB
PASI-G
EPA 7471
CMS
PASI-G
EPA 8270 by SIM
ARO
20
PASI-G
ASTM D2974-87
SKW
PASI-G
EPA 6010
DLB
PASI-G
EPA 7471
CMS
PASI-G
EPA 8270 by SIM
ARO
20
PASI-G
ASTM D2974-87
SKW
PASI-G
EPA 6010
DLB
PASI-G
EPA 7471
CMS
PASI-G
EPA 8270 by SIM
ARO
20
PASI-G
EPA 8260
SMT
64
PASI-G
ASTM D2974-87
SKW
PASI-G
EPA 8270 by SIM
ARO
20
PASI-G
ASTM D2974-87
SKW
PASI-G

Page 5 of 63
#=HO#

Green Bay, WI 54302
(920)469-2436
HITS ONLY
Project:
Pace Project No.:
4079703
Lab Sample ID
Client Sample ID
Method
Parameters
4079703001
GP-1
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 7471
ASTM D2974-87
Arsenic
Barium
Cadmium
Chromium
Lead
Silver
Mercury
Percent Moisture
Result
4079703002
GP-2
EPA 8082
EPA 8082
EPA 8082
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 7471
ASTM D2974-87

PCB, Total
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Percent Moisture
4079703003
GP-3
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 7471
ASTM D2974-87
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Percent Moisture
4079703004
GP-4
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 7471
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
1-Methylnaphthalene
2-Methylnaphthalene
Units
Report Limit
Analyzed
50.6
96.6
1.8
23.4
310
0.30J
0.11
14.9
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
%
2.3
0.57
0.57
0.57
1.1
1.1
0.0077
0.10
06/18/13 14:03
06/18/13 14:03
06/18/13 14:03
06/18/13 14:03
06/18/13 14:03
06/18/13 14:03
06/18/13 08:12
06/18/13 13:16
83.4
41.7J
125
6.4
72.1
0.19J
17.9
8.9
0.039
14.1
ug/kg
ug/kg
ug/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
%
58.2
58.2
58.2
2.0
0.49
0.49
0.49
0.98
0.0061
0.10
06/19/13 11:16
06/19/13 11:16
06/19/13 11:16
06/18/13 14:05
06/18/13 14:05
06/18/13 14:05
06/18/13 14:05
06/18/13 14:05
06/18/13 08:14
06/18/13 13:16
8.6
68.7
0.41J
13.5
25.6
0.012
13.7
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
%
2.1
0.51
0.51
0.51
1.0
0.0072
0.10
06/18/13 14:07
06/18/13 14:07
06/18/13 14:07
06/18/13 14:07
06/18/13 14:07
06/18/13 08:17
06/18/13 13:16
5.6
54.7
0.39J
13.6
11.7
0.023
17.3J
33.9
36.6
49.1
31.3
27.1
65.7
12.3J
49.0
23.0
36.5
38.9
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
2.3
0.57
0.57
0.57
1.1
0.0071
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
06/18/13 14:14
06/18/13 14:14
06/18/13 14:14
06/18/13 14:14
06/18/13 14:14
06/18/13 08:19
06/18/13 18:17
06/18/13 18:17
06/18/13 18:17
06/18/13 18:17
06/18/13 18:17
06/18/13 18:17
06/18/13 18:17
06/18/13 18:17
06/18/13 18:17
06/18/13 18:17
06/18/13 18:17
06/18/13 18:17
Qualifiers

Page 6 of 63
#=HO#

Green Bay, WI 54302
(920)469-2436
HITS ONLY
Project:
Pace Project No.:
4079703
Lab Sample ID
Client Sample ID
Method
Parameters
Result
4079703004
GP-4
EPA 8270 by SIM

EPA 8270 by SIM
EPA 8270 by SIM
ASTM D2974-87
Naphthalene
Phenanthrene
Pyrene
Percent Moisture
4079703005
GP-5
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 7471
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
ASTM D2974-87
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Mercury
Acenaphthene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Percent Moisture
4079703006
GP-6(S)
EPA 8270 by SIM

EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
1-Methylnaphthalene
Phenanthrene
Pyrene
Units
Report Limit
Analyzed
19.7J
78.0
53.1
18.0
ug/kg
ug/kg
ug/kg
%
20.3
20.3
20.3
0.10
06/18/13 18:17
06/18/13 18:17
06/18/13 18:17
06/18/13 13:16
24.5
24.3
0.68
15.4
21.2
1.8J
0.32J
0.45
232
693
915
858
1120
560
585
1180
165
2520
268
487
120
131
593
2380
1990
29.7
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
2.6
0.64
0.64
0.64
1.3
2.6
1.3
0.0092
119
119
119
119
119
119
119
119
119
119
119
119
119
119
119
119
119
0.10
06/18/13 14:16
06/18/13 14:16
06/18/13 14:16
06/18/13 14:16
06/18/13 14:16
06/18/13 14:16
06/18/13 14:16
06/18/13 08:21
06/19/13 10:11
06/19/13 10:11
06/19/13 10:11
06/19/13 10:11
06/19/13 10:11
06/19/13 10:11
06/19/13 10:11
06/19/13 10:11
06/19/13 10:11
06/19/13 10:11
06/19/13 10:11
06/19/13 10:11
06/19/13 10:11
06/19/13 10:11
06/19/13 10:11
06/19/13 10:11
06/19/13 10:11
06/18/13 13:16
141
80.6
237
252
285
247
153
314
74.1
383
174
9.3J
212
596
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
40.1
40.1
40.1
40.1
40.1
40.1
40.1
40.1
40.1
40.1
40.1
40.1
40.1
40.1
06/19/13 08:43
06/19/13 08:43
06/19/13 08:43
06/19/13 08:43
06/19/13 08:43
06/19/13 08:43
06/19/13 08:43
06/19/13 08:43
06/19/13 08:43
06/19/13 08:43
06/19/13 08:43
06/19/13 08:43
06/19/13 08:43
06/19/13 08:43
Qualifiers

Page 7 of 63
#=HO#

Green Bay, WI 54302
(920)469-2436
HITS ONLY
Project:
Pace Project No.:
4079703
Lab Sample ID
Client Sample ID
Method
Parameters
Result
4079703006
GP-6(S)
ASTM D2974-87
Percent Moisture
4079703007
GP-6(D)
EPA 8270 by SIM

EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
ASTM D2974-87
Benzo(a)pyrene
Chrysene
Fluoranthene
Pyrene
Percent Moisture
4079703008
GP-7
ASTM D2974-87
Percent Moisture
16.9 %
4079703009
GP-8
EPA 8270 by SIM

ASTM D2974-87
Percent Moisture
4079703010
GP-9
ASTM D2974-87
Percent Moisture
Units
4079703011
GP-10
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 7471
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
ASTM D2974-87
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Percent Moisture
4079703012
GP-11
EPA 6010
EPA 6010
Arsenic
Barium
Report Limit
Analyzed
0.10
06/18/13 14:21
20.3
20.3
20.3
20.3
20.3
20.3
0.10
06/18/13 19:08
06/18/13 19:08
06/18/13 19:08
06/18/13 19:08
06/18/13 19:08
06/18/13 19:08
06/18/13 14:22
13.3 %
0.10
06/18/13 14:22
4.4J ug/kg
18.6 %
20.5
0.10
06/18/13 17:25
06/18/13 14:22
16.6 %
0.10
06/18/13 14:22
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
2.1
0.54
0.54
0.54
1.1
0.0064
19.8
19.8
19.8
19.8
19.8
19.8
19.8
19.8
19.8
19.8
19.8
19.8
19.8
19.8
19.8
19.8
19.8
0.10
06/18/13 14:18
06/18/13 14:18
06/18/13 14:18
06/18/13 14:18
06/18/13 14:18
06/18/13 08:23
06/18/13 19:25
06/18/13 19:25
06/18/13 19:25
06/18/13 19:25
06/18/13 19:25
06/18/13 19:25
06/18/13 19:25
06/18/13 19:25
06/18/13 19:25
06/18/13 19:25
06/18/13 19:25
06/18/13 19:25
06/18/13 19:25
06/18/13 19:25
06/18/13 19:25
06/18/13 19:25
06/18/13 19:25
06/18/13 14:22
4.9 mg/kg
101 mg/kg
2.3
0.58
06/18/13 14:20
06/18/13 14:20
10.0J
11.6J
9.2J
12.8J
13.6J
13.6J
17.9
2.6
14.6
0.23J
5.8
6.9
0.024
20.6
16.2J
102
285
384
470
283
328
392
103
510
20.8
252
11.0J
11.4J
313
449
15.6
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
Qualifiers

Page 8 of 63
#=HO#

Green Bay, WI 54302
(920)469-2436
HITS ONLY
Project:
Pace Project No.:
4079703
Lab Sample ID
Client Sample ID
Method
Parameters
Result
4079703012
GP-11
EPA 6010
EPA 6010
EPA 6010
EPA 7471
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
ASTM D2974-87
Cadmium
Chromium
Lead
Mercury
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
1-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Percent Moisture
4079703013
GP-13
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 7471
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
ASTM D2974-87
Arsenic
Barium
Cadmium
Chromium
Lead
Silver
Mercury
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
Phenanthrene
Pyrene
Percent Moisture
4079703014
GP-14
EPA 6010
Arsenic
Units
Report Limit
Analyzed
0.78
14.3
69.9
0.10
18.5J
89.3
132
133
102
89.5
132
24.1
194
81.9
9.2J
21.4J
140
200
25.1
mg/kg
mg/kg
mg/kg
mg/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
0.58
0.58
1.2
0.0083
22.3
22.3
22.3
22.3
22.3
22.3
22.3
22.3
22.3
22.3
22.3
22.3
22.3
22.3
0.10
06/18/13 14:20
06/18/13 14:20
06/18/13 14:20
06/18/13 08:25
06/19/13 09:52
06/19/13 09:52
06/19/13 09:52
06/19/13 09:52
06/19/13 09:52
06/19/13 09:52
06/19/13 09:52
06/19/13 09:52
06/19/13 09:52
06/19/13 09:52
06/19/13 09:52
06/19/13 09:52
06/19/13 09:52
06/19/13 09:52
06/18/13 14:22
19.0
85.8
3.1
30.9
404
0.47J
0.10
393J
588J
1710
3610
3580
4710
2290
2120
4930
827
9870
1020
2010
414J
9470
7700
15.1
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
2.2
0.56
0.56
0.56
1.1
1.1
0.0073
785
785
785
785
785
785
785
785
785
785
785
785
785
785
785
785
0.10
06/18/13 14:23
06/18/13 14:23
06/18/13 14:23
06/18/13 14:23
06/18/13 14:23
06/18/13 14:23
06/18/13 08:27
06/19/13 09:17
06/19/13 09:17
06/19/13 09:17
06/19/13 09:17
06/19/13 09:17
06/19/13 09:17
06/19/13 09:17
06/19/13 09:17
06/19/13 09:17
06/19/13 09:17
06/19/13 09:17
06/19/13 09:17
06/19/13 09:17
06/19/13 09:17
06/19/13 09:17
06/19/13 09:17
06/18/13 14:22
15.4 mg/kg
4.1
06/19/13 09:18
Qualifiers

Page 9 of 63
#=HO#

Green Bay, WI 54302
(920)469-2436
HITS ONLY
Project:
Pace Project No.:
4079703
Lab Sample ID
Client Sample ID
Method
Parameters
Result
4079703014
GP-14
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 7471
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
ASTM D2974-87
Barium
Cadmium
Chromium
Lead
Silver
Mercury
Acenaphthene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Percent Moisture
4079703015
GP-22
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 7471
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
ASTM D2974-87
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Percent Moisture
Units
Report Limit
Analyzed
134
2.1
13.8
1190
0.43J
0.068
798
2340
3160
3290
4290
2180
2340
4730
565J
10600
860
1920
169J
1010
9560
7800
12.8
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
0.52
1.0
0.52
2.1
1.0
0.0072
764
764
764
764
764
764
764
764
764
764
764
764
764
764
764
764
0.10
06/18/13 14:25
06/19/13 09:18
06/18/13 14:25
06/19/13 09:18
06/18/13 14:25
06/18/13 08:29
06/19/13 09:34
06/19/13 09:34
06/19/13 09:34
06/19/13 09:34
06/19/13 09:34
06/19/13 09:34
06/19/13 09:34
06/19/13 09:34
06/19/13 09:34
06/19/13 09:34
06/19/13 09:34
06/19/13 09:34
06/19/13 09:34
06/19/13 09:34
06/19/13 09:34
06/19/13 09:34
06/18/13 14:22
5.8
45.4
0.61
14.7
82.7
0.070
29.2
24.8
125
184
257
134
186
228
52.5
171
112
89.5
137
248
136
179
8.1
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
1.9
0.46
0.46
0.46
0.93
0.0067
18.1
18.1
18.1
18.1
18.1
18.1
18.1
18.1
18.1
18.1
18.1
18.1
18.1
18.1
18.1
18.1
0.10
06/18/13 14:27
06/18/13 14:27
06/18/13 14:27
06/18/13 14:27
06/18/13 14:27
06/18/13 08:31
06/19/13 13:23
06/19/13 13:23
06/19/13 13:23
06/19/13 13:23
06/19/13 13:23
06/19/13 13:23
06/19/13 13:23
06/19/13 13:23
06/19/13 13:23
06/19/13 13:23
06/19/13 13:23
06/19/13 13:23
06/19/13 13:23
06/19/13 13:23
06/19/13 13:23
06/19/13 13:23
06/18/13 14:22
Qualifiers

Page 10 of 63
#=HO#

Green Bay, WI 54302
(920)469-2436
HITS ONLY
Project:
Pace Project No.:
4079703
Lab Sample ID
Client Sample ID
Method
Parameters
4079703016
GP-26
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 7471
ASTM D2974-87
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Percent Moisture
4079703017
GP-2(D)
ASTM D2974-87
Percent Moisture
Result
7.1
60.8
0.37J
13.4
186
0.036
10.3
Units
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
%
10.3 %
Report Limit
Analyzed
2.1
0.53
0.53
0.53
1.1
0.0058
0.10
06/18/13 14:30
06/18/13 14:30
06/18/13 14:30
06/18/13 14:30
06/18/13 14:30
06/18/13 08:37
06/18/13 14:22
0.10
06/18/13 14:22
Qualifiers

Page 11 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-1
Lab ID: 4079703001
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
8082 GCS PCB
PCB, Total
Surrogates
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7471 Mercury
Mercury
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

<29.4
<29.4
<29.4
<29.4
<29.4
<29.4
<29.4
<29.4
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
89 %
102 %
58.8
58.8
58.8
58.8
58.8
58.8
58.8
58.8
29.4
29.4
29.4
29.4
29.4
29.4
29.4
29.4
40-130
48-130
1
1
1
1
1
1
1
1
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/19/13 11:50
06/19/13 11:50
06/19/13 11:50
06/19/13 11:50
06/19/13 11:50
06/19/13 11:50
06/19/13 11:50
06/19/13 11:50
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
1336-36-3
1
1
06/18/13 12:30 06/19/13 11:50 877-09-8

06/18/13 12:30 06/19/13 11:50 2051-24-3

50.6
96.6
1.8
23.4
310
<0.68
0.30J
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
2.3
0.57
0.57
0.57
1.1
2.3
1.1
0.62
0.099
0.058
0.14
0.33
0.68
0.24
1
1
1
1
1
1
1
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/18/13 14:03
06/18/13 14:03
06/18/13 14:03
06/18/13 14:03
06/18/13 14:03
06/18/13 14:03
06/18/13 14:03
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4

0.11 mg/kg
0.0077
0.0038
06/17/13 16:14 06/18/13 08:12 7439-97-6

<9.8
<9.8
<9.8
<9.8
<3.5
<9.8
<9.8
<3.5
<9.8
<9.8
<9.8
<9.8
<9.8
<3.5
<9.8
<9.8
<9.8
<9.8
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
60 %
19.6
19.6
19.6
19.6
19.6
19.6
19.6
19.6
19.6
19.6
19.6
19.6
19.6
19.6
19.6
19.6
19.6
19.6
40-130
9.8
9.8
9.8
9.8
3.5
9.8
9.8
3.5
9.8
9.8
9.8
9.8
9.8
3.5
9.8
9.8
9.8
9.8
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 14:29
06/18/13 14:29
06/18/13 14:29
06/18/13 14:29
06/18/13 14:29
06/18/13 14:29
06/18/13 14:29
06/18/13 14:29
06/18/13 14:29
06/18/13 14:29
06/18/13 14:29
06/18/13 14:29
06/18/13 14:29
06/18/13 14:29
06/18/13 14:29
06/18/13 14:29
06/18/13 14:29
06/18/13 14:29
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0
06/18/13 06:50 06/18/13 14:29 321-60-8

Date: 06/19/2013 03:45 PM
Page 12 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-1
Lab ID: 4079703001
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
Surrogates
Terphenyl-d14 (S)
Percent Moisture
Percent Moisture
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

70 %
40-130
06/18/13 06:50 06/18/13 14:29 1718-51-0

14.9 %
0.10
0.10
06/18/13 13:16

Date: 06/19/2013 03:45 PM
Page 13 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-2
Lab ID: 4079703002
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
8082 GCS PCB
PCB, Total
Surrogates
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7471 Mercury
Mercury
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

<29.1
<29.1
<29.1
<29.1
<29.1
83.4
41.7J
125
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
88 %
96 %
58.2
58.2
58.2
58.2
58.2
58.2
58.2
58.2
29.1
29.1
29.1
29.1
29.1
29.1
29.1
29.1
40-130
48-130
1
1
1
1
1
1
1
1
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/19/13 11:16
06/19/13 11:16
06/19/13 11:16
06/19/13 11:16
06/19/13 11:16
06/19/13 11:16
06/19/13 11:16
06/19/13 11:16
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
1336-36-3
1
1
06/18/13 12:30 06/19/13 11:16 877-09-8

06/18/13 12:30 06/19/13 11:16 2051-24-3

6.4
72.1
0.19J
17.9
8.9
<0.58
<0.21
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
2.0
0.49
0.49
0.49
0.98
2.0
0.98
0.53
0.085
0.050
0.12
0.29
0.58
0.21
1
1
1
1
1
1
1
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/18/13 14:05
06/18/13 14:05
06/18/13 14:05
06/18/13 14:05
06/18/13 14:05
06/18/13 14:05
06/18/13 14:05
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4

0.039 mg/kg
0.0061
0.0030
06/17/13 16:14 06/18/13 08:14 7439-97-6

<9.7
<9.7
<9.7
<9.7
<3.5
<9.7
<9.7
<3.4
<9.7
<9.7
<9.7
<9.7
<9.7
<3.4
<9.7
<9.7
<9.7
<9.7
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
59 %
19.4
19.4
19.4
19.4
19.4
19.4
19.4
19.4
19.4
19.4
19.4
19.4
19.4
19.4
19.4
19.4
19.4
19.4
40-130
9.7
9.7
9.7
9.7
3.5
9.7
9.7
3.4
9.7
9.7
9.7
9.7
9.7
3.4
9.7
9.7
9.7
9.7
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 14:46
06/18/13 14:46
06/18/13 14:46
06/18/13 14:46
06/18/13 14:46
06/18/13 14:46
06/18/13 14:46
06/18/13 14:46
06/18/13 14:46
06/18/13 14:46
06/18/13 14:46
06/18/13 14:46
06/18/13 14:46
06/18/13 14:46
06/18/13 14:46
06/18/13 14:46
06/18/13 14:46
06/18/13 14:46
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0
06/18/13 06:50 06/18/13 14:46 321-60-8

Date: 06/19/2013 03:45 PM
Page 14 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-2
Lab ID: 4079703002
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
Surrogates
Terphenyl-d14 (S)
Percent Moisture
Percent Moisture
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

60 %
40-130
06/18/13 06:50 06/18/13 14:46 1718-51-0

14.1 %
0.10
0.10
06/18/13 13:16

Date: 06/19/2013 03:45 PM
Page 15 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-3
Lab ID: 4079703003
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
8082 GCS PCB
PCB, Total
Surrogates
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7471 Mercury
Mercury
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

<29.0
<29.0
<29.0
<29.0
<29.0
<29.0
<29.0
<29.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
90 %
102 %
58.0
58.0
58.0
58.0
58.0
58.0
58.0
58.0
29.0
29.0
29.0
29.0
29.0
29.0
29.0
29.0
40-130
48-130
1
1
1
1
1
1
1
1
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/19/13 12:07
06/19/13 12:07
06/19/13 12:07
06/19/13 12:07
06/19/13 12:07
06/19/13 12:07
06/19/13 12:07
06/19/13 12:07
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
1336-36-3
1
1
06/18/13 12:30 06/19/13 12:07 877-09-8

06/18/13 12:30 06/19/13 12:07 2051-24-3

8.6
68.7
0.41J
13.5
25.6
<0.61
<0.22
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
2.1
0.51
0.51
0.51
1.0
2.1
1.0
0.56
0.089
0.052
0.13
0.30
0.61
0.22
1
1
1
1
1
1
1
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/18/13 14:07
06/18/13 14:07
06/18/13 14:07
06/18/13 14:07
06/18/13 14:07
06/18/13 14:07
06/18/13 14:07
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4

0.012 mg/kg
0.0072
0.0036
06/17/13 16:14 06/18/13 08:17 7439-97-6

<9.7
<9.7
<9.7
<9.7
<3.4
<9.7
<9.7
<3.4
<9.7
<9.7
<9.7
<9.7
<9.7
<3.4
<9.7
<9.7
<9.7
<9.7
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
60 %
19.3
19.3
19.3
19.3
19.3
19.3
19.3
19.3
19.3
19.3
19.3
19.3
19.3
19.3
19.3
19.3
19.3
19.3
40-130
9.7
9.7
9.7
9.7
3.4
9.7
9.7
3.4
9.7
9.7
9.7
9.7
9.7
3.4
9.7
9.7
9.7
9.7
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 15:04
06/18/13 15:04
06/18/13 15:04
06/18/13 15:04
06/18/13 15:04
06/18/13 15:04
06/18/13 15:04
06/18/13 15:04
06/18/13 15:04
06/18/13 15:04
06/18/13 15:04
06/18/13 15:04
06/18/13 15:04
06/18/13 15:04
06/18/13 15:04
06/18/13 15:04
06/18/13 15:04
06/18/13 15:04
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0
06/18/13 06:50 06/18/13 15:04 321-60-8

Date: 06/19/2013 03:45 PM
Page 16 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-3
Lab ID: 4079703003
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
Surrogates
Terphenyl-d14 (S)
Percent Moisture
Percent Moisture
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

64 %
40-130
06/18/13 06:50 06/18/13 15:04 1718-51-0

13.7 %
0.10
0.10
06/18/13 13:16

Date: 06/19/2013 03:45 PM
Page 17 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-4
Lab ID: 4079703004
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
8082 GCS PCB
PCB, Total
Surrogates
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7471 Mercury
Mercury
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

<30.5
<30.5
<30.5
<30.5
<30.5
<30.5
<30.5
<30.5
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
83 %
100 %
60.9
60.9
60.9
60.9
60.9
60.9
60.9
60.9
30.5
30.5
30.5
30.5
30.5
30.5
30.5
30.5
40-130
48-130
1
1
1
1
1
1
1
1
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/19/13 12:25
06/19/13 12:25
06/19/13 12:25
06/19/13 12:25
06/19/13 12:25
06/19/13 12:25
06/19/13 12:25
06/19/13 12:25
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
1336-36-3
1
1
06/18/13 12:30 06/19/13 12:25 877-09-8

06/18/13 12:30 06/19/13 12:25 2051-24-3

5.6
54.7
0.39J
13.6
11.7
<0.67
<0.24
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
2.3
0.57
0.57
0.57
1.1
2.3
1.1
0.61
0.099
0.058
0.14
0.33
0.67
0.24
1
1
1
1
1
1
1
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/18/13 14:14
06/18/13 14:14
06/18/13 14:14
06/18/13 14:14
06/18/13 14:14
06/18/13 14:14
06/18/13 14:14
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4

0.023 mg/kg
0.0071
0.0036
06/17/13 16:14 06/18/13 08:19 7439-97-6

<10.2
<10.2
17.3J
33.9
36.6
49.1
31.3
27.1
65.7
12.3J
49.0
<10.2
23.0
36.5
38.9
19.7J
78.0
53.1
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
63 %
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
40-130
10.2
10.2
10.2
10.2
3.6
10.2
10.2
3.6
10.2
10.2
10.2
10.2
10.2
3.6
10.2
10.2
10.2
10.2
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 18:17
06/18/13 18:17
06/18/13 18:17
06/18/13 18:17
06/18/13 18:17
06/18/13 18:17
06/18/13 18:17
06/18/13 18:17
06/18/13 18:17
06/18/13 18:17
06/18/13 18:17
06/18/13 18:17
06/18/13 18:17
06/18/13 18:17
06/18/13 18:17
06/18/13 18:17
06/18/13 18:17
06/18/13 18:17
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0
06/18/13 06:50 06/18/13 18:17 321-60-8

Date: 06/19/2013 03:45 PM
Page 18 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-4
Lab ID: 4079703004
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
Surrogates
Terphenyl-d14 (S)
Percent Moisture
Percent Moisture
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

64 %
40-130
06/18/13 06:50 06/18/13 18:17 1718-51-0

18.0 %
0.10
0.10
06/18/13 13:16

Date: 06/19/2013 03:45 PM
Page 19 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-5
Lab ID: 4079703005
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
8082 GCS PCB
PCB, Total
Surrogates
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7471 Mercury
Mercury
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

<35.6
<35.6
<35.6
<35.6
<35.6
<35.6
<35.6
<35.6
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
89 %
96 %
71.2
71.2
71.2
71.2
71.2
71.2
71.2
71.2
35.6
35.6
35.6
35.6
35.6
35.6
35.6
35.6
40-130
48-130
1
1
1
1
1
1
1
1
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/18/13 12:30
06/19/13 12:42
06/19/13 12:42
06/19/13 12:42
06/19/13 12:42
06/19/13 12:42
06/19/13 12:42
06/19/13 12:42
06/19/13 12:42
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
1336-36-3
1
1
06/18/13 12:30 06/19/13 12:42 877-09-8

06/18/13 12:30 06/19/13 12:42 2051-24-3

24.5
24.3
0.68
15.4
21.2
1.8J
0.32J
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
2.6
0.64
0.64
0.64
1.3
2.6
1.3
0.69
0.11
0.065
0.16
0.37
0.76
0.27
1
1
1
1
1
1
1
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/18/13 14:16
06/18/13 14:16
06/18/13 14:16
06/18/13 14:16
06/18/13 14:16
06/18/13 14:16
06/18/13 14:16
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4

0.45 mg/kg
0.0092
0.0046
06/17/13 16:14 06/18/13 08:21 7439-97-6

232
<59.3
693
915
858
1120
560
585
1180
165
2520
268
487
120
131
593
2380
1990
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
61 %
119
119
119
119
119
119
119
119
119
119
119
119
119
119
119
119
119
119
40-130
59.3
59.3
59.3
59.3
21.1
59.3
59.3
20.9
59.3
59.3
59.3
59.3
59.3
21.0
59.3
59.3
59.3
59.3
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/19/13 10:11
06/19/13 10:11
06/19/13 10:11
06/19/13 10:11
06/19/13 10:11
06/19/13 10:11
06/19/13 10:11
06/19/13 10:11
06/19/13 10:11
06/19/13 10:11
06/19/13 10:11
06/19/13 10:11
06/19/13 10:11
06/19/13 10:11
06/19/13 10:11
06/19/13 10:11
06/19/13 10:11
06/19/13 10:11
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0
06/18/13 06:50 06/19/13 10:11 321-60-8

Date: 06/19/2013 03:45 PM
Page 20 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-5
Lab ID: 4079703005
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
Surrogates
Terphenyl-d14 (S)
Percent Moisture
Percent Moisture
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

62 %
40-130
06/18/13 06:50 06/19/13 10:11 1718-51-0

29.7 %
0.10
0.10
06/18/13 13:16

Date: 06/19/2013 03:45 PM
Page 21 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-6(S)
Lab ID: 4079703006
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Terphenyl-d14 (S)
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

<20.0
141
80.6
237
252
285
247
153
314
74.1
383
<20.0
174
9.3J
<20.0
<20.0
212
596
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
68 %
79 %
40.1
40.1
40.1
40.1
40.1
40.1
40.1
40.1
40.1
40.1
40.1
40.1
40.1
40.1
40.1
40.1
40.1
40.1
20.0
20.0
20.0
20.0
7.1
20.0
20.0
7.1
20.0
20.0
20.0
20.0
20.0
7.1
20.0
20.0
20.0
20.0
40-130
40-130
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/19/13 08:43
06/19/13 08:43
06/19/13 08:43
06/19/13 08:43
06/19/13 08:43
06/19/13 08:43
06/19/13 08:43
06/19/13 08:43
06/19/13 08:43
06/19/13 08:43
06/19/13 08:43
06/19/13 08:43
06/19/13 08:43
06/19/13 08:43
06/19/13 08:43
06/19/13 08:43
06/19/13 08:43
06/19/13 08:43
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0
2
2
06/18/13 06:50 06/19/13 08:43 321-60-8

06/18/13 06:50 06/19/13 08:43 1718-51-0

<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<49.8
<25.0
<25.0
<25.0
<25.0
<25.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
250
60.0
60.0
60.0
60.0
60.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
49.8
25.0
25.0
25.0
25.0
25.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W

Date: 06/19/2013 03:45 PM
Page 22 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-6(S)
Lab ID: 4079703006
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
p-Isopropyltoluene
Methylene Chloride
Naphthalene
n-Propylbenzene
Styrene
Tetrachloroethene
Toluene
Trichloroethene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
06/17/13 18:42
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
1634-04-4
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
179601-23-1
95-47-6
Qual

<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<50.0
<25.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
101 %
110 %
99 %
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
120
60.0
57-130
54-133
49-130
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
1
1
1
06/17/13 13:34 06/17/13 18:42 1868-53-7

06/17/13 13:34 06/17/13 18:42 2037-26-5
06/17/13 13:34 06/17/13 18:42 460-00-4
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W

Date: 06/19/2013 03:45 PM
Page 23 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-6(S)
Lab ID: 4079703006
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
Percent Moisture
Percent Moisture
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

16.9 %
0.10
0.10
06/18/13 14:21

Date: 06/19/2013 03:45 PM
Page 24 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-6(D)
Lab ID: 4079703007
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Terphenyl-d14 (S)
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

<10.2
<10.2
<10.2
<10.2
10.0J
11.6J
<10.2
9.2J
12.8J
<10.2
13.6J
<10.2
<10.2
<3.6
<10.2
<10.2
<10.2
13.6J
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
64 %
64 %
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
20.3
10.2
10.2
10.2
10.2
3.6
10.2
10.2
3.6
10.2
10.2
10.2
10.2
10.2
3.6
10.2
10.2
10.2
10.2
40-130
40-130
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 19:08
06/18/13 19:08
06/18/13 19:08
06/18/13 19:08
06/18/13 19:08
06/18/13 19:08
06/18/13 19:08
06/18/13 19:08
06/18/13 19:08
06/18/13 19:08
06/18/13 19:08
06/18/13 19:08
06/18/13 19:08
06/18/13 19:08
06/18/13 19:08
06/18/13 19:08
06/18/13 19:08
06/18/13 19:08
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0
1
1
06/18/13 06:50 06/18/13 19:08 321-60-8

06/18/13 06:50 06/18/13 19:08 1718-51-0

<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<49.8
<25.0
<25.0
<25.0
<25.0
<25.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
250
60.0
60.0
60.0
60.0
60.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
49.8
25.0
25.0
25.0
25.0
25.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W

Date: 06/19/2013 03:45 PM
Page 25 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-6(D)
Lab ID: 4079703007
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
p-Isopropyltoluene
Methylene Chloride
Naphthalene
n-Propylbenzene
Styrene
Tetrachloroethene
Toluene
Trichloroethene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
06/17/13 19:05
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
1634-04-4
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
179601-23-1
95-47-6
Qual

<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<50.0
<25.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
90 %
98 %
88 %
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
120
60.0
57-130
54-133
49-130
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
1
1
1
06/17/13 13:34 06/17/13 19:05 1868-53-7

06/17/13 13:34 06/17/13 19:05 2037-26-5
06/17/13 13:34 06/17/13 19:05 460-00-4
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W

Date: 06/19/2013 03:45 PM
Page 26 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-6(D)
Lab ID: 4079703007
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
Percent Moisture
Percent Moisture
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

17.9 %
0.10
0.10
06/18/13 14:22

Date: 06/19/2013 03:45 PM
Page 27 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-7
Lab ID: 4079703008
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Terphenyl-d14 (S)
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

<9.6
<9.6
<9.6
<9.6
<3.4
<9.6
<9.6
<3.4
<9.6
<9.6
<9.6
<9.6
<9.6
<3.4
<9.6
<9.6
<9.6
<9.6
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
63 %
63 %
19.2
19.2
19.2
19.2
19.2
19.2
19.2
19.2
19.2
19.2
19.2
19.2
19.2
19.2
19.2
19.2
19.2
19.2
9.6
9.6
9.6
9.6
3.4
9.6
9.6
3.4
9.6
9.6
9.6
9.6
9.6
3.4
9.6
9.6
9.6
9.6
40-130
40-130
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 13:19
06/18/13 13:19
06/18/13 13:19
06/18/13 13:19
06/18/13 13:19
06/18/13 13:19
06/18/13 13:19
06/18/13 13:19
06/18/13 13:19
06/18/13 13:19
06/18/13 13:19
06/18/13 13:19
06/18/13 13:19
06/18/13 13:19
06/18/13 13:19
06/18/13 13:19
06/18/13 13:19
06/18/13 13:19
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0
1
1
06/18/13 06:50 06/18/13 13:19 321-60-8

06/18/13 06:50 06/18/13 13:19 1718-51-0

<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<49.8
<25.0
<25.0
<25.0
<25.0
<25.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
250
60.0
60.0
60.0
60.0
60.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
49.8
25.0
25.0
25.0
25.0
25.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W

Date: 06/19/2013 03:45 PM
Page 28 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-7
Lab ID: 4079703008
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
p-Isopropyltoluene
Methylene Chloride
Naphthalene
n-Propylbenzene
Styrene
Tetrachloroethene
Toluene
Trichloroethene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
06/17/13 19:28
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
1634-04-4
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
179601-23-1
95-47-6
Qual

<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<50.0
<25.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
95 %
104 %
93 %
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
120
60.0
57-130
54-133
49-130
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
1
1
1
06/17/13 13:34 06/17/13 19:28 1868-53-7

06/17/13 13:34 06/17/13 19:28 2037-26-5
06/17/13 13:34 06/17/13 19:28 460-00-4
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W

Date: 06/19/2013 03:45 PM
Page 29 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-7
Lab ID: 4079703008
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
Percent Moisture
Percent Moisture
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

13.3 %
0.10
0.10
06/18/13 14:22

Date: 06/19/2013 03:45 PM
Page 30 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-8
Lab ID: 4079703009
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Terphenyl-d14 (S)
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

<10.2
<10.2
<10.2
<10.2
<3.6
<10.2
<10.2
4.4J
<10.2
<10.2
<10.2
<10.2
<10.2
<3.6
<10.2
<10.2
<10.2
<10.2
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
63 %
62 %
20.5
20.5
20.5
20.5
20.5
20.5
20.5
20.5
20.5
20.5
20.5
20.5
20.5
20.5
20.5
20.5
20.5
20.5
10.2
10.2
10.2
10.2
3.6
10.2
10.2
3.6
10.2
10.2
10.2
10.2
10.2
3.6
10.2
10.2
10.2
10.2
40-130
40-130
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 06:50
06/18/13 17:25
06/18/13 17:25
06/18/13 17:25
06/18/13 17:25
06/18/13 17:25
06/18/13 17:25
06/18/13 17:25
06/18/13 17:25
06/18/13 17:25
06/18/13 17:25
06/18/13 17:25
06/18/13 17:25
06/18/13 17:25
06/18/13 17:25
06/18/13 17:25
06/18/13 17:25
06/18/13 17:25
06/18/13 17:25
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0
1
1
06/18/13 06:50 06/18/13 17:25 321-60-8

06/18/13 06:50 06/18/13 17:25 1718-51-0

<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<49.8
<25.0
<25.0
<25.0
<25.0
<25.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
250
60.0
60.0
60.0
60.0
60.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
49.8
25.0
25.0
25.0
25.0
25.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W

Date: 06/19/2013 03:45 PM
Page 31 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-8
Lab ID: 4079703009
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
p-Isopropyltoluene
Methylene Chloride
Naphthalene
n-Propylbenzene
Styrene
Tetrachloroethene
Toluene
Trichloroethene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
06/17/13 19:51
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
1634-04-4
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
179601-23-1
95-47-6
Qual

<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<50.0
<25.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
102 %
110 %
98 %
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
120
60.0
57-130
54-133
49-130
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
1
1
1
06/17/13 13:34 06/17/13 19:51 1868-53-7

06/17/13 13:34 06/17/13 19:51 2037-26-5
06/17/13 13:34 06/17/13 19:51 460-00-4
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W

Date: 06/19/2013 03:45 PM
Page 32 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-8
Lab ID: 4079703009
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
Percent Moisture
Percent Moisture
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

18.6 %
0.10
0.10
06/18/13 14:22

Date: 06/19/2013 03:45 PM
Page 33 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-9
Lab ID: 4079703010
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Terphenyl-d14 (S)
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

<10
<10
<10
<10
<3.6
<10
<10
<3.5
<10
<10
<10
<10
<10
<3.5
<10
<10
<10
<10
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
76 %
76 %
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
20.0
10
10
10
10
3.6
10
10
3.5
10
10
10
10
10
3.5
10
10
10
10
40-130
40-130
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 16:15
06/18/13 16:15
06/18/13 16:15
06/18/13 16:15
06/18/13 16:15
06/18/13 16:15
06/18/13 16:15
06/18/13 16:15
06/18/13 16:15
06/18/13 16:15
06/18/13 16:15
06/18/13 16:15
06/18/13 16:15
06/18/13 16:15
06/18/13 16:15
06/18/13 16:15
06/18/13 16:15
06/18/13 16:15
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0
1
1
06/18/13 07:00 06/18/13 16:15 321-60-8

06/18/13 07:00 06/18/13 16:15 1718-51-0

<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<49.8
<25.0
<25.0
<25.0
<25.0
<25.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
250
60.0
60.0
60.0
60.0
60.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
49.8
25.0
25.0
25.0
25.0
25.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W

Date: 06/19/2013 03:45 PM
Page 34 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-9
Lab ID: 4079703010
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
p-Isopropyltoluene
Methylene Chloride
Naphthalene
n-Propylbenzene
Styrene
Tetrachloroethene
Toluene
Trichloroethene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
06/17/13 20:14
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
1634-04-4
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
75-01-4
179601-23-1
95-47-6
Qual

<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<50.0
<25.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
108 %
114 %
101 %
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
120
60.0
57-130
54-133
49-130
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
50.0
25.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
1
1
1
06/17/13 13:34 06/17/13 20:14 1868-53-7

06/17/13 13:34 06/17/13 20:14 2037-26-5
06/17/13 13:34 06/17/13 20:14 460-00-4
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W

Date: 06/19/2013 03:45 PM
Page 35 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-9
Lab ID: 4079703010
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
Percent Moisture
Percent Moisture
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

16.6 %
0.10
0.10
06/18/13 14:22

Date: 06/19/2013 03:45 PM
Page 36 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-10
Lab ID: 4079703011
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7471 Mercury
Mercury
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Terphenyl-d14 (S)
Percent Moisture
Percent Moisture
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

2.6
14.6
0.23J
5.8
6.9
<0.64
<0.23
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
2.1
0.54
0.54
0.54
1.1
2.1
1.1
0.58
0.093
0.055
0.13
0.31
0.64
0.23
1
1
1
1
1
1
1
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/18/13 14:18
06/18/13 14:18
06/18/13 14:18
06/18/13 14:18
06/18/13 14:18
06/18/13 14:18
06/18/13 14:18
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4

0.024 mg/kg
0.0064
0.0032
06/17/13 16:14 06/18/13 08:23 7439-97-6

20.6
16.2J
102
285
384
470
283
328
392
103
510
20.8
252
11.0J
<9.9
11.4J
313
449
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
88 %
91 %
19.8
19.8
19.8
19.8
19.8
19.8
19.8
19.8
19.8
19.8
19.8
19.8
19.8
19.8
19.8
19.8
19.8
19.8
9.9
9.9
9.9
9.9
3.5
9.9
9.9
3.5
9.9
9.9
9.9
9.9
9.9
3.5
9.9
9.9
9.9
9.9
40-130
40-130
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 19:25
06/18/13 19:25
06/18/13 19:25
06/18/13 19:25
06/18/13 19:25
06/18/13 19:25
06/18/13 19:25
06/18/13 19:25
06/18/13 19:25
06/18/13 19:25
06/18/13 19:25
06/18/13 19:25
06/18/13 19:25
06/18/13 19:25
06/18/13 19:25
06/18/13 19:25
06/18/13 19:25
06/18/13 19:25
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0
1
1
06/18/13 07:00 06/18/13 19:25 321-60-8

06/18/13 07:00 06/18/13 19:25 1718-51-0

15.6 %
0.10
0.10
06/18/13 14:22

Date: 06/19/2013 03:45 PM
Page 37 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-11
Lab ID: 4079703012
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7471 Mercury
Mercury
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Terphenyl-d14 (S)
Percent Moisture
Percent Moisture
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

4.9
101
0.78
14.3
69.9
<0.68
<0.25
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
2.3
0.58
0.58
0.58
1.2
2.3
1.2
0.63
0.10
0.059
0.14
0.34
0.68
0.25
1
1
1
1
1
1
1
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/18/13 14:20
06/18/13 14:20
06/18/13 14:20
06/18/13 14:20
06/18/13 14:20
06/18/13 14:20
06/18/13 14:20
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4

0.10 mg/kg
0.0083
0.0041
06/17/13 16:14 06/18/13 08:25 7439-97-6

<11.1
<11.1
18.5J
89.3
132
133
102
89.5
132
24.1
194
<11.1
81.9
9.2J
<11.1
21.4J
140
200
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
83 %
98 %
22.3
22.3
22.3
22.3
22.3
22.3
22.3
22.3
22.3
22.3
22.3
22.3
22.3
22.3
22.3
22.3
22.3
22.3
11.1
11.1
11.1
11.1
4.0
11.1
11.1
3.9
11.1
11.1
11.1
11.1
11.1
3.9
11.1
11.1
11.1
11.1
40-130
40-130
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/19/13 09:52
06/19/13 09:52
06/19/13 09:52
06/19/13 09:52
06/19/13 09:52
06/19/13 09:52
06/19/13 09:52
06/19/13 09:52
06/19/13 09:52
06/19/13 09:52
06/19/13 09:52
06/19/13 09:52
06/19/13 09:52
06/19/13 09:52
06/19/13 09:52
06/19/13 09:52
06/19/13 09:52
06/19/13 09:52
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0
1
1
06/18/13 07:00 06/19/13 09:52 321-60-8

06/18/13 07:00 06/19/13 09:52 1718-51-0

25.1 %
0.10
0.10
06/18/13 14:22

Date: 06/19/2013 03:45 PM
Page 38 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-13
Lab ID: 4079703013
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7471 Mercury
Mercury
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Terphenyl-d14 (S)
Percent Moisture
Percent Moisture
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

19.0
85.8
3.1
30.9
404
<0.66
0.47J
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
2.2
0.56
0.56
0.56
1.1
2.2
1.1
0.61
0.097
0.057
0.14
0.33
0.66
0.24
1
1
1
1
1
1
1
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/18/13 14:23
06/18/13 14:23
06/18/13 14:23
06/18/13 14:23
06/18/13 14:23
06/18/13 14:23
06/18/13 14:23
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4

0.10 mg/kg
0.0073
0.0037
06/17/13 16:14 06/18/13 08:27 7439-97-6

393J
588J
1710
3610
3580
4710
2290
2120
4930
827
9870
1020
2010
414J
<393
<393
9470
7700
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
67 %
70 %
785
785
785
785
785
785
785
785
785
785
785
785
785
785
785
785
785
785
393
393
393
393
140
393
393
138
393
393
393
393
393
139
393
393
393
393
40-130
40-130
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/19/13 09:17
06/19/13 09:17
06/19/13 09:17
06/19/13 09:17
06/19/13 09:17
06/19/13 09:17
06/19/13 09:17
06/19/13 09:17
06/19/13 09:17
06/19/13 09:17
06/19/13 09:17
06/19/13 09:17
06/19/13 09:17
06/19/13 09:17
06/19/13 09:17
06/19/13 09:17
06/19/13 09:17
06/19/13 09:17
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0
40
40
06/18/13 07:00 06/19/13 09:17 321-60-8

06/18/13 07:00 06/19/13 09:17 1718-51-0

15.1 %
0.10
0.10
06/18/13 14:22

Date: 06/19/2013 03:45 PM
Page 39 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-14
Lab ID: 4079703014
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7471 Mercury
Mercury
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Terphenyl-d14 (S)
Percent Moisture
Percent Moisture
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

15.4
134
2.1
13.8
1190
<0.61
0.43J
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
4.1
0.52
1.0
0.52
2.1
2.1
1.0
1.1
0.090
0.11
0.13
0.61
0.61
0.22
2
1
2
1
2
1
1
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/19/13 09:18
06/18/13 14:25
06/19/13 09:18
06/18/13 14:25
06/19/13 09:18
06/18/13 14:25
06/18/13 14:25
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4

0.068 mg/kg
0.0072
0.0036
06/17/13 16:14 06/18/13 08:29 7439-97-6

798
<382
2340
3160
3290
4290
2180
2340
4730
565J
10600
860
1920
169J
<382
1010
9560
7800
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
0 %
0 %
764
764
764
764
764
764
764
764
764
764
764
764
764
764
764
764
764
764
382
382
382
382
136
382
382
135
382
382
382
382
382
135
382
382
382
382
40-130
40-130
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
40
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/19/13 09:34
06/19/13 09:34
06/19/13 09:34
06/19/13 09:34
06/19/13 09:34
06/19/13 09:34
06/19/13 09:34
06/19/13 09:34
06/19/13 09:34
06/19/13 09:34
06/19/13 09:34
06/19/13 09:34
06/19/13 09:34
06/19/13 09:34
06/19/13 09:34
06/19/13 09:34
06/19/13 09:34
06/19/13 09:34
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0
40
40
06/18/13 07:00 06/19/13 09:34 321-60-8

06/18/13 07:00 06/19/13 09:34 1718-51-0
S4
S4

12.8 %
0.10
0.10
06/18/13 14:22

Date: 06/19/2013 03:45 PM
Page 40 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-22
Lab ID: 4079703015
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7471 Mercury
Mercury
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Terphenyl-d14 (S)
Percent Moisture
Percent Moisture
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

5.8
45.4
0.61
14.7
82.7
<0.55
<0.20
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
1.9
0.46
0.46
0.46
0.93
1.9
0.93
0.50
0.081
0.047
0.12
0.27
0.55
0.20
1
1
1
1
1
1
1
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/18/13 14:27
06/18/13 14:27
06/18/13 14:27
06/18/13 14:27
06/18/13 14:27
06/18/13 14:27
06/18/13 14:27
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4

0.070 mg/kg
0.0067
0.0033
06/17/13 16:14 06/18/13 08:31 7439-97-6

<9.1
29.2
24.8
125
184
257
134
186
228
52.5
171
<9.1
112
89.5
137
248
136
179
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
47 %
56 %
18.1
18.1
18.1
18.1
18.1
18.1
18.1
18.1
18.1
18.1
18.1
18.1
18.1
18.1
18.1
18.1
18.1
18.1
9.1
9.1
9.1
9.1
3.2
9.1
9.1
3.2
9.1
9.1
9.1
9.1
9.1
3.2
9.1
9.1
9.1
9.1
40-130
40-130
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/19/13 13:23
06/19/13 13:23
06/19/13 13:23
06/19/13 13:23
06/19/13 13:23
06/19/13 13:23
06/19/13 13:23
06/19/13 13:23
06/19/13 13:23
06/19/13 13:23
06/19/13 13:23
06/19/13 13:23
06/19/13 13:23
06/19/13 13:23
06/19/13 13:23
06/19/13 13:23
06/19/13 13:23
06/19/13 13:23
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0
1
1
06/18/13 07:00 06/19/13 13:23 321-60-8

06/18/13 07:00 06/19/13 13:23 1718-51-0

8.1 %
0.10
0.10
06/18/13 14:22

Date: 06/19/2013 03:45 PM
Page 41 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-26
Lab ID: 4079703016
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7471 Mercury
Mercury
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Terphenyl-d14 (S)
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

7.1
60.8
0.37J
13.4
186
<0.62
<0.22
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
2.1
0.53
0.53
0.53
1.1
2.1
1.1
0.57
0.091
0.053
0.13
0.31
0.62
0.22
1
1
1
1
1
1
1
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/17/13 10:05
06/18/13 14:30
06/18/13 14:30
06/18/13 14:30
06/18/13 14:30
06/18/13 14:30
06/18/13 14:30
06/18/13 14:30
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4

0.036 mg/kg
0.0058
0.0029
06/17/13 16:14 06/18/13 08:37 7439-97-6

<9.3
<9.3
<9.3
<9.3
<3.3
<9.3
<9.3
<3.3
<9.3
<9.3
<9.3
<9.3
<9.3
<3.3
<9.3
<9.3
<9.3
<9.3
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
73 %
84 %
18.6
18.6
18.6
18.6
18.6
18.6
18.6
18.6
18.6
18.6
18.6
18.6
18.6
18.6
18.6
18.6
18.6
18.6
9.3
9.3
9.3
9.3
3.3
9.3
9.3
3.3
9.3
9.3
9.3
9.3
9.3
3.3
9.3
9.3
9.3
9.3
40-130
40-130
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 16:32
06/18/13 16:32
06/18/13 16:32
06/18/13 16:32
06/18/13 16:32
06/18/13 16:32
06/18/13 16:32
06/18/13 16:32
06/18/13 16:32
06/18/13 16:32
06/18/13 16:32
06/18/13 16:32
06/18/13 16:32
06/18/13 16:32
06/18/13 16:32
06/18/13 16:32
06/18/13 16:32
06/18/13 16:32
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0
1
1
06/18/13 07:00 06/18/13 16:32 321-60-8

06/18/13 07:00 06/18/13 16:32 1718-51-0

<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
1
1
1
1
1
1
1
1
1
1
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
104-51-8
135-98-8
98-06-6
56-23-5
W
W
W
W
W
W
W
W
W
W

Date: 06/19/2013 03:45 PM
Page 42 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-26
Lab ID: 4079703016
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
p-Isopropyltoluene
Methylene Chloride
Naphthalene
n-Propylbenzene
Styrene
Tetrachloroethene
Toluene
Trichloroethene
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<49.8
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
60.0
60.0
60.0
60.0
60.0
60.0
250
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
25.0
25.0
25.0
25.0
25.0
25.0
49.8
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
96-12-8
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
108-20-3
100-41-4
87-68-3
98-82-8
99-87-6
75-09-2
1634-04-4
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W
W

Date: 06/19/2013 03:45 PM
Page 43 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-26
Lab ID: 4079703016
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
Percent Moisture
Percent Moisture
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
06/17/13 20:37
96-18-4
95-63-6
108-67-8
75-01-4
179601-23-1
95-47-6
Qual

<25.0
<25.0
<25.0
<25.0
<50.0
<25.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
101 %
109 %
98 %
60.0
60.0
60.0
60.0
120
60.0
25.0
25.0
25.0
25.0
50.0
25.0
57-130
54-133
49-130
1
1
1
1
1
1
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
06/17/13 13:34
1
1
1
06/17/13 13:34 06/17/13 20:37 1868-53-7

06/17/13 13:34 06/17/13 20:37 2037-26-5
06/17/13 13:34 06/17/13 20:37 460-00-4
W
W
W
W
W
W

10.3 %
0.10
0.10
06/18/13 14:22

Date: 06/19/2013 03:45 PM
Page 44 of 63
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079703
Sample: GP-2(D)
Lab ID: 4079703017
Collected: 06/14/13 00:00
Received: 06/15/13 12:01
Matrix: Solid

Parameters
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Terphenyl-d14 (S)
Percent Moisture
Percent Moisture
Results
Units
LOQ
LOD
DF
Prepared
Analyzed
CAS No.
Qual

<9.3
<9.3
<9.3
<9.3
<3.3
<9.3
<9.3
<3.3
<9.3
<9.3
<9.3
<9.3
<9.3
<3.3
<9.3
<9.3
<9.3
<9.3
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
78 %
90 %
18.6
18.6
18.6
18.6
18.6
18.6
18.6
18.6
18.6
18.6
18.6
18.6
18.6
18.6
18.6
18.6
18.6
18.6
9.3
9.3
9.3
9.3
3.3
9.3
9.3
3.3
9.3
9.3
9.3
9.3
9.3
3.3
9.3
9.3
9.3
9.3
40-130
40-130
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 07:00
06/18/13 15:58
06/18/13 15:58
06/18/13 15:58
06/18/13 15:58
06/18/13 15:58
06/18/13 15:58
06/18/13 15:58
06/18/13 15:58
06/18/13 15:58
06/18/13 15:58
06/18/13 15:58
06/18/13 15:58
06/18/13 15:58
06/18/13 15:58
06/18/13 15:58
06/18/13 15:58
06/18/13 15:58
06/18/13 15:58
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0
1
1
06/18/13 07:00 06/18/13 15:58 321-60-8

06/18/13 07:00 06/18/13 15:58 1718-51-0

10.3 %
0.10
0.10
06/18/13 14:22

Date: 06/19/2013 03:45 PM
Page 45 of 63
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079703
QC Batch:
MERP/3700
Analysis Method:
EPA 7471
QC Batch Method:
EPA 7471
7471 Mercury

METHOD BLANK:
4079703001, 4079703002, 4079703003, 4079703004, 4079703005, 4079703011, 4079703012, 4079703013,

4079703014, 4079703015, 4079703016
809241
Parameter
Matrix: Solid
4079703001, 4079703002, 4079703003, 4079703004, 4079703005, 4079703011, 4079703012, 4079703013,
4079703014, 4079703015, 4079703016
Blank
Reporting
Units
Result
Limit
Analyzed
Qualifiers
Mercury
mg/kg
809242
Parameter
Mercury
<0.0033
Spike
Conc.
Units
mg/kg
Parameter
Mercury
LCS
Result
.17
0.042
06/18/13 07:48
% Rec
Limits
LCS
% Rec
0.15
809243
10231800001
Units
Result
mg/kg
0.0067
92
Qualifiers
85-115
809244
MS
Spike
Conc.
MSD
Spike
Conc.
.2
MS
Result
.2
0.22
MSD
Result
MS
% Rec
0.21
91
MSD
% Rec
84
% Rec
Limits
85-115
Max
RPD RPD
5
Qual
20 M0

Date: 06/19/2013 03:45 PM
Page 46 of 63
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079703
QC Batch:
MPRP/8637
Analysis Method:
EPA 6010
QC Batch Method:
EPA 3050
6010 MET

METHOD BLANK:
4079703001, 4079703002, 4079703003, 4079703004, 4079703005, 4079703011, 4079703012, 4079703013,

4079703014, 4079703015, 4079703016
809183
Parameter
Matrix: Solid
4079703001, 4079703002, 4079703003, 4079703004, 4079703005, 4079703011, 4079703012, 4079703013,
4079703014, 4079703015, 4079703016
Blank
Reporting
Units
Result
Limit
Analyzed
Qualifiers
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
809184
Parameter
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
<0.54
<0.087
<0.051
<0.13
<0.29
<0.59
<0.21
Spike
Conc.
Units
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Parameter
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
LCS
Result
50
50
50
50
50
50
25
4.7
124
0.32J
12.1
200
<0.67
<0.24
06/18/13 13:34
06/18/13 13:34
06/18/13 13:34
06/18/13 13:34
06/18/13 13:34
06/18/13 13:34
06/18/13 13:34
LCS
% Rec
48.4
50.4
48.2
49.5
49.0
47.3
23.7
809185
4079685001
Units
Result
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
2.0
0.50
0.50
0.50
1.0
2.0
1.0
% Rec
Limits
97
101
96
99
98
95
95
Qualifiers
80-120
80-120
80-120
80-120
80-120
80-120
80-120
809186
MS
Spike
Conc.
56.4
56.4
56.4
56.4
56.4
56.4
28.2
MSD
Spike
Conc.
56.4
56.4
56.4
56.4
56.4
56.4
28.2
MS
Result
56.6
198
53.3
67.8
188
51.8
26.4
MSD
Result
MS
% Rec
57.7
210
53.5
68.0
215
52.0
26.8
92
131
94
99
-22
92
93
MSD
% Rec
94
153
94
99
26
92
95
% Rec
Limits
75-125
75-125
75-125
75-125
75-125
75-125
75-125
Max
RPD RPD
2
6
0
0
13
0
2
Qual
20
20 M0
20
20
20 M0
20
20

Date: 06/19/2013 03:45 PM
Page 47 of 63
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079703
QC Batch:
MSV/20116
Analysis Method:
EPA 8260
QC Batch Method:
EPA 5035/5030B

METHOD BLANK:
4079703006, 4079703007, 4079703008, 4079703009, 4079703010, 4079703016
809334

Parameter
Matrix: Solid
4079703006, 4079703007, 4079703008, 4079703009, 4079703010, 4079703016
Blank
Reporting
Analyzed
Units
Result
Limit
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Chlorotoluene
4-Chlorotoluene
Benzene
Bromobenzene
Bromochloromethane
Bromoform
Bromomethane
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromomethane
Diisopropyl ether
Ethylbenzene
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<49.8
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
250
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
Qualifiers
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05

Date: 06/19/2013 03:45 PM
Page 48 of 63
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079703
METHOD BLANK:
809334

Parameter
Matrix: Solid
4079703006, 4079703007, 4079703008, 4079703009, 4079703010, 4079703016
Blank
Reporting
Analyzed
Units
Result
Limit
m&p-Xylene
Methylene Chloride
n-Butylbenzene
n-Propylbenzene
Naphthalene
o-Xylene
p-Isopropyltoluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
Trichloroethene
Vinyl chloride
Toluene-d8 (S)
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%

Parameter
1,1-Dichloroethane
1,1-Dichloroethene
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzene
Bromoform
Bromomethane
Chlorobenzene
Chloroethane
<50.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
85
89
92
809335
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
120
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
60.0
49-130
57-130
54-133
Qualifiers
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
06/17/13 14:05
809336
Spike
Conc.
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
LCS
Result
2770
2670
2720
2700
2750
2660
2130
2540
2640
2750
2790
2630
2620
2690
2420
2560
2770
2530
2620
2560
LCSD
Result
2700
2610
2670
2620
2700
2590
2070
2450
2570
2540
2680
2540
2520
2620
2370
2550
2530
2480
2550
2540
LCS LCSD
% Rec % Rec
111
107
109
108
110
106
85
102
105
110
112
105
105
108
97
102
111
101
105
102
108
104
107
105
108
104
83
98
103
102
107
102
101
105
95
102
101
99
102
101
% Rec
Limits
70-130
70-130
70-130
70-130
64-130
68-130
50-150
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
63-130
41-142
70-130
70-130
57-130
Max
RPD
RPD
2
2
2
3
2
2
3
4
3
8
4
3
4
3
2
0
9
2
3
1
Qualifiers
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20

Date: 06/19/2013 03:45 PM
Page 49 of 63
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079703

Parameter
Chloroform
Chloromethane
Ethylbenzene
m&p-Xylene
Methylene Chloride
o-Xylene
Styrene
Tetrachloroethene
Toluene
Trichloroethene
Vinyl chloride
Toluene-d8 (S)
809335
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
809336
Spike
Conc.
2500
2500
2500
2500
2500
2500
2500
2500
5000
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
2500
LCS
Result
2600
2750
2620
2360
2400
2540
2740
2800
5580
2560
2760
2810
2640
2650
2690
2650
2490
2660
2690
2820
LCSD
Result
2540
2660
2550
2300
2330
2450
2660
2720
5480
2510
2640
2770
2550
2550
2630
2620
2450
2590
2660
2720
LCS LCSD
% Rec % Rec
104
110
105
94
96
101
110
112
112
102
110
113
106
106
107
106
100
106
108
113
104
103
101
102
107
102
92
93
98
106
109
110
100
106
111
102
102
105
105
98
104
106
109
102
98
102
% Rec
Limits
70-130
57-130
70-130
70-130
70-130
31-150
65-137
70-130
64-139
69-130
70-130
63-135
69-130
70-130
70-130
70-130
70-130
70-130
50-150
57-130
49-130
57-130
54-133
Max
RPD
RPD
2
3
3
2
3
4
3
3
2
2
4
2
3
4
2
1
2
3
1
4
Qualifiers
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20

Date: 06/19/2013 03:45 PM
Page 50 of 63
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079703
QC Batch:
OEXT/18642
Analysis Method:
EPA 8082
QC Batch Method:
EPA 3541
8082 GCS PCB

METHOD BLANK:
4079703001, 4079703002, 4079703003, 4079703004, 4079703005
809863

Parameter
Matrix: Solid
4079703001, 4079703002, 4079703003, 4079703004, 4079703005
Blank
Reporting
Analyzed
Units
Result
Limit

ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
809864
Parameter
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
97
79
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
Parameter
Spike
Conc.
Units
LCS
Result
809865
<29.4
<29.4
<29.4
<29.4
<29.4
<29.4
<29.4
06/19/13 10:06
06/19/13 10:06
06/19/13 10:06
06/19/13 10:06
06/19/13 10:06
06/19/13 10:06
06/19/13 10:06
06/19/13 10:06
06/19/13 10:06
LCS
% Rec
<25.0
<25.0
<25.0
<25.0
<25.0
<25.0
507
500
4079703001
Units
Result
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
50.0
50.0
50.0
50.0
50.0
50.0
50.0
48-130
40-130
Qualifiers
% Rec
Limits
101
102
84
Qualifiers
70-130
48-130
40-130
809866
MS
Spike
Conc.
588
MSD
Spike
Conc.
588
MS
Result
<29.4
<29.4
<29.4
<29.4
<29.4
<29.4
594
MSD
Result
MS
% Rec
<29.4
<29.4
<29.4
<29.4
<29.4
<29.4
602
101
98
83
MSD
% Rec
102
101
89
% Rec
Limits
40-149
48-130
40-130
Max
RPD RPD
Qual
31
31
31
31
31
31
31

Date: 06/19/2013 03:45 PM
Page 51 of 63
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079703
QC Batch:
OEXT/18628
Analysis Method:
EPA 8270 by SIM
QC Batch Method:
EPA 3546

METHOD BLANK:
4079703001, 4079703002, 4079703003, 4079703004, 4079703005, 4079703006, 4079703007, 4079703008,

4079703009
809525
Parameter
Matrix: Solid
4079703001, 4079703002, 4079703003, 4079703004, 4079703005, 4079703006, 4079703007, 4079703008,
4079703009
Blank
Reporting
Units
Result
Limit
Analyzed
Qualifiers
1-Methylnaphthalene
2-Methylnaphthalene
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
Naphthalene
Phenanthrene
Pyrene
Terphenyl-d14 (S)
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
809526
Parameter
1-Methylnaphthalene
2-Methylnaphthalene
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
Naphthalene
<2.9
<8.3
<8.3
<8.3
<8.3
<8.3
<3.0
<8.3
<8.3
<2.9
<8.3
<8.3
<8.3
<8.3
<8.3
<8.3
<8.3
<8.3
61
70
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Spike
Conc.
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
40-130
40-130
LCS
Result
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
06/18/13 10:41
% Rec
Limits
LCS
% Rec
223
205
253
248
265
200
228
223
234
230
262
243
218
248
236
194
67
61
76
74
80
60
68
67
70
69
78
73
65
74
71
58
Qualifiers
47-130
48-130
55-130
55-130
66-130
55-130
56-130
53-130
51-130
52-130
58-130
55-130
62-130
58-130
54-130
41-130

Date: 06/19/2013 03:45 PM
Page 52 of 63
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079703
809526
Parameter
Phenanthrene
Pyrene
Terphenyl-d14 (S)
ug/kg
ug/kg
%
%
Parameter
1-Methylnaphthalene
2-Methylnaphthalene
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
Naphthalene
Phenanthrene
Pyrene
Terphenyl-d14 (S)
Spike
Conc.
Units
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
333
333
213
220
809527
4079703008
Result
<3.4
<9.6
<9.6
<9.6
<9.6
<9.6
<3.4
<9.6
<9.6
<3.4
<9.6
<9.6
<9.6
<9.6
<9.6
<9.6
<9.6
<9.6
LCS
% Rec
LCS
Result
% Rec
Limits
64
66
71
76
Qualifiers
60-130
51-130
40-130
40-130
809528
MS
Spike
Conc.
384
384
384
384
384
384
384
384
384
384
384
384
384
384
384
384
384
384
MSD
Spike
Conc.
384
384
384
384
384
384
384
384
384
384
384
384
384
384
384
384
384
384
MS
Result
228
217
261
260
271
186
236
187
225
259
270
235
219
249
231
216
222
214
MSD
Result
MS
% Rec
215
222
263
252
258
153
194
150
195
239
237
198
195
191
202
227
199
187
59
57
68
68
71
48
61
49
58
67
70
61
57
65
60
56
58
56
67
65
MSD
% Rec
56
58
68
66
67
40
50
39
51
62
62
52
51
50
53
59
52
49
62
54
% Rec
Limits
42-130
34-130
31-130
32-130
39-131
29-130
35-130
21-142
12-134
35-130
37-130
23-130
29-137
32-130
17-134
24-130
27-135
24-130
40-130
40-130
Max
RPD RPD
6
2
1
3
5
20
19
22
14
8
13
17
11
27
13
5
11
13
Qual
32
35
35
25
38
30
33
44
33
37
38
27
50
32
28
40
46
49

Date: 06/19/2013 03:45 PM
Page 53 of 63
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079703
QC Batch:
OEXT/18629
Analysis Method:
EPA 8270 by SIM
QC Batch Method:
EPA 3546

METHOD BLANK:
4079703010, 4079703011, 4079703012, 4079703013, 4079703014, 4079703015, 4079703016, 4079703017
809529

Parameter
Matrix: Solid
4079703010, 4079703011, 4079703012, 4079703013, 4079703014, 4079703015, 4079703016, 4079703017
Blank
Reporting
Analyzed
Units
Result
Limit
Qualifiers
1-Methylnaphthalene
2-Methylnaphthalene
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
Naphthalene
Phenanthrene
Pyrene
Terphenyl-d14 (S)
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
809530
Parameter
1-Methylnaphthalene
2-Methylnaphthalene
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
Naphthalene
Phenanthrene
<2.9
<8.3
<8.3
<8.3
<8.3
<8.3
<3.0
<8.3
<8.3
<2.9
<8.3
<8.3
<8.3
<8.3
<8.3
<8.3
<8.3
<8.3
78
84
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Spike
Conc.
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
333
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
40-130
40-130
LCS
Result
06/18/13 11:16
06/18/13 11:16
06/18/13 11:16
06/18/13 11:16
06/18/13 11:16
06/18/13 11:16
06/18/13 11:16
06/18/13 11:16
06/18/13 11:16
06/18/13 11:16
06/18/13 11:16
06/18/13 11:16
06/18/13 11:16
06/18/13 11:16
06/18/13 11:16
06/18/13 11:16
06/18/13 11:16
06/18/13 11:16
06/18/13 11:16
06/18/13 11:16
% Rec
Limits
LCS
% Rec
295
272
336
331
356
245
311
268
304
316
363
312
286
322
305
274
280
88
82
101
99
107
73
93
80
91
95
109
94
86
97
91
82
84
Qualifiers
47-130
48-130
55-130
55-130
66-130
55-130
56-130
53-130
51-130
52-130
58-130
55-130
62-130
58-130
54-130
41-130
60-130

Date: 06/19/2013 03:45 PM
Page 54 of 63
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079703
809530
Parameter
Pyrene
Terphenyl-d14 (S)
Units
ug/kg
%
%
Spike
Conc.
333
LCS
% Rec
LCS
Result
311
% Rec
Limits
93
90
91
Qualifiers
51-130
40-130
40-130

Date: 06/19/2013 03:45 PM
Page 55 of 63
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079703
QC Batch:
PMST/8584
Analysis Method:
ASTM D2974-87
QC Batch Method:
ASTM D2974-87

SAMPLE DUPLICATE:
4079703001, 4079703002, 4079703003, 4079703004, 4079703005
809919
Parameter
Percent Moisture
Units
%
4079739003
Result
7.1
Dup
Result
Max
RPD
RPD
6.9
Qualifiers
10

Date: 06/19/2013 03:45 PM
Page 56 of 63
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079703
QC Batch:
PMST/8585
Analysis Method:
ASTM D2974-87
QC Batch Method:
ASTM D2974-87

SAMPLE DUPLICATE:
4079703006, 4079703007, 4079703008, 4079703009, 4079703010, 4079703011, 4079703012, 4079703013,

4079703014, 4079703015, 4079703016, 4079703017
810007
Parameter
Percent Moisture
Units
%
4079739001
Result
7.2
Dup
Result
Max
RPD
RPD
7.2
Qualifiers
10

Date: 06/19/2013 03:45 PM
Page 57 of 63
#=QL#

Green Bay, WI 54302
(920)469-2436
QUALIFIERS
Project:
Pace Project No.:
4079703
DEFINITIONS
S - Surrogate
LABORATORIES
PASI-G
BATCH QUALIFIERS
Batch: MSV/20118
[M5]
Batch: MSSV/5759
[IP]
Batch: MSSV/5760
[IP]
ANALYTE QUALIFIERS
M0
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
S4
Surrogate recovery not evaluated against control limits due to sample dilution.
Non-detect results are reported on a wet weight basis.

Date: 06/19/2013 03:45 PM
Page 58 of 63
#=CR#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079703
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
4079703001
4079703002
4079703003
4079703004
4079703005
GP-1
GP-2
GP-3
GP-4
GP-5
EPA 3541
EPA 3541
EPA 3541
EPA 3541
EPA 3541
OEXT/18642
OEXT/18642
OEXT/18642
OEXT/18642
OEXT/18642
EPA 8082
EPA 8082
EPA 8082
EPA 8082
EPA 8082
GCSV/9725
GCSV/9725
GCSV/9725
GCSV/9725
GCSV/9725
4079703001
4079703002
4079703003
4079703004
4079703005
4079703011
4079703012
4079703013
4079703014
4079703015
4079703016
GP-1
GP-2
GP-3
GP-4
GP-5
GP-10
GP-11
GP-13
GP-14
GP-22
GP-26
EPA 3050
EPA 3050
EPA 3050
EPA 3050
EPA 3050
EPA 3050
EPA 3050
EPA 3050
EPA 3050
EPA 3050
EPA 3050
MPRP/8637
MPRP/8637
MPRP/8637
MPRP/8637
MPRP/8637
MPRP/8637
MPRP/8637
MPRP/8637
MPRP/8637
MPRP/8637
MPRP/8637
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
ICP/7673
ICP/7673
ICP/7673
ICP/7673
ICP/7673
ICP/7673
ICP/7673
ICP/7673
ICP/7673
ICP/7673
ICP/7673
4079703001
4079703002
4079703003
4079703004
4079703005
4079703011
4079703012
4079703013
4079703014
4079703015
4079703016
GP-1
GP-2
GP-3
GP-4
GP-5
GP-10
GP-11
GP-13
GP-14
GP-22
GP-26
EPA 7471
EPA 7471
EPA 7471
EPA 7471
EPA 7471
EPA 7471
EPA 7471
EPA 7471
EPA 7471
EPA 7471
EPA 7471
MERP/3700
MERP/3700
MERP/3700
MERP/3700
MERP/3700
MERP/3700
MERP/3700
MERP/3700
MERP/3700
MERP/3700
MERP/3700
EPA 7471
EPA 7471
EPA 7471
EPA 7471
EPA 7471
EPA 7471
EPA 7471
EPA 7471
EPA 7471
EPA 7471
EPA 7471
MERC/4611
MERC/4611
MERC/4611
MERC/4611
MERC/4611
MERC/4611
MERC/4611
MERC/4611
MERC/4611
MERC/4611
MERC/4611
4079703001
4079703002
4079703003
4079703004
4079703005
4079703006
4079703007
4079703008
4079703009
GP-1
GP-2
GP-3
GP-4
GP-5
GP-6(S)
GP-6(D)
GP-7
GP-8
EPA 3546
EPA 3546
EPA 3546
EPA 3546
EPA 3546
EPA 3546
EPA 3546
EPA 3546
EPA 3546
OEXT/18628
OEXT/18628
OEXT/18628
OEXT/18628
OEXT/18628
OEXT/18628
OEXT/18628
OEXT/18628
OEXT/18628
EPA 8270 by SIM

EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
MSSV/5759
MSSV/5759
MSSV/5759
MSSV/5759
MSSV/5759
MSSV/5759
MSSV/5759
MSSV/5759
MSSV/5759
4079703010
4079703011
4079703012
4079703013
4079703014
4079703015
4079703016
4079703017
GP-9
GP-10
GP-11
GP-13
GP-14
GP-22
GP-26
GP-2(D)
EPA 3546
EPA 3546
EPA 3546
EPA 3546
EPA 3546
EPA 3546
EPA 3546
EPA 3546
OEXT/18629
OEXT/18629
OEXT/18629
OEXT/18629
OEXT/18629
OEXT/18629
OEXT/18629
OEXT/18629
EPA 8270 by SIM

EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
EPA 8270 by SIM
MSSV/5760
MSSV/5760
MSSV/5760
MSSV/5760
MSSV/5760
MSSV/5760
MSSV/5760
MSSV/5760
4079703006
4079703007
GP-6(S)
GP-6(D)
EPA 5035/5030B
EPA 5035/5030B
MSV/20116
MSV/20116
EPA 8260
EPA 8260
MSV/20118
MSV/20118

Date: 06/19/2013 03:45 PM
Page 59 of 63
#=CR#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079703
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
4079703008
4079703009
4079703010
4079703016
GP-7
GP-8
GP-9
GP-26
EPA 5035/5030B
EPA 5035/5030B
EPA 5035/5030B
EPA 5035/5030B
MSV/20116
MSV/20116
MSV/20116
MSV/20116
EPA 8260
EPA 8260
EPA 8260
EPA 8260
MSV/20118
MSV/20118
MSV/20118
MSV/20118
4079703001
4079703002
4079703003
4079703004
4079703005
GP-1
GP-2
GP-3
GP-4
GP-5
ASTM D2974-87
ASTM D2974-87
ASTM D2974-87
ASTM D2974-87
ASTM D2974-87
PMST/8584
PMST/8584
PMST/8584
PMST/8584
PMST/8584
4079703006
4079703007
4079703008
4079703009
4079703010
4079703011
4079703012
4079703013
4079703014
4079703015
4079703016
4079703017
GP-6(S)
GP-6(D)
GP-7
GP-8
GP-9
GP-10
GP-11
GP-13
GP-14
GP-22
GP-26
GP-2(D)
ASTM D2974-87
ASTM D2974-87
ASTM D2974-87
ASTM D2974-87
ASTM D2974-87
ASTM D2974-87
ASTM D2974-87
ASTM D2974-87
ASTM D2974-87
ASTM D2974-87
ASTM D2974-87
ASTM D2974-87
PMST/8585
PMST/8585
PMST/8585
PMST/8585
PMST/8585
PMST/8585
PMST/8585
PMST/8585
PMST/8585
PMST/8585
PMST/8585
PMST/8585

Date: 06/19/2013 03:45 PM
Page 60 of 63
Page 61 of 63
Page 62 of 63
Page 63 of 63
#=CL#

Green Bay, WI 54302
(920)469-2436

June 19, 2013
Mitchell Banach

Sincerely,
Steven Mleczko
Project Manager
Enclosures

Page 1 of 19
#=CP#

Green Bay, WI 54302
(920)469-2436
CERTIFICATIONS
Project:
Pace Project No.:
4079704



Page 2 of 19
#=SS#

Green Bay, WI 54302
(920)469-2436
SAMPLE SUMMARY
Project:
Pace Project No.:
4079704
Lab ID
Sample ID
Matrix
Date Collected
Date Received
4079704001
GP-1
Water
06/14/13 00:00
06/15/13 12:01
4079704002
GP-2
Water
06/14/13 00:00
06/15/13 12:01
4079704003
GP-3
Water
06/14/13 00:00
06/15/13 12:01
4079704004
GP-4
Water
06/14/13 00:00
06/15/13 12:01
4079704005
GP-6
Water
06/14/13 00:00
06/15/13 12:01
4079704006
GP-17
Water
06/14/13 00:00
06/15/13 12:01
4079704007
GP-18
Water
06/14/13 00:00
06/15/13 12:01
4079704008
GP-19
Water
06/14/13 00:00
06/15/13 12:01
4079704009
GP-26
Water
06/14/13 00:00
06/15/13 12:01
4079704010
TRIP BLANK
Water
06/14/13 00:00
06/15/13 12:01

Page 3 of 19
#=SA#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079704
Lab ID
Sample ID
4079704001
GP-1
4079704002
4079704003
4079704004
GP-2
GP-3
GP-4
Analytes
Reported
Method
Analysts
Laboratory
EPA 8082
BLM
10
PASI-G
EPA 6010
DLB
PASI-G
EPA 7470
CMS
PASI-G
EPA 8270 by HVI
RJN
20
PASI-G
EPA 8082
BLM
10
PASI-G
EPA 6010
DLB
PASI-G
EPA 7470
CMS
PASI-G
EPA 8270 by HVI
RJN
20
PASI-G
EPA 8082
BLM
10
PASI-G
EPA 6010
DLB
PASI-G
EPA 7470
CMS
PASI-G
EPA 8270 by HVI
RJN
20
PASI-G
EPA 8082
BLM
10
PASI-G
EPA 6010
DLB
PASI-G
EPA 7470
CMS
PASI-G
EPA 8270 by HVI
RJN
20
PASI-G

Page 4 of 19
#=HO#

Green Bay, WI 54302
(920)469-2436
HITS ONLY
Project:
Pace Project No.:
4079704
Lab Sample ID
Client Sample ID
Method
Parameters
Result
4079704001
GP-1
EPA 6010
EPA 6010
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
Barium, Dissolved
Chromium, Dissolved
Acenaphthene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
4079704002
GP-2
EPA 6010
EPA 6010
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
Arsenic, Dissolved
Barium, Dissolved
Acenaphthylene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
4079704003
GP-3
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 7470
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
Arsenic, Dissolved
Barium, Dissolved
Cadmium, Dissolved
Chromium, Dissolved
Lead, Dissolved
Mercury, Dissolved
Acenaphthene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
Units
Report Limit
Analyzed
62.5
2.9J
0.0095J
0.016J
0.029J
0.027J
0.026J
0.020J
0.022J
0.035J
0.0078J
0.077
0.0096J
0.016J
0.011J
0.015J
0.049J
0.069
0.074
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
5.0
5.0
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
06/18/13 12:11
06/18/13 12:11
06/19/13 09:33
06/19/13 09:33
06/19/13 09:33
06/19/13 09:33
06/19/13 09:33
06/19/13 09:33
06/19/13 09:33
06/19/13 09:33
06/19/13 09:33
06/19/13 09:33
06/19/13 09:33
06/19/13 09:33
06/19/13 09:33
06/19/13 09:33
06/19/13 09:33
06/19/13 09:33
06/19/13 09:33
5.0J
61.8
0.0037J
0.0056J
0.015J
0.021J
0.072
0.013J
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
20.0
5.0
0.045
0.045
0.045
0.045
0.045
0.045
06/18/13 12:14
06/18/13 12:14
06/19/13 09:51
06/19/13 09:51
06/19/13 09:51
06/19/13 09:51
06/19/13 09:51
06/19/13 09:51
69.7
596
4.6J
184
81.0
0.34
0.0060J
0.011J
0.034J
0.031J
0.032J
0.023J
0.031J
0.041J
0.079
0.0054J
0.018J
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
20.0
5.0
5.0
5.0
7.5
0.20
0.048
0.048
0.048
0.048
0.048
0.048
0.048
0.048
0.048
0.048
0.048
06/18/13 12:16
06/18/13 12:16
06/18/13 12:16
06/18/13 12:16
06/18/13 12:16
06/17/13 14:21
06/19/13 10:09
06/19/13 10:09
06/19/13 10:09
06/19/13 10:09
06/19/13 10:09
06/19/13 10:09
06/19/13 10:09
06/19/13 10:09
06/19/13 10:09
06/19/13 10:09
06/19/13 10:09
Qualifiers

Page 5 of 19
#=HO#

Green Bay, WI 54302
(920)469-2436
HITS ONLY
Project:
Pace Project No.:
4079704
Lab Sample ID
Client Sample ID
Method
Parameters
Result
4079704003
GP-3
EPA 8270 by HVI

EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
4079704004
GP-4
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 6010
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
Arsenic, Dissolved
Barium, Dissolved
Cadmium, Dissolved
Chromium, Dissolved
Lead, Dissolved
Selenium, Dissolved
Silver, Dissolved
Acenaphthylene
Fluoranthene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Units
Report Limit
Analyzed
0.0093J
0.014J
0.049
0.062
0.081
ug/L
ug/L
ug/L
ug/L
ug/L
0.048
0.048
0.048
0.048
0.048
06/19/13 10:09
06/19/13 10:09
06/19/13 10:09
06/19/13 10:09
06/19/13 10:09
11.2J
160
1.2J
36.5
15.1
6.7J
3.0J
0.0051J
0.0065J
0.015J
0.029J
0.095
0.0095J
0.0081J
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
20.0
5.0
5.0
5.0
7.5
20.0
10.0
0.049
0.049
0.049
0.049
0.049
0.049
0.049
06/18/13 12:22
06/18/13 12:22
06/18/13 12:22
06/18/13 12:22
06/18/13 12:22
06/18/13 12:22
06/18/13 12:22
06/19/13 10:27
06/19/13 10:27
06/19/13 10:27
06/19/13 10:27
06/19/13 10:27
06/19/13 10:27
06/19/13 10:27
Qualifiers

Page 6 of 19
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079704
Sample: GP-1
Parameters
8082 GCS PCB
PCB, Total
Surrogates
Arsenic, Dissolved
Barium, Dissolved
Cadmium, Dissolved
Chromium, Dissolved
Lead, Dissolved
Selenium, Dissolved
Silver, Dissolved
7470 Mercury, Dissolved
Mercury, Dissolved
Lab ID: 4079704001

Results
Units
Collected: 06/14/13 00:00

LOQ
LOD
Received: 06/15/13 12:01
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

<0.29
<0.29
<0.29
<0.29
<0.29
<0.29
<0.29
<0.29
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
76 %
94 %
0.58
0.58
0.58
0.58
0.58
0.58
0.58
0.58
0.29
0.29
0.29
0.29
0.29
0.29
0.29
0.29
37-130
34-130
1
1
1
1
1
1
1
1
06/17/13 08:08
06/17/13 08:08
06/17/13 08:08
06/17/13 08:08
06/17/13 08:08
06/17/13 08:08
06/17/13 08:08
06/17/13 08:08
06/18/13 13:49
06/18/13 13:49
06/18/13 13:49
06/18/13 13:49
06/18/13 13:49
06/18/13 13:49
06/18/13 13:49
06/18/13 13:49
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
1336-36-3
1
1
06/17/13 08:08 06/18/13 13:49 877-09-8

06/17/13 08:08 06/18/13 13:49 2051-24-3
P2
L2

<4.2
62.5
<0.48
2.9J
<2.7
<5.2
<1.7
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
20.0
5.0
5.0
5.0
7.5
20.0
10.0
4.2
1.1
0.48
1.4
2.7
5.2
1.7
1
1
1
1
1
1
1
06/17/13 09:00
06/17/13 09:00
06/17/13 09:00
06/17/13 09:00
06/17/13 09:00
06/17/13 09:00
06/17/13 09:00
06/18/13 12:11
06/18/13 12:11
06/18/13 12:11
06/18/13 12:11
06/18/13 12:11
06/18/13 12:11
06/18/13 12:11
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4

<0.10 ug/L
0.20
0.10
06/17/13 10:06 06/17/13 14:17 7439-97-6
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Terphenyl-d14 (S)
0.0095J
<0.0038
0.016J
0.029J
0.027J
0.026J
0.020J
0.022J
0.035J
0.0078J
0.077
0.0096J
0.016J
0.011J
0.015J
0.049J
0.069
0.074
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
74 %
107 %
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
39-130
73-155
0.0042
0.0038
0.0053
0.0052
0.0054
0.0074
0.0088
0.011
0.0068
0.0060
0.0057
0.0042
0.0064
0.0039
0.0067
0.0036
0.0042
0.0058
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/19/13 09:33
06/19/13 09:33
06/19/13 09:33
06/19/13 09:33
06/19/13 09:33
06/19/13 09:33
06/19/13 09:33
06/19/13 09:33
06/19/13 09:33
06/19/13 09:33
06/19/13 09:33
06/19/13 09:33
06/19/13 09:33
06/19/13 09:33
06/19/13 09:33
06/19/13 09:33
06/19/13 09:33
06/19/13 09:33
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0
1
1
06/18/13 07:44 06/19/13 09:33 321-60-8

06/18/13 07:44 06/19/13 09:33 1718-51-0

Date: 06/19/2013 03:26 PM
Page 7 of 19
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079704
Sample: GP-2
Parameters
8082 GCS PCB
PCB, Total
Surrogates
Arsenic, Dissolved
Barium, Dissolved
Cadmium, Dissolved
Chromium, Dissolved
Lead, Dissolved
Selenium, Dissolved
Silver, Dissolved
Mercury, Dissolved
Lab ID: 4079704002

Results
Units
Collected: 06/14/13 00:00

LOQ
LOD
Received: 06/15/13 12:01
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

<0.28
<0.28
<0.28
<0.28
<0.28
<0.28
<0.28
<0.28
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
79 %
90 %
0.56
0.56
0.56
0.56
0.56
0.56
0.56
0.56
0.28
0.28
0.28
0.28
0.28
0.28
0.28
0.28
37-130
34-130
1
1
1
1
1
1
1
1
06/17/13 08:08
06/17/13 08:08
06/17/13 08:08
06/17/13 08:08
06/17/13 08:08
06/17/13 08:08
06/17/13 08:08
06/17/13 08:08
06/18/13 14:06
06/18/13 14:06
06/18/13 14:06
06/18/13 14:06
06/18/13 14:06
06/18/13 14:06
06/18/13 14:06
06/18/13 14:06
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
1336-36-3
1
1
06/17/13 08:08 06/18/13 14:06 877-09-8

06/17/13 08:08 06/18/13 14:06 2051-24-3
P2
L2

5.0J
61.8
<0.48
<1.4
<2.7
<5.2
<1.7
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
20.0
5.0
5.0
5.0
7.5
20.0
10.0
4.2
1.1
0.48
1.4
2.7
5.2
1.7
1
1
1
1
1
1
1
06/17/13 09:00
06/17/13 09:00
06/17/13 09:00
06/17/13 09:00
06/17/13 09:00
06/17/13 09:00
06/17/13 09:00
06/18/13 12:14
06/18/13 12:14
06/18/13 12:14
06/18/13 12:14
06/18/13 12:14
06/18/13 12:14
06/18/13 12:14
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4

<0.10 ug/L
0.20
0.10
06/17/13 10:06 06/17/13 14:19 7439-97-6
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Terphenyl-d14 (S)
<0.0039
0.0037J
<0.0049
<0.0048
<0.0050
<0.0068
<0.0081
<0.010
<0.0062
<0.0055
<0.0052
0.0056J
<0.0059
0.015J
0.021J
0.072
0.013J
<0.0053
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
78 %
108 %
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
0.045
39-130
73-155
0.0039
0.0035
0.0049
0.0048
0.0050
0.0068
0.0081
0.010
0.0062
0.0055
0.0052
0.0039
0.0059
0.0036
0.0061
0.0033
0.0039
0.0053
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/19/13 09:51
06/19/13 09:51
06/19/13 09:51
06/19/13 09:51
06/19/13 09:51
06/19/13 09:51
06/19/13 09:51
06/19/13 09:51
06/19/13 09:51
06/19/13 09:51
06/19/13 09:51
06/19/13 09:51
06/19/13 09:51
06/19/13 09:51
06/19/13 09:51
06/19/13 09:51
06/19/13 09:51
06/19/13 09:51
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0
1
1
06/18/13 07:44 06/19/13 09:51 321-60-8

06/18/13 07:44 06/19/13 09:51 1718-51-0

Date: 06/19/2013 03:26 PM
Page 8 of 19
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079704
Sample: GP-3
Parameters
8082 GCS PCB
PCB, Total
Surrogates
Arsenic, Dissolved
Barium, Dissolved
Cadmium, Dissolved
Chromium, Dissolved
Lead, Dissolved
Selenium, Dissolved
Silver, Dissolved
Mercury, Dissolved
Lab ID: 4079704003

Results
Units
Collected: 06/14/13 00:00

LOQ
LOD
Received: 06/15/13 12:01
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

<0.27
<0.27
<0.27
<0.27
<0.27
<0.27
<0.27
<0.27
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
82 %
77 %
0.54
0.54
0.54
0.54
0.54
0.54
0.54
0.54
0.27
0.27
0.27
0.27
0.27
0.27
0.27
0.27
37-130
34-130
1
1
1
1
1
1
1
1
06/17/13 08:08
06/17/13 08:08
06/17/13 08:08
06/17/13 08:08
06/17/13 08:08
06/17/13 08:08
06/17/13 08:08
06/17/13 08:08
06/18/13 14:23
06/18/13 14:23
06/18/13 14:23
06/18/13 14:23
06/18/13 14:23
06/18/13 14:23
06/18/13 14:23
06/18/13 14:23
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
1336-36-3
1
1
06/17/13 08:08 06/18/13 14:23 877-09-8

06/17/13 08:08 06/18/13 14:23 2051-24-3
P2
L2

69.7
596
4.6J
184
81.0
<5.2
<1.7
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
20.0
5.0
5.0
5.0
7.5
20.0
10.0
4.2
1.1
0.48
1.4
2.7
5.2
1.7
1
1
1
1
1
1
1
06/17/13 09:00
06/17/13 09:00
06/17/13 09:00
06/17/13 09:00
06/17/13 09:00
06/17/13 09:00
06/17/13 09:00
06/18/13 12:16
06/18/13 12:16
06/18/13 12:16
06/18/13 12:16
06/18/13 12:16
06/18/13 12:16
06/18/13 12:16
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4

0.34 ug/L
0.20
0.10
06/17/13 10:06 06/17/13 14:21 7439-97-6
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Terphenyl-d14 (S)
0.0060J
<0.0038
0.011J
0.034J
0.031J
0.032J
0.023J
0.031J
0.041J
<0.0059
0.079
0.0054J
0.018J
0.0093J
0.014J
0.049
0.062
0.081
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
70 %
90 %
0.048
0.048
0.048
0.048
0.048
0.048
0.048
0.048
0.048
0.048
0.048
0.048
0.048
0.048
0.048
0.048
0.048
0.048
39-130
73-155
0.0041
0.0038
0.0052
0.0051
0.0053
0.0072
0.0087
0.011
0.0066
0.0059
0.0056
0.0041
0.0062
0.0038
0.0065
0.0036
0.0041
0.0057
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/19/13 10:09
06/19/13 10:09
06/19/13 10:09
06/19/13 10:09
06/19/13 10:09
06/19/13 10:09
06/19/13 10:09
06/19/13 10:09
06/19/13 10:09
06/19/13 10:09
06/19/13 10:09
06/19/13 10:09
06/19/13 10:09
06/19/13 10:09
06/19/13 10:09
06/19/13 10:09
06/19/13 10:09
06/19/13 10:09
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0
1
1
06/18/13 07:44 06/19/13 10:09 321-60-8

06/18/13 07:44 06/19/13 10:09 1718-51-0

Date: 06/19/2013 03:26 PM
Page 9 of 19
#=AR#

Green Bay, WI 54302
(920)469-2436
ANALYTICAL RESULTS
Project:
Pace Project No.:
4079704
Sample: GP-4
Parameters
8082 GCS PCB
PCB, Total
Surrogates
Arsenic, Dissolved
Barium, Dissolved
Cadmium, Dissolved
Chromium, Dissolved
Lead, Dissolved
Selenium, Dissolved
Silver, Dissolved
Mercury, Dissolved
Lab ID: 4079704004

Results
Units
Collected: 06/14/13 00:00

LOQ
LOD
Received: 06/15/13 12:01
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual

<0.31
<0.31
<0.31
<0.31
<0.31
<0.31
<0.31
<0.31
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
73 %
83 %
0.62
0.62
0.62
0.62
0.62
0.62
0.62
0.62
0.31
0.31
0.31
0.31
0.31
0.31
0.31
0.31
37-130
34-130
1
1
1
1
1
1
1
1
06/17/13 08:08
06/17/13 08:08
06/17/13 08:08
06/17/13 08:08
06/17/13 08:08
06/17/13 08:08
06/17/13 08:08
06/17/13 08:08
06/18/13 14:40
06/18/13 14:40
06/18/13 14:40
06/18/13 14:40
06/18/13 14:40
06/18/13 14:40
06/18/13 14:40
06/18/13 14:40
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
1336-36-3
1
1
06/17/13 08:08 06/18/13 14:40 877-09-8

06/17/13 08:08 06/18/13 14:40 2051-24-3
P2
L2

11.2J
160
1.2J
36.5
15.1
6.7J
3.0J
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
20.0
5.0
5.0
5.0
7.5
20.0
10.0
4.2
1.1
0.48
1.4
2.7
5.2
1.7
1
1
1
1
1
1
1
06/17/13 09:00
06/17/13 09:00
06/17/13 09:00
06/17/13 09:00
06/17/13 09:00
06/17/13 09:00
06/17/13 09:00
06/18/13 12:22
06/18/13 12:22
06/18/13 12:22
06/18/13 12:22
06/18/13 12:22
06/18/13 12:22
06/18/13 12:22
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4

<0.10 ug/L
0.20
0.10
06/17/13 10:06 06/17/13 14:23 7439-97-6
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
1-Methylnaphthalene
2-Methylnaphthalene
Naphthalene
Phenanthrene
Pyrene
Surrogates
Terphenyl-d14 (S)
<0.0042
0.0051J
<0.0052
<0.0051
<0.0053
<0.0073
<0.0087
<0.011
<0.0067
<0.0059
0.0065J
<0.0042
<0.0063
0.015J
0.029J
0.095
0.0095J
0.0081J
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
60 %
91 %
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
0.049
39-130
73-155
0.0042
0.0038
0.0052
0.0051
0.0053
0.0073
0.0087
0.011
0.0067
0.0059
0.0056
0.0042
0.0063
0.0039
0.0066
0.0036
0.0042
0.0057
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/18/13 07:44
06/19/13 10:27
06/19/13 10:27
06/19/13 10:27
06/19/13 10:27
06/19/13 10:27
06/19/13 10:27
06/19/13 10:27
06/19/13 10:27
06/19/13 10:27
06/19/13 10:27
06/19/13 10:27
06/19/13 10:27
06/19/13 10:27
06/19/13 10:27
06/19/13 10:27
06/19/13 10:27
06/19/13 10:27
06/19/13 10:27
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
218-01-9
53-70-3
206-44-0
86-73-7
193-39-5
90-12-0
91-57-6
91-20-3
85-01-8
129-00-0
1
1
06/18/13 07:44 06/19/13 10:27 321-60-8

06/18/13 07:44 06/19/13 10:27 1718-51-0

Date: 06/19/2013 03:26 PM
Page 10 of 19
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079704
QC Batch:
MERP/3699
Analysis Method:
EPA 7470
QC Batch Method:
EPA 7470
7470 Mercury Dissolved

METHOD BLANK:
4079704001, 4079704002, 4079704003, 4079704004
809199

Parameter
Matrix: Water
4079704001, 4079704002, 4079704003, 4079704004
Blank
Reporting
Units
Result
Limit
Mercury, Dissolved
ug/L
809200
Parameter
<0.10
Mercury, Dissolved
ug/L
Parameter
Mercury, Dissolved
Spike
Conc.
Units
Units
ug/L
0.20
LCS
Result
5
4079685014
Result
Qualifiers
06/17/13 14:00
LCS
% Rec
4.9
809201
Analyzed
% Rec
Limits
97
Qualifiers
85-115
809202
MS
Spike
Conc.
MSD
Spike
Conc.
MS
Result
4.9
MSD
Result
MS
% Rec
5.0
MSD
% Rec
% Rec
Limits
Max
RPD RPD
2
Qual
20

Date: 06/19/2013 03:26 PM
Page 11 of 19
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079704
QC Batch:
MPRP/8636
Analysis Method:
EPA 6010
QC Batch Method:
EPA 3010
6010 MET Dissolved

METHOD BLANK:
4079704001, 4079704002, 4079704003, 4079704004
809163

Parameter
Matrix: Water
4079704001, 4079704002, 4079704003, 4079704004
Blank
Reporting
Units
Result
Limit
Arsenic, Dissolved
Barium, Dissolved
Cadmium, Dissolved
Chromium, Dissolved
Lead, Dissolved
Selenium, Dissolved
Silver, Dissolved
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
809164
Parameter
<4.2
<1.1
<0.48
<1.4
<2.7
<5.2
<1.7
Arsenic, Dissolved
Barium, Dissolved
Cadmium, Dissolved
Chromium, Dissolved
Lead, Dissolved
Selenium, Dissolved
Silver, Dissolved
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Parameter
Arsenic, Dissolved
Barium, Dissolved
Cadmium, Dissolved
Chromium, Dissolved
Lead, Dissolved
Selenium, Dissolved
Silver, Dissolved
Spike
Conc.
Units
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
20.0
5.0
5.0
5.0
7.5
20.0
10.0
LCS
Result
500
500
500
500
500
500
250
4079685014
Result
Qualifiers
06/18/13 11:59
06/18/13 11:59
06/18/13 11:59
06/18/13 11:59
06/18/13 11:59
06/18/13 11:59
06/18/13 11:59
LCS
% Rec
492
508
494
507
495
487
243
809165
Analyzed
% Rec
Limits
98
102
99
101
99
97
97
Qualifiers
80-120
80-120
80-120
80-120
80-120
80-120
80-120
809166
MS
Spike
Conc.
MSD
Spike
Conc.
MS
Result
495
553
491
504
497
495
245
MSD
Result
MS
% Rec
502
554
493
509
497
499
248
MSD
% Rec
% Rec
Limits
Max
RPD RPD
1
0
0
1
0
1
1
Qual
20
20
20
20
20
20
20

Date: 06/19/2013 03:26 PM
Page 12 of 19
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079704
QC Batch:
OEXT/18613
Analysis Method:
EPA 8082
QC Batch Method:
EPA 3510
8082 GCS PCB

METHOD BLANK:
4079704001, 4079704002, 4079704003, 4079704004
809133

Parameter
Matrix: Water
4079704001, 4079704002, 4079704003, 4079704004
Blank
Reporting
Units
Result
Limit
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%

Parameter
<0.12
<0.12
<0.12
<0.12
<0.12
<0.12
<0.12
97
77
809134
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
0.25
0.25
0.25
0.25
0.25
0.25
0.25
34-130
37-130
Analyzed
Qualifiers
06/18/13 11:30
06/18/13 11:30
06/18/13 11:30
06/18/13 11:30
06/18/13 11:30
06/18/13 11:30
06/18/13 11:30
06/18/13 11:30
06/18/13 11:30
809135
Spike
Conc.
2.5
LCS
Result
<0.12
<0.12
<0.12
<0.12
<0.12
<0.12
2.7
LCSD
Result
<0.12
<0.12
<0.12
<0.12
<0.12
<0.12
1.6
LCS LCSD
% Rec % Rec
108
101
93
63
57
46
% Rec
Limits
70-130
34-130
37-130
Max
RPD
RPD
52
Qualifiers
20
20
20
20
20
20
20 L0,R1

Date: 06/19/2013 03:26 PM
Page 13 of 19
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079704
QC Batch:
OEXT/18634
Analysis Method:
EPA 8270 by HVI
QC Batch Method:
EPA 3510
8270 Water PAH by HVI

METHOD BLANK:
4079704001, 4079704002, 4079704003, 4079704004
809563

Parameter
1-Methylnaphthalene
2-Methylnaphthalene
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
Naphthalene
Phenanthrene
Pyrene
Terphenyl-d14 (S)
Matrix: Water
4079704001, 4079704002, 4079704003, 4079704004
Blank
Reporting
Units
Result
Limit
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%

Parameter
1-Methylnaphthalene
2-Methylnaphthalene
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Chrysene
Fluoranthene
Fluorene
Naphthalene
Phenanthrene
<0.0040
<0.0068
<0.0043
<0.0039
<0.0054
<0.0053
<0.0055
<0.0075
<0.0090
<0.012
<0.0069
<0.0061
<0.0058
<0.0043
<0.0065
<0.0037
<0.0043
<0.0059
69
116
809564
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050
39-130
73-155
Analyzed
Qualifiers
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
06/19/13 07:26
809565
LCS
Result
Spike
Conc.
.2
.2
.2
.2
.2
.2
.2
.2
.2
.2
.2
.2
.2
.2
.2
.2
.2
0.11
0.11
0.15
0.15
0.17
0.21
0.19
0.20
0.19
0.21
0.21
0.19
0.19
0.15
0.19
0.14
0.17
LCSD
Result
0.11
0.11
0.15
0.15
0.18
0.20
0.19
0.20
0.19
0.21
0.21
0.19
0.19
0.15
0.19
0.12
0.17
LCS LCSD
% Rec % Rec
54
54
75
75
87
103
93
99
94
107
104
93
95
76
93
69
87
54
53
74
73
89
101
95
100
94
106
106
93
93
77
93
61
86
% Rec
Limits
23-130
22-130
31-130
31-130
26-130
47-130
41-130
37-130
37-130
51-130
50-130
34-130
49-130
30-130
36-130
24-130
39-130
Max
RPD
RPD
1
1
1
2
2
2
3
2
0
1
2
0
2
1
1
11
0
Qualifiers
49
50
34
37
35
27
28
27
29
26
26
30
26
34
29
40
30

Date: 06/19/2013 03:26 PM
Page 14 of 19
#=QC#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079704

Parameter
Pyrene
Terphenyl-d14 (S)
809564
Units
ug/L
%
%
809565
Spike
Conc.
LCS
Result
.2
0.22
LCSD
Result
0.21
LCS LCSD
% Rec % Rec
108
68
101
106
66
101
% Rec
Limits
47-130
39-130
73-155
Max
RPD
RPD
2
Qualifiers
25

Date: 06/19/2013 03:26 PM
Page 15 of 19
#=QL#

Green Bay, WI 54302
(920)469-2436
QUALIFIERS
Project:
Pace Project No.:
4079704
DEFINITIONS
S - Surrogate
LABORATORIES
PASI-G
BATCH QUALIFIERS
Batch: GCSV/9716
[M5]
Batch: MSSV/5762
[M5]
ANALYTE QUALIFIERS
L0
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
L2
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results may be biased low.
P2
Re-extraction or re-analysis could not be performed due to insufficient sample amount.
R1
RPD value was outside control limits.

Date: 06/19/2013 03:26 PM
Page 16 of 19
#=CR#

Green Bay, WI 54302
(920)469-2436

Project:
Pace Project No.:
4079704
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
4079704001
4079704002
4079704003
4079704004
GP-1
GP-2
GP-3
GP-4
EPA 3510
EPA 3510
EPA 3510
EPA 3510
OEXT/18613
OEXT/18613
OEXT/18613
OEXT/18613
EPA 8082
EPA 8082
EPA 8082
EPA 8082
GCSV/9716
GCSV/9716
GCSV/9716
GCSV/9716
4079704001
4079704002
4079704003
4079704004
GP-1
GP-2
GP-3
GP-4
EPA 3010
EPA 3010
EPA 3010
EPA 3010
MPRP/8636
MPRP/8636
MPRP/8636
MPRP/8636
EPA 6010
EPA 6010
EPA 6010
EPA 6010
ICP/7675
ICP/7675
ICP/7675
ICP/7675
4079704001
4079704002
4079704003
4079704004
GP-1
GP-2
GP-3
GP-4
EPA 7470
EPA 7470
EPA 7470
EPA 7470
MERP/3699
MERP/3699
MERP/3699
MERP/3699
EPA 7470
EPA 7470
EPA 7470
EPA 7470
MERC/4609
MERC/4609
MERC/4609
MERC/4609
4079704001
4079704002
4079704003
4079704004
GP-1
GP-2
GP-3
GP-4
EPA 3510
EPA 3510
EPA 3510
EPA 3510
OEXT/18634
OEXT/18634
OEXT/18634
OEXT/18634
EPA 8270 by HVI

EPA 8270 by HVI
EPA 8270 by HVI
EPA 8270 by HVI
MSSV/5762
MSSV/5762
MSSV/5762
MSSV/5762

Date: 06/19/2013 03:26 PM
Page 17 of 19
Page 18 of 19
Page 19 of 19

Phase II ESA

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Phase II ESA

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Phase II

Environmental Site Assessment

Phase II Environmental Site Assessment

This report prepared by:

This report reviewed by:

5201 E. Terrace Drive, Suite 200

The current presence of a 10,000-gallon underground storage tank (UST) system,

The former presence of a gasoline house, as identified on historical fire insurance

The former operation of a railway power house, as identified on historical fire

Phase II ESA Scope

Retained a drilling contractor and installed 26 soil probes to a maximum depth of 12

Submitted soil and groundwater samples to a Wisconsin certified laboratory for

Analyzed soils with potentially hazardous concentrations of lead by toxicity

The current presence of a 10,000-gallon underground storage tank (UST) system in

The former presence of a gasoline house, as identified on historical fire insurance

The former operation of a railway power house, as identified on historical fire

Site Location and Project Numbers

Wisconsin Department of Administration

Drilling and Laboratory Contractors

Phase II ESA Scope

Retained a drilling contractor and installed 26 soil probes to a maximum depth of 12

Submitted soil and groundwater samples to a Wisconsin certified laboratory for

Analyzed soils with potentially hazardous concentrations of lead by toxicity

Former Brass Foundry

PCBs, Pb, and Cr in former cistern during

Former Oil Dipping

Not previously investigated. Analysis

Not previously investigated. Analysis

Former North Scrap

Not previously investigated. Analysis

Former West Coal Bin

Not previously investigated. Analysis

Former East Coal Bin

Not previously investigated. Analysis

Former South Scrap

Not previously investigated. Analysis

Former Paint Shop

Not previously investigated. Analysis

Former Oil House

Former Gasoline House

Not previously investigated. Analysis

Not previously investigated. Analysis

Former Machine Shop

Previously investigated by Ivertech in

Former Railway Power

No information available regarding

No environmental screening data collected

Soil probe locations are shown on Figures 2 and 3.

General Soil Description

GP-4 and GP-5

Sand and slag fill from 0-2 ft bgs. Medium

Asphalt and gravel fill from 0-1.5 ft bgs,

Asphalt and gravel fill from 0-2 ft bgs, pea

Medium brown silty clay from 0-1.5 ft bgs,

Asphalt and gravel fill from 0-1 ft bgs, silty

Concrete and clayey sand or gravel fill from

GP-13 and GP14

Dark brown fill and slag from 0-2 ft bgs with

GP-15 and GP16

Concrete and sand fill from 0-2 ft bgs, black

General Soil Description

Asphalt and gravel fill from 0-2 ft bgs,

Asphalt and gravel fill from 0-2 ft bgs, black

Gravel fill from 0-1 ft bgs, black gravel fill