l [B-JGT-J-DIFA)

0 415

Serial No. [

CHEMICAL ENGINEERING
Paper-[

('M:-:-ax-im_u_m_M:-:-a-rks:-.-.-2-o'o)

om

(Time Allowei: Three Hours)

INSTRUCTIONS

xa

ra

ce

.c

Candidates should attempt Question Nos. 1 and 5

which are compulsory, and THREE of the
remaining questions, selecting at least
ONE question from each Section.
The number of marks carried by e,.ach question is
indicated at the end of the question.
Answers must be written in ENGLISH only.
Assume suitable data, if considered necessary, and
indicate the same clearly.
Neat sketches may be drawn, wherever required.

1.

.e

SECTION-A

Answer any FOUR of the following : -

JQX4=40

w
w

(a) Classify fluids rheologically on the basis of their

stress-strain relationship. Explain them with
examples.

10

(b) Discuss flow pattern caused by a turbine type

impelter in an agitated tank. Mention ways to

prevent swirling and vortex formation in the
10
agitated tank.
(I)

(Contd.)

(c) (i)

om

Define capacity and effectiveness of a screen.

Derive an expression for the overall
effectiveness of a screen.
5
(ii) State Rittinger's law of crushing. Mention its
limitations.
5

(d) Discuss, the mechanism of nucleate boiling. How

does it differ from film boiling?
10

(a) (i)

ce

Differentiate between differential and

cumulative analysis to find the average size
of a sample.
5
(ii) What is a ball mill ? Derive an expression
for its critical speed.
5

ra

2.

.c

(c) Discuss, with the help of a sketch, the principle

of a steam jet ejector for creating vacuum.
10

(b) Determine an expression for terminal velocity of

xa

solid particles settling in a fluid s~ream under

hindered condition. How will you modify it when
the container is of limited size ?
10

.e

(c) Explain the construction and operation of a plate

and frame filter press.

w
w

State the difference between washing and nonwashing plate.

10

(d) What is an ultrafine grinder ? Explain its principle

3.

and operation.

10

(a) Draw boiling curve and explain various regjmes

occurring therein. What is the significance of
critical heat flux point on the curve?
10
(2)

(Comd.)

(b) Compare forward feed double effect evaporator

with backward feed dQuble effect evaporator.

10

om

(c) What is boiling point elevation? Discuss its effect

on the capacity and steam economy of an
evaporator.
10

{a)

Discuss clearly the concept of film transfer

coefficient and overall transfer coefficient in mass

ce

4.

.c

(d) Briefly describe the procedure to calculate radiant

heat load of an oil fired furnace.
I0

ra

transfer.

How does penetration theory of mass transfer differ

from surface renewal theory ?
I0

Define 'relative volatility'. How can it be

.e

(c) (i)

xa

(b) Explain the construction and operation of a packed

I0
extraction tower.

w
w

used to draw equilibrium curve of a binary

system?
5

(ii) Mention limitations of McCabe-Thiele

method. How are these overcome in PonchonSavarit method ?
s

(d) With a neat drying rate curve, explain various zones

of drying. Mention the mechanism of moisture
movement in each zone.
(3)

I0
(Corud.)

SECTION-8
5.

Answer any FOUR of the following : -

10x4=40

(a) Explain stepwise procedure for the design of an

om

elliptical head for a cylindrical vessel.

{b) Discuss failure of vessels based on the theory of
plasticity.

.c

(c) Name various supports generally used for process

ce

vessels. Give their advantages and disadvantages.

(d) Develop an expression for frequency response of

Discuss procedure for plotting of open loop transfer

(e)

ra

a transportation lag. Show it graphically thro' a

sketch.

6.

(a)

xa

function by root locus method.

What is pervaporation? Explain it with the help

of a neat sketch and also indicate its areas of

application.

.e

10

w
w

(b) Discuss various types of membranes. Mention

procedure of immersion precipitation process for

the production of a membrane.

I0

(c) Describe dialysis and electrodialysis processes.

Give their areas of applications.
Briefly explain the working of an instrument based
on electrodialysis.
10
(4)

(Contd.)

(d) What is Super Critical Fluid Extraction ? Compare

super critical fluid with the conventional fluid as

a solvent. Give areas of application of super critical

10

7.

om

fluid extraction process.

(a) Describe Coate's theoretical analysis for bending

stress at the head-shell junction of a vessel.

10

.c

(b) Explain the design equations for calculating the

thickness of cylindrical and spherical shells. How

ce

will you select a standard plate for the fabrication

of a shell ?

10

ra

(c) Estimate the thickness of the shell and head of

a process vessel. The vessel is a cylinder having

ellipsoidal heads (major to minor axis ratio

xa

2 : I) at its bottom and top ends. The_ inside

diameter and length of the vessel are I 5 m and

2 m respectively. The vessel is to operate at a

.e

pressure of 14 MN/m 2 (absolute}. The allowable

stress for the material (plain carbon steel) is

w
w

85 MNim 2. Weld is fully radiographed. A corrosion

allowance of 2 mm may be taken.

Take design pressure as 10% above operating

10

pressure.

(d) What are the various stresses on a tall vessel to

be installed in a seismic zone ?

(5}

10
(Contd.)

8.

{a) How do you measure liquid level if the liquid

contains suspended solid particles ? Suggest a
suitable measuring instrument and explain its
working principle.
I0

Negative and positive feedback control

systems
5

.c

(i)

om

(b) Explain the following:-

ra

ce

(ii) Servo and regulatory control problems. 5

(c) Develop a transfer function between pressure drop
and the manometer reading for a mercury
manometer. State the assumptions made.
I0
(d) Explain the working of a PID control system. Draw
a pneumatic control cir:cuit for this system and give

w
w

.e

xa

its characteristics.

(6)

I0

,. ~s ...L.~~

313

B-JGT-J-DIF B

CHEMICA L ENGINEE RING

om

Paper II

ra

ce

.c

INSTRUCTIO NS
Candidates should attempt questions no. I and
5 whick are compulsory, and any THREE of the
remaining quetltions, selecting at least ONE
question from each Section.
The number of marks carried by each questifm
is indicated at the end of the question.
An.swers must be written in ENGUSH.

xa

Assume suitable data, if considered necessary,

and indicate the saiJU' clearly.
Symbols and notations have their usual meanings.

SECTlON A

w
w

.e

Neat sketches may be drawn, wherever required.

I.

Answer any four ofthe following (maximum UiO words

each):
4><10==40

(a)

Explain ahout excess air requirement

adiabatic flame temperature.

(b)

Distinguish between an ideal mixed flow reactor

and an ideal plug flow reacWr. In which reactor
will you get better conversion ? Write down the
design equation of each ideal reactor.

B-JGT-J-DIFB

and

[Contd.]

(d)

Pure oxygen is mixed with air to produce an

ellriched air containing 50% by volume of oxygen.
Determine the ratio of air to oxygen used.

(e)

Explain about temperature effects and runaway

reactions.

(a)

Explain aOOut recycle, bypass, purge and Kopp's

Rule.

ce

.c

om

Compare and il!UEtrate the interpretation of

kinetic data by integral method of analysis with
that of differential method of analysis.

10

(b)

The analysis of gas entering the secondary

converter in a contact sulphuric acid plant is 4%
of 802, 13% of 0 2 and 83% N 2 (volume basis). In
a converter S02 is oxidised to 803. The gases
leaving the converter contain 045% S02 on S03
20
free basis. Calculate % conversion of S0 2.

(c)

An aqueous solution of245% by weight sulphuric

acid, has a specific gravity of 1011. Express the
composition of sulphuric acid in normality.

10

If the density of gaseous ammonia at 473 K and

50 bar is 243 kg!M" 3, estimate its fugacity.

20

w
w

.e

xa

ra

2.

(c)

S.

(a)

(b)

Calculate the fraction of pure ethane that would

dehydrogenate at 750 K and 5 atm, if the
following reaction takes place at equilibrium :
~G 7 GO K = >J2576 kJ.

6-JGT -J-D1FB

20

[Contd.J

Find the first order rate constant. for the

disappearance of A in the gas reaction 2A --~> R if,
on holding the pressure constant, the volume of
reaction mixture, starting with 80% A, decreases
by 20% in 3 minutes.
20

(b}

A gaseous feed of pure A (one mole/litre) enters a

mixed flow reactor of 2 litres volume and reacts
as follows :

2A--~>

om

(a)

R - rA::: 005c! molellitre.sec.

.c

4.

outlet
20

w
w

.e

xa

ra

ce

Find what feed rate will give an

concentration of CA "' 05 mole/litre.

B-JGT-J-DIFB

IContd.]

r
I

SECTION B

Explain about atmospheric distillation of crude

oiL

(b)

Explain about edible oils extraction. Compare

and contrast Soaps vs, Detergents.

(c)

Explain about the reason

depletion and acid rain.

(d)

Discuss about solid wastes hazards and their

disposal techniques.

(e)

Explain about net present value by discounted

cash flow.

Ia)

Give an account of coal chemicals.

15

(b)

Discuss manufacture of ammonia (NH 3) with a

neal flow sheet.

15

Explain how poly vinyl chloride is manufactured.

10

ra

ce

.c

layer

Explain the extent of environmental legislation in the

country. Bring out the specific features relevant W
water and air protection and those relating to forest
conservation.
40

w
w

7.

ozone

.e

{o)

for

om

(a)

6.

Answer any four of the following (maximum 150 words

each):
4x10=40

xa

5.

(a)

8.

(b)

Discuss about the estimation methods of fixed

and working capital requirement fo~: a process
industry.

20

Explain about HAZOP and HAZAN.

20

B-JGT -J-OIFB