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George W. Woodruff School of Mechanical Engineering, Georgia Institute of Technology, 801 Ferst Drive, Atlanta, GA 30332-0405, USA
School of Materials Science and Engineering, Georgia Institute of Technology, 771 Ferst Drive, Atlanta, GA 30332-0245, USA
art ic l e i nf o
a b s t r a c t
Article history:
Received 3 April 2015
Received in revised form
20 October 2015
Accepted 24 October 2015
Available online 31 October 2015
Changes in temperature can have a large effect on the fretting damage response for materials with
properties that are highly temperature sensitive, such as austenitic stainless steel. The fretting damage
response of thin sheets of AISI 301 stainless steel in the full hard condition in contact with AISI 52100
steel is investigated for temperatures ranging from 20 C to 250 C. Changes in material resistance to
fatigue damage and wear are characterized by determination of mechanical properties and oxidation
behavior with changing temperature. The drivers for wear and fatigue are evaluated via nite element
analysis over a range of temperatures. The net effect of changes in the wear and fatigue damage drivers
and resistance with changing temperature is discussed.
& 2015 Elsevier B.V. All rights reserved.
Keywords:
Fretting
Fatigue
Frictional energy dissipation
Stainless steel
Glaze oxide
1. Introduction
Fretting is a low amplitude oscillatory motion between contacting bodies which results in damage of the materials in contact.
Wear and fatigue damage can occur, with the type and extent of
damage being sensitive to many parameters [1]. Changes in temperature affect many aspects of the interaction, including the
mechanical properties and oxidation behavior, which in turn affect
the friction response and the extent of fatigue damage.
The mechanical properties of austenitic stainless steels are
highly temperature sensitive. Austenitic stainless steel is comprised austenite in the annealed state, and can undergo a transformation to martensite due to a combination of thermal treatment and/or mechanical loading. Martensite has a higher hardness
than austenite, resulting in an increase in strength. The occurrence
of the transformation in regions of high deformation results in
local hardening and reduction in the local plastic instability, thus
increasing ductility [2]. The stability of the austenite increases
with increasing temperature, and is sensitive to the composition
[36]. The temperature above which martensite cannot be formed
by mechanical loading, Md, has been reported as 100 C for 301
stainless steel [7,8]. Therefore, the benecial effects associated
n
Corresponding author at: George W. Woodruff School of Mechanical Engineering, Georgia Institute of Technology, 801 Ferst Drive, Atlanta, GA 30332-0405,
USA. Tel.: 1 404 894 3074.
E-mail address: rick.neu@gatech.edu (R.W. Neu).
http://dx.doi.org/10.1016/j.wear.2015.10.007
0043-1648/& 2015 Elsevier B.V. All rights reserved.
Table 1
Material composition in weight percent.
Element Weight Percent
Mn
Cr
Si
Ni
Mo
Cu
Al
0.15
0.931.05
2.00
0.250.45
16.018.0
1.351.60
1.00
0.150.35
0.05
0.025 Max
0.03
0.015 Max
6.08.0
0.25 Max
0.10
0.10 Max
0.30 Max
0.0015 Max
0.050 Max
Table 2
Elastic constants used for material models.
E (GPa)
Stationary specimen
Backing plate
Moving specimen
PTFE layer
3. Modeling method
3.1. Model formulation
A nite element model of the experimental conguration was
created using ABAQUS/Standard to determine the local cyclic
stressstrain behavior and local frictional energy dissipation. The
geometry of the model is shown in Fig. 2. The model is twodimensional plane-strain and consists of three bodies with two
contact interactions. A Lagrangian contact formulation was used
for contact between the moving specimen and the stationary
specimen to enforce exact stick. A Penalty contact formulation was
used for contact between the stationary specimen and the PTFE
layer to aid convergence. A compliant layer was added to the sides
of the backing plate to account for the compliance of the test
conguration. The sides of the compliant layers and the bottom of
the backing plate were constrained against motion. Normal force
and displacement boundary conditions were applied to a reference
node in a rigid layer at the top of the moving specimen. A mesh
size of 2 2 m2 was used at the contact interface between the
20 C
250 C
20 C
250 C
167
195
210
0.5
142
182
200
0.03
0.30
0.30
0.30
0.46
0.30
0.30
0.30
0.46
specimen and the PTFE used was 0.04 for 20 C and 0.03 for
250 C, which was in agreement with the literature [28].
Simulations were performed for three cycles, which was found
to be sufcient to stabilize the model response, which was
determined by a negligible difference in plastic strain between
cycles three and four for the most highly loaded test condition.
Model results for the third cycle were used for analysis.
3.2. Fretting damage modeling
The results from the model were used to calculate damage
parameters to determine the changes in damage drivers with
changing test conditions. The stressstrain and slip results from
the simulation of each test condition were exported from ABAQUS
and post-processed using MATLAB. The FatemiSocie (FS) criticalplane based multiaxial fatigue damage parameter [29] was used to
indicate the local driver for fatigue damage as a function of location over the model. The FS parameter was found in previous work
[16] to better correlate the fretting damage for the 20 C conditions investigated here than the SmithWatsonTopper parameter
[30]. The FS value was averaged over a 15 m radius, approximately equal to the grain size, to account for strain gradient sensitivity. The local energy dissipation per cycle, adapted from the
Ruiz Fretting Damage Parameter (FDP) [31], was used to indicate
Fig. 3. Plain fatigue response of 301 stainless steel (full hard) at 20 C and 250 C,
R 0.05.
the local driver for wear over the surface of the stationary
specimen.
4. Experimental results
4.1. Baseline material performance
The stress-life results for plain fatigue of 301 stainless steel at
20 C and 250 C are shown in Fig. 3. The increase in temperature
resulted in a decrease in the fatigue limit by approximately 510%.
The decrease in the fatigue strength was more signicant at lower
cycles to failure. The larger reduction in fatigue strength at lower
cycles to failure is attributed to the reduction in ductility which
occurs due to the increase in temperature. This reduction in ductility
between 20 C and 250 C was found to be 80% in previous work [9].
This has a more signicant effect for shorter lives because of the
larger plastic strain amplitude for the higher stress amplitudes.
4.2. Friction response
The COF evolution at 20 C and 250 C for various displacement
amplitudes and normal forces is shown in Fig. 4. The COFs were
obtained from the ratio of tangential to normal force measured in
the gross slip stage of the hysteresis loops. Tests conducted at
20 C had a low initial COF which increased to reach a maximum
value after 102103 cycles and then remained approximately
constant for the remaining duration of the test. For tests conducted at 250 C, the COF typically reached a maximum value early
in the test, at less than 10 cycles, before decreasing to a stabilized
value prior to reaching 102 cycles. Tests conducted in the mixed
slip regime had different contact condition evolution which is
related to this difference in COF evolution. At 20 C, a mixed slip
running condition consisted of an initial period of gross slip followed by a transition to stabilized partial slip. Conversely, a mixed
slip running condition at 250 C consisted of an initial period of
partial slip followed by a transition to stabilized gross slip. The
difference in behavior is related to the formation of a glaze oxide
on the surface in the tests conducted at elevated temperature. This
is discussed in a subsequent section.
The stabilized values of the maximum tangential force ratio
(TFR), dened as the ratio of the magnitude of the maximum tangential force during a cycle to the imposed normal force, for each
condition at 20 C and 250 C is shown in Fig. 5. The steady state
slip amplitude was determined as half of the width of the stabilized
Fig. 4. COF evolution for tests conducted at (a) 20 C and (b) 250 C.
10
Fig. 5. Steady state tangential force ratio versus steady state slip amplitude.
Fig. 7. Wear volume versus temperature including results from the literature for
fretting of annealed 304 stainless steel against itself [24].
200 m as a function of temperature is shown in Fig. 7. A signicant decrease in the wear rate was found to occur between
20 C and 250 C. This is in agreement with results for fretting of
annealed 304 stainless steel against itself [24]. This is attributed to
a transition in the oxide composition from Fe2O3 to Fe3O4, which
was identied via X-ray diffraction (XRD) in our earlier work [9].
Fretting at elevated temperature resulted in the formation of a
glaze oxide layer that resulted in the decrease in wear, partially
due to a decrease in the COF. The measured increase in total
volume (negative wear volume) is attributed to impacted iron
oxide, which has a higher volume than iron [24]. The decrease in
the wear volume was greater than the decrease in the amount of
dissipated energy at elevated temperature, thus the wear resistance of the material increased.
Cross-sections of 301 stainless steel subjected to fretting at 20 C
and 550 C are shown in Fig. 8. The specimen subjected to fretting at
20 C was etched to show the phase distribution. A layer of martensite (dark phase) was formed at the surface due to fretting.
Martensite is also present throughout the sample due to prior cold
work. The glaze oxide layer responsible for the decreased friction
and wear rate was observed on the sample subjected to fretting at
550 C. Of the fretting scars and cross-sections inspected by optical
and scanning electron microscopy, no clearly distinguishable cracks
were detected in the microstructurally-altered volumes where
fretting had occurred.
4.4. Fatigue damage due to fretting
The subsequent fatigue lives for specimens subjected to fretting
using a normal force of 255 N at 20 C and 250 C are shown in
Fig. 9. Fatigue tests were conducted on the fretting damaged
specimens at a stress amplitude of 468 MPa, which is 85% of the
room temperature fatigue strength, both based on R0.05. Fatigue
damage due to fretting was found to be more severe at 250 C than
at 20 C for displacement amplitudes below 60 m. The fatigue
damage due to fretting was found to be less severe for tests conducted at 250 C than at 20 C for displacement amplitudes of
60 m and above. The 20 C results do not seem to demonstrate
the expected benecial effects associated with high wear at the
higher displacement amplitudes as typically shown in a Vingsbo
plot [32]. This is due to the signicant wear depth for the 20 C
tests which causes a reduction in the cross-section of the specimens by as much as 20%. This causes a decrease in the subsequent
fatigue life due to the increased stresses and appears as an
increase in the level of fatigue damage, however it is an artifact
11
Fig. 8. Subsurface structure from fretting at (a) 20 C and (b) 550 C [9] (reprinted with permission from Elsevier).
5. Modeling results
Fig. 9. Uniaxial fatigue life after fretting with a 255 N normal force.
Fig. 10. Subsequent fatigue life versus the steady state maximum tangential force.
which only occurs for specimens which are thin relative to the
wear depth [16].
The subsequent fatigue lives as a function of the maximum
steady state tangential force is shown in Fig. 10. It would be
expected that if wear did not have a signicant effect on the level
of fatigue damage due to fretting then the maximum steady state
tangential force would correlate well with the level of fatigue
damage due to fretting [16]. There is not a strong correlation, thus
suggesting that the wear behavior may play an important role in
the level of fatigue damage due to fretting for these conditions and
12
Fig. 11. Frictional energy dissipation accumulation for a (a) partial slip condition and (b) gross slip condition.
Fig. 12. Frictional energy dissipation per cycle on the surface of the stationary specimen in terms of (a) the total dissipation and (b) dissipation per unit contact area.
values for the 375 N normal force. The increased contact area
resulting from the higher normal force causes a reduction in the
pressure, which is enhanced by the presence of the compliant
PTFE layer, helps explain this result.
A comparison of the model prediction for fatigue damage and
the experimental subsequent fatigue lives is shown in Fig. 14. The
subsequent fatigue results are presented as the inverse of subsequent life so that it is proportional to fatigue damage. The
prediction for the level of fatigue damage was fairly consistent for
the tests conducted at 20 C for all displacements. It was expected
that the actual fatigue damage would be more severe than the
prediction at high amplitudes because of the reduction in thickness, rather than the expected result for a thick specimen which
would have a higher damage than predicted due to the benecial
effects of wear. This suggests that the detrimental effect of thickness reduction and the benecial effects of material removal
nearly offset one another.
The actual level of fatigue damage at 250 C was relatively
higher than predicted by the model, especially at the lower displacement amplitudes. This is due to the reduction in fatigue
strength of the material at elevated temperature. At higher displacements, the predicted level of damage increases because the
COF values increase with increasing amplitude. However, the
actual level of fatigue damage did not continue to increase with
increasing displacement. The glaze oxide layer which is more
prominent at higher displacements may have provided a protective effect.
6. Discussion
The changes that occur with changing temperature can be
categorized as being either a change in material resistance or a
7. Conclusions
The inuence of temperature on the fatigue damage in 301
stainless steel sheets due to fretting against 52100 steel was
investigated. Using experimental observations and measurements
coupled with nite element modeling, the drivers for damage and
changes in the material resistance as temperature are increased
from 20 C to 250 C were elucidated:
1. The resistance of the 301 stainless steel to wear improved at the
higher temperature due to the formation of a glaze oxide layer.
The glaze oxide layer formed as a result of a change in the oxide
composition from Fe2O3 to Fe3O4.
13
Acknowledgments
This project was conducted with the nancial support of the
Victor-Reinz Division of Dana Holding Corporation.
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