1318010049

2017 5 6


ABSTRACT

Key words:

II

II 8


III


[Panax notoginseng (Burk.) F.H.Chen]

600

10 1

324

3 (
,HCH) ( ,
DDT) pentachloronitrobenzene PCNB)

78
9 20 70
80
30

456

11

1 7


12

2.
2.1

2.1.1 GC7890B 1448JSS075

TurboVap II: 1048JSS064

Biotage /Caliper TDL-40C:1648JSS032
TDL-80-2B:XQJS15045
JJ-300 XQJS936
KS501 0848JSS171 JYL-
C012
2.1.2
2015-s0417-01)
27
2.2
HP-5MS 99.99%
99.999% 0.8ml/min 250 C
300 C

70 C 1 10 C 180 C 5
5 C 220 C 100 C
280 C 8

2 7

2 7
8


2.3 2015 2341

- 1.9

2.3.1 100g/ml

1.0g/ml 1.0g/ml

10ng/ml 20ng/ml 50ng/ml 100ng/ml

1
y=321.42x+101.87, r=1 ,

2.3.1 2.0g 50ml

15ml 10ml 5.0g , 300r/min

3 7


30min, 3000r/min 2min

2.3.2 4ml 10ml

1ml
3000r/min 2min,

2.5

X= Cs
V
1000
m

x mg/kg
Cs
ng/ml
V ml
m g
3.
1
1

1 15
2 16
3 17
4 18
5 19
6 20
7 21
8 22
9 23
10 24
11 25

4 7

4 7
8


12 26
13 27
14
0.1mg/kg.

27 10
37% 6 22%

3.1
2
3 4 2 PCNB
11.071min

3.2 3 4

5 7


4.

6 7

6 7
8


2013

90%

2 GB/T 19086-

2008

7 7


1% 3

14 15

GAP

8 7

8 7
8


16 17

9 7