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DISEO EXPERIMENTAL

PISCO FACTORES REPOSO- MADURAC

MES 0

Alambique con espacio


de cabeza MES 1.5

MES 3

MES 0

Alambique sin espacio


de cabeza MES 1.5

MES 3
PISCO PURO
QUEBRANTA

MES 0

Falca con espacio de


cabeza MES 1.5

MES 3

MES 0
Falca sin espacio de
cabeza MES 1.5

MES 3

REPOSO MADURACIN - SEGUIMIENTO


Reposo a Temperatura: Ambiente
Se evala grado alcohlico y Ac. Total (expresado en mg Ac. Actico/100
ml AA)
Se evalan
1. los siguientes componentes voltiles mediante cromatografa de gases:
Acetaldeh 2. Iso-Butiraldehdo
3.
dosteres: Acetato de etilo y acetato de 4. Metanol
isoamilo
5. Furfural 6. Alcoholes superiores: n-propanol, iso-butanol, 2
7. Total congenricos 2-feniletanol
8. Acidez voltil: Ac. Actico, Ac. Propinico, Ac. I

DCA con arreglo factorial 4x3


REPOSO- MADURACIN

R1
R2
R3

R1
R2
R3

R1
R2
R3

R1
R2
R3

R1
R2
R3

R1
R2
R3

R1
R2
R3

R1
R2
R3

R1
R2
R3

R1
R2
R3
R1
R2
R3

R1
R2
R3

gases:

periores: n-propanol, iso-butanol, 2 butanol, n-butanol, amlicos y


l: Ac. Actico, Ac. Propinico, Ac. Iso-butrico y Ac. Iso-valrico
Grado
REPETICION TRATAMIENTO TIEMPO pH
alcoholico
1 ALAMBIQUE CON ESPACIO DE CABEZA MES 0 43.10 4.41
2 ALAMBIQUE CON ESPACIO DE CABEZA MES 0 43.10 4.39
3 ALAMBIQUE CON ESPACIO DE CABEZA MES 0 42.70 4.40
1 ALAMBIQUE CON ESPACIO DE CABEZA MES 1.5 43.30 4.34
2 ALAMBIQUE CON ESPACIO DE CABEZA MES 1.5 43.20 4.31
3 ALAMBIQUE CON ESPACIO DE CABEZA MES 1.5 43.20 4.32
1 ALAMBIQUE CON ESPACIO DE CABEZA MES 3 42.90 4.32
2 ALAMBIQUE CON ESPACIO DE CABEZA MES 3 43.00 4.27
3 ALAMBIQUE CON ESPACIO DE CABEZA MES 3 42.80 4.24
1 ALAMBIQUE SIN ESPACIO DE CABEZA MES 0 43.10 4.41
2 ALAMBIQUE SIN ESPACIO DE CABEZA MES 0 43.10 4.39
3 ALAMBIQUE SIN ESPACIO DE CABEZA MES 0 42.70 4.40
1 ALAMBIQUE SIN ESPACIO DE CABEZA MES 1.5 43.40 4.33
2 ALAMBIQUE SIN ESPACIO DE CABEZA MES 1.5 43.50 4.31
3 ALAMBIQUE SIN ESPACIO DE CABEZA MES 1.5 43.00 4.31
1 ALAMBIQUE SIN ESPACIO DE CABEZA MES 3 43.00 4.32
2 ALAMBIQUE SIN ESPACIO DE CABEZA MES 3 43.10 4.29
3 ALAMBIQUE SIN ESPACIO DE CABEZA MES 3 42.80 4.27
1 FALCA CON ESPACIO DE CABEZA MES 0 43.20 4.61
2 FALCA CON ESPACIO DE CABEZA MES 0 43.50 4.53
3 FALCA CON ESPACIO DE CABEZA MES 0 43.30 4.59
1 FALCA CON ESPACIO DE CABEZA MES 1.5 43.20 4.57
2 FALCA CON ESPACIO DE CABEZA MES 1.5 43.60 4.50
3 FALCA CON ESPACIO DE CABEZA MES 1.5 43.20 4.57
1 FALCA CON ESPACIO DE CABEZA MES 3 43.00 4.56
2 FALCA CON ESPACIO DE CABEZA MES 3 43.30 4.49
3 FALCA CON ESPACIO DE CABEZA MES 3 42.90 4.49
1 FALCA SIN ESPACIO DE CABEZA MES 0 43.20 4.61
2 FALCA SIN ESPACIO DE CABEZA MES 0 43.50 4.53
3 FALCA SIN ESPACIO DE CABEZA MES 0 43.30 4.59
1 FALCA SIN ESPACIO DE CABEZA MES 1.5 43.50 4.56
2 FALCA SIN ESPACIO DE CABEZA MES 1.5 43.60 4.49
3 FALCA SIN ESPACIO DE CABEZA MES 1.5 43.40 4.54
1 FALCA SIN ESPACIO DE CABEZA MES 3 43.00 4.56
2 FALCA SIN ESPACIO DE CABEZA MES 3 43.30 4.47
3 FALCA SIN ESPACIO DE CABEZA MES 3 43.20 4.47
Ac. Total (mg ac. Acetato de iso-
Acetaldehido iso-Butiraldehido Acetato de etilo Total Esteres
acetico/100ml AA) amilo
65.02 4.5276 1.5504 20.7132 0.1741 20.8873
74.28 5.9158 1.8617 21.5224 0.0000 21.5224
74.70 6.6855 2.2470 22.7851 0.0000 22.7851
52.19 5.7528 1.6799 22.4656 0.4744 22.9400
62.33 5.9987 1.9085 22.6225 0.2171 22.8395
65.18 7.0196 1.6252 21.7217 0.0000 21.7217
66.25 5.3124 1.4457 21.7287 0.0000 21.7287
65.39 6.3034 2.0112 21.8543 0.1961 22.0504
66.24 6.4013 1.6925 21.4067 0.0000 21.4067
65.02 4.5276 1.5504 20.7132 0.1741 20.8873
74.28 5.9158 1.8617 21.5224 0.0000 21.5224
74.70 6.6855 2.2470 22.7851 0.0000 22.7851
77.90 5.3092 1.6274 22.3414 0.0000 22.3414
63.43 6.0357 1.9551 22.9370 0.2115 23.1485
65.20 6.8244 2.0366 22.4889 0.0000 22.4889
65.42 5.3043 1.5872 21.9303 0.1844 22.1147
62.84 5.7879 1.7058 20.3861 0.0000 20.3861
59.53 6.3089 1.5831 20.7736 0.0000 20.7736
61.35 8.6069 1.8081 37.0352 0.6502 37.6854
61.38 5.8142 1.1984 22.0173 0.0000 22.0173
58.67 5.0129 1.6410 22.3907 0.0000 22.3907
65.46 10.5779 1.4007 42.2480 0.8156 43.0636
61.69 7.0159 1.4958 22.9286 0.0000 22.9286
66.13 6.1741 1.7591 26.4258 0.0000 26.4258
64.28 8.1795 1.1145 34.3528 0.6599 35.0127
65.60 5.3906 1.1355 19.4681 0.0000 19.4681
55.12 5.4149 1.6252 22.7801 0.3083 23.0884
61.35 8.6069 1.8081 37.0352 0.6502 37.6854
61.38 5.8142 1.1984 22.0173 0.0000 22.0173
58.67 5.0129 1.6410 22.3907 0.0000 22.3907
62.35 9.4081 2.3654 39.9886 0.8001 40.7887
64.44 6.2534 1.3949 22.6427 0.2770 22.9197
63.31 5.8306 1.6143 24.3283 0.0000 24.3283
61.94 7.8751 1.1122 33.5510 0.6699 34.2209
65.57 5.3979 0.7654 20.1318 0.2034 20.3352
70.67 5.0039 1.4685 22.4764 0.0000 22.4764
Total alcoholes
Metanol n-propanol iso-butanol n-butanol amlicos 2-fenil etanol
superiores
60.2986 22.7033 29.5843 0.9530 127.3565 5.3310 185.9282
64.7463 23.9861 31.0980 1.0237 134.5802 6.5853 197.2733
65.9127 24.4181 31.6863 1.0860 136.4124 7.1510 200.7537
64.4460 24.3297 31.6538 1.0738 135.9796 7.0171 200.0540
65.0698 23.8706 31.4016 0.9631 134.7620 7.0449 198.0422
62.4591 23.2977 30.0955 1.0919 129.3026 6.6788 190.4665
61.3121 22.8760 29.9744 0.9373 128.7718 7.0653 189.6248
62.6390 23.0887 30.2032 1.2033 130.6627 7.1881 192.3459
60.4451 22.4853 29.3404 0.9215 126.0748 7.0179 185.8399
60.2986 22.7033 29.5843 0.9530 127.3565 5.3310 185.9282
64.7463 23.9861 31.0980 1.0237 134.5802 6.5853 197.2733
65.9127 24.4181 31.6863 1.0860 136.4124 7.1510 200.7537
64.2014 24.0750 31.1130 1.0789 133.7550 5.5765 195.5983
67.1553 24.2958 32.1417 1.0116 137.9198 6.7371 202.1059
64.7436 23.8642 31.0946 1.0017 133.7902 6.8948 196.6455
61.4771 23.0585 30.3134 0.9915 129.9114 6.6557 190.9305
58.0084 21.4976 27.9586 0.8788 120.6837 6.3365 177.3552
57.4163 21.1087 27.6424 0.8672 118.4026 6.5692 174.5901
60.2370 23.5308 32.9454 0.9568 139.3118 6.3022 203.0471
63.4013 24.4819 32.2828 0.9622 137.9826 5.6264 201.3358
59.2870 22.3338 29.1574 0.9295 124.2657 5.2652 181.9516
70.5938 27.5516 38.2466 1.2061 162.4453 7.7146 237.1642
65.5530 25.2171 33.1127 1.0509 142.1135 7.0995 208.5936
68.9741 25.7718 33.6429 1.0367 144.4706 7.6179 212.5398
57.2579 21.9564 30.9832 0.9376 131.0660 6.2684 191.2116
53.8839 20.8303 27.4104 0.9171 118.1909 5.9116 173.2603
59.2088 22.3566 29.0850 0.9552 124.8166 5.7433 182.9567
60.2370 23.5308 32.9454 0.9568 139.3118 6.3022 203.0471
63.4013 24.4819 32.2828 0.9622 137.9826 5.6264 201.3358
59.2870 22.3338 29.1574 0.9295 124.2657 5.2652 181.9516
65.0866 25.1564 35.5940 1.0415 149.0927 5.7813 216.6658
63.9861 24.5840 32.0472 1.0349 137.9938 6.5665 202.2264
63.5554 23.7700 31.1057 0.9945 133.1843 6.8553 195.9098
54.3689 21.0651 29.8643 0.9086 127.3261 5.5169 184.6810
55.4743 21.3883 28.2723 0.9184 121.7663 5.8642 178.2094
58.4826 21.8790 28.7622 0.9303 123.2368 6.4584 181.2666
Furfural Ac. Actico Ac. Propionico Ac.iso-Butrico Ac.iso-Valrico Total Acidez Voltil Total congenricos

3.3294 46.1377 9.9031 0.5111 1.9583 58.5102 335.0316


3.7599 50.3731 12.1081 0.6143 2.0702 65.1657 360.2451
3.7795 50.7246 12.8444 0.5848 2.0709 66.2247 368.3882
3.3702 52.7542 14.6927 0.5027 2.0479 69.9976 368.2404
3.6948 51.4899 13.1632 0.5887 2.2825 67.5243 365.0778
3.5279 47.3067 11.7220 0.5891 2.0400 61.6578 348.4778
3.0379 47.7885 12.9898 3.2367 1.8950 65.9100 348.3715
3.2848 47.0235 12.8319 3.2141 2.0485 65.1180 353.7527
3.4512 47.1107 12.5923 0.5796 2.0064 62.2889 341.5256
3.3294 46.1377 9.9031 0.5111 1.9583 58.5102 335.0316
3.7599 50.3731 12.1081 0.6143 2.0702 65.1657 360.2451
3.7795 50.7246 12.8444 0.5848 2.0709 66.2247 368.3882
3.3411 46.2661 10.3141 0.5469 1.9371 59.0642 351.4829
3.7934 50.6126 12.3532 0.7222 2.1607 65.8487 370.0426
3.7588 51.5106 13.1016 0.5459 2.0125 67.1706 363.6683
3.1582 44.9011 11.8026 0.6135 2.0392 59.3564 343.9284
3.1432 44.2418 11.6645 2.8378 1.7953 60.5394 326.9259
3.1494 44.1810 11.8172 0.5520 1.8625 58.4127 322.2341
2.5326 46.5652 12.3345 0.5694 1.9028 61.3718 375.2890
2.8426 43.4536 10.3498 0.5210 1.9082 56.2327 352.8424
3.1226 45.8010 10.3837 0.4880 2.0233 58.6961 332.1020
3.0430 56.6617 15.3478 0.6468 2.1510 74.8073 440.6505
2.9705 52.2895 14.1131 3.4225 2.2707 72.0958 380.6533
3.3713 54.8053 14.6913 0.6232 2.1334 72.2532 391.4974
2.4610 46.6834 12.8365 2.9530 1.9169 64.3897 359.6269
2.3904 44.2308 11.7794 2.8861 1.7582 60.6544 316.1833
2.9626 39.5547 11.1844 0.5159 1.6874 52.9424 328.1991
2.5326 46.5652 12.3345 0.5694 1.9028 61.3718 375.2890
2.8426 43.4536 10.3498 0.5210 1.9082 56.2327 352.8424
3.1226 45.8010 10.3837 0.4880 2.0233 58.6961 332.1020
2.8700 47.6484 11.5548 0.5872 2.1501 61.9406 399.1251
2.8554 49.2081 12.7032 0.5369 1.9617 64.4099 364.0459
3.2145 50.5601 13.0532 0.6145 2.0080 66.2358 360.6888
2.3424 42.9104 11.1324 0.5137 1.7377 56.2942 340.8947
2.4777 44.3972 11.5726 0.5490 1.8476 58.3664 321.0262
2.8754 47.0488 12.5994 3.2132 1.9552 64.8166 336.3901

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