Professional Documents
Culture Documents
CALIBRATION BATH
USER MANUAL
HART
SCIENTIFIC
©Copyright, 1993-1998
Hart Scientific
799 East Utah Valley Drive
American Fork, Utah 84003
Telephone (801) 763-1600 • Fax (801) 763-1010
Internet: http://www.hartscientific.com
2
WARNING
To ensure the safety of operating personnel, and to avoid damage to this unit:
DO NOT operate this unit without a properly grounded, properly polarized power cord.
DO NOT connect this unit to a non-grounded, non-polarized outlet.
WARNING
EXTREMELY COLD TEMPERATURES PRESENT
in this equipment.
F R E E Z E R B U R N S AND FROSTBITE
may result if personnel fail to observe safety precautions.
WARNING
HIGH T E M P E R A T U R E S P R E S E N T
in this equipment.
FIRES AND S E V E R E B U R N S
may result if personnel fail to observe safety precautions.
WARNING
Fluids used in this bath may produce
NOXIOUS OR TOXIC F U M E S
under certain circumstances.
Consult the fluid manufacturer's M S D S (Material Safety Data Sheet).
PROPER VENTILATION A N D
S A F E T Y PRECAUTIONS MUST B E O B S E R V E D .
WARNING
CALIBRATION EQUIPMENT SHOULD ONLY BE USED BY TRAINED PERSONNEL.
TABLE OF CONTENTS
1 Introduction 9
2.3 Warranty 12
3 Safety Guidelines 13
4 Quick Start 15
4.1 Unpacking 1 5
4.2 SetUp 1 5
4.3 Power 15
4.4 Setting the Temperature 15
5 Installation 17
5.1 Bath Environment 17
5.2 "Dry-out" Period 17
5.3 Bath Preparation and Filling 17
5.4 Probe 17
5.5 Power 18
6 Bath Use 19
6.1 General 19
6.2 Comparison Calibration 19
6.3 Calibration of Multiple Probes 20
8 General Operation 25
8.1 Overview 25
8.2 Bath Fluid 25
8.2.1 Temperature Range 25
8.2.2 Viscosity 26
8.2.3 Specific Heat 26
5
8.2.4 Thermal Conductivity 26
3.2.5 Thermal Expansion 26
3.2.6 Electrical Resistivity 26
8.2.7 Fluid Lifetime 26
8.2.8 Safety 26
8.2.9 Cost 27
8.2.10 Commonly Used Fluids 27
8.2.10.1 Water 27
8.2.10.2 Ethylene Glycol 27
8.2.10.3 Methanol 27
8.2.10.4 Mineral Oil 27
8.2.10.5 Silicone Oil 27
8.3 Stirring 27
8.4 Power 27
8.5 Heater 28
8.6 Cooling 28
8.7 Temperature Controller 29
Controller Operation 31
9.1 Bath Temperature 31
9.2 Reset Cut-out 31
9.3 Temperature Set-point 31
9.3.1 Programmable Set-points 31
9.3.2 Set-point Value 33
9.3.3 Set-point Vernier 33
9.4 Temperature Scale Units 33
9.5 Secondary Menu 34
9.6 Heater Power 34
9.7 Proportional Band 34
9.8 Cut-out 35
9.9 Controller Configuration 36
9.10 Probe Parameters Menu 36
9.10.1 R0 36
9.10.2 ALPHA 36
9.11 Operating Parameters 36
9.11.1 Cut-out Reset Mode 36
9.12 Serial Interface Parameters 37
9.12.1 B A U D Rate 37
9.12.2 Sample Period 37
9.12.3 Duplex Mode 37
9.12.4 Linefeed 37
9.13 IEEE-488 Parameters Menu 38
9.13.1 I E E E - 4 8 8 Address 38
9.14 Calibration Parameters 38
9.14.1 CTO 38
9.14.2 COandCG 38
9.14.3 H and L 38
11 Calibration Procedure 45
11.1 Calibration Points 45
11.2 Measuring the Set-point Error 45
11.3 Computing R and ALPHA
0 45
11.4 Calibration Example 45
12 Charging Instructions 47
12.0.1 Bypass Adjustment 47
13 Maintenance 49
14 Trouble Shooting 51
14.1 Troubleshooting 51
14.1.1 The heater indicator LED stays red but the temperature does not increase 51
14.1.2 The controller display flashes "cut-out" and the heater does not operate 51
14.1.3 The display flashes "cut-out" and an incorrect process temperature 51
- 4.1.4 The displayed process temperature is in error and the controller remains in the
cooling or heating state at any set-point value 52
14.1.5 The controller controls or attempts to control at an inaccurate temperature 52
14.1.6 The controller shows that the output power is steady but the process
temperature is unstable 52
The controller alternately heats for a while then cools 52
'- \ The controller erratically heats then cools, control is unstable 52
14.1.9 The bath does not achieve low temperatures 52
7
14.2 Wiring Diagrams
Introduction
Introduction
T h e Hart Scientific Model 7030 is a versatile, preci- The Model 7030 consists of a constant level test well,
sion temperature calibration bath. Its operating tem- pump system, an integrated cooling and heating sys-
:e-=:_-e ange is - 3 0 to 150 C. It is capable of rapid
r C tem, precision temperature controller, temperature
heating and cooling rates, and highly stable and ac- control probe, and cabinet. The recommended heat
h a t e settings. It is designed for calibration of immer- transfer fluid will function throughout the temperature
sion temperature devices up to 13 inches long. range of the bath.
Table 1 Specifications
Accuracy ±1.0°C
Recommended Heat Transfer Silicone oil; Hart Model 5012 (Dow 200.10), 1.4 gal.
Fluid Recommended fluid will cover full temperature range of bath.
Exterior Dimensions 14" W x 35" H x 17" F-B
35.6cm x 88.9cm x 43.2cm
Shipping Weight 120 l b s / 5 7 kg
• mains voltage within ± 1 0 % of nominal charge for repair or replacement of the instrument due
to defects in material or workmanship. The warranty
• vibrations in the calibration environment
will not apply if the product has not been used accord-
should be minimized
ing to the instruction manual or has been tampered
• altitude does not effect the performance or with by the user. For service or assistance, please
safety of the unit contact the manufacturer.
Hart Scientific, Inc.
2.3 Warranty 799 East Utah Valley Drive
American Fork, UT 84003
The 7030 bath is covered by a 1 year warranty that
takes effect 10 days after the product is shipped. The Ph: 801-763-1600 . Fax:801-763-1010
manufacturer will provide parts and labor without E-Mail: support@hartscientific.com
3 Safety Guidelines
• Ooerate the bath in room temperatures be- gized for a "dry-out" period of 1 -2 hours before
tween 5-50°C (41-122°F). Allow sufficient air it can be assumed to meet all of the safety re-
circulation by leaving at least 6 inches of space quirements of the IEC 1010-1.
between the bath and nearby objects. Over-
• The bath is equipped with operator accessible
nead clearance needs to allow for safe and
fuses. If a fuse blows, it may be due to a power
easy insertion and removal of probes for cali-
surge or failure of a component. Replace the
bration.
fuse once. If the fuse blows a second time, it is
• If the bath is used at higher temperatures likely caused by failure of a component part. If
where fluid vaporization is significant, a fume this occurs, contact Hart Scientific Customer
hood should be used. Service. Always replace the fuse with one of
the same rating, voltage, and type. Never re-
• The bath is a precision instrument. Although it
place the fuse with one of a higher current rat-
has been designed for optimum durability and
ing.
trouble free operation, it must be handled with
care. The instrument should not be operated in • If a mains supply power fluctuation occurs, im-
excessively dusty or dirty environments. Do mediately turn off the bath. Power bumps from
not operate near flammable materials. brown-outs and black-outs can damage the
compressor. Wait until the power has stabi-
The bath generates extreme temperatures.
lized before re-energizing the bath.
Precautions must be taken to prevent per-
sonal injury or damage to objects. Probes may • This bath is not designed to be lifted. There-
be extremely hot or cold when removed from fore, moving the bath once it has been in-
the bath. Cautiously handle probes to prevent stalled should be kept to a minimum. Never
personal injury. Carefully place probes on a move a bath that is full of fluid. This action
heat resistant surface or rack until they are at could be extremely dangerous and could
room temperature. result in personal injury to the person mov-
ing the bath. The fluid can splash causing in-
Use only a grounded A C mains supply of the
jury or if the bath and cart tip, the fluid could
appropriate voltage to power the bath. T h e
cause damage to the surrounding area and
bath requires 17 amps at 115 V A C (±10%) 60
personal injury to personnel. If the bath must
Hz or optionally 8 amps at 230 V A C (±10%) 50
be moved, be sure to drain the fluid to prevent
Hz.
any injury. The bath is not designed to be lifted.
Before initial use, after transport, and anytime The wheels allow it to be rolled. If the unit must
the instrument has not been energized for be lifted, call Hart Scientific Customer Service.
more than 10 days, the bath needs to be ener-
4 Quick Start
CAUTION The control probe must be inserted through the lid
into the bath and plugged into the socket at the back
READ SECTION 6 ENTITLED BATH USE before
of the bath.
placing the bath in service.
Incorrect handling can damage the bath and
void the warranty. 4.3 Power
Plug the bath power cord into a mains outlet of the
This section gives a brief summary of the steps re-
proper voltage, frequency, and current capability.
auired to set up and operate the 7030 bath. This
This should be 115 V A C (±10%), 60 Hz, 17 A (230
should be used as a general overview and reference
V A C [±10%], 50 Hz, 8 A optional). Set the H E A T E R
and not as a substitute for the remainder of the man-
switch on the front panel to position L O W and turn the
ual. Please read Section 5 through 8 carefully before
bath on using the front panel P O W E R switch. The
operating the bath.
bath will turn on and begin to heat or cool to reach the
previously programmed temperature set-point. The
4.1 Unpacking front panel L E D display will indicate the actual bath
temperature.
Unpack the bath carefully and inspect it for any dam-
age that may have occurred during shipment. If there
is shipping damage, notify the carrier immediately. 4.4 Setting the Temperature
Verify that all components are present: In the following discussion a solid box around the
word SET, UP, EXIT or D O W N indicates the panel
• 7030 Bath
button while the dotted box indicates the display read-
• Controller Probe ing. Explanation of the button or display reading is to
the right of each button or display value.
• Manual
To view or set the bath temperature set-point proceed
If you are missing any item, please call customer
as follows. T h e front panel L E D display normally
service at 1-801-763-1600.
shows the actual bath temperature.
Set up of the bath requires careful unpacking a n d When S E T is pressed the display will show the set-
oiacement of the bath, filling the bath with fluid, install- point memory that is currently being used and its
ing the probe and connecting power. Consult Section value. Eight set-point memories are available.
5 for detailed instructions for proper installation of the
Dath. Be sure to place the bath in a safe, clean and
level location. SET I Access set-point selection
To fill the bath, remove the ambient guard (Figure 4). I. ?S.O ! Set-point 1, 25.0°Ccurrently
B e sure the drain is fully closed (clockwise—Figure used
3). Pour in the heat transfer fluid until it is 4 inches
from the top. Normal care should be taken to maintain Press S E T to select this memory and access the set-
: e a - ' e s s Use a funnel and immediately clean up point value.
spills. Only clean, unpolluted oil should be used.
, ' , - e - : - e ;=:- s * ed to the specific level, replace the
:
SET Access set-point value
ambient guard.
! C BS 0 0 i Current value of set-point 1,
' * • • • : 25.00°C
• \
Press U P or D O W N to change the set-point value. ^4.13 [ I Bath temperature display
Increment display The bath will heat or cool until it reaches the new set-
point temperature. Set the heater switch to position
• • \
I C 3 0.00 i New set-point value HIGH to allow the bath to more quickly reach a higher
temperature. The high power setting may be neces-
Press S E T to accept the new value and display the sary to control at high temperatures.
vernier value. The bath begins heating or cooling to When setting the set-point temperature be careful not
the new set-point. to exceed the temperature limit of the bath fluid. The
over-temperature cut-out should be correctly set for
added safety. S e e Section 9.8.
Store new set-point, access vernier
\ If operating the bath below 55°C set the C O O L I N G
0.0 0 0 0 0 ! Current vernier value power switch to O N . The cooling temperature may re-
quire adjustment to provide the proper amount of cool-
Press EXIT and the bath temperature will be dis- ing. See Section 8.6.
played again.
To obtain optimum control stability adjust the propor-
tional band as discussed in Section 9.7.
Return to the temperature display
5 Installation
CAUTION 5.3 Bath Preparation and
READ SECTION 6 ENTITLED BATH USE before Filling
placing the bath in service.
The Model 7030 Bath is not provided with a fluid. Vari-
Incorrect handling can damage the bath and
ous fluids are available from Hart Scientific and other
void the warranty.
sources. D O W 200.10 silicone oil is the recom-
mended fluid. This fluid is usable throughout the
This bath is not designed to be lifted. Therefore, mov- bath's temperature range.
ing the bath once it has been installed should be kept
Fluids are discussed in detail in Section 8.2.
to a minimum.
To fill the bath, remove the ambient guard (Figure 4).
Never move a bath that is full of fluid. This action
Be sure the drain is fully closed (clockwise—Figure
could be extremely dangerous and could result
3). Pour in the heat transfer fluid until it is four inches
in personal injury to the person moving the bath.
from the top (Figure 4). Care should be taken to main-
If the bath must be moved, be sure to drain the fluid to tain cleanliness. Use a funnel and immediately clean
prevent any injury. The side of the bath with the up spills. Only clean, unpolluted oil should be used in
compressor is heavier than the tank side. To safely the bath. When the bath is filled to the specific level,
move the bath, two people are required. replace the ambient guard.
5.5 Power Be sure the stirring motor power cord is plugged into
the S T I R R E R socket at the back of the bath.
With the bath power switch off, plug the bath into an
A C mains outlet of the appropriate voltage, frequency,
and current capacity. Normally this will be 115 V A C
(±10%), 60 Hz, 17 A (230 V A C [±10%], 50 Hz, 8 A op-
tional).
6 Bath Use
READ B E F O R E PLACING THE BATH IN SERVICE 6.2 Comparison Calibration
The information in this section is for general informa- Comparison calibration involves testing a probe (unit
tion only. It is not designed to be the basis for calibra- under test, UUT) against a reference probe. After in-
tion laboratory procedures. Each laboratory will need serting the probes to be calibrated into the bath, allow
to write their own specific procedures. sufficient time for the probes to settle and the tem-
perature of the bath to stabilize.
6.3 Calibration of Multiple the probes. Using the reference probe as the guide,
be sure that the temperature has stabilized before
Probes starting the calibration.
Fully loading the bath with probes increases the time
required for the temperature to stabilize after inserting