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Received 14 July 2003; received in revised form 15 February 2005; accepted 11 April 2005
Abstract
Most of cold rolled deep drawability steel sheets finds application in areas where forming is critical. Deep drawing sheet steel requires
good mechanical properties and microstructures, as well as sufficient anti-aging characteristics. Therefore, deep drawing steels are produced
by controlling these metallurgical factors and optimizing steelmaking, hot rolling, cold rolling and annealing processes.
This paper explains the effect the microstructure and mechanical properties of hot rolling conditions on continuously annealed sheet
properties in certain chemical composition. Experiments have been conducted to investigate the effect of hot rolling conditions. Consequently,
it became clear that hot rolling conditions play an important role in producing continuous annealed deep drawing quality steels.
© 2005 Elsevier B.V. All rights reserved.
0924-0136/$ – see front matter © 2005 Elsevier B.V. All rights reserved.
doi:10.1016/j.jmatprotec.2005.04.097
18 G. Erdem, Y. Taptik / Journal of Materials Processing Technology 170 (2005) 17–23
Fig. 2. Effects of finishing and coiling temperatures on the microstructure of the hot band sheet steel.
were analyzed for each trial. The microstructures shown in that ferrite ASTM No. decreases with increasing finishing and
Fig. 2 are the representative microstructures of trials. As coiling temperatures. In Fig. 3, Carbide Index No.1 decreases
expected [5,6], the change in the grain size is dependent on with increasing finishing and coiling temperatures. Carbide
finishing temperature and, on the other hand, the morphology index number is similar to ferrite ASTM number. Carbide
of cementite is strongly dependent on coiling temperature. size increases with decreasing index number.
The ferrite grain size decreases with decreasing finishing According to 700 ◦ C annealing temperature in CAL pro-
temperature and mixed grain structure is obtained when hot cess, hot band microstructure with high coiling temperature
rolling was conducted at a temperature below Ar3 [7,8]. and finishing temperature (Trial IV, B) resulted in the final
Trial I has a relatively coarse grain structure and resulted annealed microstructure shown in Fig. 5. After hot rolling
in mixed grain sizes. When the hot bands were rolled both surfaces of steels were inspected in recoiling line and
at 930 ◦ C (finishing temperature), large sizes on ferrite then they were pickled in HCl acid (18%, 65 ◦ C, 240 m/min)
grain were observed. The flaky cementite particles were in order to remove the surface oxides. Because of the high
obtained along grain boundaries with increasing coiling coiling temperature for these steels, tension leveller was used
temperature. On the other hand, when hot bands were coiled before the pickling to ensure full-scale removal. The coils
at 730 ◦ C, very coarse cementite particles were observed. were rolled to a final gauge of 0.80 mm on four-stand tandem
Trial IV (B) has coarse cementite particles and coarse grain cold rolling mill and the amount of deformation in cold rolling
structure due to high finishing and coiling temperatures. process is 71%. It can be seen that sufficient recrystalliza-
This diagram also shows the relation between change in tion is completed in case of these process conditions. Finally,
microstructure of hot rolled sheet steel and the rolling process the full hard materials were annealed in continuous anneal-
parameters. ing line after electrolytic cleaning process. Fig. 1 shows the
Effects of finishing and coiling temperatures for the fer- schematic illustration of experimental procedure.
rite grain and carbide size are shown in Figs. 3 and 4. For
plotting the grain size and carbide index, a mean grain size
and carbide index were calculated. It can be seen in Fig. 2 1 It is based on NKK CAL Process Knowhow Book, January 1995.
20 G. Erdem, Y. Taptik / Journal of Materials Processing Technology 170 (2005) 17–23
Fig. 5. Annealed microstructure of hot band with high coiling and finishing temperature: (a) ferrite grain size (100×) and (b) carbide size (500×).
G. Erdem, Y. Taptik / Journal of Materials Processing Technology 170 (2005) 17–23 21
Fig. 6. The effect of finishing temperature for (a) yield strength, (b) tensile strength and (c) elongation. The effect of coiling temperature for (d) yield strength,
(e) tensile strength and (f) elongation.
are severe at the head and tail end of the coil because of heat annealing. The coarsening of carbide was found to contribute
radiation. This excessive cooling leads to undesirable carbide greatly to the grain growth by weakening the dragging effect
morphologies and finely dispersed aluminium nitride precip- of the precipitates.
itation which degrades the formability of the final product Although the middle of the coil has of a lower tempera-
at these positions [9]. By applying high finishing and coil- ture than the head or tail of the coil, it is possible to uniform
ing temperature with no water, the coarsening of carbide and properties when the coil was cooled because heat losses are
the growth of ferrite grain were achieved. The large grain severe at the head and tail of coil. The mechanical tests were
size of hot band aids the grain growth after cold rolling and performed after the coil was cooled. The temperature in Fig. 6
22 G. Erdem, Y. Taptik / Journal of Materials Processing Technology 170 (2005) 17–23
Fig. 7. The change of yield strength (a and d), tensile strength (b and e) and elongation, (c and f) depending on finishing and coiling temperature for whole coil
length. (O) Middle of coil, (B) head of coil and (S) tail of coil.
correspond to the average values is used for obtaining Fig. 7. low carbon Al-killed steel sheets which are finished and
Therefore, uniform mechanical properties for the whole coil coiled at high temperature in hot rolling lie within range of
length were observed as seen in Fig. 7. Besides, the tempera- 210–230 N/mm2 for yield strength, 310–330 N/mm2 for ten-
ture difference between the edges and center was reduced to sile strength, 45–46% for elongation and 1.4–1.6 for r mean
10–20 ◦ C from 40 to 50 ◦ C with coil box. value at 700 ◦ C constant heating temperature. Therefore,
Although mechanical properties of continuously annealed mechanical properties with low yield and tensile strength, and
products are largely affected by a heating temperature, the high r mean value and elongation for continuously annealed
mechanical properties of continuously annealed cold rolled steel are obtained.
G. Erdem, Y. Taptik / Journal of Materials Processing Technology 170 (2005) 17–23 23
4. Conclusion References
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