Professional Documents
Culture Documents
Experiment Instructions
Please read and follow the safety regulations before the first installation!
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Table of Contents
1 Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
2 Description . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
3 Safety . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
4 Theory . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
5 Experiments . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16
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6 Appendix . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23
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1 Introduction 1
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1 Introduction 2
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1
10
1 Evaporator 11
2 Column
3 Hand valve and flowmeter 12
for cooling water
4 Differential pressure gauge
5 Condenser
6 Reflux divider
7 Vacuum gauge
8 Vacuum pump
9 Top product container
10 Control cabinet with 13
system diagram
11 Water outlet
12 Hand valve for regulating
the vacuum pump
13 Water inlet
2 Description 3
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2 Description 4
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2 Description 5
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2 Description 6
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· Heater controls:
- ON/OFF switch (18)
- The indicator lamp (20) lights up when
the heater is on.
- „Low Level“ warning lamp (21)
The evaporator tank is fitted with a
level switch. If the evaporator does not
contain at least the minimum amount
All Rights Reserved G.U.N.T. Gerätebau GmbH, Barsbüttel, Germany 07/2014
1 Actual value
2 Setting value · Setting temperature T13 on the controller
3 Operating buttons
4 „Manual operation“ indicator lamp When it is switched on the controller is in normal
5 Unit
display mode.
Operating the „EXIT“ button toggles between the
Fig. 2.6 Temperature Controller controller’s automatic and manual modes.
Exit button
The indicator LED (5) lights when the
controller is in manual mode.
Arrow buttons In this mode the control ratio of the controller can
be adjusted directly using the two „arrow keys“.
PGM button
2 Description 7
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If the indicator LED (5) does not light up, the con-
troller is in automatic mode.
1
5
2
In this mode the required setpoint can be adjusted
4
using the two „arrow keys“.
3
REMARK: The controller only updates the new
setpoint after approx. 2 seconds!
All Rights Reserved G.U.N.T. Gerätebau GmbH, Barsbüttel, Germany 07/2014
1 Actual value
2 Setting value
3 Operating buttons
5 „Manual operation“ indicator lamp
6 Unit
2 Description 8
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the evaporator
· Fill the evaporator with a suitable test liquid.
Make sure that the minimum liquid level is
reached.
Warning! The heater will not activate if the
evaporator is underfilled.
Observe the „Low Level“ warning lamp
min. 2 litres to ensure that the heater activates
min. 5 litres to allow a meaningful experiment without
the heater cutting out prematurely
· Open the water supply and provide a suitable
runoff for the cooling water
· Connect the unit to the mains electricity supply
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3 Safety
DANGER of burns!
The evaporator, column and pipes get hot during
experiments due to the nature of the process.
Do not touch system components when in operation.
When emptying the hot bottom product be sure to
drain it into suitable heat-resistant containers and
wear protective gloves at all times.
3 Safety 10
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WARNING!
The choice of chemicals for distillation and rectifi-
cation is limited by the resistance of the materials
used in the construction of the equipment. Use
only those chemicals which do not attack
- VITON,
-
All Rights Reserved G.U.N.T. Gerätebau GmbH, Barsbüttel, Germany 07/2014
PVDF,
- PTFE and
- stainless steel 1.4305!
WARNING!
The electrical components and the control cabinet
must be protected from moisture and humidity and
especially from aggressive media.
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4 Theory
1
has the fraction x1, is brought to the boil, it will give
0.8 off steam. Substance A has a different fraction y1
0.6
in the steam than it does in the liquid mixture AB.
0.52
If we enter the corresponding values for the vapour
0.4
in steam
4 Theory 12
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4.1.1 Distillation
4 Theory 13
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4.1.2 Rectification
Bottom
The result is an exchange of material and heat be-
Bottom product
tween the rising vapours and the falling liquid.
The high-boiling component condenses first from
the rising vapours. The resulting condensation
heat causes more low-boiling component to evap-
Fig. 4.4 Rectification, schematic orate in turn. The result is that the liquid flowing
back to the bottom of the column is enriched with
high-boiling components. The vapours at the top
4 Theory 14
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Condenser
Column head
Reflux
Top product
Evaporator (low-boiling)
Bottom product
(high-boiling)
Aftercooler
4 Theory 15
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4 Theory 16
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5 Experiments
5.1.1 Preparation
5 Experiments 17
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6 Appendix
6 Appendix 23
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6.2 Tables
6 Appendix 24
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6 Appendix 25
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Test mixture
All Rights Reserved G.U.N.T. Gerätebau GmbH, Barsbüttel, Germany 07/2014
Concentration %
Heating power %
Reflux ratio %
Distillate concentration %
6 Appendix 26
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6 Appendix 27