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OBJECTIVE
To determine the optimum alum dose for turbidity removal from water using jar
test.
INTRODUCTION
Apparatus
Beakers, plastic pipette, burette, retort stand and clamp, filter funnel, automated
mixer and turbidity measurement machine.
Materials
Kaolin (clay) suspension, 2.0 g/l alum solution, sulphuric acid and sodium hydroxide
solution
EXPERIMENTAL PROCEDURE
Note: Prior to the jar test procedure, each 500 ml sample must be corrected to the
required pH using H2SO4 or NaOH. In order to obtain the correct amount of
acid or alkali for each sample, a separate titration must be carried out for
each alum dose- pH combination. The pH and turbidity of the sample before
treatment must be determined.
M 1V 1 = M 2V 2
Six 1 litre beakers were filled with 500 ml of the given kaolin (clay) suspension (SS
about 50 mg/l). A burette was filled with 50 ml alum solution of concentration 2.0 g/l.
The certain amount of H2SO4 or NaOH that would yield a final pH of 7 – 7.1 was
added to the beakers. The alum solution corresponding to doses of 0 (control), 5, 10,
20, 40 and 60 mg/l were added to the beakers. The samples were then mixed at high
speed (80 rpm) for 1 minute. The mixing speed was reduced to 30 rpm and the
mixing was continued for 15 minutes. The stirrer was stopped and the flocs was
allowed to settle for 20 minutes. The turbidity of the supernatant was determined.
Graph of turbidity versus alum dose was plotted.