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Determination of the sphericity of granular


food materials

Article in Journal of Food Engineering · June 2005


DOI: 10.1016/j.jfoodeng.2004.06.014

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Mustafa Bayram
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Journal of Food Engineering 68 (2005) 385–390
www.elsevier.com/locate/jfoodeng

Determination of the sphericity of granular food materials


Mustafa Bayram *

Faculty of Engineering, Department of Food Engineering, University of Gaziantep, 27310-Gaziantep, Turkey

Received 2 February 2004; accepted 21 June 2004

Abstract

In the present study, a new dimensional method and equation were developed to calculate the sprecity (/s) of certain shapes
(sphere, cubes, rectangular solid and cylinder) and some granular food materials (wheat, bean, intact red lentil, chickpea and coarse
bulgur).
It was found that increase in /s value caused deviation from the absolute sprecity (/s = 0). Sprecity was constant and independ-
ent of size for certain shapes at 0, 0.00271 and 0.00155 for sphere, cube and cylinder (length = diameter), respectively. Also, the
sphericities of wheat, bean, intact red lentil, chickpea and coarse bulgur were determined as 0.01038, 0.00743, 0.00641, 0.00240
and 0.01489, respectively (P < 0.05). As expected, chickpea had the best and coarse bulgur had the worst sprecity due to their specific
shapes.
Ó 2004 Elsevier Ltd. All rights reserved.

Keywords: Sprecity; Wheat; Bean; Lentil; Chickpea; Bulgur

1. Introduction The equivalent diameter is sometimes defined as the


diameter of a sphere of equal volume. For granular
The shape of an individual particle is conveniently ex- materials, however, it is difficult to determine exact vol-
pressed in terms of sprecity /s, which is independent of ume and surface area of a particle to obtain the equiva-
particle size. For a spherical particle of diameter Dp, lent diameter, and Dp is usually taken to be the nominal
/s = 1; for a nonspherical particle, the sprecity is defined size based on screen analyses, visual length measure-
by the relation in Eq. (1). For a cylinder where the diam- ments or microscopic examination. The surface area
eter equals to length, /s is calculated to be 0.874 and for may be found from adsorption measurements or from
a cube, /s is calculated as 0.806 (McCabe, Smith, & the pressure drop in a bed of particles and Eq. (1) used
Harriott, 1985, 2001; Geankoplis, 1983; Perry, 1984; to calculate /s. For many crushed materials /s is be-
Holdich, 2002). tween 0.6 and 0.8, but for particles rounded by abrasion
/s  6V p =Dp S p ð1Þ /s may be as high as 0.95 (Geankoplis, 1983; Perry,
1984; McCabe et al., 1985, 2001; Holdich, 2002).
where /s, Vp, Dp and Sp are sprecity, volume of one par- As explained above, the main problem in having
ticle, equivalent or nominal diameter of particle and sur- irregular shape granular materials is the calculation
face area of one particle, respectively. of the exact volume and surface area. High-level mathe-
matical formulas should be used to calculate the
*
Corresponding author. Tel: +90 342 360 1200x2303; fax: +90 342
volume and surface area. Additionally, instead of a cal-
360 11 05. culation method, advanced experimental methods can
E-mail address: mbayram@gantep.edu.tr be used (Geankoplis, 1983; McCabe et al., 1985, 2001).

0260-8774/$ - see front matter Ó 2004 Elsevier Ltd. All rights reserved.
doi:10.1016/j.jfoodeng.2004.06.014
386 M. Bayram / Journal of Food Engineering 68 (2005) 385–390

Therefore, the determination of the solid mechanical 2.3. Drawing of shapes


and handling properties of any granular food material
using sprecity is very difficult and also not very practical. All drawings on a 1:1 scale were made using Auto-
The present study deals with (1) the derivation of a CAD 2000 Engineering Drawing Software (AutoDesk,
sprecity equation, (2) the determination of the sprecity USA).
values of certain shapes i.e. sphere, cubes, rectangular
solids and cylinders having different dimensions, (3)
2.4. Calculation of sprecity
the application of the sprecity equation to some granu-
lar food products.
Sprecity was calculated using Microsoft Office Excel
Software (Microsoft, USA).

2. Materials and methods


2.5. Statistical analysis
2.1. Materials
An ANOVA analysis was performed for average
Wheat (Triticum durum, Fırat-98, harvesting year diameters and sprecity value to determine significant dif-
2003), bean (Tokat species, harvesting year 2003), red ferences (P < 0.05). DuncanÕs multiple range tests were
lentil (Kızıltepe species, harvesting year 2003), chickpea
(Elbistan species, harvesting year 2003) and coarse bul-
gur (produced from Triticum durum ‘‘Fırat-98’’, harvest-
ing year of wheat and processing year for bulgur 2003)
were obtained from Arbel Legumes and Cereals Co.
(Mersin, Turkey). The population of each sample was
10.

2.2. Measurement of dimensions

Dimensions were measured using a micrometer


Fig. 1. Illustration of measuring sides for certain shapes. (For sphere:
(Mitutoyo, No: 505-633, Japan) in millimetre. Measure-
D is diameter. For cube and rectangular solid: D1, D2, D3 are edges;
ments were carried out through crossing the origin of D4, D5, D6, D7 are diagonals; D8, D9, D10, D11, D12, D13 are cross-sides.
the materials by determining orifin with measuring the For cylinder: D1 is diameter; D2 is length; D3, D4, D5, D6, D7, D8, D9,
distance of a line through the origin. D10 are diagonals.)

Table 1
Dimensional values and formulas for certain shapes
Shapes Dimensional values and formulas N /s
Sphere D as a given 1 0 (size independent and constant)

Cube D1 = D2 = D3 as given 13 0.00271 (size independent and constant)


D4 ¼ D5 ¼ D6 ¼ D7 ¼ ð3D21 Þ1=2
D8 ¼ D9 ¼ D10 ¼ D11 ¼ D12 ¼ D13 ¼ ð2D21 Þ1=2

Rectangular solid D1,D2,D3 as given 13 Size dependent and changes with dimensions
D4 ¼ D5 ¼ D6 ¼ D7 ¼ ðD21 þ D22 þ D23 Þ1=2
D8 ¼ D9 ¼ ðD21 þ D23 Þ1=2
D10 ¼ D11 ¼ ðD22 þ D23 Þ1=2
D12 ¼ D13 ¼ ðD21 þ D22 Þ1=2

Cylinder D1,D2 as given 10 Size dependent and changes with dimensions


D4 ¼ D5 ¼ D6 ¼ D7 ¼ D8 ¼ D9 ¼ D10 ¼ ðD21 þ D22 Þ1=2

Cylinder (for length = diameter) D1 = D2 as given 10 0.00155 (size independent and constant)
D4 ¼ D5 ¼ D6 ¼ D7 ¼ D8 ¼ D9 ¼ D10 ¼ ð2D21 Þ1=2
For sphere: D is diameter. For cube and rectangular solid: D1, D2, D3 are edges; D4, D5, D6, D7 are diagonals; D8, D9, D10, D11, D12, D13 are cross-
sides. For cylinder: D1 is diameter; D2 is length; D3, D4, D5, D6, D7, D8, D9, D10 are diagonals. N shows the number of measurement, i.e. the number
of measured diameters.
M. Bayram / Journal of Food Engineering 68 (2005) 385–390 387

Table 2
Illustration of actual and equivalent shapes, and Sphericity values for certain shapes
Shapes Actual shape Equivalent spherical shape Dimensions N D /s
Sphere D=2 1 2 0
D=5 5 0
D = 111 111 0

Cube D1 = D2 = D3 = 2 2.833 0.00271


D4 = D5 = D6 = D7 = 3.464
D8 = D9 = D10 =
D11 = D12 = D13 = 2.828

D1 = D2 = D3 = 10 13 14.164 0.00271
D4 = D5 = D6 = D7 = 17.321
D8 = D9 = D10 = D11 =
D12 = D13 = 14.142

D1 = D2 = D3 = 7 9.915 0.00271
D4 = D5 = D6 = D7 = 12.124
D8 = D9 = D10 = D11 = D12 =
D13 = 9.899

Rectangular solid D1 = 3, D2 = 2, D3 = 1 2.998 0.00603


D4 = D5 = D6 = D7 = 3.742
D8 = D9 = 3.162
D10 = D11 = 2.236
D12 = D13 = 3.606

D1 = 8, D2 = 5, D3 = 4 13 8.273 0.00477
D4 = D5 = D6 = D7 = 10.247
D8 = D9 = 8.944
D10 = D11 = 6.403
D12 = D13 = 9.434

D1 = 5, D2 = 5, D3 = 2 5.929 0.00488
D4 = D5 = D6 = D7 = 7.349
D8 = D9 = 5.385
D10 = D11 = 5.385
D12 = D13 = 7.071

Cylinder D1 = 1, D2 = 2 2.089 0.00313


D4 = D5 = D6 = D7 =
D8 = D9 = D10 = 2.236

D1 = 3, D2 = 7 10 7.093 0.00377
D4 = D5 = D6 = D7 =
D8 = D9 = D10 = 7.615

D1 = 2, D2 = 11 10.244 0.00720
D4 = D5 = D6 = D7 =
D8 = D9 = D10 = 11.18

Cylinder (for length = diameter) D1 = D2 = 1 1.331 0.00155


D4 = D5 = D6 = D7 =
D8 = D9 = D10 = 1.414

D1 = D2 = 2 10 2.663 0.00155
D4 = D5 = D6 = D7 =
D8 = D9 = D10 = 2.828

D1 = D2 = 7 9.320 0.00155
D4 = D5 = D6 = D7 =
D8 = D9 = D10 = 9.899
For sphere: D is diameter. For cube and rectangular solid: D1, D2, D3 are edges; D4, D5, D6, D7 are diagonals; D8, D9, D10, D11, D12, D13 are cross-
sides. For cylinder: D1 is diameter; D2 is length; D3, D4, D5, D6, D7, D8, D9, D10 are diagonals. N shows the number of measurement, i.e. the number
of measured diameters.
388 M. Bayram / Journal of Food Engineering 68 (2005) 385–390

carried out to determine homogeneous groups (SPSS 8.0 Front views D1


D1 D1
Statistical Software, SPSS Inc., USA). D3 D2 D3 D4

crease or joint joint


3. Results and discussion
D4 Top views D3
3.1. Derivation of sprecity equation D6 D5

D7 D2 D2
In the present model, equivalent or nominal diameter
for irregular shape materials was accepted as the average
dimension to obtain an equivalent sphere. Differences (for wheat and bean) (for intact red lentil) (for chickpea)
between average diameter and actual measured dimen- Fig. 2. Illustration of measuring sides for wheat, bean, lentil and
sions were determined with the sum of square of differ- chickpea (D1. . .7 show different dimensions for each material where
ences. When this difference is divided by the square of notated in shapes).
product of the average diameter and number of meas-
urements, it gives a fraction for the approach of the
slope to an equivalent sphere i.e. sprecity. Therefore, It should be noted that, due to its similarity to a
Eq. (2) was derived as sphere i.e. /s = 0, a cylinder (/s = 0.00155) with equal
RðDi  DÞ
2 diameter and length was more spherical than a cube
/s ¼ 2
ð2Þ (/s = 0.00271) (Tables 1 and 2). It was also correlated
ðDN Þ
with the literature reports for a cube and cylinder i.e.
where /s is the sprecity value, Di is any measured dimen- sprecity is 1, 0.874 and 0.804 for sphere, cylinder and
sion, D is average dimension or equivalent diameter and cube, respectively (Geankoplis, 1983; Perry, 1984; McC-
N is the number of measurements. Increase in the N in- abe et al., 1985, 2001; Holdich, 2002).
creases the accuracy. Eq. (2) was also used to determine the sphericities of
As a note, in Eq. (1), /s for a sphere was 1, while in some granular food materials i.e. wheat, bean, intact red
Eq. (2), /s for a sphere was 0. In other word, an increase lentil, chickpea and coarse bulgur. The goal of the selec-
in /s value using Eq. (2) shows the deviation from the tion of these five materials was important due to their
sprecity i.e. the opposite to Eq. (1). different shapes, these being a long ellipsoid, a wide
The applicability and proof of Eq. (2) was carried out ellipsoid, a disc, a sphere and an irregular shape, respec-
using the following shapes: sphere, cube, rectangular tively. The experiments were made on 10 granules for
solid and cylinder. The measured dimensions of certain each material and their averages were determined, and
shapes are illustrated in Fig. 1 and Table 1. As examples, then statistically analysed (P < 0.05, Fig. 2, Tables 3
dimensions were given and their equivalent sphere and 4).
shapes are shown in Table 2. It should be noted that, As expected, due to the spherical shape of chickpea, it
for a sphere that had any dimension or diameter, its had the best /s-value (0.00240, the nearest value to zero
sprecity value was always zero and it was size independ- or sphere) (P < 0.05, Table 4). Then, intact red lentil had
ent (Eq. (2), Tables 1 and 2). Therefore, a sphere is a the second best spherical shape (/s = 0.00641, P < 0.05,
perfect shape for sprecity. Table 3).
A cube had a constant sprecity value of 0.00271 and it The shapes of the wheat and bean kernels are ellip-
was also size independent, similar to the sphere (Eq. (2), soid. But, former is long in contrast to the latter one.
Tables 1 and 2). Its equivalent sphere was illustrated in Due to its length, the sprecity of wheat (/s = 0.01038)
Table 2 as an example. Rectangular solids have different was lower than that of bean (/s = 0.00743, P < 0.05, Ta-
edge dimensions; therefore their sprecity depends on ble 3).
their dimensions ratio. For a cylinder, where the diame- Bulgur is an irregular shaped granular food product
ter equals to length, sprecity was calculated as 0.00155. and it is obtained by cooking, drying, dehulling and
It was constant for any cylinder of equal diameter and grinding operations (Bayram, 2000; Bayram & Öner,
length. In other words, the sprecity of a cylinder (diam- 2002; Bayram, Kaya, & Öner, 2004a, 2004b). The grind-
eter = length) is size independent and constant (0.00155) ing operation causes bulgur to have an irregular shape.
similar to a sphere and cube. If the diameter and length Dimensions for the bulgur granules were measured
of cylinder was not equal to each other, the sprecity was along different axes (12 dimensions were measured). Its
changed based on dimensions (Table 2) similar to a rec- sprecity was the lowest one, as expected, i.e.
tangular solid. /s = 0.01489 (Table 4, P < 0.05).
M. Bayram / Journal of Food Engineering 68 (2005) 385–390 389

Table 3
Results for dimensions and sphericity values for wheat, bean and red lentil
Granular Parameters Samples
food
1 2 3 4 5 6 7 8 9 10
products
Wheat Dimensions D1 3.65 3.60 3.45 3.50 3.25 3.40 3.50 3.10 3.10 3.05
D2 = D3 5.30 5.40 5.20 5.40 5.35 5.10 5.60 5.45 5.30 5.30
D4 3.15 2.95 3.15 3.45 2.80 3.05 3.10 3.55 2.70 2.60
D5 = D6 5.05 4.80 5.10 5.00 5.05 4.80 4.60 4.60 4.30 4.85
D7 7.35 7.40 7.50 7.00 7.20 7.00 7.40 7.50 6.95 7.25

N 7
D 4.979 4.907 4.957 4.964 4.864 4.750 4.914 4.893 4.564 4.743
/s 0.00902 0.01039 0.01010 0.00742 0.01110 0.00907 0.01065 0. 01075 0.01228 0.01305

Average D for 10 4.854a


samples
Average /s for 10 0.01038a
samples

Bean Dimensions D1 5.80 4.90 5.50 4.85 5.50 5.45 5.05 5.50 5.45 5.40
D2 = D3 9.20 9.70 8.95 8.70 9.15 8.50 8.50 8.45 9.50 8.40
D4 7.40 7.55 6.85 7.60 7.40 8.00 7.75 7.70 7.55 7.45
D5 = D6 10.40 10.25 9.05 11.15 9.80 10.00 10.00 10.15 10.60 9.65
D7 12.80 12.90 11.65 12.6 12.30 12.20 12.10 12.50 12.45 11.75

N 7
D 9.314 9.321 8.571 9.250 9.014 8.950 8.843 8.986 9.379 8.671
/s 0.00719 0.00881 0.00628 0.00981 0.00679 0.00671 0.00760 0. 00744 0.00724 0.00644

Average D for 10 9.030b


samples
Average /s for 10 0.00743b
samples

Intact red lentil Dimensions D1 2.85 2.70 2.75 2.60 2.60 2.45 2.50 2.65 2.35 2.50
D2 4.30 4.45 4.25 4.35 4.15 3.75 3.85 4.10 3.90 3.90
D3 = D4 3.60 3.65 3.55 3.55 3.40 3.15 3.05 3.20 3.20 3.05

N 4
D 3.588 3.613 3.525 3.513 3.388 3.125 3.050 3.288 3.163 3.125
/s 0.00511 0.00736 0.00567 0.00779 0.00655 0.00542 0.00598 0.00626 0.00754 0.00642

Average D for 10 3.344c


samples
Average /s for 10 0.00641b
samples
Different superscript letters indicate statistically significant differences exist at a = 0.05 for average diameter and sphericity values for 10 samples.
Means for groups in homogeneous subsets are displayed. Based on Type III Sum of Squares. DuncanTest was applied. N shows the number of
measurement i.e. the number of measured diameters. D1. . .12 show the dimensions for each material where noted in Fig. 2.

4. Conclusions also be measured using image analysis or microscopic


methods for very fine granular products.
Due to important problems in available measuring According to the present method and Eq. (2), the
and calculation methods to determine exact volume sprecity values of certain shapes were constant and inde-
and surface area for granular materials, use of Eq. (1) pendent to size at 0, 0.00271 and 0.00155 for sphere,
is very difficult. Therefore, Eq. (2) in the present study cube and cylinder (length = diameter), respectively. As
can be used easily for solid mechanics and handling expected, the order of sprecity of granular food mate-
operations to determine the sprecity of granular materi- rials were chickpea > intact red lentil > bean > wheat >
als instead of Eq. (1). Measurements of dimensions can coarse bulgur.
390 M. Bayram / Journal of Food Engineering 68 (2005) 385–390

Table 4
Results for dimensions and sphericity values for chickpea and coarse bulgur
Granular Parameters Samples
food
1 2 3 4 5 6 7 8 9 10
products
Chickpea Dimensions D1 7.85 7.85 7.65 7.55 7.95 8.05 7.65 8.55 8.20 8.30
D2 8.80 8.60 8.50 8.70 8.60 9.40 9.90 10.10 10.15 10.15
D3 7.90 7.60 8.20 7.45 8.00 7.75 7.75 8.00 8.15 7.70

N 3
D 8.183 8.017 8.117 7.900 8.183 8.400 8.433 8.883 8.833 8.717
/s 0.00095 0.00094 0.00063 0.00172 0.00043 0.00243 0.00505 0.00334 0.00370 0.00477

Average D for 10 8.367d


samples
Average /s for 10 0.00240c
samples

Coarse bulgur Dimensions D1 4.70 5.50 4.80 5.55 5.65 4.10 4.00 4.75 4.50 5.05
D2 2.50 2.65 2.80 2.80 2.90 2.80 2.40 2.40 2.65 2.85
D3 1.45 1.85 1.60 1.80 1.40 1.20 1.40 1.40 1.55 1.30
D4 4.15 5.25 4.65 5.30 5.45 3.90 3.85 4.60 4.30 5.00
D5 2.60 5.10 4.45 5.15 5.30 3.80 3.60 4.50 4.05 4.85
D6 2.25 4.90 4.10 5.30 5.10 3.45 3.45 4.25 3.85 4.35
D7 2.15 1.95 2.90 2.85 3.35 2.95 2.65 2.65 2.75 3.55
D8 2.35 2.10 3.15 2.95 3.65 3.05 2.85 2.75 2.95 3.05
D9 2.40 1.90 3.20 3.10 3.50 3.40 3.00 2.90 3.05 3.45
D10 3.30 2.85 1.65 1.90 1.55 1.30 1.55 1.55 1.65 1.45
D11 3.20 2.95 1.80 2.10 1.90 1.55 1.85 1.65 1.85 1.75
D12 1.70 3.10 2.15 2.05 2.15 1.80 1.90 1.85 2.00 2.05

N 12 12 12 12 12 12 12 12 12 12
D 2.519 3.085 2.865 3.142 3.223 2.562 2.500 2.712 2.704 2.977
/s 0.01156 0.01703 0.01344 0.01759 0.01878 0.01342 0.01054 0.01734 0.01211 0.01713

Average D for 10 2.829e


samples
Average /s for 10 0.01489d
samples
Different superscript letters indicate statistically significant differences exist at a = 0.05 for average diameter and sphericity values for 10 samples.
Means for groups in homogeneous subsets are displayed. Based on Type III Sum of Squares. DuncanTest was applied.N shows the number of
measurement i.e. the number of measured diameters. D1. . .7 show the dimensions for each material where notated in Fig. 2.

Acknowledgement Bayram, M., Öner, M. D., & Kaya, A. (2004b). Influence of soaking
on the dimensions and colour of soybean for bulgur production.
Journal of Food Engineering, 61, 331–339.
I wish to thank Arbel Legume and Cereal Co. Mer- Geankoplis, C. J. (1983). Transport processes and unit operations (2nd
sin, Turkey for provision of the samples. ed.). Boston: Allyn and Bacon Inc. pp. 132–135.
Holdich, R. (2002). Fundamentals of particle technology. UK: Midland
References Information Technology and Publishing pp. 5–6.
McCabe, W. L., Smith, J. C., & Harriott, P. (1985). Unit operations of
Bayram, M. (2000). Bulgur around the world. Cereal Foods World, 45, chemical engineering (4th ed.). NY: McGraw-Hill Co. p. 137, 222,
80–82. 798.
Bayram, M., & Öner, M. D. (2002). The new old wheat: convenience McCabe, W. L., Smith, J. C., & Harriott, P. (2001). Unit operations of
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