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PII: S2352-7102(17)30753-2
DOI: https://doi.org/10.1016/j.jobe.2018.04.032
Reference: JOBE477
To appear in: Journal of Building Engineering
Received date: 27 November 2017
Revised date: 30 April 2018
Accepted date: 30 April 2018
Cite this article as: T.J. Chandni and K.B. Anand, Utilization of Recycled Waste
as Filler in Foam concrete, Journal of Building Engineering,
https://doi.org/10.1016/j.jobe.2018.04.032
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Utilization of Recycled Waste as Filler in Foam concrete
CHANDNI. T. J1 and K. B. ANAND2*
Department of Civil Engineering, Amrita School of Engineering, Coimbatore, Coimbatore
Amrita Vishwa Vidyapeetham, India
Email addresses: tjchandni@gmail.com (Chandni.T.J),
kb_anand@amrita.edu (K.B.Anand)
*
Corresponding author.
Abstract
The rapid urbanization has led to the enormous increase in wastes being disposed of. This paper
aims at identifying the possibility of using recycled materials such as crushed glass and plastic
wastes in foam concrete as a substitute filler for fine river sand. A protein based foaming agent
has been adopted for the study. The workability and strength of different mixes, made using
preformed foam, at varying densities using powdered glass and plastic wastes have been
investigated. Analysis of foam concrete mixes to identify air-void distribution and its
relationship to strength has been done. Effect of superplasticizer inclusion and the corresponding
change in the water to solids ratio on compressive strength has also been carried out. The study
showed that incorporation of recycled wastes is effective to produce foam concrete of strength
that will permit its use for bearing wall applications. Incorporation of PCE based superplasticizer
Keywords: Foam concrete; Sustainable material; Recycled waste; Air-void structure; Water to
solids ratio
1
Post Graduate Student
2
Professor
1. Introduction
replacing some of the solid material in the mix by air voids. Foam concrete is a type of cement-
based mortar which contains millions of evenly distributed and consistently sized air bubbles or
controlled low strength, and excellent thermal insulation, consuming only minimal aggregate.
The density of foam concrete is influenced by the amount of foam added and normally ranges
from 400 kg/m3 to 1600 kg/m3 with compressive strengths varying from 1MPa to 15MPa. Table
1 summarizes some of the recent studies on foam concrete with respect to the constituent aspects
Density,
E.K. Kunhanandan Nambiar, Sand Spreadability,
Organic
K. Ramamurthy, [2] Class F Fly ash Flowability
Compressive Strength,
Zhongwei Liu, et. al. [3] Protein Flowability Pore structure
Sand
E.K. Kunhanandan Nambiar,
Organic Class F Fly ash Pore structure
K. Ramamurthy, [4]
Flowability,
Siong Kang Lim, et. al. [5] Synthetic Sand Spreadability Compressive Strength
Compressive Strength,
E.K. Kunhanandan Nambiar, Sand Fresh density,
Synthetic Water absorption
K. Ramamurthy, [6] Class F Fly ash Spreadability
Strength, Shrinkage
Bing, et. al. [7] Protein Class F Fly ash
Sand Strength, Elastic modulus,
Ameer A. Hilal, et. al. [8] Protein Spreadability
Fly ash- Category S Thermal properties
Sand Compressive Strength, Air void
Ameer A. Hilal, et. al. [9] Protein
Fly ash- Category S structure, Hydration products
Typically, three types of foaming agents are used for the production of foam concrete, namely
synthetic, protein and organic based foaming agents. These foaming agents facilitate the
formation of stable air bubbles by reducing the surface tension of the solution. It has been
observed [1] that for a protein-based foaming agent, the air voids were smaller and more uniform
in size at higher foam concrete densities than synthetic based foaming agents. The density and
stability of foam produced with four synthetic surfactants were studied [10] by the free drainage
test as prescribed in Defence Standard 42–40 [11] and foam stability test based on ASTM C 796-
97 [12]. Studies also indicate that in foam concrete mixes, foam addition considerably reduces
the mix consistency and increased foam volumes necessitate higher water to solids ratio [2]. As
per a study [3] for the same foam concrete density, a higher w/c ratio would result in a lower
relative viscosity and a weaker bubble-maintaining capacity in cement paste resulting in the
bubbles to combine easily into larger ones. It was also reported [4] that higher strength was
The type of filler material used also influences various properties of foam concrete. As the filler
materials become finer, it produces more uniform and narrower air-void distribution thereby
increasing the compressive strength [5]. Compared to sand filler foam concrete mixes, the fly ash
based mixes required relatively higher water to solids ratio and lower foam volume because of its
fineness [6]. It has been reported [7] that the incorporation of silica fume and polypropylene fiber
improved the compressive strength and the shrinkage resistance of foam concrete. Ameer A.
Hilal et al. [8,9] also observed that mineral admixtures such as fly ash and silica fume in
combination with a super-plasticizer improved the compressive strength of foam concrete.
distribution of air voids. Addition of ultrafine GGBS as partial cement replacement showed a
Many researchers have studied about ways in which recycled wastes can be utilized in normal
concrete. Yahya Jani and William Hogland [14], reviewed the previous works done on concrete
with waste glass as an aggregate replacement and concluded that as the particle size increases,
the alkali-silica reaction expansion also increases causing cracks in concrete. Finer waste glass
aggregate produces a pozzolanic reaction which helps in improving the mechanical properties of
the cement paste. It has been observed [15] that concrete with cement replaced by glass powder
(at 15% and 30% level) yielded higher compressive strength and low porosity due to the slow
pozzolanic reaction of glass powder. Due to the reduction in pore size and connectively, a higher
resistance against water and chloride ingress was also observed, In the experimental
investigations on ASR expansions of glass sand mortar [16], it was observed that brown glass
showed more resistance to alkali-silica reaction than green glass. This has been attributed to the
preferential occurrence of reaction in the internal cracks of green glass particles. Malek Batayneh
et al. [17] observed that plastic waste as a substitute for sand decreased the strength of concrete,
whereas adoption glass waste increased the strength. Harini et al. [18] observed that inclusion of
plastic waste as fine aggregate reduced the density of concrete and also assisted in arresting
microcracks.
Varieties of waste materials have been tried in foam concrete as fine filler, viz., fly ash [6,19,20],
incinerator bottom ash, foundry sand and quarry finer [21], expanded polystyrene and Lytag
fines [22,23], lime [24], chalk and crushed concrete [25]. The primary intention in these attempts
was to utilize the waste generated in industrial processes to reduce the density of foam concrete.
The primary objective of this study is to develop a sustainable product using recyclable waste
materials thereby attempting to partially solve the problems caused by the disposal of such
waste. The waste materials have been considered as the potential replacement for aggregates in
foam concrete. Glass and plastic wastes were adopted in this study as large volumes of these
types of wastes are generated in both commercial and household activities. Research attempts
have been made to determine the feasibility of using these recycled wastes in concrete but not in
foam concrete. Glass waste and plastic waste have the advantage over other waste materials, viz.,
pozzolanic property and lower density respectively. Also, the use of the protein-based foaming
agent, which helps in the production of a stable foam, orients this study towards sustainability.
The current study aims at determining the potential use of these recycled wastes in foam concrete
by (i) Assessing the fresh state properties; (ii) Investigating the compressive strength at various
densities; (iii) Studying the relationship between the strength and air-void distribution; (iv)
3. Experimental Details
In this study, the primary experiment variables are the types of filler materials, i.e. the recycled
glass powder and plastic powder; the types of superplasticizers used, i.e. Poly Carboxylate Ether
(PCE) and Sulphonated Naphthalene Formaldehyde (SNF); and the water to solids ratio to obtain
foam concrete of required density and consistency. For each of the designed mixes fresh and
3.1.1 Binder
Locally available 53 Grade Ordinary Portland Cement of specific gravity 2.98, conforming to IS
3.1.2 Filler
Two types of recycled wastes in the powdered form were used in the study
(a) Recycled glass powder – crushed waste soda-lime glass (of window panels and bottles),
of particle size finer than 90μm and specific gravity 2.36. The chemical composition of
Oxide % by weight
Na2O 11.07
MgO 1.59
Al2O3 0.66
SiO2 70.65
CaO 15.14
Fe2O3 0.77
TiO2 0.12
(b) Recycled thermoplastic powder – derived from polypropylene based molded furniture
(after useful life and damaged) of particle size finer than 1.18mm and specific gravity
0.9.
The particle size distribution of the filler materials are shown in Figure 1.
110
100
90
Weight passing (%) 80
70
60
50 plastic powder
40 Glass powder
30
20
10
0
0.01 0.1 1 10
Sieve size (mm)
3.1.3 Foam
The foam was generated by using a foam generator by diluting the foaming agent with water and
then aerating to create the foam. A vegetable protein-based liquid foaming agent of specific
gravity 1.2 and having a pH value of 7.5 was used in this study. Foam density was measured
immediately after the generation of foam while foam stability was measured by free drainage test
as prescribed in Defence Standard 42-40 [11]. The foam generation pressure controls the mixing
of air with foaming liquid and hence the foam density varies with foam generation pressure. For
foam concrete, ASTM C 796 [12] specifies the foam unit weight to be in the range of 32 to
64kg/m3. For evaluating the relative characteristics of foam produced with the foaming agent, a
series of trials were carried out with two surfactant concentrations (foaming agent to water ratio),
viz., 1:40 and 1:35; and aeration pressure ranging from 100KPa to 350KPa. A stable foam
density 40kg/m3 was obtained with a dilution of 1:35 and aeration pressure of 250KPa (using the
Superplasticizers belonging to two families, i.e. Poly Carboxylate Ether (PCE) and Sulphonated
Naphthalene Formaldehyde (SNF) were used in the study. The specific gravity of PCE was 1.1
ASTM C 796 [12] suggests a method of estimating foam volume necessary to make cement
slurry of given water-cement ratio and target density. Foam concrete was prepared by the
addition of pre-formed foam (with density 40 kg/m3) into the cement-based slurry, as per
equation 1. For a target design density (D kg/m3) of foam concrete, at a particular water to solids
ratio, the quantity of cement (c kg/m3) and filler (f kg/m3) was obtained by varying the foam
volume. Initially, cement and filler were weighed and dry mixed in a mortar mixer and then
water (w kg/m3) was added incrementally to obtain a homogeneous mix. The required quantity of
foam (F kg/m3) was added to the wet mix and mixed until the foam was uniformly distributed
D = c + f +w + F - - - - - - - - - (1)
The actual densities of the mixes produced were ensured to vary only within ±50 kg/m3 from the
design densities.
A series of trials were carried out for each mix, by varying the water to solids ratio and the foam
volume to obtain workable mix. Mix proportioning was done based on volume. As the specific
gravity of glass powder was higher than plastic powder, it was yielding foam concrete of higher
densities. In this study, design densities for glass filler foam concrete (GFC) were fixed as 1200
kg/m3, 1400 kg/m3 and 1600 kg/m3 with cement : filler ratio as 1:1. For plastic filler foam
concrete (PFC), the design densities were 800 kg/m3, 1000 kg/m3 and 1200 kg/m3 with cement:
filler ratio 1:0.33. The variation in the cement to filler ratios was due to the large difference in
the specific gravities of the two types of fillers. Table 3 shows the range of water to solids ratio
and foam volume adopted for the trials for both fillers at each of the design densities.
Table 3: Range of water to solids ratio and foam volume for the trial mixes
1200 35 - 25
Glass 1400 0.35 - 0.60 25 - 15
1600 15 – 5
800 50 - 40
Plastic 1000 0.35 - 0.70 35 - 25
1200 20 - 10
Fresh state characteristics of foam concrete which are to be tested are the fresh density and the
spreadability. The fresh density test was done as per ASTM C796 [12]. It was evaluated by
determining the density of the freshly produced foam concrete immediately after its production.
Spreadability of foam concrete was determined by the flow cone/ mini-slump test. It was done by
filling the mix in slump cone (of top diameter 2mm, bottom diameter 5.7mm, height 3.8mm) and
raising it. The percentage of spread was obtained after measuring the spread diameter.
Compressive Strength test was conducted for cubes of size 50mm x 50mm x 50mm using the
Universal Testing Machine of capacity 400kN. For each mix, 4 specimens were cast and de-
molded after 24 hours. The cubes were water cured for 28 days before testing. After 28 days of
water curing, the specimens were dried, and dry density was estimated. This was done to check
Air-void distribution of foam concrete was observed through the optical microscopic study with
the help of an image analysis software. For this, 50mm cubes were cut parallel to the cast face
smoothened and treated with 2 coats of black ink. After drying, talc powder was applied to the
surface to highlight the air voids. The specimen was then subjected to image analysis. A
magnification of 50x was selected and each image covering 5.72 mm2 (2.6 mm × 2.2 mm). A
total of 24 specimens were tested, 12 with each type of filler. 10 images were captured from the
cut surfaces of each mix. From the total area (57.2 mm2) of each mix analyzed, the total number
of voids, as well as the diameter of each void, was measured and classified.
The effect of reduced water to solids ratios was studied by adding superplasticizers. For this
study, highest density mixes were selected from each of the filler type (1600 kg/m3 and 1200
kg/m3 for GFC and PFC respectively) without changing the foam content. Two different families
Formaldehyde (SNF), were added at a dosage of 1.5% by weight of cement. With the addition of
plasticizers, there was a reduction in water/solid ratio and the density was maintained through a
marginal increase in solids. An earlier study [2] reports a reduction of 23% in the water to solids
cement. Use of PCE based superplasticizer for foam concrete have not been reported. 50mm
cube specimens were cast for each mix of both the filler types and were subjected to water curing
In this study, the foam volume was chosen to obtain foam concrete density close to the design
density. It was observed that the type of filler affects the water to solids ratio for obtaining a mix
of density ratio (fresh density to design density) value of one and of suitable workability. From
the trials, the water to solids ratio for producing workable mixes, for GFC was observed to be
ranging from 0.45 to 0.55 whereas for PFC it was from 0.65 to 0.75. The composition of the
mixes selected for GFC and PFC at the respective design densities along with spread values are
shown in Table 4.
Design Fresh
W/S Cement Filler Water Foam Spread
Filler Mix Density Density
ratio
kg/m3 kg kg kg % kg/m3 %
GFC12 1200 0.55 376 376 414 30 1212 112
Glass GFC14 1400 0.50 455 455 455 20 1394 112
GFC16 1600 0.45 542 542 488 10 1579 100
PFC8 800 0.75 353 116 352 40 803 112
Plastic PFC10 1000 0.65 447 147 386 25 1030 125
PFC12 1200 0.65 543 179 469 15 1250 125
The higher requirement of water to solids ratio for PFC mixes may be because of the lower
specific gravity and angular shape of the plastic powder. The foam volume decreases steeply
with an increase in foam concrete density whereas the water solids ratio decreases marginally for
both the fillers. From the trials, for both fillers, the spread value was observed to be increasing
with increase in the water to solids ratio at a particular density. In low-density mixes requiring
higher foam content, reduction in spread values was observed. A reported study involving low-
density mixes [6] indicates that there are more bubbles and their adhesion with the solid particles
The compressive strength mainly depends on the water to solids ratio, cement content, foam
volume and the type of fillers. Table 5 shows the average compressive strength (based on testing
6 samples) of GFC and PFC respectively, at the selected design densities for each filler type.
All the mixes showed compressive strength within the range of 1.5 N/mm2 to 10 N/mm2
observed for sand-filler foam concrete of 800kg/m3 to 1600 kg/m3 densities as reported [27]. The
strength ranges achieved indicate their suitability for different classes of application from
insulation to masonry blocks. The maximum compressive strength of 10.26 N/mm2 was obtained
for GFC at a design density of 1600 kg/m3. This may be because of the lower foam content at
higher densities. As the density of foam concrete increased, the volume of foam added was
reduced which means that lesser volume of the mix was occupied by the pores. For GFC, the
foam volume has decreased from 30% to 10% for design densities from 1200 kg/m3 to 1600
kg/m3 whereas, in the case of PFC, foam volume decreased from 40% to 15% for design
densities from 800 kg/m3 to 1200 kg/m3. GFC showed higher strength than PFC because of the
higher design densities and lower water to solids ratio for the former mixes. At all the design
densities attempted in the study, the derived strength was sufficient for it to be recommended for
masonry blocks. Studies on normal concrete utilizing glass powder as the fine aggregate [14, 28]
report an increase in strength due to the pozzolanic reaction of glass filler. This factor also would
have contributed along with the fine particle size of glass filler in attaining the higher strength of
GFC. For the same design density of 1200 kg/m3, the compressive strength of PFC was found to
be marginally higher than that of GFC. It may be attributed to the higher foam volume in the
latter. The range of strength obtained at low densities indicates its suitability for insulation
blocks.
The strength of foam concrete is influenced by the air void distribution. For both fillers, it was
observed that the voids were uniformly distributed with most of the voids being in a uniform size
range at all design densities. Figures 2(a) and 2(b) show typical normal images of the specimen
cut surface for air-void analysis before and after preparation. Figures 3 (a) and (b) show the
typical microscopic images (with 50X magnification) of GFC and PFC respectively.
(a) Before preparation (b) After preparation
Figure 2: Typical images of cut surface for air-void analysis
In the case of GFC, the voids were found to be more uniformly distributed, regular in shape and
less interconnected. This may be due to the higher fineness of glass powder filler. It has been
reported that finer filler material results in a uniform distribution of bubbles [6]. For PFC, as the
foam volume increases i.e. as foam concrete density decreases, the number of bigger sized pores
also increases suggesting merging of pores at higher foam volume. A similar observation was
observed and reported in an earlier research work [4]. The pores were of irregular shape at all
densities in general for PFC specimens. The total sectional area of voids and its percentage based
on the observed area of all mixes are presented in Table 6. Figure 4 and Figure 5 show the air-
60
GFC12
40 GFC14
GFC16
20
0
0 100 200 300 400 500 600 700 800 900 1000 1100
Figure 4: Relation between Cumulative frequency and air void size of GFC
100
Cumulative Frequency (%)
80
60
PFC8
PFC10
40
PFC12
20
0
0 100 200 300 400 500 600 700 800 900 1000 1100
Figure 5: Relation between Cumulative frequency and air void size of PFC
For both fillers, the percentage of area occupied by voids showed an increase with a reduction in
density. The reduction in the void area of GFC was from 31.3% to 13.3% for GFC12 to GFC16. In
PFC8, air voids constituted 44.7% of the total area analyzed and only 19.5% in case of PFC12.
Air-void parameter D90 values (indicate that only 10% of voids are larger than this size)
correlates well with the strength of foamed concrete and hence were taken into consideration for
the analysis. Figure 6 shows the relationship between air void parameter and the 28-day
12
10
Compressive Strength (N/mm2 )
Glass Filler
8
Plastic Filler
1600 kg/m³
6
1400 kg/m³
1200 kg/m³
4
1200 kg/m³
1000 kg/m³
2
800 kg/m³
0
600 700 800 900
Pore Diameter (μm)
It was observed that as the density increases, there was a reduction in pore diameter resulting in
increased strength for both fillers, similar to the observation of Ameer A. Hilal et al. [9]. For
GFC, only a small variation in D90 value was observed at different densities. The decrease in
pore diameter was higher for PFC, but a corresponding significant increase in strength was not
observed. The compressive strength was observed to increase with a reduction in the percentage
of area occupied by air voids and the D90 value. This can explain the slightly higher
studied for the selected mixes, the mix composition of which is presented in Table 7. With the
addition of plasticizers, there was a reduction in water/solid ratio and the density was maintained
through the marginal increase in solids. Increase in cement content ranged between 9 to 16% for
different mixes. The corresponding 28 day compressive strength results are tabulated in Table 7.
Table 7: Mix Details and Compressive strength of modified GFC16 and PFC12 mixes
Type of
SP
Filler Average
(1.5%
(Design Mix W/S Foam Cement Filler Water Compressive
by CoV
Density designation Ratio (%) (kg) (kg) (kg) Strength
weight
kg/m3) (N/mm2)
of
cement)
The introduction of PCE resulted in 37% and 33% reduction of the water to solids ratio in GFC
and PFC respectively, whereas SNF caused a reduction of only 24% and 30%. Hence it can be
concluded that PCE is more efficient in reducing the water to solids ratio, the reduction being
more prominent in GFC. It was observed that by the inclusion of PCE, foam concrete with both
fillers showed a higher strength. This increase in the strength was more significant for GFC when
compared to PFC. Addition of SNF also resulted in an increase in strength for GFC and no
appreciable change for PFC when compared with mixes without superplasticizer. Figure 7 and
Figure 8 show the air-void size distribution of GFC and PFC respectively.
100
Cumulative Frequency (%)
80
60
GFC16 - P
40
GFC16 - S
GFC16
20
0
0 200 400 600 800 1000 1200
Figure 7: Relation between Cumulative frequency and air void size of GFC16 mixes
100
Cumulative Frequency (%)
80
60
PFC12 - P
40
PFC12 - S
PFC12
20
0
0 200 400 600 800 1000 1200
Figure 8: Relation between Cumulative frequency and air void size of PFC12 mixes
A higher D90 value indicates the presence of more number of bigger sized pores and thus a
decrease in the compressive strength. The inclusion of superplasticizer has resulted in a decrease
in the D90 value for GFC. In the case of PFC mixes not much changes were observed with
respect to the D90 value on the addition of both superplasticizers. Even though both families of
mixes. Table 8 shows the mix parameters and properties for GFC16 and PFC12 mixes with and
without superplasticizers.
In all the mixes except PFC12 - S, the number and the percentage of area occupied by the voids
have decreased by the inclusion of superplasticizers. A reduction in the number and size of voids
in GFC was observed when PCE was introduced. For GFC specimens, the pores were more
regular in shape, whereas for PFC mixes there was no appreciable difference in the shape and
size of voids with respect to reference mixes. PCE based superplasticizer was effective in
enhancing the strength of foam concrete for structural applications. Strength enhancement up to
2.8 times could be achieved. Beneficial influence on the void structure has been reported [9] in a
study on sand filler based foam concrete prepared by addition of superplasticizer. Marginally
higher cement content, void structure enhancement and improved cement paste microstructure
However, such a beneficial improvement in the air-void structure was not observed in PFC
5. Conclusion
Many earlier studies have focused on utilization of waste generated in industrial processes,
whereas the current study primarily looks at wastes that are generated at commercial and
household level, particularly very low specific gravity filler like waste plastic in powder form.
The following conclusions drawn are applicable to the range of parameters investigated.
The water to solids ratio which influences the consistency of the mix depends on the type
of filler. Optimal water to solids ratio of plastic filler foam concrete was higher than glass
filler foam concrete by 18% indicating that low specific gravity fillers require higher
Glass filler foam concrete showed higher compressive strength compared to plastic filler
foam concrete. Recycled glass filler foam concrete showed sufficient compressive
strength that will permit its use for bearing wall applications. Based on density, plastic
filler foam concrete yielded strengths suited either for insulation or load bearing
application.
The air-voids were found to be uniformly distributed for both the fillers with the majority
of the voids falling in a uniform size range. The inclusion of superplasticizer has resulted
in lowering the D90 value (i.e. lesser number of bigger pores) for GFC, which
reduction in water to solids ratio along with the marginal increase in cement content
improved the compressive strength (up to 2.8 times). Only PCE based superplasticizer
was efficient in enhancing the strength of foam concrete for structural applications.
Both families of superplasticizers did not show much influence in improving the strength
Funding
This research did not receive any specific grant from funding agencies in the public, commercial
or not-for-profit sectors.
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