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  • Práctica 12. "Síntesis 5,5-Difenilhidantoína".: Añadir Y Mezclar: + 1G Bencilo + 0.5G Urea + 3Ml Naoh 30% + 15Ml Etoh

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    Paoli Ruiz
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    Diagrama P12 Farmoquímica

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    D12

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    Diagrama P12 Farmoquímica

    Copyright:

    © All Rights Reserved
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    9 views1 page

    Práctica 12. "Síntesis 5,5-Difenilhidantoína".: Añadir Y Mezclar: + 1G Bencilo + 0.5G Urea + 3Ml Naoh 30% + 15Ml Etoh

    Uploaded by

    Paoli Ruiz
    Diagrama P12 Farmoquímica

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Flag for inappropriate content
    of 1

    Nombre: Ruiz García Paola Michelle Fecha: 18/Mayo/2018

    Grupo: 5FM1 Práctica 12. “Síntesis 5,5-difenilhidantoína”.

    Añadir y mezclar:

    + 1g Bencilo
    + 0.5g Urea
    + 3mL NaOH 30%
    + 15mL EtOH

    Calentar y reflujar Eliminar EtOH


    Mezcla por 2 horas con destilación

    Enfriar a T ambiente
    +25 mL agua.

    Filtrar al vacío y acidular con HCl concentrado

    Recristalizar de EtOH

    Hacer cromatografía AcOEt/hexano (1:3)

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