COV Factor Detn - 20170925

15 June 2017
STANDART 2 OKTANONE
LOT NO MKDK1191V
MW 128.21
REGENT GRADE 98
MW CO 28
25
Berat Sampel : 0.2622 g
20 f(x) = 40.4781207093x - 17.8435803639
R² = 0.9993325543
15
g CO = 0.2570
ug CO = 5.6117
10
1 ml Stock Solution ug CO = 5.6117 5
mL Abs ug CO 0
0 0.439 0 0.4 0.5 0.6 0.7 0.8 0.9
2 0.718 11.2234 -5
3 0.865 16.8351
4 0.989 22.4468
Done by: Santoso/Robi

7093x - 17.8435803639
43
6 0.7 0.8 0.9 1 1.1

20 Juli 2017
STANDARD 2 OKTANONE
LOT NO MKDK1191V
MW 128.21
REGENT GRADE 98
MW CO 28
g CO = 0.2570
ug CO = 5.6117
1 ml Stock Solution ug CO = 5.6117
mL Abs ug CO I II AVG
0 0.577 0 0.577 0.577 0.577
1 0.728 5.6117 0.728 0.728 0.728
2 0.834 11.2234 0.834 0.834 0.834
3 0.978 16.8351 0.978 0.978 0.978
4 1.116 22.4468 1.116 1.116 1.116
5 1.262 28.0585 1.262 1.262 1.262
6 1.403 33.6702 1.403 1.403 1.403
Done by: Santoso
TCA TOLUENE Bottle # 4; Lot # K46165125 449
DNPH TOLUENE Bottle # 4; Lot # K46165125 449
SOLVENT TOLUENE Bottle # 19; Lot # K46165125 449
Ethanol = Technical Grade (TG)
40
35
f(x) = 40.997296276x - 23.5648071017
30 R² = 0.9987911108
25
20
15
10
0
0.500 0.600 0.700 0.800 0.900 1.000 1.100 1.200 1.300 1.400 1.500
-5
11 Juli 2017
STANDART 2 OKTANONE
LOT NO MKDK1191V
MW 128.21
REGENT GRADE 98.0
MW CO 28.0
25
f(x) = 31.086247344x - 10.2379260987
20
R² = 0.9998081787
15
ug CO = 0.2570
ug CO = 5.6117
10
mL Abs ug CO
0 0.332 0 0
1 0.504 5.6117 0.2 0.3 0.4 0.5 0.6 0.7 0.8
2 0.694 11.2234 -5
3
4 1.051 22.4468
5 1.108 28.0585
5 1.133 28.0585
6 1.295 33.6702
REGENT GRADE 98.0

MW CO 28.0
40
Berat Sampel : 0.2622 g 35
f(x) = 35.7721827512x - 12.4332629696
30
R² = 0.9974653788
25
ug CO = 0.2570
ug CO = 5.6117 20
15
5
mL Abs ug CO
0 0.332 0 0
1 0.504 5.6117 0.2 0.4 0.6 0.8 1
2 0.694 11.2234 -5
5 1.108 28.0585
5 1.133 28.0585
6 1.295 33.6702
REGENT GRADE 98.0

MW CO 28.0
40
30 f(x) = 35.3699228673x - 12.2860709418

R² = 0.9982553415
25
ug CO = 0.2570
ug CO = 5.6117 20
15
5
mL Abs ug CO
0 0.332 0 0
1 0.504 5.6117 0.2 0.4 0.6 0.8 1
2 0.694 11.2234 -5
5 1.133 28.0585
6 1.295 33.6702
086247344x - 10.2379260987
98081787
0.5 0.6 0.7 0.8 0.9 1 1.1
1827512x - 12.4332629696
53788
0.6 0.8 1 1.2 1.4

9228673x - 12.2860709418
53415
0.6 0.8 1 1.2 1.4

12 Juli 2017
STANDART 2 OKTANONE
LOT NO MKDK1191V
MW 128.21
REGENT GRADE 98
MW CO 28
30
25 f(x) = 35.7766673991x - 14.4591865718
R² = 0.9936682326
20
g CO = 0.2570
ug CO = 5.6117 15
10
5
mL Abs ug CO
0 0.373 0 0
1 0.582 5.6117 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1
2 0.747 11.2234 -5
4 1.033 22.4468
5 1.168 28.0585
Done by: Santoso

73991x - 14.4591865718
326
0.6 0.7 0.8 0.9 1 1.1 1.2 1.3

12 Juli 2017
STANDART 2 OKTANONE
LOT NO MKDK1191V
MW 128.21
REGENT GRADE 98
MW CO 28
30
25 f(x) = 35.7766673991x - 14.4591865718
R² = 0.9936682326
20
g CO = 0.2570
ug CO = 5.6117 15
10
5
mL Abs ug CO
0 0.373 0 0
1 0.582 5.6117 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1
2 0.747 11.2234 -5
4 1.033 22.4468
5 1.168 28.0585
Done by: Santoso

73991x - 14.4591865718
326
0.6 0.7 0.8 0.9 1 1.1 1.2 1.3

15 Juli 2017
STANDART 2 OKTANONE
LOT NO MKDK1191V
MW 128.21
REGENT GRADE 98
MW CO 28
65
55 f(x) = 38.3504483339x - 21.0684243158
R² = 0.9976687266
45
g CO = 0.2570
ug CO = 5.6117 35
25
15
mL Abs ug CO
0 0.559 0 5
2 0.853 11.2234
4 1.137 22.4468 -50.4 0.6 0.8 1 1.2 1.4 1.6
5 1.274 28.0585
6 1.412 33.6702
8 1.681 44.8936
10 2.051 56.117
Done by: Santoso

Toluene 38
483339x - 21.0684243158
7266
1 1.2 1.4 1.6 1.8 2 2.2

16 Juli 2017
STANDART 2 OKTANONE
LOT NO MKDK1191V
MW 128.21
REGENT GRADE 98
MW CO 28
65
55
f(x) = 40.7770353855x - 24.8176643134
R² = 0.999861017
45
g CO = 0.2570
ug CO = 5.6117 35
25
15
mL Abs ug CO
0 0.610 0 5
2 0.892 11.2234
4 1.154 22.4468 0.400
-5 0.600 0.800 1.000 1.200 1.400 1.600
5 1.291 28.0585
6 1.429 33.6702
8 1.711 44.8936
10 1.990 56.1170
Done by: Santoso

Toluene 19
70353855x - 24.8176643134
61017
1.000 1.200 1.400 1.600 1.800 2.000 2.200

19 Juli 2017
STANDARD 2 OKTANONE
LOT NO MKDK1191V
MW 128.21
REGENT GRADE 98
MW CO 28
g CO = 0.2570
ug CO = 5.6117
0 0.615 0 0.613 0.616 0.615
1 0.761 5.6117 0.763 0.759 0.761
2 0.953 11.2234 0.953 0.953 0.953
3 1.0755 16.8351 1.077 1.074 1.076
4 1.24 22.4468 1.240 1.240 1.240
5 1.394 28.0585 1.393 1.395 1.394
Done by: GILBERT

30
f(x) = 35.9226565497x - 22.1209167078

25 R² = 0.9980674906
20
15
10
0
0.500 0.600 0.700 0.800 0.900 1.000 1.100 1.200 1.300 1.400 1.500
-5
17 September 2017
STANDARD 2 OKTANONE
LOT NO MKDK1191V
MW 128.21
REGENT GRADE 98
MW CO 28
g CO = 0.2570
ug CO = 5.6117
0 0.557 0 0.577 0.577 0.577
1 0.766 5.6117 0.728 0.728 0.728
2 0.899 11.2234 0.834 0.834 0.834
3 0.969 16.8351 0.978 0.978 0.978
4 1.236 22.4468 1.116 1.116 1.116
5 1.335 28.0585 1.262 1.262 1.262
6 1.479 33.6702 1.403 1.403 1.403
Done by: Santoso
40
35
30 f(x) = 36.5449335128x - 20.9680233666

R² = 0.9863770784
25
20
15
10
0
0.400 0.600 0.800 1.000 1.200 1.400 1.600
-5
17 September 2017
STANDARD 2 OKTANONE
LOT NO MKDK1191V
MW 128.21
REGENT GRADE 98
MW CO 28
g CO = 0.2570
ug CO = 5.5800
0 0.518 0 0.518 0.516 0.517
1 0.707 5.58 0.707 0.704 0.706
2 0.855 11.16 0.855 0.854 0.855
3 0.997 16.74 0.997 0.995 0.996
4 1.184 22.32 1.184 1.182 1.183
5 1.315 27.9 1.315 1.312 1.314
Done by: willy
30
25 f(x) = 35.057499156x - 18.630102549

R² = 0.9976937036
20
15
10
0
0.400 0.500 0.600 0.700 0.800 0.900 1.000 1.100 1.200 1.300 1.400
-5
17 September 2017
STANDARD 2 OKTANONE
LOT NO MKDK1191V
MW 128.21
REGENT GRADE 98
MW CO 28
g CO = 0.2570
ug CO = 5.6117
0 0.530 0 0.530 0.532 0.531
1 0.705 5.6117 0.705 0.712 0.709
2 0.903 11.2234 0.912 0.903 0.908
3 1.064 16.8351 1.068 1.064 1.066
4 1.204 22.4468 1.208 1.024 1.116
5 1.391 28.0585 1.395 1.391 1.393
Done by: willy
30
f(x) = 32.8670920814x - 17.7258387993
25 R² = 0.997846184
20
15
10
0
0.400 0.600 0.800 1.000 1.200 1.400 1.600
-5
17 September 2017
STANDARD 2 OKTANONE
LOT NO MKDK1191V
MW 128.21
REGENT GRADE 98
MW CO 28
g CO = 0.2570
ug CO = 5.6117
0 0.731 0 0.583 0.582 0.583
1 0.831 5.6117 0.723 0.723 0.723
2 0.945 11.2234 0.889 0.888 0.889
3 1.067 16.8351 0.987 0.986 0.987
4 1.201 22.4468 1.125 1.124 1.125
5 1.289 28.0585 1.261 1.260 1.261
Done by: Santoso

30
25 f(x) = 48.7109634747x - 35.2012970851

R² = 0.9974848217
20
15
10
0
0.700 0.800 0.900 1.000 1.100 1.200 1.300 1.400
-5
22 September 2017
STANDARD 2 OKTANONE
LOT NO MKDK1191V
MW 128.21
REGENT GRADE 98
MW CO 28
g CO = 0.2570
ug CO = 5.6117
mL Abs ug CO
0 0.542 0
1 0.69 5.6117
2 0.854 11.2234
3 1.008 16.8351
4 1.156 22.4468
5 1.402 28.0585
Done by: Andrew

30
f(x) = 33.3059517241x - 17.3449565241
25 R² = 0.9923472617
20
15
10
0
0.400 0.600 0.800 1.000 1.200 1.400 1.600
-5
22 September 2017
STANDARD 2 OKTANONE
LOT NO MKDK1191V
MW 128.21
REGENT GRADE 98
MW CO 28
Date Prepared 17-Sep-17
Prepared by Santoso
g CO = 0.2570
ug CO = 5.6117
mL Abs ug CO
0 0.542 0
1 0.69 5.6117
2 0.854 11.2234
3 1.008 16.8351
4 1.156 22.4468
Done by: Andrew

25
f(x) = 36.2878040823x - 19.62123347

20
R² = 0.9997139033
15
10
0
0.500 0.600 0.700 0.800 0.900 1.000 1.100 1.200
-5
16 Juli 2017
STANDART 2 OKTANONE
LOT NO MKDK1191V
MW 128.21
REGENT GRADE 98
MW CO 28
65
55
f(x) = 102.5834748034x - 69.7630719078
R² = 0.9948205659
45
g CO = 0.2570
ug CO = 5.6117 35
25
15
mL Abs ug CO
0 0 5
2 0.775 11.2234
4 0.913 22.4468 -50.75 0.8 0.85 0.9 0.95 1 1.05 1.1
5 0.961 28.0585
6 1.015 33.6702
8 1.107 44.8936
10 1.224 56.1170
Done by: Santoso

Toluene 19
48034x - 69.7630719078
59
0.9 0.95 1 1.05 1.1 1.15 1.2 1.25

25 September 2017
STANDART 2 OKTANONE
LOT NO MKDK1191V
MW 128.21
REGENT GRADE 98
MW CO 28
65
55
f(x) = 39.6794987861x - 28.2637142769
R² = 0.9972931338
45
g CO = 0.2570
ug CO = 5.6117 35
25
15
mL Abs ug CO
0 0.706 0 5
2 1.032 11.2234
4 1.278 22.4468 0.600
-5 0.800 1.000 1.200 1.400 1.600 1.800
5 1.403 28.0585
6 1.520 33.6702
8 1.864 44.8936
10 2.133 56.1170
Done by: Santoso

Toluene 19
7861x - 28.2637142769
38
1.200 1.400 1.600 1.800 2.000 2.200 2.400

27 September 2017
STANDART 2 OKTANONE
LOT NO MKDK1191V
MW 128.21
REGENT GRADE 98
MW CO 28
40
30 f(x) = 39.0329559519x - 26.6692979059

R² = 0.9916320991
25
g CO = 0.2570
ug CO = 5.6117 20
15
5
mL Abs ug CO
0 0.660 0 0
0 0.692 0 0.600 0.700 0.800 0.900 1.000 1.100 1.200 1.300
1 0.859 5.6117 -5
2 0.933 11.2234
3 1.160 16.8351
4 1.238 22.4468
5 1.440 28.0585
6 1.530 33.6702
6 1.519 33.6702
Toluene 19
9519x - 26.6692979059
91
900 1.000 1.100 1.200 1.300 1.400 1.500 1.600

29 September 2017
STANDART Nonanal
LOT NO MKBR0585V
MW 142.24
REGENT GRADE 95
MW CO 28
45
Berat Sampel 0.2946 gr 40

35 f(x) = 38.3545786695x - 20.154155289
30 R² = 0.9920381361
g CO = 0.2799 25
ug CO = 5.5093 20
15

5
mL Abs ug CO 0
0 0.485 0
-50.400 0.600 0.800 1.000 1.200
1 0.682 5.5093
2 0.837 11.0186
4 1.126 22.0372
5 1.267 27.5465
7 1.485 38.5651
Toluene Spectroscopy
6695x - 20.154155289
61
0.800 1.000 1.200 1.400 1.600

30 September 2017
STANDART Nonanal
LOT NO MKBR0585V
MW 142.24
REGENT GRADE 95
MW CO 28
25
Berat Sampel 0.2946 gr f(x) = 42.9557946637x - 18.395380396

20
R² = 0.9925530758
15
g CO = 0.2799
ug CO = 5.5093 10
5
0
mL Abs ug CO
0.400 0.500 0.600 0.700 0.800
0 0.449 0
-5
1 0.537 5.5093
3 0.798 16.5279
4 0.955 22.0372
6637x - 18.395380396
758
0.600 0.700 0.800 0.900 1.000

15 June 2017
STANDART 2 OKTANONE
LOT NO MKDK1191V
MW 128.21
REGENT GRADE 98
MW CO 28
25
20 f(x) = 40.4781207093x - 17.8435803639
R² = 0.9993325543
15
g CO = 0.2570
ug CO = 5.6117
10
mL Abs ug CO 0
0 0.439 0 0.4 0.5 0.6 0.7 0.8 0.9
1 0.718 11.2234 -5
2 0.865 16.8351
3 0.989 22.4468
Done by: Santoso/Robi

7093x - 17.8435803639
43
6 0.7 0.8 0.9 1 1.1

03 Oktober 2017
STANDART Nonanal
LOT NO MKBR0585V
MW 142.24
REGENT GRADE 95
MW CO 28
25
Berat Sampel 0.2946 gr f(x) = 42.9557946637x - 18.395380396

20
R² = 0.9925530758
15
g CO = 0.2799
ug CO = 5.5093 10
5
0
mL Abs ug CO
0.400 0.500 0.600 0.700 0.800
0 0.449 0
-5
1 0.537 5.5093
2 0.798 16.5279
3 0.955 22.0372
6637x - 18.395380396
758
0.600 0.700 0.800 0.900 1.000

30 Agustus 2018
STANDART Nonanal
LOT NO MKBR0585V
MW 142.24
REGENT GRADE 95
MW CO 28
35
Berat Sampel 0.2946 gr 30 f(x) = 41.1901024243x - 18.064031942

R² = 0.9969810081
25
20
g CO = 0.2799
ug CO = 5.5093 15
10
mL Abs ug CO 0
0 0.444 0 0.400 0.500 0.600 0.700 0.800 0.900 1.000 1
-5
1 0.548 5.5093
2 0.715 11.0186
3 0.862 16.5279
4 0.986 22.0372
5 1.091 27.5465
5 1.098 27.5465
6 1.242 33.0558
43x - 18.064031942
1
0.700 0.800 0.900 1.000 1.100 1.200 1.300

COV Factor Detn - 20170925

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COV Factor Detn - 20170925

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15 June 2017

1 ml Stock Solution ug CO = 5.6117 5

Done by: Santoso/Robi

6 0.7 0.8 0.9 1 1.1

Berat Sampel : 0.2622 g

1 ml Stock Solution ug CO = 5.6117

1 ml Stock Solution ug CO = 5.6117 5

REGENT GRADE 98.0

1 ml Stock Solution ug CO = 5.6117 10

REGENT GRADE 98.0

30 f(x) = 35.3699228673x - 12.2860709418

1 ml Stock Solution ug CO = 5.6117 10

0.5 0.6 0.7 0.8 0.9 1 1.1

0.6 0.8 1 1.2 1.4

0.6 0.8 1 1.2 1.4

Done by: Santoso

0.6 0.7 0.8 0.9 1 1.1 1.2 1.3

Done by: Santoso

0.6 0.7 0.8 0.9 1 1.1 1.2 1.3

Done by: Santoso

1 1.2 1.4 1.6 1.8 2 2.2

Done by: Santoso

1.000 1.200 1.400 1.600 1.800 2.000 2.200

Berat Sampel : 0.2622 g

1 ml Stock Solution ug CO = 5.6117

Done by: GILBERT

f(x) = 35.9226565497x - 22.1209167078

Berat Sampel : 0.2622 g

1 ml Stock Solution ug CO = 5.6117

30 f(x) = 36.5449335128x - 20.9680233666

Berat Sampel : 0.2622 g

1 ml Stock Solution ug CO = 5.58

25 f(x) = 35.057499156x - 18.630102549

Berat Sampel : 0.2622 g

1 ml Stock Solution ug CO = 5.6117

Berat Sampel : 0.2622 g

1 ml Stock Solution ug CO = 5.6117

Done by: Santoso

25 f(x) = 48.7109634747x - 35.2012970851

Berat Sampel : 0.2622 g

1 ml Stock Solution ug CO = 5.6117

Done by: Andrew

Berat Sampel : 0.2622 g

1 ml Stock Solution ug CO = 5.6117

Done by: Andrew

f(x) = 36.2878040823x - 19.62123347

Done by: Santoso

0.9 0.95 1 1.05 1.1 1.15 1.2 1.25

Done by: Santoso

1.200 1.400 1.600 1.800 2.000 2.200 2.400

30 f(x) = 39.0329559519x - 26.6692979059

1 ml Stock Solution ug CO = 5.6117 10

900 1.000 1.100 1.200 1.300 1.400 1.500 1.600

Berat Sampel 0.2946 gr 40

1 ml Stock Solution ug CO = 5.5093 10

0.800 1.000 1.200 1.400 1.600

Berat Sampel 0.2946 gr f(x) = 42.9557946637x - 18.395380396

0.600 0.700 0.800 0.900 1.000

1 ml Stock Solution ug CO = 5.6117 5

Done by: Santoso/Robi

6 0.7 0.8 0.9 1 1.1

Berat Sampel 0.2946 gr f(x) = 42.9557946637x - 18.395380396

0.600 0.700 0.800 0.900 1.000