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��l� Designation: D 4253 - 93 AMERICAN SOCIETY FOR TESTING AND MATERIALS

1916 Race St. Philadelphia, Pa 19103


Reprinted from the Annual Book of ASTM Standards. Copyright ASTM
If not listed in the current combined index, will appear in the next edition.

Standard Test Methods for


Maximum Index Density and Unit Weight of Soils Using a
Vibratory Table 1
NOTE- The incorrect material was printed as the 1991 version. The standard was corrected editorially and year date changed February
1993.

I. Scope 1.4 The test method to be used should be specified by the


1.1 These test methods cover the determination of the individual assigning the test.
maximum index density/unit weight of cohesionless, free- 1.4.1 The type of table to be used (Method I or 2) is likely
draining soils using a vertically vibrating table. to be decided based upon available equipment.
1.2 Systems of Units: NOTE I-There is considerable evidence to show that electromag-
1.2.1 The testing apparatus described in this standard has netic tables yield slightly higher values of maximum index density/unit
been developed and manufactured using values in the weight.
gravimetric or inch-pound system. Therefore, test apparatus 1.4.2 It is recommended that both the dry and wet
dimensions and mass given in inch-pound units are regarded methods (Test Methods IA and IB or 2A and 2B) be
as the standard. performed when beginning a new job or encountering a
1.2.2 It is common practice in the engineering profession change in soil types, as the wet method can yield significantly
to concurrently use pounds to represent both a unit of mass higher values of maximum index density/unit weight for
(lbm) and a unit of force (lbf). This implicitly combines two some soils. Such a higher maximum index density, when
separate systems of units; that is, the absolute system and the considered along with the minimum index density/unit
gravitational system. It is scientifically undesirable to com- weight, Test Methods D 4254, will be found to significantly
bine the use of two separate sets of inch-pound units within a affect the value of the relative density (5. 7) calculated for a
single standard. This standard has been written using the soil encountered in the field. While the dry method is often
gravitational system of units when dealing with the inch- preferred because results can usually be obtained more
pound system. In this system the pound (lbf) represents a quickly, as a general rule the wet method should be used if it
unit of force (weight). However, balances or scales measure is established that it produces maximum index densities/unit
mass; and weight must be calculated. In the inch-pound weights that would significantly affect the use/application of
system, it is common to assume that I !bf is equal to I lbm. the value of relative density.
While reporting density is not regarded as nonconformance 1.5 These test methods are applicable to soils that may
with this standard, unit weights should be calculated and contain up to 15 %, by dry mass, of soil particles passing a
reported since the results may be used to determine force or No. 200 (74-µm) sieve, provided they still have cohesionless,
stress. free-draining characteristics (nominal sieve dimensions are
I .2.3 The terms density and unit weight are often used in accordance with Specification E 11 ). Further, these test
methods are applicable to soils in which 100 %, by dry mass,
interchangeably. Density is mass per unit volume whereas
of soil particles pass a 3 in. (75 mm) sieve (see Table I).
unit weight is force per unit volume. In this standard density
1.5.1 Soils, for the purpose of these test methods, shall be
shall be given only in SI units. After the density has been regarded as naturally occurring cohesionless soils, processed
determined, calculation for determining unit weights shall be particles, or composites or mixtures of natural soils, or
given. mixtures of natural and processed particles, provided they
1.3 Four alternative procedures are provided to determine are free draining.
the maximum index density/unit weight, as follows: 1.6 These test methods will typically produce a higher
1.3.1 Test Method IA-Using oven-dried soil and an maximum dry density/unit weight for cohesionless, free-
electromagnetic, vertically vibrating table. draining soils than that obtained by impact compaction in
1.3.2 Test Method IE-Using wet soil and an electromag- which a well-defined moisture-density relationship is not
netic, vertically vibrating table.
1.3.3 Test Method 2A-Using oven-dried soil and an TABLE Required Mass of Specimen-4
eccentric or cam-driven, vertically vibrating table. Maximum Size of Soil Mass of Specimen Size of Mold to be
I .3.4 Test Method 2B-Using wet soil and an eccentric or Particle, in. (mm) Required, (kg) Used, tt3 (cm3)
cam-driven vertically vibrating table. 3 (75) 34 0.500 (14 200)
1112(38.1) 34 0.500 (14 200)
3/, (19.0) 11 0.100 (2830)
3/e (9.5) 11 0.100 (2830)
I
These test methods are under the jurisdiction of ASTM Committee D-18 on
No. 4 (4. 75) or less 11 0.100 (2830)
Soil and Rock and are the direct responsibility of Subcommittee 018.03 on
Texture, Plasticity, and Density Characteristics of Soils. A The mass of the sample should be at least two (preferably four) times these
Current edition approved Feb. 2, 1993. Published April 1993. Originally values, since normally the wet and dry method is performed and more than one
published as D 4253 - 83 . Last previous edition D 4253 - 91. trial is done in the dry method preferably using non-tested soil (see 11.1.11 ).
-
4t D 4253
apparent. However, for some soils containing between 5 and particle segregation and breakdown.
15 % fines, the use impact compaction (Test Methods D 698 3.1.1.2 minimum index void ratio, emin-the reference
or D 1557) may be useful in evaluating what is an appro- void ratio of a soil at the maximum index density/unit
priate maximum index density/unit weight. weight.
1. 7 For many types of free-draining, cohesionless soils, 3.1.1.3 minimum index density/unit weight, Pctmin or
these methods cause a moderate amount of degradation 'Yctmin-the reference dry density/unit weight of a soil in the
(particle breakdown) of the soil. When degradation occurs, loosest state of compactness at which it can be placed using a
typically there is an increase in the maximum index density/ standard laboratory procedure which prevents bulking and
unit weight obtained, and comparable test results may not be minimizes particle segregation.
obtained when different size molds are used to test a given 3.1.1.4 maximum index void ratio, emax-the reference
soil. void ratio of a soil at the minimum index density/unit
1.8 This standard does not purport to address all of the weight.
safety problems, if any, associated with its use. It is the 3.1.1.5 given void ratio. e-the in situ or stated void ratio
responsibility of the user of this standard to establish appro- of a soil deposit or fill.
priate safety and health practices and determine the applica- 3.1.1.6 dry density/unit weight, Pd or 'Yd-the dry density/
bility of regulatory limitations prior to use. unit weight of a soil deposit or fill at the given void ratio.
3.1.1. 7 relative density, Dct-the ratio, expressed as a
2. Referenced Documents percentage, of the difference between the maximum index
void ratio and any given void ratio of a cohesionless,
2.1 ASTM Standards: free-draining soil; to the difference between its maximum
C 127 Test Method for Specific Gravity and Absorption of and minimum index void ratios. The equation is as follows:
Coarse Aggregate2
D 422 Method for Particle-Size Analysis of Soils3
D 653 Terminology Relating to Soil, Rock and Contained (I)
Fluids3
D 698 Test Method for Laboratory Compaction Charac- or, in terms of corresponding dry densities
teristics of Soil Using Standard Effort ( 12 400 ft-lbf/ft3
(600 kN-m/m3)) Dd = Pdma,(Pd - Pdmin) X lOO (2)
D 854 Test Method for Specific Gravity of Soils3 PiPdmax - Pdmin)

D 1557 Test Method for Laboratory Compaction Charac- in terms of corresponding or dry unit weights
teristics of Soil Using Modified Effort (56 000 ft-lbf/ft3
(2700 kN-m/m3)) _ 'Ydmax('Yd - 'Ydmin)
Dd - (3)
D 2166 Method for Laboratory Determination of Water 'Yd('Ydmax - 'Ydmin)
(Moisture) Content of Soil, Rock, and Soil-Aggregate 3.1.1.8 percent compaction or relative compaction.
Mixtures3 Re-the ratio, expressed as a percentage, of the dry density/
D 2487 Test Method for Classification of Soils for Engi- unit weight of a given soil to its maximum index density/unit
neering Purposes3 weight. The equation is:
D 2488 Practice for Description and Identification of Soils
(Visual-Manual Procedure)3
R c = _.!!.!!___ x 100 (4)
D 4254 Test Methods for Minimum Index Density of Soils
Pdmax
and Calculation of Relative Density3
or
04753 Specification for Evaluating, Selecting, and Speci-
fying Balances and Scales for Use in Soil and Rock 'Yd
Testing3 Rc=--X 100 (5)
E 11 Specification for Wire-Cloth Sieves for Testing 'Ydmax

Purposes4 3.1. l.9 density index, Id-the ratio, expressed as a per-


E 380 Practice for Use of the International System of centage, of the difference between any given dry density/unit
Units (SI) (the Modernized Metric System)4 weight and the minimum index density/unit weight of a
given cohesionless soil to the difference between its max-
3. Terminology imum and minimum index densities/unit weights. The
equation is:
3.1 Description of Terms Specific to This Standard:
3.1.1 Except as listed below, all definitions are in accor-
dance with Terminology D 653. Id = Pd - Pdmin X lOO (6)
Pdmax - Pdmin
3.1.1.1 maximum index density/unit weight, Pdmax or
'Yctmax-the reference dry density/unit weight of a soil in the or
densest state of compactness that can be attained using a
standard laboratory compaction procedure that minimizes _ 'Yd - 'Ydmin
Id- (7)
'Y dmax - 'Y dmin

2 Annual Book of ASTM Standards, Vol 04.02. 4. Summary of Test Methods


3 Annual Book of ASTM Standards, Vol 04.08.
4 Annual Book of ASTM Standards, Vol 14.02.
4.1 The maximum index density/unit weight of a given

2
�i D 4253

free-draining soil is determined by placing either oven-dried be used when the test results are to be applied in conjunction
or wet soil in a mold, applying a 2-lb/in. 2 ( 14-kPa) surcharge with design or special studies and there is not enough soil to
(dead weight) to the surface of the soil, and then vertically use the standard molds. Such test results should be applied
vibrating the mold, soil, and surcharge. Use either an with caution as maximum index densities/unit weights
electromagnetic, eccentric, or cam-driven vibrating table obtained with the special molds may not agree with those
having a sinusoid-like time-vertical displacement relation- that would be obtained using the standard molds.
ship at a double amplitude of vertical vibration (peak-
to-peak) of about 0.013 in. (0.33 mm) for 8 min at 60 Hz or 6. Apparatus
about 0.019 in. (0.48 mm) for 10 min at 50 Hz. The 6.1 Mold Assembly-An example of a typical mold as-
maximum index density/unit weight is calculated by di- sembly is shown in Fig. I. Individual components and
viding the oven-dried mass/weight of the densified soil by its accessories shall be as follows:
volume (average height of densified soil times area of mold). 6.1.1 Standard Molds-Cylindrical metal molds having
. 5. Significance and Use nominal volumes of 0.100 ft3 (2830 cm ') and 0.500 ft3
(14 200 cm3). The molds shall conform to the requirements
5.1 For many cohesionless, free-draining soils, the max-
shown in Fig. 2. The actual volume of the molds shall be
imum index density/unit weight is one of the key compo-
within ± 1.5 % of the specified nominal volume.
nents in evaluating the state of compactness of a given soil
6.1.2 Special Molds-Cylindrical metal molds having a
mass that is either naturally occurring or placed by man (fill).
S.1.1 Relative density and percent compaction are com- capacity less than 0.100 ft3 (2830 cm3), an inside diameter
equal to or greater than 23/4 in. (70 mm), but less than 4 in.
monly used for evaluating the state of compactness of a given
soil mass. Density/unit weight index is also sometimes used. ( 100 mm) and conforming to the design methodology
See Section 3 for descriptions of terms. presented in Fig. 3. Such molds may only be used when the
5.2 It is generally recognized that either relative density or test results are to be used in conjunction with design or other
percent compaction is a good indicator of the state of special studies or both, and there is not enough soil to use the
0.100 ft3 (2830 cm3) mold.
compactness of a given soil mass. However, the engineering 6.1.3 Guide Sleeves-One guide sleeve with clamp as-
properties, such as strength, compressibility, and perme-
ability of a given soil, compacted by various methods to a sembly, or. other suitable attachment devices [see Fig. 4(a)],
given state of compactness can vary considerably. Therefore, for each size mold. For easy centering of the guide sleeve
considerable engineering judgment must be used in relating above the mold, two of the three set screws on the clamp
the engineering properties of soil to the state of compactness. assembly should be provided with lock nuts.
5.3 An absolute maximum density/unit weight is not 6.1.4 Surcharge Base Plates-One surcharge base plate
necessarily obtained by these test methods. for each standard size mold, conforming to the requirements
of Fig. S.
NOTE 2-In addition, there are published data to indicate that these 6.1.S Surcharge Weights-One surcharge weight for each
test methods have a high degree of variability." However, the variability
size mold. See Fig. S for tolerances related to the 0.100 ft3
bt:
c�n greatly reduced by careful calibration of equipment, including the (2830 cm3) and 0.500 ft3 (14 200 cm3) molds. For special
vibrating table, and careful attention to proper test procedure and
technique. molds, similar tolerances should be maintained. The total
mass of the surcharge base plate and surcharge weight shall
5.4 The double amplitude of vertical vibration has been be equivalent to a surcharge pressure of 2.00 ± 0.02 lb/in.2
found to have a significant effect on the density obtained. 5 (13.8 ± 0.1 kPa) for the mold being used. For special molds,
For a particular vibrating table and mold assembly, the the surcharge weight can be composed of a single solid mass
maximum index density/unit weight ofa given material may of metal.
be obtained at a double amplitude of vibration other than 6.1.6 Surcharge Base-Plate Handle-A device used to
the double amplitude of0.013 ± 0.002 in. (0.33 ± 0.05 mm) initially place and then to remove the surcharge base plate
at a frequency of 60 Hz or 0.019 ± 0.003 in. (0.48 ± 0.08 upon completion of densification. An example of such a
mm) at SO Hz required in this method; that is, dry handle is given in Fig. 4(b); however, any convenient
density/unit weight may initially increase with increasing hooking device may be used.
double amplitude of vibration, reach a peak, and then 6.2 Dial-Indicator Gage Holder and Dial Indicator-A
decrease with further increases in double amplitude of device used, in conjunction with the guide brackets, to
vibration. Furthermore, the relationship between the peak
measure the difference in elevation between the top surfaces
density/unit weight and optimum double amplitude of
of the mold and surcharge base plate after densification [Fig.
vibration (double amplitude of vibration where peak density/
4(c)]. The dial indicator shall have a 2-in. (SO-mm) or greater
unit weight occurred) can vary with various soil types and
travel, with 0.00 I-in. (0.025-mm) graduations and mounted
gradations. For this reason, these methods allow the use of
so that the dial stem is parallel with the vertical axis of the
double amplitudes of vibration other than that described
mold. The dial indicator may be of the clockwise-movement
above, in special circumstances as provided in 11.1.6.3.
type where the dial pointer reads zero when the stem is
S.S The use of the standard molds (6.1.1) has been found
extended, or of the counterclockwise type where the dial
to be satisfactory for most soils requiring maximum index-
pointer reads zero when the stem is all the way in.
density /unit weight testing. Special molds (6.1.2) shall only
6.3 Balancets), of sufficient capacity to determine the
total mass of the specimen and mold, having sufficient
s E.T. Selig and R. S. Ladd, eds., Evaluation of Relative Density and its Role in accuracy that the mass of the soil is determined to the nearest
Geotechnical Projects Involving Cohesionless Soils, ASTM STP 523, ASTM, I 973. 0.1 %. Examples of balances capable of satisfying these

'
�I D 4253

Hoisting handle

Surcharge weight

Clomp assembly

��=,,-- Soil specimen

,'-.-�..,,.-- Guide brackets

Deck

f -16 UNC Drilled hole

FIG. 1 Schematic Drawing of a Typical Mold Assembly

requirements for most conditions have specifications as attached and rigidly supported during the test. The table
follows: shall be capable of vertically vibrating the mold assembly
6.3.1 For 0.500-ft3 (14 200-cm3) molds, use a balance with a sinusoid-like time-vertical displacement relationship
having a minimum capacity of 40-kg and meeting the at an average double amplitude (peak-to-peak displacement)
requirements of Specification D 4753 for Class GP 10. of 0.013 ± 0.002 in. (0.33 ± 0.05 mm) at a frequency of 60
6.3.2 For 0. IOO-ft3 (2830-cm3) molds, use a balance of at Hz or 0.019 ± 0.003 in. (0.48 ± 0.08 mm) at 50 Hz under
least 15-kg capacity and meeting the requirements of Speci- test conditions. The table shall have the capability for
fication D 4753 for Class GP 5. adjustment of the frequency of vibration (between O to 60
6.3.3 For special molds that are less than O. J-ft3 Hz) or double amplitude of vibration, or both, between
(2830-cm3}, use a balance having a minimum capacity of at about 0.005 in. (0.15 mm) and 0.013 in. (0.33 mm) at 60 Hz
least 2-kg and meeting the requirements of Specification or about 0.007 in. (0.20 mm) and 0.019 in. (0.48 mm) at 50
D 4753 for a Class GP 2. Hz for use with Test Methods IA, IB, 2A, or 2B (11.2.3).
6.4 Hoist-A rope, chain, or cable hoist of at least 140-kg The table shall have the capability for adjustment of the
capacity when either the 0.1 OO-ft3 (2830-cm3) or 0.500-ft3 double amplitude of vibration between about 0.008 in. (0.20
( 14 200 cm3) size molds are being used. mm) and 0.025 in. (0.64 mm) at 60 Hz or about 0.012 in.
6.5 Drying Oven, thermostatically controlled, preferably (0.30 mm) and 0.036 in. (0.91 mm) at 50 Hz for use in
of the forced-draft type, capable of maintaining a uniform conjunction with design or other special studies ( 11.1.6.3).
temperature of 110 ± 5°C throughout the drying chamber. 6.9.1 Use one of the following table types:
6.6 Sieves, 3-in. (75-mm), Jlh-in. (37.5-mm}, 3/4-in. ( 19- 6.9.1.1 Electromagnetic Vibrating Table-A steel table
mm), 3/s-in. (9.5-mm), No. 4 (4.75-mm}, and No. 200 conforming to the requirements of 6.9 with a vertically
(75-µm) sieves conforming to the requirements of Specifica- vibrating, cushioned steel deck generally about 30 by 30 in.
tions E 11. (760 by 760 mm), actuated by an electromagnetic vibrator of
6.7 Calibration Bar, metal, about 3 by 12 by 1/4 in. (75 by the solid-impact type with a net mass over 45 kg. The table
300 by 6 mm), optional (see 10.4). shall be mounted to a concrete floor or slab of mass weighing
6.8 Other equipment such as mixing pans, a large metal about 450 kg.
scoop, a hair-bristled dusting brush, a timing device indi- 6.9.1.2 Eccentric or Cam-Driven Vibrating Table, con-
cating minutes and seconds, a micrometer with at least a I forming to the requirements of 6.9. The mass required to
in. (25-mm) travel and with 0.001-in. (0.025-mm) gradua- support cam-driven tables and eliminate vibrations in other
tions, and a metal straight edge (for trimming excess soil after areas may be as large as 4500 kg.
it has been placed in the mold, if the minimum index Norn 4-See Footnote 5 (not Note 5) for examples of electromag-
density/unit weight by Test Methods D 4254 is being deter- netic and cam-driven vibratory tables.
mined).
6.9 Vibrating Table, shall be mounted to a concrete floor 7. Precautions
or mass of sufficient size and configuration that excess 7.1 Safety Precautions-Use of vibratory tables in certain
vibrations are not transmitted to other testing areas. The acoustic environments may produce noise levels above those
vertically vibrating deck of the table shall be of sufficient size considered acceptable. In areas where such conditions are
and rigidity that the mold assembly being used can be known to exist or where acoustic monitoring surveys have

4
--- .. ----------------------------

�� D 4253

+
lo
"
I 1� Dia. hole

= ......�.� -. ====�
Approx. i dia. c These handles cast on
� .so cu. ft. mold only
r-r--r-..---1-----.--,.--,

No1e 1-Tolerances are ±1/o• in. (±0.4 mm) unless otherwise noted.
Dimensions, in. (mm)
Size Mold
ft3 (cm3) A ( +0_005 in. ) B ( +0.005 in. )
-o.ooo -0.000 c D E F
0.100 (2830) 6.000 (152.4) 5_112 (155.2) 71/e (181.0) 61/2 (105.1) 112 (12.7) 11/e (28.6)

0.500 (14 200) 11.000 (279.4) 9.092 (230.9) 121/e (308.0) 9112 (241.3) 5/e (15.9) 2 (50-8)

FIG. 2 Details of Molds

not been conducted, suitable hearing protection devices shall sample and the grain-size distribution (gradation) of the
be used. In addition, testing personnel should also adhere to sample (see Table I).
any additional personal safety requirements in accordance 8.2.1 Using a visual method or Test Method D 422
with individual laboratory policies. (depending upon the complexity of the gradation of the
sample and operator experience}, determine the percentage
8. Sampling and Test Specimen of particles retained on the 3-in. (75-mm}, 11/i-in. (37.5-
mm}, 3/4-in. (19.0 mm), 3/s-in. (9.5-mm), No. 4 (4.75-mm),
8.1 Prior to testing, the sample should be stored in a
and No. 200 (75-µm) sieves.
manner to prevent freezing, contamination with other
8.2.2 The determination of the maximum index density/
matter, loss of soil, or loss of identification. unit weight should not be performed in accordance with this
8.2 The required size of the test specimen and mold is a test method unless the requirements of 1.5 are met. If these
function of the maximum particle size contained in the conditions are met, then the mold size and specimen mass

5
-
41 D 4253

Guide sleeve
Metric Equivalents
in. mm
1,8 3.2
�4 6.4
lt2 13
21'4 70

Clomp
assembly

Guide
brackets

c::
E

2}141 .
min min.

H=(0.7 to 1.3) times diameter


FIG. 3 Special Cylindrical Metal Molds

required can be determined according to the maximum mented aggregations; avoiding the reduction of the natural
particle size as prescribed in Table 1. size of the particles.
8.2.3 When it is applicable to use special molds, 100 % of
the sample shall pass the 3/4-in. (19 .0-mm) sieve and have less
than 10 % retained on the 3/s-in. (9.5-mm) sieve. 9. Preparation of Apparatus
8.2.3.1 The selected test specimen shall have a mass not 9. I For a mold assembly in which the alignment of the
less than that determined using the following equation: guide sleeve on top of the mold is controlled by the position
Mr = 0.0024 Vm of the set screws, assemble the guide sleeve on top of the
mold and tighten the clamp assemblies so that the inner wall
where:
of the sleeve is in line with the inner wall of the mold.
Mr = mass required in kg, and
Vm = volume of mold in cm 3. Tighten the lock nuts on the two set screws so equipped.
8.3 Select a representative specimen of soil that meets the Loosen the set screw having no lock nut and remove the
requirements of 8.2, using a splitter, riffle, or other method guide sleeve.
such as quartering. 9.2 Determine and record the mass of the empty mold,
8.4 If Test Methods IA or 2A are being performed, dry using the appropriate balance specified in 6.3.
the specimen in the drying oven, maintained at 110 ± 5°C to 9.3 Check that the vibrating table is in good working
a constant mass. It is often desirable to obtain the water condition and that parts are not loose or worn. Make any
content of the field sample. If this is the case, determine the necessary adjustments or repairs.
water content in accordance with Test Method D 2216. 9.4 Check that one set of initial dial readings is within
8.4.1 After drying, thoroughly break up the weakly ce- ±0.005 in. (0.15 mm) of the value obtained in 10.4, that is,

6
41 D 4253

f d Std. Notch for


machine bolt Ii f ting hook
Guide sleeve
See
� Rubber gasket

Cylindrical mold,
cost silicon
aluminum
Bevel 20• from
vertical
f - 16 NC x -r long
(a) (bl
Surcharge Bose Plate Handle
Typical Clomp Assembly for Guide Sleeve
for Guided Surcharge Weights. ( I Re qui red)

screws

Dial it),dicator g�ge


0.001 graduation
2" travel minimum
Gage stem

• <1)
a:,.,_
0
z

Col I ar 1" std steel pipe


used with o.50 cu ft mold

(c}
Holder for Dial Indicator Gage
NOTE 1- This piece shall be a steel bar, 1112 by 'h in. (38.1 by 12.7 mm) of a length necessary to produce the indicated dimension from the inside of the guide sleeve.
Weld three clamp assemblies to the guide sleeve at equal spacing.
NOTE 2- These dimensions must be changed to fit the dial gage indicator used.
NOTE 3-Tolerances are ±1/64 in. (±0.4 mm) unless otherwise noted.

Size Mold, ft3 (cm3) A, in. (mm) B, in. (mm) Guide Sleeve
0.100 (2830 cm3) 112 (12.7) 13/e (34.9) Steel tubing, 6 in. (150 mm) ID 1/• in. (6.4 mm) wall, 12 in. long (305 mm)

0.500 (14 200 cm3) •le (15.9) 11/2 (38.1) Steel pipe, 11 in. (280 mm) ID •lo in. (9.5 mm) wall, 8 in. (200 mm) long

FIG. 4 Details of Apparatus Components

the dial-gage zero has not been changed. As required, adjust difference between the volumes calculated from the two
the dial gage or reperform the calibration ( 10.4). Alterna- methods exceeds 0.5 % of the nominal value of the mold
tively, a reference bracket [similar to that shown in Fig. 6] being calibrated, then the calibration should be repeated.
may be used and, if required, adjust the dial gage to the Failure to obtain agreement between the two calibration
reference bracket reading. methods within the stated tolerances, even after several trials,
is an indication that the mold is badly deformed and should
10. Calibration be replaced. If both calibration methods are performed, the
10.1 The following calibrations of test apparatus should volume obtained by the water-filling method should be
be performed before initial use and at intervals not exceeding assigned to the mold (as this method more accurately reflects
each 1000 tests, or annually, whichever occurs first. the conditions over the entire mold).
10.2 Molds-Determine the volume of each mold by 10.2.1 Direct Measurement Method-The volume of the
either the direct-measurement method of the water-filling mold is calculated from the average of at least three internal
method as provided in 10.2.1 and 10.2.2. The volume diameter and three height measurements, evenly spaced
obtained by either method should be within ± 1.5 % of the throughout the mold, made to the nearest 0.00 I in. (0.025
nominal value. It is recommended that both the direct- mm). Calculate and record the height, in m or cm to three
measurement and water-filling methods be used. If the significant digits (in accordance with Practice E 380). Calcu-

7
4ITT}1 D 4253

Steel rod

I
l
I Lead filled to
specific weight

1"
,._�...L.�.L.4...L.,t.""""'i""""'i1"L--�..£....,f.�����-Saw cut 2
( at 4 places)
3 Alignment pins

== ;
(typical) equally � �--.--;::r
spaced '//////� �
Circular I
surcharge I
311
-16-NC, Ti3 Deep
11
bcseplcte
I. D val bottom drill

Nore 1-AII plates shall be 112-in. (12.7-mm) thick steel.


Nore 2- Top plates for weights may be torch-cut, but edges must be ground as smooth as practicable. Surcharge base plates must be machined to the specified
diameter.
Nore 3-Hoisting handles shall have the same shape as the surcharge base plate handle (see Fig. 4 (b)).
Size Mold, ft3 (cm3) o, in. (mm) H, in. (mm) Standard Pipe, in. (mm) Total Weight Required, lb (kg)
0.100 (2830) 5••!,a (151) 9.0 (230) 4.0 (100) 56.5 ± 0.5 (25.6 ± 0.2)

0.500 (14 200) 107/a (276) 6.0 (150) 10 (250) 190 ± 2 (86.2 ± 0.9)

FIG. 5 Circular Surcharge Weight and Base Plate

late and record the cross-sectional, Am, (m2 or cm2) and I 0.2.2.1 For mass measurements in grams, the calculated
volume, Vms (m3 or cm3) to four significant digits (in volume in cm3 is obtained by multiplying the mass of water,
accordance with Practice E 380). in grams, used to fill the mold by the unit volume of water,
10.2.2 Water-Filling Method-Completely fill the mold from Table 2.
with water. Slide a glass plate carefully over the top surface 10.2.2.2 If only the water-filling method is used to deter-
(rim) of the mold as to ensure that the mold is completely mine the volume of the mold, then the cross-sectional area of
filled with water. A thin film of grease or silicone lubricant the mold must be calculated by dividing its measured
on the rim of the mold will make a watertight joint between volume (l 0.2.2) by its measured height (l 0.2.1 ).
the glass plate and rim of the mold. Determine the mass and 10.3 Surcharge Base Plate-Calculate and record the
temperature of the water required to fill the mold. The average thickness of the surcharge base plate (Tp) to the
temperature should be determined to the nearest degree nearest 0.00 l in. (0.025 mm) from at least four measure-
Celsius. The mass of the water must be determined to at least ments using a vernier or micrometer caliper. Calculate and
the nearest 5 g for the 0.100 ft3 (2830 cm3) mold and to the record this thickness, TP in same units that dial gage is
nearest 50 g for the 0.500 ft3 (14 200 cm3) mold. From Table recorded.
2, obtain the unit volume of water in milliliters per gram at 10.4 Initial Dial Reading-This value may be obtained
the observed temperature. Calculate and record the volume using the calibration bar, as provided in 10.4.1 or without the
of the mold (m3 or cm3) to the appropriate number of bar, as provided in 10.4.2, if the contact area between the
significant digits as follows: mold guide bracket and the collar of the dial gage holder

8
...

41 D 4253

______ 1

20
.. J ----- �

40 I
TOP

4-}61 IF) Drill holes thru


5 010 • 820 cs

2-1.150 ! ::: Dia


drilled ho�s O O
thru "'"'

All material for bracket


to be .51 brass stock. Break al!. sharp edges
to a li chamfer

FACE

',--
)--

1.75
3.0
�"'7 Silver solder
/

RIGHT SIDE

FIG. 6 Dial Gauge Calibration Standard (Reference Bracket)

(Figs. 2 and 4) has been machined level or made level by the guide brackets and the holder. Obtain six dial indicator
use of brass inserts. readings, three on each the left and the right sides, and
10.4.1 Initial Dial Reading with Calibration Bar-Deter- average these six readings. To compute the initial dial
mine the thickness of the calibration bar to 0.001 in. (0.025 reading, Ri, for clockwise-reading dial indicators, subtract the
mm) using a micrometer. Place the calibration bar across a thickness of the calibration bar from the average of the six
diameter of the mold along the axis of the guide brackets. dial indicator readings. To compute counterclockwise-
Insert the dial-indicator gage holder in each of the guide reading dial indicators, Rj, add the thickness of the calibra-
brackets on the mold with the dial gage stem on top of the tion bar to the average of the six dial indicator readings.
calibration bar and on the axis of the guide brackets. The dial 10.4.2 Initial Dial Reading Without Calibration Bar-
gage holder should be placed in the same position in the Insert the dial indicator gage holder in each of the guide
guide brackets each time by means of matchmarks on the brackets with the dial gage stem in contact with the rim of

9
�fill, D 4253

TABLE 2 Volume of Water per Gram Based on TemperatureA NOTE 5-If the minimum index density/unit weight is also being
Temperature
performed, the soil shall be placed in accordance with the appropriate
Volume of Water, mL/g method specified in Test Methods D 4254. The mass of the mold plus
•c "F soil shall also be determined and recorded.
12 53.6 1.00048
14 57.2 1.00073 J 1.1.3 Place the appropriate surcharge base plate on the
16 60.8 1.00103 surface of the soil and twist it slightly several times so that it
18 64.4 1.00138 is firmly and uniformly in contact with the surface of the
20 68.0 1.00177
1.00221
soil. Remove the surcharge base-plate handle.
22 71.6
24 75.2 1.00268 11.1.4 Attach the mold to the vibrating table.
26 78.8 1.00320 11.1.5 Firmly attach the guide sleeve to the mold and
28 82.4 1.00375 lower the appropriate surcharge weight onto the surcharge
30 86.0 1.00435
32 89.6 1.00497 base plate.
11.1.6 Setting for double amplitude of vibration.
A Values other than shown may be obtained by referring to the Handbook of
Chemistry & Physics. Chemical Rubber Publishing Co., Cleveland, Ohio. 11.1.6.1 Test Method IA-Set the vibrator control
(rheostat) at the setting determined in 10.� for the m_old
assembly being used to obtain a double amplitude of vertical
the mold (at its center) on both sides of the guide brack:ts.
vibration ofO.O 13 ± 0.002 in. (0.33 ± 0.05 mm) at 60 Hz or
Obtain six sets of dial indicator readings, three on each side
0.019 ± 0.003 in. (0.48 ± 0.08 mm) at 50 Hz.
of each guide bracket. The average of these twelve readings is
the initial dial gage reading, R;. 11.1.6.2 Test Method 2A-Set the eccentric or cam at the
setting determined in 10.5 for the mold assembly being used
I 0.5 Vibrating Table-The calibration shall consist of
to obtain a double amplitude of vertical vibration of 0.013 ±
determining, under simulated test conditions and_ for each
mold size being used, the required rheostat, eccentnc, or cam 0.002 in. (0.33 ± 0.05 mm) at 60 Hz or 0.019 ± 0.003 in.
(0.48 ± 0.08 mm) at 50 Hz.
setting for the electro-magnetic, eccentric, or cam-drive?
11.1.6.3 As stated in 4.4, there is a relationship between
table, respectively, such that the mold has a double ampli-
density/unit weight and double amplitude of vibration, and
tude of vertical vibration of 0.013 ± 0.002 in. (0.33 ± 0.05
mm) at 60 Hz or 0.019 ± 0.003 in. (0.48 ± 0.08 mm) at 50 the peak density/unit weight occurs at an optimum double
Hz The double amplitude of vibration should be measured amplitude of vibration which may not be the same as the
on. the mold to the nearest 0.0005 in. (0.015 mm). It is maximum index density/unit weight obtained at the double
recommended that during each calibration a relationship amplitude of vibration prescribed in 11. I .6.1 and 11. � .6.2.
between the double amplitude of vertical vibration versus the Therefore, this method allows the use of a double amplitude
of vertical vibration other than those prescribed in 11.1.6.1
rheostat, eccentric, or cam setting be establis�ed.
or 11.1.6.2 if the following conditions are met:
10.5.1 While there are many different equipment config-
(a) Test results are to be used in conjunction with design
urations that can be used to measure this double amplitude
of vibration, it is not easily measured unless one has or special studies or both, and
considerable experience. Typical calibration procedure and (b) The double amplitude of vertical. vibration u_sed
equipment requirements have been given in the Geotechnical should be: (a) the optimum double amplitude of vertical
Testing Journal.6 vibration (see the Appendix for a recommended method to
10.5.2 In addition to the calibration frequency recom- obtain the optimum double amplitude of vibration), (b) less
mended in I 0.1 the vibrating table should also be calibrated than 0.025 in. (0.64 mm) at 60 Hz or 0.037 in. (0.94 mm) at
before reuse after any event (including repairs) which might 50 Hz, and (c) greater than 0.008 in. (0.20 mm� at 60 Hz or
affect its operation and whenever the test results are ques- 0.012 in. (0.30 mm) at 50 Hz (except when filling the mold
tionable. for the wet method, 11.2.3). In terms of nominal peak
acceleration, these values are greater than about 1.5 g (14
m/s2) and less than about 4.8 g (45 m/s2).
11. Procedure NOTE 6-The nominal peak acceleration can be calculated using the
I I.I Dry Method-Test Methods IA or 2A. following equation:
11.1.1 Mix the oven-dried sample to provide an even AP= 0.0511(2Y)F2
distribution of particle sizes; that is, having as little segrega- where:
tion as possible. A = nominal peak acceleration in g,
J l .1.2 Fill the mold with soil and level the surface of the 2Y = double amplitude of vertical vibration in inches, and
soil using methods that minimize segregation. A s�O?P or F p = frequency in cycles per second, Hz.
pouring device (funnel) should be used to place the_ soil in !he 11.1. 7 Vibrate the mold assembly and specimen for 8 ±
mold. The sides of the mold may be struck a few times using I/4 min at 60 ± 2 Hz or for 12 ± 1/4 min at 50 ± 2 Hz.
a metal bar, rubber hammer, or similar item to settle the soil Remove the surcharge weight and guide sleeve from the
so that the surcharge base plate can be easily placed into mold. Check that the surcharge base plate is firmly and
position and there is no surge of air from the mold when uniformly in contact with the surface of the soil; that is, does
vibration is initiated. not wobble when pressed at the edges. If it wobbles, this
should be noted on the report form (data sheet).
6 Kaufman, L. P., Strickland, E. A., and Benavidez, A. A., "Suggested Method
11.1.8 To obtain and record dial indicator gage readings
for the Calibration of Vibrating Tables for Maximum Index Density Testing," on opposite sides of the surcharge base plate place the
Geotechnica/ Testing Journal, GTJODJ, Vol 2, No. 3, Sept. 1979, pp. 152-157. indicator gage holder in each of the guide brackets. Brush

JO
�I D 4253

aside any fines that might have collected on the surcharge TABLE 3 Dial Reading Conversion Factors for Volume
base plate where these readings will be taken. Calculations
11.1.9 Remove the surcharge base plate from the mold Factor
and detach the mold from the vibratory table. During this Dial Reading Units
Volume Requirements
step, prevent (as much as possible) any fines that have mm in.
collected on the surfaces of the surcharge base plate and the m3 6.102 x 10•
106
rim of the mold from entering the mold. If the mass of these cm3 103 0.06102
fines is greater than about 0.2 % of the total mass of the
specimen, determine the mass and note it on the report form
(data sheet). using means which prevent, as much as possible, the removal
11. J .10 Determine and record the mass of the mold and of soil.
soil using a balance meeting the requirements of 6.3: To 11.2.4 Assemble the surcharge base plate, surcharge
calculate and record the mass of the soil filling the mold weight, and guide sleeve as specified in 11.1.3 and 11.1.5.
subtract the mass of the empty mold from the mass of the 11.2.5 Vibrate the mold assembly and specimen as speci-
mold and soil. Alternately, the contents of the mold may be fied in 11.1.6 through 11.1. 7. After the vibration period,
emptied into a pan and weighed. Calculate the maximum- remove the surcharge weight and guide sleeve from the mold.
index density/unit weight, Pdmax, in accordance with Sec- Remove any free water appearing above, on, and around the
tion 12. surcharge base plate.
11.1.11 Steps 11.1.1 through 11.1.10 should be repeated 11.2.6 Obtain and record dial indicator-gage readings in
until consistent values of maximum index density/unit accordance with 11.1.8.
weight (preferably within 2 % ) are obtained. If excessive 11.2. 7 Remove the surcharge base plate and detach the
degradation (particle breakdown) of the soil is suspected, a mold from the vibratory table in accordance with 11.1.9. If a
sufficient quantity of representative soil sample should be determination of the specimen water content is desired,
provided (if possible), so that a single test specimen is not determine and record the mass of the mold and soil.
repeatedly subjected to step 11.1. 7. Carefully remove the entire wet specimen from the mold,
11.2 Wet Method-Test Methods IB or 2B. placing it in a pan of known mass for oven drying. Wash all
11.2.1 The wet method may be conducted on oven-dried particles clinging to the inside of the mold and bottom of the
soil to which sufficient water is added or, if preferred, on wet base plate into the plan. Dry the specimen in a drying oven,
soil from the field. Mix the sample to provide an even maintained at 110 ± 5°C to a constant mass (Test Method
distribution of particle sizes and water content with as little D 2216). Determine and record its oven-dried mass, using a
segregation as possible. If water is added to dry soil, allow a balance meeting the requirements of 6.3.
minimum soaking period of about 1h h. The amount of
water added should be sufficient enough that free water does 12. Calculation
not accumulate in the mixing pan, and the specimen will 12.1 Calculate the maximum dry density of the test
become basically saturated during the densification process. specimen as follows:
Pdmax = MJV
NOTE 7-The following equation can be used to estimate the amount
of water required to be added to an oven-dried soil or, initially, try about where:
1000 mL for every 4.5 kg of soil. Pdmax = dry maximum index density of the specimen,
mg/m3 or g/cm3
Ms = mass of dry specimen, mg or g and
V = volume of specimen, m3 or cm3
where: V = Ve - Ac (H) X Factor (see Table 3), m3 or cm3
Mw = mass of water in grams, Ve = calibrated volume of mold m3 or cm3 and
Pd = estimated dry density after initial placement in mold Ac = calibrated cross sectional area of mold, m2 or cm2
in mg/m3. This typically ranges between 1.6 and 1.9 and
mg/m3• H = R; - R, + TP for clockwise-reading dial indicators or
Ms = mass of test specimen in grams, H = R; - R, + TP for counterclockwise-reading dial
Pw = density of water, I mg/m3, and indicators
G. = specific gravity of soil. R; = initial dial gage reading mm or in.
11.2.2 Attach the mold to the vibrating table. R, = average of final dial gage readings on opposite sides
11.2.3 With the vibrating table turned on, slowly fill the of the surcharge base plate after completion of the
mold with wet soil using a scoop or shovel. After each vibration period, mm or in., and
increment of soil is added, inspect to see if a small amount of = thickness of surcharge base plate, mm or in.
TP
free water has accumulated on the soil surface. If not, add a 12.1.1 Calculate the dry maximum index unit weight of
sufficient amount of water by squeezing from a sponge, the specimen as follows:
pouring from a small container, or by other means. During
this process, which is to take 5 to 6 minutes, the double 'Ydmax = 9.807 X Pdmax• kN/m3 or 62.43 X Pdmax• lbf/ft3
amplitude or the frequency or both, of vibration must be where:
adjusted to prevent excessive boiling and fluffing of the soil. 'Ydmax= dry maximum index unit weight, kN/m3 or lbf/ft3
During and just after the final minute of vibration, any water 9.807 = conversion factor, mg/m3 or g/cm3 to kN/m3, and
appearing above the surface of the soil should be removed 62.43 = conversion, mg/m3 or g/cm3 to lbf/ft3•

11
�t O 4253

12.1.2 Calculate the average maximum index density/unit different from that specified in 11.1.6.1 or 11.1.6.2.
weight from the trials of the dry method which agree within 13.1.5 The maximum index density, Pdmax, mg/m3 or
2 %. This value is to be reported as the maximum-index g/cm3 to three significant digits (in accordance with Practice
density /unit weight unless it is established that the wet E 380) or maximum/index unit weight, 'Ydmax in lbf/ft3
method produces a maximum-index density/unit weight (kN/m3).
higher than the dry method, which would significantly affect 13.1.6 Any abnormalities such as loss of material, segre-
the use of application and of the maximum-index density/ gation, excessive tilting of base plate, and the like.
unit weight in which case the result of the wet method should
be used. 14. Precision and Bias
12.2 Calculate the minimum-index void ratio, emin• as 14.1 Criteria for judging the acceptability of maximum-
follows: index density/unit weight test results are given in Table 4.
emm. = PwGavg _ I
s2 = _I_ iN1 (x - x)2
N-1
where:
14.1.1 Variations Between Laboratories (Variability):
Pw = density of water equal to mg/m3, and 14.1.1.1 The standard deviation, S, is calculated from the
Gavg = weighed average specific gravity of soils composed of equation:
particles larger and smaller than the No. 4 (4.75- where:
mm) sieve,
N= number of determinations,
x = individual value of each determination, and
G =----- x = numerical average of the determinations.
avg R, Pi 14.1.2 Variations Between Duplicate Tests (Reproduc-
--+-- ibility):
IOOG, IOOG2 14.1.2.1 The combined standard deviation, S', is calcu-
G1 = apparent specific gravity of the soil particles retained lated from the equation:
on the No. 4 (4.75-mm) sieve as determined by Test I
Method C 127, S2 = - i D2
2K
G2 = specific gravity of the soil particles passing the No. 4 where:
(4.75-mm) sieve as determined by Test Method D 854, D = difference between duplicate tests, and
R 1 = percentage of soil particles from the sample retained K = number of pairs of duplicate tests.
on the No. 4 (4.75-mm) sieve, and
P1 = percentage of soil particles from the sampling passing 15. Keywords
the No. 4 (4.75-mm) sieve and Pdmax is in units of
15.1 maximum index density; maximum index unit
mg/m3 or g/cm3•
12.3 If the minimum index density/unit weight, Pdmin or weight; relative density; vibrating table
'Ydmin• has been determined in accordance with Test Methods
D 4254; and the soil deposit or fill dry density/unit weight, Pd TABLE 4 Precision of Maximum-Index Density/Unit Weight Tests
Results A
or 'Yd, or void ratio, e, is known, the relative density, Dd, can
be calculated as: Standard Deviation
Combined Standard Acceptable
Deviation, S' Range of Two
_ Pdmax(Pd - Pdmin) Results
Dd - x IOO , or Unit Unit Expressed as
Pd(Pdmax - Pdmin) Density Density
Weight Weight Percent of
(mg/m3) (mg/m3)
'Ydmax('yd - 'Ydmin) (lb/ft3) (lb/ft3) Mean Values
Dd = or Multilaboratory
'Yi 'Y dmax - 'Y dmin) precision
e -e fine to medium 2.4 0.038 8.3
Dd = max X 100 sands
emax - emin gravelly sands 4.5 0.072 13.0
Single operator
13. Report precision:
fine to medium 0.8 0.013 2.7
13.1 The report shall include the following information: sands
13.1.1 Origin of material used in text. gravelly sands 1.4 0.022 4.1
13.1.2 Description of appearance of test specimen, based A All values shown in this table are based on average test results on a limited
on Practice D 2488 (Test Method D 2487 may be used as an variety of different soils (Footnote 5) and are subject to future revision.
alternative). 8
This column indicates a limiting range of values that shall not be exceeded by
13.1.3 The Test Methods (IA, lB, 2A, or 28) and size of the difference between any two results, expressed as a percentage of the average
value. Approximately 95 % of the test results from the cooperative test programs
mold used. do not exceed the limiting acceptable ranges shown (assuming normally distrib-
13.1.4 Double amplitude of vertical vibration used if uted data).

12
�I D 4253

APPENDIX

(Nonmandatory Information)

XI. RECOMMENDED METHOD TO OBTAIN THE OPTIMUM DOUBLE AMPLITUDE OF VIBRATION


X 1.1 To reduce testing problems, the dry method (Test indicated in Table XI or between those already tried shall be
Method A) should be used. The size of mold used should be used.
in accordance with 8.2. X 1.5 From the data obtained in X 1.4, plot the dry
X 1.2 For the mold size and vibrating table being used, density/unit weight values as ordinates with corresponding
establish the relationship between the double amplitude of double amplitude of vibration values as abscissas. Draw a
vertical vibration of the mold assembly, and the rheostat, smooth curve connecting the plotted points. The double
eccentric, or cam setting under simulated test conditions. amplitude of vibration corresponding to the peak of this
X 1.3 Select between four and six test specimens from the curve is termed the optimum double amplitude of vibration,
sample using a splitter, riffie, or other method, such as while the peak dry density/unit weight is termed the op-
quartering, and dry each specimen. An unused portion of timum index density/unit weight.
material shall be used for each trial to eliminate any X 1.6 For soils susceptible to degradation, the optimum
cumulative degradation effects of the soil. index density/unit weight may not be clearly defined, that is,
Xl.4 Using the procedure outlined in Section 11 (except density/unit weight may continue to increase with increasing
for 11.1.6) perform about four trials with the double ampli-
double amplitude of vibration beyond a reasonable value of
tude of vibration varying between about 0.008 in. (0.2 mm)
0.025 in. (0.64 mm) at 60 Hz or 0.037 in. (0.93 mm) at 50
and 0.025 in. (0.64 mm) for 60 Hz. See Table X 1 for a
Hz. For this case, a selected optimum double amplitude
typical set of double amplitude of vibration values which
value ofO.O 15 in. (0.38 mm) at 60 Hz or 0.022 in. (0.56 mm)
may be used. If a peak dry density/unit weight is not clearly
defined (see X 1.5) then additional trials using other values as at 50 Hz shall be used.

TABLE X1.1 Typical Set of Double Amplitude of Vibration Values


Frequency of
Double Amplitude of Vibration, in. (mm)
Vibration
50 Hz 0.012 (0.30) 0.017 (0.43) 0.022 (0.56) 0.026A (0.66) 0.030A (0. 76) 0.036 .. (0.91)
60 Hz 0.008 (0.20) 0.012 (0.30) 0.015 (0.38) O.D18 (0.46) 0.021 (0.53) 0.025 .. (0.64)
A For some electromagnetic tables, double amplitudes of vibration of 0.025 in. (0.64 mm) and above may be harmful to the electromagnets. This can be checked by
inserting a strip of paper between the electromagnets in accordance with the manufacturer's instructions.

The American Society tor Testing and Materials takes no position respecting the validity of any patent rights asserted in connection
with any item mentioned in this standard. Users of this standard are expressly advised that determination of the validity of any such
patent rights, and the risk of infringement of such rights, are entirely their own responsibility.

This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years and
if not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standards
and should be addressed to ASTM Headquarters. Your comments will receive careful consideration at a meeting of the responsible
technical committee, which you may attend. It you feel that your comments have not received a fair hearing you should make your
views known to the ASTM Committee on Standards, 1916 Race St., Philadelphia, PA 19103.

13

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