Professional Documents
Culture Documents
PROCESS
Karen M. B. Taminger and Robert A. Hafley
NASA Langley Research Center, Hampton, VA
Proceedings of the 3rd Annual Automotive Composites Conference, September 9-10, 2003, Troy, MI. Society of Plastics
Engineers (2003).
provide better opportunity for optimization of designs by Direct laser deposition, one of the most mature of the SFF
allowing more time for determining details. processes, was introduced around 1991 and has been the
focus of extensive research activity at many institutions. A
SFF also offers the potential for improved performance laser beam, typically either CO2 or Nd:YAG, is used to
through control of microstructures and compositions at a create a small molten pool on a metallic substrate in an
much finer scale than parts machined from thick products. inert atmosphere. Metallic powder is fed into the molten
Typical thick sections have high degrees of microstructural pool to build up a part, resulting in fully dense, structural
inhomogeneity, leading to anisotropic mechanical parts directly produced from CAD models without molds,
properties. This is a direct result of differences in cooling tooling, or machining (except for some finish machining to
rates and an inability to impart work evenly through a thick get final tolerances and surface finishes). Feedstock
section. Working with smaller billets in conjunction with material is usually pre-alloyed powder, although elemental
layer-additive processes can result in more optimal powder blends are also used. This process results in near
microstructural features, potentially improving the net shaped parts with fine grained microstructures due to
mechanical properties of the resultant part as compared to rapid solidification kinetics and a small melt pool. [1, 5]
a similar part machined from a thick section billet. Finally,
compositional gradients offer improved performance and Most commercial laser based systems have limited size
reduced cost by allowing grading from an inexpensive build envelopes and operate at low deposition rates,
material for the bulk of the product to an expensive limiting application on large parts. Typically, these
material at the surface for enhanced wear resistance, processes use a tightly (approximately 0.05 cm (0.02 inch)
corrosion resistance, etc. diameter) focused beam which enables fine details to be
fabricated. However, there is a tradeoff between feature
Solid Freeform Fabrication Processes size and deposition rate, with fine feature size resulting in
low deposition rates (8 to 33 cm3/hr (0.5 to 2 in3/hr) and
Rapid prototyping is an emerging field which encompasses low powder capture efficiencies, typically less than 50%.
numerous different techniques and resulting product forms. Energy efficiency of laser processes tends to be low; less
Of specific interest are processes that are capable of than 10% of the input energy is converted to beam energy,
producing fully dense metallic and hybrid parts in which and much of the beam energy may be reflected from the
the resulting parts may be used for loaded structure. part (up to 98% in the case of highly reflective materials
Binderless processes are attractive because they eliminate such as aluminum and copper). Diode laser based systems
contaminants and minimize secondary processing. Layer have improved energy efficiencies approaching 40% but
additive techniques offer the potential for graded still exhibit the same reflectance losses as other lasers. [1]
microstructures and compositions, and production of near-
net shapes with minimal secondary processing required.
Electron Beam Deposition
Over the past several years, a number of SFF processes
Electron beam freeform fabrication (EBF3) is an emerging
have been developed to directly produce structural metallic
cross-cutting technology for producing structural metal
parts. Several processes such as Selective Laser Sintering
parts. The process can be used to build a complex,
(SLS) and Electron Beam Melting (EBM) operate in a
unitized part in a layer-additive fashion, although the more
powder bed, tracing the part in a layer of powder with a
immediate payoff is for use as a manufacturing process for
high energy beam and repeating for subsequent layers. [1,
adding details to components fabricated from simplified
2] These processes may require secondary processing to
castings and forgings or plate products. Figure 1 shows a
produce fully-dense components. Other emerging SFF
schematic of the primary elements of an EBF3 system.
processes that focus on low heat inputs include Precision
EBF3 employs a high power electron beam in a vacuum
Metal Deposition (PMD), laser deposition with flat wire
environment (1x10-4 torr or lower). Wire feedstock is used
[3], and ultrasonic consolidation (UC) of layered metal
foils to form 3-D parts using ultrasonic welding, a solid
state process. [4] Direct laser deposition processes, Wire feed Electron beam gun
including Direct Metal Deposition (DMD), Laser Additive
Manufacturing (LAM) and Laser Engineered Net Shaping
(LENS™), feed powder directly into a molten pool created
Electron beam
by a laser. [1, 5] Electron beam freeform fabrication
Deposit
(EBF3) is another recently developed process, similar to
direct laser deposition but employing a focused electron
beam and wire feedstock. [6, 7, 8] Many of these
processes are complementary and selection of the
Substrate
appropriate process is dependent upon the desired
applications.
Figure 1. Schematic of the EBF3 process.
Proceedings of the 3rd Annual Automotive Composites Conference, September 9-10, 2003, Troy, MI. Society of Plastics
Engineers (2003).
due to difficulties feeding powder in a vacuum, since the A fundamental examination of the effect of processing
carrier gas used to assist powder delivery will be ionized in parameters (translation speed and wire feed rate) for 2219
the electron beam. Operation in a vacuum ensures a clean Al was conducted to establish some basic processing-
process environment and eliminates the need for a microstructure-mechanical property relationships. In this
consumable shield gas, as is typically used in laser work, one of these two variables was continuously
deposition systems. The EBF3 process is nearly 100% changed, while the beam power and the other variable were
efficient in feedstock consumption and approaches 95% held constant. The resulting deposit dimensions,
efficiency in power usage. The electron beam couples well microstructures, and tensile properties were documented.
with any electrically conductive material, including highly Over the range of parameters tested, microstructures varied
reflective alloys, such as aluminum and copper. A variety from a fine-grain equiaxed grain structure to a
of weldable alloys can be processed using EBF3; further solidification microstructure with larger grain sizes and
development is required to determine if non-weldable dendritic grown, as shown in Figure 2. This shows the
alloys can also be deposited. Demonstrated deposition rates range of microstructures obtained over a wide processing
for EBF3 are 330 to 2500 cm3/hr (20 to 150 in3/hr), with envelope. The light bands are dendrites formed in the
lower resolution in the ability to build fine details. interpass region where portions of a previously deposited
Experiments are planned with fine diameter wires to layer remelted during deposition of the following layer.
attempt to construct fine details and large diameter wires to
increase deposition rate. EBF3 offers viable solutions to Increasing translation speed resulted in a decrease in both
issues of deposition rate, process efficiency, and material width and height of the deposited layer. Higher translation
compatibility for insertion into the production speed produced more rapid cooling and resulted in a
environment. homogeneous microstructure with smaller equiaxed grains
(see Figure 2). Increasing the wire feed rate resulted in a
Recent work with the EBF3 system at NASA Langley narrowing of the deposit width and an increase in the
Research Center has focused on understanding the process deposit height. At higher wire feed rates, the cooling rate
and characterizing the resulting microstructures and increased providing a smaller equiaxed grain structure with
mechanical properties to optimize the process for 2219 Al good homogeneity and no evidence of dendrite growth in
and Ti-6-4. Aluminum alloy 2219, which has a nominal the interpass region as compared to the microstructure
composition of Al-6 wt % Cu, is a common aerospace developed at the lower wire feed rate. [7]
alloy with excellent weldability and good strength and
toughness. Ti-6Al-4V is also commonly used in aerospace Figure 3 shows the ultimate tensile strength, 0.2% offset
structures for high temperature applications and where its yield strength, and total elongation to failure for EBF3
excellent strength and corrosion resistance are required. 2219 Al deposits as compared to typical handbook data for
Extensive work has been done with Ti-6-4 in the laser sheet and plate products. [9] The data for the as-deposited
deposition arena, providing a baseline for comparison with 2219 Al were averaged over duplicate tests for seven
the EBF3 process. combinations of beam power, translation speed, and wire
feed rate. Despite the wide range of processing conditions,
Figure 2. Microstructures of EBF3 2219 Al deposits showing range of microstructures achievable: (a) low translation speed
results in inhomogeneous microstructure and larger grains, and (b) higher translation speed produces more homogeneous
microstructure with smaller equiaxed grains. [7]
Proceedings of the 3rd Annual Automotive Composites Conference, September 9-10, 2003, Troy, MI. Society of Plastics
Engineers (2003).
450
2219 - O typical
400 As-deposited
2219 - T4 typical
Deposit+T62
350
2219 - T62 typical
300
Strength (MPa)
250 25
200 20
Elongation (%)
150 15
100 10
50 5
0 0
Yield Ultimate Elongation
Figure 3. Tensile properties at room temperature of EBF3 deposited 2219 Al as compared to typical handbook values for
2219 Al sheet and plate. [9]
the majority of the as-deposited 2219 Al data fell in a Similar work is now underway with Ti-6-4. The Ti-6-4
tight band, as shown by the range bars in Figure 3. The microstructure comprises extremely large columnar grains
properties of as-deposited 2219 Al were intermediate to growing epitaxially from the substrate, as shown in Figure
those for annealed (O temper) and solutionized and 4a. At higher magnification, as shown in Figure 4b,
naturally aged (T4 temper) 2219 Al sheet and plate. The alpha-beta laths typical of the microstructures of
2219 Al deposits that were heat treated to the T62 temper alpha+beta titanium alloys can be seen. Brice and
also had a very tight data range and were equivalent to coworkers [8] have also researched Ti-6-4 EBF3
typical handbook properties for 2219-T62 sheet and plate deposition with similar results; the room temperature
product. [7, 9] tensile properties of Ti-6-4 deposits were comparable to
(a) (b)
Figure 4. Microstructures of EBF3 Ti-6-4 deposits showing range of microstructures achievable: (a) low magnification shows
columnar grain structure, and (b) high magnification shows alpha-beta laths.
Proceedings of the 3rd Annual Automotive Composites Conference, September 9-10, 2003, Troy, MI. Society of Plastics
Engineers (2003).
or better than properties for wrought products. They also
reported that a Ti-6-4 F-22 AMAD bracket produced by All parts built to date have been near-net shape, requiring
EBF3 successfully completed a two lifetime broad a final finishing step to obtain final surface finish and
spectrum fatigue test with adequate residual tensile contour. Four identical pylons were finished using a
strength. [8] variety of techniques and compared to an as-built pylon to
demonstrate the ability to perform finishing operations.
In addition to processing-microstructure-property The 2219 Al EBF3 parts were successfully finished using
correlation, process programmability and control are conventional milling, wire electric discharge machining
currently being explored. Several 2219 Al parts (EDM), glass bead blasting, and electron beam glazing.
demonstrating different deposition schemes are shown in The as-built EBF3 part had good localized surface finish
Figure 5. Low and high deposition rates have been (smoothness) but larger long range surface irregularity
achieved, ranging from rates of 160 cm3/hr to 1300 cm3/hr (waviness) and mild tensile residual stresses.
(10 in3/hr to 80 in3/hr), with a change in deposit width Machinability of the EBF3 parts was comparable to
from 0.25 cm to 1.25 cm (0.1 to 0.5 inches) for the low standard wrought product for both the milling and wire
and high deposition rates, respectively. The cylinder in EDM processes. Milling resulted in the best surface
Figure 5a shows an EBF3 part built using a high finish over long and short ranges and induced
deposition rate. The square box in Figure 5b compressive residual stresses. Wire EDM induced high
demonstrates the ability to change the motion vector of compressive residual stresses in the EBF3 2219 Al, but the
the part without a corresponding change to the wire feed surface finish required additional work to achieve
orientation so that the entry point of the wire varies from adequate smoothness. Bead blasting was not aggressive
the leading edge to the side or trailing edge of the molten enough to eliminate EBF3 surface features, but succeeded
pool. This had very little impact on the deposit except for in inducing compressive residual stresses. Electron beam
a slight pushing of the puddle by the entering wire. This glazing (using a defocused electron beam with the same
flexibility is significant because it enables simplified EBF3 equipment) produced a flat surface with fine-
programming and construction of detailed parts. The grained equiaxed microstructure at the surface, but did not
airfoil-shaped pylon in Figure 5c demonstrates an ability significantly change the residual stress state of the as-built
to program and build a part with more complex curvature part. These experiments demonstrated that EBF3 parts
than the other round or square shapes built. The vase- can be finished using conventional machining operations.
shaped part shown in Figure 5d demonstrates the ability In addition, electron beam glazing is promising for
to build an unsupported overhang (50 degrees on the part production of net shaped parts using EBF3 and secondary
shown) in either an expanding or contracting wall. processing in the same equipment.
Finally, a mixer in Figure 5e has been built to show
transition from a circular part to a fluted edge.
(a) (b)
5 cm
10 cm
8 cm
20 cm
10 cm
Figure 5. 2219 Al shapes built using EBF3 demonstrate different deposition schemes: (a) high deposition rate, (b) varied wire
feed angle, (c) complex curvature, (d) unsupported overhangs, and (e) transition from one geometry to another.
Proceedings of the 3rd Annual Automotive Composites Conference, September 9-10, 2003, Troy, MI. Society of Plastics
Engineers (2003).
Future Plans titanium alloys have demonstrated the potential for
achieving a wide microstructural range with properties
Researchers at NASA Langley Research Center are comparable to those of wrought product forms. EBF3
developing the EBF3 process for manufacture and repair offers viable solutions to issues of deposition rate, process
of aerospace structures. Materials of interest include efficiency, and material compatibility for insertion into
aluminum alloys for subsonic aircraft and spacecraft, and the production environment. Although further process
titanium alloys, nickel-based alloys, titanium aluminides, development and understanding is required, no barriers
and metal matrix composites (including titanium matrix are evident to prevent the maturation of EBF3 into a
composites) for hot structures and launch vehicles. In competitive commercial process.
addition, we have interest in high strength steels such as
Vascomax and 15-5 PH for production of wind tunnel References
models.
[1] Sears, J.W., “Direct Laser Powder Deposition –
Future efforts will concentrate on understanding and ‘State of the Art’,” KAPL Report No. KAPL-P-
improving various aspects of the EBF3 process. Closed 000311, (1999).
loop control and modeling of the process are important to [2] “Electron Beams: Useful for More than Just
ensure high quality and repeatability for certification of Microscopes,” European Tool and Mouldmaking,
the process for applications on primary or secondary March/April 2002, http://www.tool-
aerospace structures. A deeper understanding of the moldmaking.com/magazine/magdetail.php?company
processing-microstructure-property relationships is =2355&x=11&y=15, accessed 3 July 2003.
necessary to support this development for continued [3] Rabinovich, J., “Net Shape Manufacturing With
process refinement. Process techniques will be developed Metal Alloys,” Advanced Materials & Processes,
to enable building parts with complex geometry, 161:1, 47 & 86, (2003).
improved surface quality, and minimized residual [4] White, D.R., “Ultrasonic Consolidation of Aluminum
stresses. Expanding the range of deposition rates and Tooling,” Advanced Materials & Processes, 161:1,
levels of detail achievable in a single system are also of 64-65, (2003).
interest to enhance the process flexibility. Finally, [5] Sandia National Lab Laser Engineered Net Shaping
development of processing parameters for other material CRADA No. SC96/01462, (1999).
systems and exploitation of the layer-additive nature of [6] Dave, V.R., Matz. J.E., and Eagar, T.W., Electron
the process to develop functionally graded parts will Beam Solid Freeform Fabrication of Metal Parts,”
broaden the utility of the EBF3 process. Ultimately, our Proceedings of 6th SFF Symposium, 64-71, (1995).
goal is to develop the EBF3 process into a robust [7] Taminger, K.M.B. and Hafley, R.A.,
industrial process for application in a variety of industries. “Characterization of 2219 Aluminum Produced by
Electron Beam Freeform Fabrication,” Proceedings
Summary of 13th SFF Symposium, 482-489, (2002).
[8] Brice, C.A., et al., “Rapid Prototyping and Freeform
EBF3 is a new layer additive process with high potential Fabrication via Electron Beam Welding Deposition,”
for use in numerous structural metallic applications. Proceeding of Welding Conference, (2002).
EBF3 offers cost and lead time reductions in production of [9] Mayer, L.W., Alcoa Green Letter: Alcoa Aluminum
parts and performance improvements through optimized Alloy 2219, (1967).
alloy chemistries and microstructures. Microstructures
and mechanical properties obtained in aluminum and
Proceedings of the 3rd Annual Automotive Composites Conference, September 9-10, 2003, Troy, MI. Society of Plastics
Engineers (2003).