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sveNDSEN 1,898,405
METHOD OF PREPARING A LEAD CARBONATE PRODUCT
Filed Sept. 12, 1928
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Patented Feb. 21, 1933 1898,405
and sixty pounds of soda ash, eight pounds thereof and plates to recover the grid and lugs
of sodium acetate and fifty gallons of boiling Verized the filling in the form of a pull
hot water are added. The door it is closed caibonate and ieadmixture consisting mainly of lead
and the drum is rotated for about an hour, in tumbling said plates peroxide which consists
low pressure steam being introduced during gether with an aqueousin solution a rotary drum to 8 5
of alkali
the process in order to raise the temperature carbonate and a minor proportion of a lead
of the menstruum to about the boiling point solvent compound and separating the pulver
and maintain it at that temperature. Dur
ing this operation, the filling material is sub ized5. mixture
The
from the metal parts.
method of producing a pulverized
stantially completely removed from the mixture of lead carbonate and lead peroxide
grids, thoroughly pulverized and the lead from the filling of storage
sulfate substantially completely converted without substantially breakingbattery up the
plates
metal
30 into lead carbonate. The solution is de lic part of the plate into small particles which
canted off from the solid material which is consists in Supplying said plates together
washed several times with water, each addi with a substantial quantity of soda ash, a
tion of washing water being decanted off after relatively small amount
settling. By this method the filling of the and a substantial quantityofofsodium hot
acetate
Water to a
plates is converted into a pulverized mixture rotary drum, maintaining the reaction mix
of lead carbonate and lead peroxide contain ture at a high temperature and rotating the
ing a small amount of spongy lead. This drum.
powdered material is separated from the
grids and lugs by agitating with water and myinhand testimony whereof I have hereunto set
and Seal this 30th day of August,
40 decanting the pulverized material with the 1928.
water. This pulverized mixture is collected SWEND S. SVENDSEN.
and dried in a centrifuge and may suitably
be converted into litharge or red lead, in the
known manner, by heating in a suitable roast
ing furnace to the appropriate temperature.
The grids contain a greater proportion of 110
antimony than do the lugs. The lugs are,
therefore, separated from the grid metal and
both are melted separately.
Although the present invention has been
50 described in connection with the details of the
specific embodiment it must be understood
that such details are not intended to be limita
tive of the invention, except in so far as in
55 cluded in the accompanying claims.
claim:
1. The method of treating storage battery
plates to remove the filling of the plates and
to convert the lead sulfate of the filling into
60 lead carbonate which consists in tumbling
said plates upon each other in a solution of
an alkali metal carbonate.
2. The method of disintegrating storage
battery plates to recover the grid and lugs
65 thereof and the filling in the form of a pull
verized mixture consisting mainly of lead