Time (sec.

) Temperature (°C) TIME TEMP

0 94 0 91
30 94 30 89
60 95 60 87.5
90 95 90 86.5
120 94 120 85
150 93 150 84
180 92 180 83
210 91 210 81
240 90 240 80
270 89 270 78.5
300 88 300 77.5
330 86 330 76
360 85 360 75
390 84 390 74
420 83 420 74
450 81 450 74 COOLING CURVE OF UNKNOW
480 80 480 73.5 100
510 79 510 73 90
540 79 540 72.5 80
70
570 79 570 72

Temperature (°C)
60
600 79 600 72 50
630 79 630 71 40
660 78.5 660 71 30
690 78 690 70.5 20
10
720 78 720 70 0
750 78 750 69 0 60 120 180 240 300 360 420 480 540 60
780 78 780 68.5
810 77.5 810 68 Time (sec)
840 77 840 67
870 74 870 66
900 72 900 65.5
930 70 930 65
960 960
Cooling curve of
990 990
100
1020 1020
90
80
70
Temperature (°C)

60
50
40
30
20
10
0
0 60 20 80 40 00 60 20 80
 60

Temperature (°
50
40
30
20
10
0
0 60 0 0 0 0 0 0 0
12 18 24 30 36 42 48

Tim
LING CURVE OF UNKNOWN SOLUTION

0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0
18 24 30 36 42 48 54 60 66 72 78 84 90 96 102

Time (sec)

Cooling curve of unknown solvent

20 80 40 00 60 20 80 40 00 60 20 80 40 00 60 20
 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0
12 18 24 30 36 42 48 54 60 66 72 78 84 90 96 102

Time (sec)