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Statement of problem. Fracture of an interim fixed partial denture (FPD) may jeopardize the success of the interim
prosthodontic treatment phase and cause patient discomfort.
Purpose. The purpose of this study was to compare the fracture toughness of a polymethyl methacrylate (PMMA)
resin and a bis-acryl composite (BAC) resin reinforced with stainless steel wire, glass fiber, and polyethylene fiber.
Material and methods. Four groups (n=13) of each of the 2 materials were prepared for the single-edge notch 3-
point-bending test. Three groups had the different reinforcements, and the group without reinforcement served as the
control. Using a universal testing machine, peak load to fracture was recorded and fracture toughness (KIC) was calcu-
lated in MNm-1.5. Median KIC values were compared by means of nonparametric ANOVA (Kruskal-Wallis test, α=.05).
Results. For the controls, the fracture toughness for PMMA resin (KIC=27.9) was significantly lower (P<.01) than for
BAC resin (KIC=31.2). Glass fibers and stainless steel wire reinforcements produced significantly higher fracture tough-
ness for both PMMA (KIC=34.4, P<.01, and KIC=39.0, P<.001, respectively) and BAC resin (KIC=42.3, P<.001, and
KIC=44.0, P<.001, respectively), but the polyethylene fibers did not (KIC=25.8, P>.10, for PMMA resin and KIC=33.1,
P>.10, for BAC resin). There was no significant difference between the fracture toughness of the wire and glass fiber
reinforcements for both interim materials (P>.10 in both instances).
Conclusions. Of the 3 reinforcement methods evaluated, wire and glass fiber reinforced the PMMA and BAC resin
materials best. (J Prosthet Dent 2008;99:461-467)
Clinical Implications
When esthetics and space are of concern, glass fiber seems to be the most
appropriate method for reinforcing interim FPDs made from PMMA and
BAC resins. Wire provides the clinician with a less expensive option in areas
of the mouth where esthetics are not crucial and adequate space is avail-
able. All 3 reinforcements evaluated prevent catastrophic failure.
Presented at the South African Division of the International Association for Dental Research, Pretoria, South Africa, September
2006.
The following manufacturers and suppliers provided the products used in this study: Stick Tech, 3M ESPE, Istrodent, and Millners
Dental Suppliers.
a
Principal Specialist and Associate Professor, Department of Restorative Dentistry, University of the Western Cape.
b
Former Resident, Department of Restorative Dentistry, University of the Western Cape.
c
Stomatologist and Professor, Operative Dentistry, Faculty of Dentistry, University of Limpopo.
Geerts et al
462 Volume 99 Issue 6
Polymethyl methacrylate (PMMA), ing test. This test determines critical the specimens. Three of the 4 groups
polyethyl methacrylate, bis-acryl values of stress intensity (KIC) when were reinforced; 1 group without re-
composite (BAC), and epimine resin standardized precracked specimens inforcement served as the control.
are materials commonly used to fab- are loaded until fracture. These loads The reinforcements used were: (1) 1-
ricate interim fixed partial dentures are used to calculate toughness.25 Nu- mm-diameter smooth stainless steel
(FPDs).1 These materials must be merous fracture resistance tests have wire (KC Smith & Co, Monmouth,
strong enough to withstand mastica- been performed for resins reinforced UK), (2) glass fiber (everStick C&B
tory forces, particularly for long-span with steel wire, polyethylene, or glass fiber; Stick Tech Ltd, Turku, Finland),
FPDs, for long-term use, or for pa- fiber.5,8-15,17-21 However, none have and (3) polyethylene fiber (Construct
tients with parafunctional habits.2,3 compared the reinforcement effect braided polyethylene fiber; Kerr Corp,
Different methods of enhancing the of steel wire, polyethylene, and glass Orange, Calif ).
physical properties of interim FPDs fiber on PMMA and BAC resins in a A custom-made stainless steel
have been developed.4 Positive re- single study. mold was used to produce standard-
sults have been achieved with the use The purpose of this study was to ized specimens (Fig. 1). The precrack,
of metal and fiber reinforcements.5-12 compare the fracture toughness of 2 perpendicular to the specimen length,
These studies demonstrate that metal types of materials frequently used for was created by inserting a straight-
wires incorporated into polymers pro- interim FPDs, with and without rein- edged surgical blade (No. 11; Swann-
duce higher transverse strength, but forcement. Stainless steel wire, poly- Morton Ltd, Sheffield, UK), with a
fibers have been demonstrated to be ethylene fiber, and glass fiber were blade edge radius of less than 0.3 μm,
more effective in improving strength.12 used as the 3 materials for reinforce- half the length of the mold; the slot
Various types of fibers have been in- ment. The null hypothesis was that (A=3 mm) extended up half the height
vestigated, including glass, carbon, the 3 reinforcement materials would of the specimen (W=6 mm) to give A/
aramid, and polyethylene fibers. The not significantly alter the fracture W= 0.5 (Fig. 2). The mold used in this
eventual strength of the reinforced toughness of the 2 resins. study could be disassembled com-
resin is influenced by the quantity and pletely so that no force was required
orientation of the fibers, position, fi- MATERIAL AND METHODS to remove the polymerized specimens
ber impregnation, and adhesion of from the mold.
the fibers to the polymer matrix.13-17 Four groups (n=13) of specimens The control groups were fabri-
The degree of adhesion between fi- were prepared from a BAC resin (Pro- cated as follows: the BAC resin was
ber and polymer affects the degree of temp 3 Garant; 3M ESPE, Seefeld, mixed using the automix gun system
reinforcement. The better the bond, Germany) and a PMMA resin (Cold- provided by the manufacturer. For
the better the transfer of stress from pac; The Motloid Co, Chicago, Ill) for the PMMA resin, 0.58 g of powder
the weak polymer matrix to the fibers a single-edge notch 3-point bending was weighed using a precision stan-
with a higher tensile strength.18,19 Uni- test conforming to the British Stan- dard scale (Model TS400 D; Ohaus
directional fibers enhance strength dard 5477 (1977).26 The dimensions Corp, Pine Brook, NJ) and 0.25 ml
and stiffness in 1 direction, while of the specimens were 3 mm x 6 mm x of liquid was measured using a pi-
randomly oriented fibers enhance 26 mm. The depth of the precrack was pette (Pipetman, L 116956; Gilson,
mechanical properties in all direc- 3 mm, which was half the height of Inc, Paris, France) and mixed. This
tions.15 Interim FPDs reinforced with
impregnated fibers demonstrate high-
er fracture resistance than those rein-
forced with nonimpregnated fibers.20
Silanized glass fibers bond readily to
polymers.21 Compared to other types
of fibers, adhesion of polyethylene fi-
bers to polymers is less effective.22
The fracture mechanism approach
is considered a reliable indicator of
the performance of brittle materials.23
A fracture toughness test measures
the resistance of a material to crack
extension.24 Different tests have been
used to quantify the fracture tough- 1 Custom-made stainless steel mold, demonstrating
ness of dental materials. One such test stops (a) with depth of 1.5 mm for positioning of rein-
is the single-edge notch 3-point bend- forcement and position of scalpel (b) to create precrack.
Table I. Descriptive statistics for fracture toughness (KIC in MNm-1.5) for 8 groups (n=13)
PMMA Resin BAC Resin
PMMA = polymethyl methacrylate resin, BAC = bis-acryl composite resin, IQR = interquartile range,
wire = stainless steel wire, PE = polyethylene fiber, glass = glass fiber
55.00
60
46.25
50
37.50
40
28.75
30
20.00
20 BAC Glass PE Wire
PMMA Glass PE Wire
3 Side-by-side box plot of fracture toughness (KIC in 4 Side-by-side box plot of fracture toughness (KIC in
MNm-1.5) for 4 PMMA groups. Dots represent outliers. MNm-1.5) for 4 BAC groups. Dot represents 1 outlier. BAC
PMMA = polymethyl methacrylate resin, glass = glass = bis-acryl composite resin, glass = glass fiber, PE = poly-
fiber, PE = polyethylene fiber, wire = stainless steel wire. ethylene fiber, wire = stainless steel wire.
Purpose. The aim of this study was to investigate the deviations of the implant positions of both impressions and
casts using different impression materials and techniques. Furthermore, the existence of a correlation between the
deviations of the impression and those of the cast was investigated.
Materials and Methods. A reference model was fabricated with 5 Frialit-2 implants parallel to each other. In a stan-
dardized experimental setting, 5 stone casts were produced with 5 different techniques using polyether (A) or polyvi-
nyl siloxane (B through E). In 3 groups, a direct technique was used with a medium-viscosity material or a putty-tray
material in combination with a light-viscosity syringe material (A to C). In 2 groups, an indirect technique (either
1-step [group D] or 2-step [group E]) was used with a putty-tray material in combination with a light-viscosity syringe
material. The center-to-center distances were measured for impressions and casts in the horizontal plane using a com-
puter-aided microscope, and the relative and absolute deviations compared to the reference model were calculated.
Analysis of variance followed by the post-hoc Scheffe test (parametric data) or the Kruskal-Wallis test followed by
pair-wise Mann-Whitney tests (nonparametric data) were used for statistical analyses. Deviations of impressions were
compared with their respective casts using paired t tests and the Pearson correlation coefficient.
Results. No significant differences for the relative deviations were found for impressions (–5 to –8 µm) or casts (+7 to
+16 µm). Group E produced significantly higher absolute deviations for impressions (38 µm) and casts (39 µm) com-
pared to the other groups (11 to 18 µm and 17 to 23 µm, respectively). A significant correlation between deviation of
the impression and its respective cast was found for every group (r = 0.40 to 0.80) except group D.
Conclusion. The distortions in the horizontal plane of the casts obtained from the impression techniques of groups
A to D would probably not affect the clinical fit of implant-retained superstructures. Because of the high variation of
deviations (–113 to +124 µm), the 2-step technique cannot be recommended. The method to measure both impres-
sion and cast provided a better understanding of how inaccuracies are caused.
Geerts et al