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Article history: Expansive soils have long been recognized as problematic because they cause failure to civil structures
Received 6 January 2013 constructed above them. The main problem of these soils can be attributed to poor understanding of the vol-
Received in revised form 6 May 2013 ume changes caused by moisture fluctuations. Current swell and shrinkage characterization models are lim-
Accepted 7 July 2013
ited by both the lack of standardized tests and tests that employ volume changes in uniaxial direction. In the
Available online 13 July 2013
present research, a comprehensive laboratory investigation was undertaken to study the volume change re-
Keywords:
lated swell–shrinkage behaviors of five different types of expansive clayey soils sampled from various regions
SWCC in Texas, USA. Extensive experimental programs consisting of basic, chemical and mineralogical soil proper-
Expansive soils ties were first determined. Three-dimensional free swell and shrinkage tests were performed on all soils at
Swelling and shrinkage various compaction moisture content conditions. Soil–water characteristic curves (SWCCs) of all test soils
Unsaturated soils were determined by studying the suction potentials of these soils over a wide range of moisture contents.
Clay mineralogy Volume change measurements of soils showed a good correlation with soil properties, including plasticity
and soil compaction properties. SWCC results also showed a clear variation in SWCC profiles of soils with re-
spect to soil plasticity. Overall, a large database of soil properties was developed and is presented here. It in-
cludes physical and mineralogical properties, as well as engineering swell, shrinkage and SWCC test results.
Published by Elsevier B.V.
from five sites, namely Fort Worth, Paris, San Antonio, El Paso and Table 2
Houston, Texas, USA. The experimental program was mainly com- Chemical measurements and clay mineralogy of test soils.
prised of tests to determine basic soil properties, such as plasticity Item Soil types
and compaction properties; clay mineralogy data; and engineering
Fort San Paris Houston El Paso
characteristics, including volume change related swell and shrinkage Worth Antonio
strain properties. A brief summary of the laboratory procedures,
Specific surface area (m2/g) 314 269 431 236 167
equipments used and results obtained are presented in the following Cationic exchange capacity 117 96 133 76 57
sections. (meq/100 g)
Total potassium (%) 0.96 1.08 0.78 1.56 3.78
2.1. Basic soil property tests % illite 16 18 13 26 63
% kaolinite 34 40 17 38 29
% montmorillonite 50 42 70 36 8
All representative soil samples were subjected to various physical
property measurements, including grain size and hydrometer tests,
Atterberg limits, and Proctor compaction tests. All test results are helps in replacing them. Hence, the cation exchange process involv-
presented in Table 1. Based on the physical soil characteristics, four ing this saturating solution makes it appropriate for the reliable esti-
soils were characterized as high plasticity clays, and one soil was clas- mation of CEC of a soil.
sified as lean or low plastic clay. The specific surface area or SSA of a soil sample is the total surface
Generally, soils that exhibit plastic behavior over a wide range of area of soil particles contained in a unit mass of soil. This property of
moisture contents and have high liquid limits tend to undergo larger the soil is primarily dependent on the particle size distribution of the
swelling and shrinking. As per the expansive soil characterization, soil mass. Typically, soils with a large number of smaller particle sizes
soils sampled from the Fort Worth, Houston, San Antonio and Paris have higher specific surface areas. It should be noted here that a clay-
sites were considered as high swelling potential, and soil from El ey soil with a high specific surface area has a high water holding ca-
Paso was considered as a low swell potential material. Four of the pacity and greater swell potential due to the large surface area that
five soils are classified as A-7-6 as per the American Association of is negatively charged and attracts dipole-natured water.
State Highway and Transportation Officials (ASSHTO) classification This test method involves saturating the prepared soil sample,
system and CH as per Unified Soil Classification System (USCS). equilibrating them in a vacuum over a calcium chloride–EGME
Also, an attempt is made to determine the clay mineralogy of (CaCl2–EGME) solvate, and then determining the weight when the
these soils based on chemical measurements, including specific sur- equilibrium (constant weight) is reached. The specific surface is
face area, cation exchange capacity and total potassium. then determined from the mass of retained EGME in comparison to
the amount retained by pure montmorillonite, which is assumed to
2.2. Chemical tests have a surface area of 810 m2/g (Carter et al., 1986). This test method
was fully evaluated for its potential application in the geotechnical
Three chemical property related tests known as cation exchange field by Cerato and Lutenegger (2002), and they concluded that the
capacity (CEC), specific surface area (SSA), and total potassium (TP) method is applicable to a wide range of soils with different clay min-
were studied here, and details of these test procedures are briefly eralogies and is capable of determining the specific surface area rang-
discussed here. ing from 15 to 800 m2/g.
Cation exchange capacity or CEC can be used to determine the min- Potassium is the interlayer cation in the clay mineral, illite, and
eral composition since a high CEC value indicates the presence of the this stable clay mineral is the only one that possesses potassium in
clay mineral such as montmorillonite and a low CEC indicates the pres- its structure (Mitchell and Soga, 2005). Hence, measuring the amount
ence of non-expansive clay mineral such as kaolinite. CEC of a soil can be of potassium ion in the soil gives a direct indication of the presence of
defined as the capacity or the ability of the soil to exchange free cations the clay mineral, illite. The test procedure formulated by Knudsen et
that are available in the exchange locations. It may also be understood al. (1982) was followed to determine the amount of total potassium
simply as a measure of the quantity of readily exchangeable cations present in the soil. The method involves a double acid digestion tech-
neutralizing negative charge in the clay mineral (Chapman, 1965). nique developed originally by Jackson (1958), which uses two acids,
The CEC test method involves the addition of a saturating solution hydrofluoric acid and perchloric acid, to break the mineral structure
to the soil sample, followed by removal of the adsorbed cations, using of the soil and then extract the potassium ions from the structure.
an extracting solution. In the method used here, ammonium acetate Once the potassium is extracted, its concentration in the solution
(NH4OAc) is the saturating solution, which has the ability to replace can be obtained with the help of a spectrophotometer or any other
all the exchangeable cation locations with the ammonium (NH+ 4 ) cat- appropriate device.
ion. This is possible because of the low valence (1+) of this cation that These chemical test results, along with interpreted clay mineralogy,
makes it more stable and electro-negatively stronger than higher va- are presented in Table 2. Interpretations were made based on the anal-
lence cations such as Ca2+, Al3+ and others. While replacing the sim- ysis of chemical measurements induced by the clay mineral fractions
ilar valence cations such as Na+, the higher atomic weight of NH+ 4 of a given soil. Details of this analysis can be found in Chittoori and
Puppala (2011). The interpreted clay mineralogy data is presented in
Table 1 Table 3. Overall, it can be mentioned that both Fort Worth and Paris
Basic soil properties.
102 16.0
Table 4
Volumetric shrinkage strain test results of five expansive soils.
100 15.7
Max. Dry Density
Moisture Parameter Shrinkage strain (%)
a) b)
Fig. 3. (a) Typical photograph of a soil specimen surface area with cracks after test; (b) threshold image of the surface area showing only cracks.
190 A.J. Puppala et al. / Engineering Geology 164 (2013) 187–194
35
a) Vertical Swell Strain Results
Wet of OMC OMC Dry of OMC 18
Volumetric Shrinkage Strain (%)
15
25
15 9
10 6
5 3
0
Fort Worth San Antonio Paris Houston El Paso 0
0 20 40 60 80 100
Fig. 4. Volumetric shrinkage strain test results of five soils. Time (hr.)
b) Radial Swell Strain Results
7
Dry of OMC OMC Wet of OMC
6
0
0 20 40 60 80 100
Time (hr.)
20
a) b)
Fig. 8. Pressure plate testing: (a) initial setup of testing specimens and (b) closed pressure vessel with air pressure applied.
192 A.J. Puppala et al. / Engineering Geology 164 (2013) 187–194
soil types (Fort Worth, San Antonio, Paris and Houston soils), have conditions (Snethen, 1979; Hamberg, 1985; Lytton, 2004). Therefore,
experienced large volumetric swell strain (more than 10%) at OMC soil suction was measured on present soils at different moisture con-
condition, and these magnitudes considered are characterized as a tents, which were later used to establish soil–water characteristic
very high degree of expansion potential as per the free swell strain curves (SWCCs). The SWCC describes a unique relationship between
characterization methodology given by Chen (1983). As expected, El the matric suctions and compaction moisture contents of a given
Paso clay exhibited the lowest swell strain results due to the low plas- soil type. In unsaturated soil mechanics, the SWCC, known to depend
ticity properties (low PI) as well as low amounts of montmorillonite on the size and distribution of pore structures in the soils, is used in
mineral content. direct and indirect interpretations of soil strength, permeability and
volume change related characteristics (Fredlund et al., 1994). A few
2.4.3. Suction and SWCC measurements tests utilizing matric and total suction tests performed on the test
Expansive soils are often characterized by the soil suction charac- soils, using the filter paper method, showed that both suctions are
terization methods due to their common occurrence in unsaturated similar, indicating that the osmotic suction is small and practically
0.25 0.25
0.20 0.20
0.15 0.15
0.10 0.10
0.05 0.05
0.00 0.00
1 10 100 1,000 10,000 100,000 1,000,000 1 10 100 1,000 10,000 100,000 1,000,000
Suction (kPa) Suction (kPa)
0.40 0.35
0.35 0.30
0.30 0.25
0.25
0.20
0.20
0.15
0.15
0.10
0.10
0.05 0.05
0.00 0.00
1 10 100 1,000 10,000 100,000 1,000,000 1 10 100 1,000 10,000 100,000 1,000,000
Suction (kPa) Suction (kPa)
e) El Paso Soil
0.25
By Pressure Plate By Filter Paper
Gravimetric Water Content
0.20
0.15
0.10
0.05
0.00
1 10 100 1,000 10,000 100,000 1,000,000
Suction (kPa)
negligible. As a result, matric suction methods are followed in the rest from low to high suction conditions. The combined SWCC test results
of the experimental program. of all soils from pressure plate and filter paper methods are presented
Filter paper and pressure plate methods are commonly used to de- in Figs. 9 and 10.
termine ‘soil–water characteristic curves (SWCCs)’ of unsaturated SWCCs of all four high plastic soils exhibited similar characteris-
soils, which provide a relationship between the matric suction and tics. The only noticeable difference is that the saturated moisture
compaction moisture content conditions of the soils. Hence, SWCC content (at zero suction) of Houston clay is much lower than the
studies were planned and performed on all five test soils. The limita- other soils. This lower value indicates less ability to hold up water
tion of the present pressure plate device used here was that it can or moisture content, which implies that they do not undergo large
only measure matric suctions up to 1000 kPa. Hence, for high suction swelling when hydrated. Overall, trends noted in the engineering
ranges, the filter paper method was followed, as this method can pro- swell, shrinkage and SWCC studies show a direct relationship with
vide suctions larger than 1000 kPa (Bulut et al., 2001). Overall, both the chemical analysis results in particular specific surface area results
pressure plate and filter paper test methods were utilized in the de- and related clay mineralogy interpretations.
velopment of complete SWCC profiles of the test soils. As seen by the above described experimental program, a large da-
Fig. 8 shows the photographs of a typical pore water extraction tabase of soil properties comprised of physical, mineralogical and en-
testing setup using a pressure plate apparatus. The primary compo- gineering volume change properties and SWCC profiles was prepared.
nents of the system are a steel plate pressure vessel and a saturated These test results were analyzed and studied for both evaluating the
High Air Entry (HAE) ceramic plate. As shown, a small water reservoir existing swell and shrinkage strain predictions and developing new
is formed beneath the plate using an internal screen and a neoprene models for predicting swell and shrinkage related volume changes
diaphragm. The water reservoir is vented to the atmosphere through in soils. These analyses and results will be included in the future
an outflow tube located on top of the plate, thus allowing the air pres- paper.
sure in the vessel and the water pressure in the reservoir to be sepa-
rated across the air–water interfaces bridging the saturated pores of 3. Summary and conclusions
the HAE material (Lu and Likos, 2004).
Soil specimens were initially saturated, typically by applying a The following lists a few of the major conclusions obtained from
partial vacuum to the air chamber and then allowing the specimens the present experimental program:
to imbibe water from the underlying reservoir through the ceramic
disk. Air pressure in the vessel was then increased to some desired 1. Among tested soils, three soils from Fort Worth, Paris and San
level while pore water was allowed to drain from the specimens in Antonio contained moderate to large amounts of montmorillonite,
pursuit of moisture equilibrium. The outflow of water was monitored and these soils exhibited high plasticity index property. The soil
until it ceased, the pressure vessel was then opened, and the water from Houston contained a moderate amount of montmorillonite,
contents of the soil specimens were measured, thus generating a but still exhibited high plasticity index. The only exception was
one point on the soil–water characteristic curve. Subsequent incre- the soil from El Paso, which had low plasticity index property
ments in air pressure were applied to generate addition points on and contained low amounts of montmorillonite.
the curve using the other specimen. 2. Both volume change related swell and shrinkage studies have
For the filter paper method, a filter paper, Schleicher and Schuell yielded test results that are not only repeatable due to low
No. 589-WH type, was suspended in the headspace above the soil standard deviations, but also reliable, as they show the trends
specimen so that the moisture transfer from soil occurred in the that are expected for different types of expansive soils. These
vapor phase. The equilibrium amount of water absorbed by the filter tests, the shrinkage tests in particular, provide shrinkage strain
paper is presented as a function of the pore-air relative humidity and potentials as a function of moisture content and dry unit weight
the corresponding total soil suction. The water content of the filter conditions.
paper was later measured after the test reached equilibrium condi- 3. Soils with high plasticity properties experienced large volume
tion after undergoing the vapor transmittal for a period of ten days. changes during swell and shrinkage strain characterizations stud-
The suction was estimated from the moisture content of the filter ies. This reconfirms the well established notion that high plastic
paper using a calibration curve established by Bulut et al. (2001). By soils are indeed mostly highly expansive.
measuring the soil suctions at various compaction moisture content 4. Largest magnitudes of shrinkage volumetric strains were mea-
conditions, the soil–water characteristic curves were then drawn sured at wet of optimum moisture content conditions, and largest
magnitudes of volumetric swell strains were recorded at dry of op-
timum moisture content conditions. These trends are expected as
Fort Worth San Antonio Paris El Paso Houston
0.50 soils compacted at these moisture conditions are either close to
dry conditions or full saturation conditions, and swell or shrinkage
0.45
tests are expected to provide large and small magnitudes.
5. SWCCs of all four high PI soils exhibited similar suction character-
Gravimetric Water Content
0.40
0.35 istics. The only noticeable difference is that the saturated moisture
content (at zero suction) of Houston clay is much lower than the
0.30
other three soils. This lower value indicates less ability to hold up
0.25 water or moisture content, which implies that they do not undergo
0.20 large swelling when hydrated.
0.15
0.10 Acknowledgments
0.05
This research was conducted in cooperation with the Texas
0.00 Department of Transportation. The authors would like to acknowledge
1 10 100 1,000 10,000 100,000 1,000,000
Suction (kPa) TxDOT engineers for excellent cooperation throughout the research.
Also, the authors would like to acknowledge National Science
Fig. 10. Combined plots of soil–water characteristic curves of five soils. Foundation (Program Director: Dr. Richard J. Fragaszy) for the NSF
194 A.J. Puppala et al. / Engineering Geology 164 (2013) 187–194
Grant No.1031214, which assisted researchers in parts of soil Jackson, M.L., 1958. Soil chemical analysis. Prentice Hall, Englewood Cliffs, N.J.
Kormonik, A., David, D., 1969. Prediction of swell pressure of clays. Journal of Soil
characterization studies reported here. Mechanics and Foundation Division ASCE 95 (SM1), 209–225.
Lu, N., Likos, W.J., 2004. Unsaturated Soil Mechanics. John Wiley & Sons, New York.
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