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Article history: The intensity of light signal transmitted through an optical fiber, whose cladding over a finite length is
Received 31 July 2009 removed, is used as a sensor of refractive index of liquids, in which the fiber is immersed. The transmitted
Received in revised form light intensity is measured as a function of liquid refractive index for different lengths of the unclad
28 November 2009
section of the fiber and at each unclad length its sensitivity to change in refractive index of liquid is
Accepted 4 December 2009
monitored. The liquid refractive index studied ranges from below the refractive index of the cladding
Available online 16 December 2009
to above that of the core. A plot of normalized light intensity as a function of liquid refractive index
for a short unclad length shows a local maximum at a liquid refractive index equal to the refractive
Keywords:
Liquid refractive index sensor
index of the fiber core. This maximum becomes less prominent as length of unclad region increases and
Fiber optic refractive index sensor finally disappears. These observations are interpreted in terms of frustrated total internal reflection of
Frustrated total internal reflection light rays. Sensitivity to refractive index differential, of the sensor response, increases with increase in
FTIR refractive index of the liquid pair, below that of the fiber core. In this range of refractive index, we observe
a maximum in this sensitivity at an intermediate unclad length of the fiber. When liquid refractive index
equals core refractive index, at the rising edge of the local maximum observed in sensors of shorter unclad
length, the sensitivity maximum disappears. The sensitivity to refractive index differential diminishes
as liquid refractive index exceeds fiber core refractive index. Measurements have been performed with
five different unclad sensor lengths and a core diameter of 400 and 800 m. The results for the two core
diameters show similar qualitative features.
© 2009 Elsevier B.V. All rights reserved.
0925-4005/$ – see front matter © 2009 Elsevier B.V. All rights reserved.
doi:10.1016/j.snb.2009.12.009
266 A. Mukherjee et al. / Sensors and Actuators B 145 (2010) 265–271
at higher (6.0 and 8.0 cm) unclad lengths. Fig. 3(b) shows data at
8.0 cm unclad length. In Fig. 4 we show R as a function of liquid
RI for both core diameters in the range where these local maxima
are observed at smaller unclad lengths. The maximum in each case
has been reproduced several times. The maximum is sharper for
an unclad length of 1.5 cm as compared to that of 3.0 and 4.5 cm
for both fiber core diameters. In each of these three maxima for
400 m fiber core, the height of the falling edge of the intensity
ratio profile is 0.11, while those of the rising edge is 0.11 in 1.5 cm
unclad length and ∼0.029 (these numbers are in arbitrary units) in
the other two.
Experimental data on intensity ratio for a given fiber diame-
ter and a given unclad length are verified to be free from possible
differences in fiber alignment that may result from change in test
liquid. The fiber is held rigidly on both ends by stable mechanical
support. The intensity ratio for a given core diameter and different
unclad lengths are made free from possible alignment differences
by adjusting them to same intensity ratio in air. If the core diame-
ter is different then perfectly equivalent alignment in air will also
not give same intensity ratio. The relative locations of the plots for
400 and 800 m core diameter fibers in Fig. 3(a) and (b), therefore
do not have any physical significance and are adjusted merely for
clarity of the figures.
In addition to the presence of the above-mentioned maxima, the
plots for 400 m core diameter fiber (Figs. 3 and 4) show a mini-
mum at a liquid RI equal to core RI and a switchover from negative
to positive slope as the liquid RI exceeds RI of the fiber core. This
feature has been reported by Cusano et al. [15] who use a fully
clad single mode fiber to monitor RI of polymer-based composites
deposited on the fiber. They make measurements with liquid sam-
ples for purposes of calibration. The quantity that monitors the RI of
the liquid is the intensity of reflected light at the liquid–fiber inter-
face. They observe, just as we do, a negative slope in the range of
liquid RI below the fiber RI (∼1.37–1.48) and a positive slope when
RI of test liquid exceeds that of fiber. An earlier report from our
group [23] that used the experimental arrangement described in
this paper, also noted this switchover. That report was less detailed
and the fibers and the process of uncladding were not as well char-
Fig. 3. Plot of intensity ratio (R) as a function of liquid refractive index (RI, n) with acterized.
fibers of two different core diameters (400 and 800 m core radius) of two different
unclad lengths ((a) 1.5 cm and (b) 8.0 cm). Feature to note is the presence of maxima
3.3. Sensitivity maximum at intermediate unclad length
in (a) and its absence in (b).
Fig. 4. Plot of intensity ratio (R) with fibers of different unclad lengths (core diameters of the two fibers are 400 and 800 m) as a function of liquid refractive index in the
region where the maxima of interest are observed at smaller unclad length. The value of the unclad length is indicated on each figure. x-Axis of each figure indicates liquid
refractive index. y-Axis indicates intensity ratio in arbitrary units (see text).
and (b) (range on y-axis: 0–0.6 and 3.65–3.85, respectively), further by the effect of frustrated total internal reflection, as discussed
increases in Fig. 5(c) and (d) (range on y-axis: −6 to 10 and 14–20, below. A non-monotonic dependence of transmitted light inten-
respectively) where we are on the two edges of the local maximum sity on liquid RI is then superimposed on the monotonic profile. As
observed for smaller unclad lengths, and then in Fig. 5(e) as we liquid RI exceeds core RI, total internal reflection does not take place
go past the point where nliquid ∼ ncore the sensitivity becomes very and evanescent wave no longer participates in the sensing mech-
small (range on y-axis:1.6–2.0). The absolute values of R are depen- anism. A minimum in transmitted light intensity at nliquid = ncore is
dent on the alignment of the fiber, but, as already stated, we have observed because, then light rays do not sense any optical inhomo-
taken care in correcting for different alignments by adjusting the geneity at the core–liquid interface.
alignment to equalize the intensity ratio to the same value in air. The evanescent waves within the cladding layer associated with
The values of R/n in Fig. 5(a)–(e) are then on equal footing. the guided modes experience two discontinuities: both along the
We have performed experiments, corresponding to those direction of propagation, one at the beginning and the other at
reported above, in our laboratory on fiber sensors whose cladding the end of the unclad region. The evanescent wave entering the
have not been fully removed, but have been unclad to differ- unclad region encounter conditions akin to that in the well known
ent thickness values. The results show a systematic dependence frustrated total internal reflection (FTIR) [33], i.e., propagating
of experimental results on cladding thickness for a given unclad modes in the larger core region (with RI = ncore ) are evanescent
length. The maximum sensitivity at an intermediate unclad length within the thin barrier region (cladding layer with RI = ncladding )
is also observed. These results will be reported in a separate com- followed by an extended region with higher RI (=nliquid ∼ ncore )
munication. where they become propagating modes again. The guided modes
of the fiber tunnel through the barrier and become propagating
3.4. Interpretation of results modes within the liquid-filled unclad region. These new prop-
agating modes re-enter the guiding core region by the reverse
Energy loss from light propagating in a partially cladding- process at the second interface of the unclad region, leading to the
stripped fiber with shorter unclad lengths in the range of unclad enhanced transmission intensity through the fiber. As the unclad
lengths we study show, in the local maxima we observe with region is made longer, fewer propagating modes are able to cou-
nliquid ∼ ncore for shorter unclad lengths, a non-monotonic depen- ple back into the fiber at the second interface. We note that only
dence on liquid RI. The dependence is monotonic at larger unclad around nliquid = ncore the direction of propagation vectors within
lengths, where the local maxima disappear. This is an interesting the core and of the new propagating modes are collinear (as is
experimental result. We are not aware of a similar report in the well known in FTIR geometry) leading to efficient coupling back
literature. into the fiber [33a ]. Hence, light couples back into the fiber most
A monotonic dependence on liquid RI (<core RI) with a more efficiently in the regime where nliquid ∼ ncore . The peak in the plot
rapid rate of energy loss as liquid RI exceeds cladding RI is a result of I/I0 as function of RI that we observe (Figs. 3 and 4) is the
of an increase in the extent of evanescent field in the liquid under result. FTIR has recently been used in the design of a fiber-optic
test. As liquid RI approaches core RI, this increase is accompanied RI sensor. The sensor principle is based on FTIR effect caused by
A. Mukherjee et al. / Sensors and Actuators B 145 (2010) 265–271 269
Fig. 5. Plot of sensitivity of intensity ratio to liquid refractive index change as a function of unclad length of 400 m core diameter fiber for five different liquid pairs with
refractive indices in different RI regions. The liquid pair and their refractive indices are indicated on each figure ((a)–(e)).
refractive index change of a medium surrounding an optical fiber (b), (d), and (e)) owes its origin to the presence of local maxima we
tip [34]. interpret above in terms of FTIR. In Fig. 5(c) R/n (i) is positive at
The deviation of the plot of RI sensitivity as a function of unclad lower unclad lengths for the liquid pair studied (ii) has the largest
length for the liquid pair in the rising part of the local maximum positive value in the shortest unclad fiber length which has the most
(Fig. 5(c)) from the pattern with a maximum at an intermediate prominent maximum (Fig. 4(a) and (f)) and (iii) becomes negative
unclad length we observe for other liquid pairs studied (Fig. 5(a), at larger unclad lengths (Fig. 4(d), (e), (i), and (j)). In the other four
270 A. Mukherjee et al. / Sensors and Actuators B 145 (2010) 265–271
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