Professional Documents
Culture Documents
5MTPA
Palletizing Plant at 13636 T/Day
sohar – 568.16 T/Hr
Sultanate of Oman
Technology:
Grate Kiln {formerly
known as Allis-Chalmers
Raw Material:
Kiln} Iron ore,
Brief: Pellets are Limestone,
transforms of Mineral Anthracite &
resources of superior Bentonite.
quality feed as raw
materials to D.R.I & Blast Fuel: Natural Gas
Furnace process
For Steel making……
Vale’s Industrial Empire
Vale Oman
Palletizing Plant
Iron Ore Fines Utilization….. Via …..Pelletisation
Analyze Process
capability
Stimulate Process
Performance
Prepare Process
Plan
We
are
here
Vale Oman Palletizing Complex:-
Process
Control
Dept.
Vale Oman Process Flow Chart
Thickener
Iron Ore Bentonite
Feed Additives
Chips/Chunks
Fuel
Balling
P P T D D
H H P D D Roller
2 1 H 2 1 Feeder
Rotary Kiln
Traveling
Grate
Annular
Cooler
CONTENTS:-
Process : Control :
Lot: The quantity of Raw material/ Finished Products indicated to be of the same category and offered
for inspection at one time. A lot may consist of the whole or a part of the quantity ordered for.
Sub-lot: The quantity of ore/pellets in each of the parts into which a lot is divided for the purpose of
sampling.
Increment: The quantity of ore/pellets obtained by a sampling device at one time from a lot or sub-lot.
Unit Sample: The quantity of ore/pellets collected at one time from the conveyor (Unit sample is larger
than the increment).
Gross sample: The total quantity of ore/pellets consisting of all increments or unit samples taken from
a sub-lot.
Size sample: The sample taken for the determination of the size distribution of the lot or sub-lot.
Moisture sample: The sample taken for the determination of moisture content of the lot or sub-lot.
Laboratory sample: The quantity of ore/pellets obtained by reducing a gross sample following a
specified procedure for determining chemical composition of a lot or sub-lot.
Composite sample (For the lot): The quantity obtained by mixing together proportional quantities of
ore/pellets representing the mass of each sub-lot which a lot has been divided.
Sampler: Person responsible for performing the sampling operations.
Sampling method: That part of the sampling procedure dealing with the method prescribed for withdrawing
samples.
Random sample: Sample in which the different fractions of the material have
an equal probability of being represented.
Sampling plan: Description of the location, number of units and/or quantity of material
that should be collected, and associated acceptance criteria.
Sampling record: Written record of the sampling operations carried out on a particular
material for a defined purpose. The sampling record should contain the batch number,
date and place of sampling, reference to the sampling protocol used, a description of the
containers and of the materials
sampled, notes on possible abnormalities, together with any other relevant observations,
and the name and signature of the inspector.
Need for Sampling:
Introduction : According to ISO/IEC 10725, “sampling” is defined as “a procedure whereby a part of
a substance, material or product is taken to provide for testing or calibration a representative sample of
the whole.
Sampling may also be required by the appropriate specification for which the substance, material or
product is to be tested.” In other words, the goal of sampling is to select and obtain a test portion of the
material in some manner, such that the sub-sample is representative of the larger amount of material.
Sampling is often a major source of error and if a truly representative sample of the batch is
not obtained, then the subsequent analysis will give a wrong figure. It is the aim therefore
to develop correct sampling protocols, considered to be an essential requirement for
obtaining valid results within Prospect.
Shipment sampling.
Stockpile sampling.
Automatic samplers.
Sectional sampling.
Trench sampling.
Or n
Pellets
Iro
e
• Sampling from conveyors: When ore/pellets is moved on conveyors, one of the most reliable methods
of manual sampling is stopped belt method. Whenever it is practicable to stop the conveyor belt
periodically, a large quantity of iron ores known as unit sample may be drawn by stopping the belt. The
sample shall be collected from the full width and thickness of the ore/pellet stream over a suitable length
of the conveyor. In case it is not possible to stop the conveyor the sample shall be taken from a specified
place on a conveyor or at a specified transfer point of conveyor.
• Shipment sampling: In order to get gross sample, the ore/pellets shall be sampled as far as possible
when in motion. That is from the conveyor during loading or immediate discharge during unloading at
regular interval.
• Stockpile sampling: The ore/pellets from stockpiles shall be carried out as far as possible, when they
are in motion, that is, during the formation of the stock piles or during the shifting of the stockpiles to
the other places. Sampling from the stationary stockpile shall not be conducted, as this would introduce
significant bias in sampling.
• Sampling during production: The ore/pellets shall be collected as per stopped belt method from the
conveyor or at the convenient discharge point of the conveyor.
Trench sampling: Along a randomly chosen line on the ore surface of the sub-lot, a
trench shall be dug, right down to the ground level leaving about 0.3 meter
walking space at the ground level. From the trenches so dug, the required number
of increment shall be collected with the help of suitable sampling scoop, at
various points randomly spread over the two exposed sides of the trenches. In
case of large stockpiles, in addition to the trench, the sides of the piles may also
be opened to expose the ore down to the bottom, at places where the trench does
not expose the ore inside.
Automatic samplers: In Grinding Section & Product pellet area, the automatic
samplers have been provided. By simple button pressing at the required interval
the sample will be collected.
Sectional Sampling: 4 unit samples in the case of fines and calibrated ores and at least
8 unit samples in the case of sized ore and lumps are to be collected from each
sub-lot. For this purpose, the requisite number of points shall be chosen at
random on the entire surface of the stockpiles. At each of the selected points, a
circle of suitable diameter (minimum three times the largest particle size) shall
be marked. The material over the area of this circle and along entire height of the
stockpile from top to bottom shall be collected in stages. This can be done by
taking initially ores up to a depth of 50 cm and covering the hole so formed by a
plate for removing the ores lying on the sides of the hole. Then after removing
the plate further depth can be reached in the same manner and the ores can be
collected from the freshly formed hole.
SAMPLE PREPARATION
• Before analyzing any raw material for Physical/Chemical/Metallurgical properties it is very important to mention here about the sampling and
sample preparation. The sample should be collected which is a well representative of the total raw material ready for dispatch and well prepared
before analysis. In order to collect representative sample for correct analysis, sampling and sample preparation is a very important tool for
preparing a sample for analysis.
• The primary object of sampling of any material is to draw an inference about the quality of the lot on the basis of information derived from the
sample. If the consignment is of uniform nature the inference so drawn is almost precise, which gives an accurate estimate of the quality, but
when the material is heterogeneous in nature as is often the case with any raw material, the method by which a sample obtained becomes critical
in inferring about the quality of the consignment.
• The efficiency of sampling largely depends on the degree of homogeneity of the material and size of the sample. In case of heterogeneous material,
the size of the sample should be more for accurate estimate of the quality.
• Preparation of a final sample for physical, chemical and metallurgical properties is an important aspect, because the sample prepared in
accordance with the below mentioned procedure will fetch accurate analysis otherwise erratic results.
•
• There are different methods of sample preparation.
• Riffle divider
• Reduction by Riffle divider: The final sample shall be well mixed and poured into the riffle. This process shall be repeated using different sizes of
riffles according to the size of the ore.
• After the cone is formed, it shall be flattened by pressing the top of the cone with the smooth surface of the scoop.
Then it is cut into quarters by two lines which intersect at right angles at the center of the cone.
• The bulk of the sample is reduced by rejecting any two diagonally opposite quarters
Coning Quartering
Process Control - Raw Material Sampling Tools :
Process control: Instruments for Monitoring Temperatures ,
Differential Pressures , Gas Flows & Level Sensors
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Raw Material Handling systems:
( Sampling of Iron ore , Lime stone, Anthracite)
• In general, for any industry a right amount of input is necessary to produce an effective output as yield. In our pellet
plant we are getting the iron ore fines as the input from Brazil through shipment, we need an handling system for
transporting of the raw material from Port area to our plant, and hence we are making use of equipments like
Stackers, Reclaimers & Conveyors for serving the purpose.
Limestone
Stockpile
Capacity:6.000T
Anthracite
Stockpile
Capacity:15.000T
Process Control Sampling Plan:
• Vale Oman has Raw material’s Storage capacity of 1712.000T( Iron ore),where sampling is challenging task to meet the
Homogeneity of the sample. Process Control Dept. aims to execute such a difficult task where there is a higher
a) Segregation errors
This occurs when particles are exposed to gravitational, rotational, vibratory or
aeration operations (or other types of mechanical motion), usually resulting in fine
particles migrating to the bottom and larger particles being concentrated at the top.
This type of error is thus dependent upon the previous history of the powder and
usually occurs with free or easily flowing powders, having a significant range of
particle size. This type of error can be minimized by suitable mixing and building up
the sample from a large number of increments.
b) Statistical errors
This is type of error is caused by observing a sample instead of the
whole lot. Although this type of error cannot be prevented, it is
likely that the size of statistical errors can generally be controlled by taking a
large enough random sample from the entire lot.
Process Sampling at Stockpiles
We need to trench
the entire the pile , Dividing the
so as to have Entire Mass in to
Random uniformity &
Layers a
Composite sample
sampling homogenization in has to be drawn.
of entire sampling
area
10 Mtrs
Top Layer
Middle Layer
Bottom Layer
Stocked Raw materials are transported
through conveyors in to Plant Storage Bins:-
has to be followed
The term H.G.G refers to Hot Gas Generator used to remove moisture from the mixed raw material (Iron ore, Lime
stone, Anthracite) before it enters grinding mill , Grinding refers to the size reduction of a material by tumbling it in a
revolving cylinder. There are two types of grinding processes (1) Vertical and (2) Horizontal. But we are using
Horizontal grinding process. This occurs when the ore and a grinding media are tumbled together. The grinding media
used are Hi-Chrome Steel balls. These balls are of different diameters distributed through out the Ball Mill.
The media method of size reduction depends primarily on impact or compression fracture of the ore caused by the
impact action of heavier steel balls. Such impacts caused by the impacts or point-to-point contacts occur between the
ore and the balls or between the balls and the mill shell liners. It is important that the balls are large enough so that as
many points of contacts as possible occur and sufficient impacting action is provided which will result in the proper
breaking of the ore particle.
Grinding
Media Mill
Diaphragm
Mill
Liners
• The grinding mill liners are provided with lifters. As the mill cylinder is rotated the lifters lift the balls to give
them a proper cascade pattern and the energy to do breaking. The cascade pattern is determined by the
rotating speed of the mill cylinder and the mill diameter. The energy consumed in grinding is therefore
proportional to the weight of media, the diameter and rotational speed of the mill.
• The size of the ball media is determined by the size of the incoming feed particles. Larger sized ore requires a
larger ball size for good impact efficiency. As the ore is gradually reduced size, the media itself wears out and
the balls are reduced in size. These smaller balls are also necessary, as these balls are still adequate in size to
cause fracture because many more points of contact occur and many more balls are present per unit volume.
It is imperative to add bigger size balls for two reasons.
• To keep up the number of bigger size balls to break the large ore particles.
• To maintain the required number of balls in the mill to provide the power required for grinding. The media
should be added as and when required as the balls are continuously being worn away.
• Another mechanism of size reduction that occurs in the mill together with impact grinding is abrasive
grinding or attrition grinding or grinding by rubbing as the ore particles and media slide and rub against each
other as the ball mill rotates.
Dimensions
D=6.6M
L=12M
• Cascade Pattern – Here the lifters lifts the balls giving them the proper cascading energy for
breaking up the ore initially.
• Impact Pattern - Once the balls lifted up and after attaining a definite height it falls down on
the ore creating fractures. More the intensity of the balls finer be the size reduction.
• Attrition Pattern – This takes place along with the impact grinding, here due to rubbing /
sliding of the ore particles and the media against each other, size reduction takes place on the
mill rotation.
• The discharge of the ball mill passed through the SEPOL a Dynamic separator to
separate the fine particles from coarse particles, it acts as a classifier. The
Dimensions:
W x H x D/mm = 340 x 660 x 240
Sample collecting container volume = 51
Mixing & Blending Area:
( Sampling of Mixed material & Bentonite ) Paddles
Intensive
Mixer
Make:Lodige
capacity: 650
T/Hr
Length:5 Mtr
Dia:1.85Mtr
• Mixer is provided for mixing of iron ore concentrate & bentonite on continuous basis.
• Ploughshare shovels rotate in special arrangement along the horizontal shaft inside a horizontal,
cylindrical mixing drum. The size, number, positioning, geometric shape and peripheral speed of the
mixing elements are coordinated for three-dimensional movement of the components inside the
mixing drum. The resultant turbulence, with constant, total product mobility caused by the mixing
elements, prevents the formation of dead or static zones and results in gentle, precision mixing
within the shortest possible time.
• Mixing elements lift product during radial movement from the wall of the drum thereby preventing
particles from becoming squashed between the wall and the shovel. The hurling and whirling
process is, therefore, highly suitable for mixing processes in which the components have widely
differing bulk densities, particle sizes, rheological features and – relevant to pharmaceutical
production – highly different mass fractions.
Process Sampling Mixing & Blending Area:
Feed Rate of
WF’s-
AL3112.01,02
Bentonite
Sampling for
Moisture%
Grind% &
Swelling Index
• Thickening is a process of reducing the liquid content and thereby increasing the solid density within the slurry.
The mechanism is all based on the settling rate. The settling is even controlled by the rotation of the rake arms. The
rotation of the rake arms makes the denser particles to be dragged to the central portion and the light particles move
to the periphery. Almost clear water is taken as the overflow. Thickener is essentially a conical tank like structure.
It has a central shaft at the axis of the conical tank. The rake arms are attached to a sprocket that rotates about the
central shaft. There are four arms, two long and two short, all 90° apart. The longer arms are responsible for the
settling action. The shorter arms mainly deal with the central portion. But the central area is a denser portion
subjecting more torque on the arms. The shorter arms handle such denser matter reducing the torque on longer
arms.
Process sampling at Thickener area
Slurry Sampling
at Thickener
under flow for
Density & % of
solids checking as
per ISO:2591
CBBS extracts a representative sample from the falling flow of material off a belt conveyor. It’s
carriage-mounted cutter traverses through the material flow, collecting the product sample as
it goes, before discharging it into a hopper positioned outside the material flow
Blending Area to Balling Feed. Sample will be collected at - CT.3113.01. Capacity : 2.5kgs & feed rate
of conveyor: 900Tph.Samples are collected in a box later carried to Quality Lab manually.
Palletizing Disc Area: (Sampling of Green Ball )
Agglomeration:
As the Mixed Material is fed to the
Balling disc, it gets lifted upwards due to the rotation of
the disc. The material gets lifted up as long as the friction
between the ore particles and the disc bed is more than
the gravitational force. Once the gravitation force on the
ore particles is more than the frictional force, the particles
roll down. As the particles roll down, they agglomerate.
The agglomeration of the particles continues as long as
the rolling movement is sustained, resulting in formation
of the balls.
Feed Rate
Moisture content
powder seed binder droplet liquid bridges solid bridges
Sidewall height
Powder layering
Surface Area of the Particle
Spheronizing
Granule Green pellet
snowball“-structure
Brief: The traveling grate is used primarily to dry and preheat green balls for feeding into the rotary kiln,
where they are indurated. The traveling grate provides the means for efficient heat transfer with high,
medium and low temperature gases. These gases transfer heat by convection so intimate gas solids contact
is required for effective heat transfer.
Dried green balls do not have the physical properties necessary to survive direct feeding to the rotary kiln
and must be semi-indurated. For acceptable semi-induration, it is necessary for green balls to be
substantially heated and fluxstone carbonates (if used) to be substantially calcined. Good gas-solids contact
is required to cause bonding to occur and to remove CO2 so that calcination of the fluxstone can proceed at
reasonable rates. This semi-induration or preheating is accomplished by flowing the gases exiting the
annular cooler and rotary kiln through the bed of dried balls in the tempered preheat and preheat zones
respectively of the traveling grate.
Process Sampling at Traveling Grate
Checking Gapping of Roller
Classifiers CS3131.01-07 &
Roller Feeder AL3131.01
Internal view of
Traveling Grate
AIR HEATER
Analyzing of Process Parameters
Temperatures
&
Differential Pressures
&
Gas Flows, at Indurations Duct,
The rotary kiln is a downwards-sloping cylinder from the traveling grate to the annular cooler. The speed of rotation
controls the rate of solids flow through the rotary kiln and imparts a mixing action to the pellet burden. The mixing action
is important because it creates a homogeneous pellet product. All of the pellets are exposed to the burner flame for an equal
amount of time.
This residence time is sufficient to uniformly indurate all pellets, thereby minimizing the ball-to-ball quality differences
inherent in pellets discharging from the static bed processing typical of a SG.
At the discharge end of the rotary kiln is a single burner, which utilizes the hot recuperated (secondary) air from the
annular cooler for combustion. The burner can be designed to fire a single fuel or a combination of fuels. Oil, Natural gas
(LBG/Coke oven gas/ BF gas/ Corex gas) or coal can be used singly or in varying mixtures. Because of the single burner,
controlling the induration process is a simple temperature loop. Grate-Kiln plant processing Hematite ore may have few
additional burners in pre heating zone. This is very different from a SG system that may require up to 50 burners.
Process control Monitoring Kiln
The HEAD sampling equipment samples pellet from the end of a belt conveyor. This product collects accurate
representative samples when mounted on the end of a belt conveyor carrying the product. Sampler installations are designed
per application.
When activated an electric motor drives the slotted sample cutter through the product flow to collect a sample of the material.
The sample is discharged via gravity to a sample collection point. Sample collection is initiated in response to either an
operator’s manual command or a signal automatically generated by controller logic, usually time-based but which could also
be volume or quantity based.
In our process Head Samplers are provided at conveyor TR.1010.12 & TR.1010.13- Product Pellet Carrying Conveyor at
Transfer tower CT-1010.10&CT-1010.11.Capacity : 6.5kgs & feed rate of conveyor : 750Tph.Samples are collected in a
Pellets are coated with external additives like Limestone or Dolomite with
Equipment safety:
Follow caution signs and warnings
Follow manufacture recommended work practices
Check all equipments before starting and give it a change incase it asks for.
Skilled supervision is required.
Use all the rotating machinery provided with appropriate protection devices such as coupling guard as well as emergency stop buttons.
Equipment must be locked out prior to removal of equipment guards.
Electrical safety:
Never assume a electrical line to be dead unless it is tested and declared so.
Lockout and tag electrical /mechanical controls before performing any inspection, maintenance, lubrication.
Any work on electrical installations to be carried out in accordance with safety instructions.
Installation, maintenance and repair of electrical equipment to be done when permitted by authorized persons.
Sparks from electrical equipment (cable, wire, motor, hose etc) if observed to be reported to shift supervisor and maintenance
department to be notified immediately.
• Conveyor safety:
• Ensure the conveyor horns function properly.
• Ensure conveyor zero speed switch function properly.
• Stop the conveyor when there is a need to pass anything over it or under it.
• Personnel must never ride on the conveyor belts.
• All walkways along the conveyed must be free of material, tools, oil or grease.
• Ensure all pull chords function properly.
• Loose clothes should not be worn near conveyors.
• Do not lean over the conveyor while taking samples
• If the conveyor maintenance is to be taken, make certain the equipment is
locked out according to the electrical lock out system and a work permit has to
be obtained prior to work commencing.
• To ensure safety, have the equipment controlled by the local field control
panel.
• Safety training:
• All should be aware of plant design philosophy and potential hazards.
• All grades of personnel must be involved in elaborating emergency
procedures.
• Reporting all unsafe conditions to their supervisors.
• Identification of dangerous material and areas.
• Identification of hazardous substances.
• Identification of prohibitive and restricted areas.
• First training and emergency preparedness.
• Issuing of Safety work permits.
Gas safety:
Carbon monoxide is highly toxic when inhaled, it acts by combining with hemoglobin of
red blood cells to form carboxyhaemoglobin. This results in oxy-hemoglobin
dissociation and oxygen transport in blood.
An individual can work safely for 8 hrs in a 500-ppm exposure of CO gas.
At high concentration of 0.4% i.e. 4000 ppm CO can prove fatal in less than an hour.
Respiratory Protective equipments (RPPE) should be used in personal emergencies for
evacuation purposes and during clean up of the area.
Remove the person immediately from the contaminated area to fresh air location and
keep him comfortably warm. Tight fitting clothes, shoes and the belt of victim should be
loosened. Inform OHC, Safety, Transport, and Utility for necessary action at their end.
Incase of gas leaks, All sources of ignition should be kept away.SCBA to be used while
sampling and attending leaks. Incase of fire, Dry chemical Powder and CO2
extinguisher are suitable to fight small fire of CO.In case of large fire brigade
should be called to attend the fire call.
Presentation By:
A.Srik@nthKaundiny@
Process Control Dept.
V@le Om@n Pellet Plant –
Sohar-Sultanate of Om@n