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Pencucian Endapan
Why it should be
washed?
• Most precipitate produced in the
presence of one or more soluble
substance
• The soluble substances are not
volatile at the temperature
which the precipitate heated
• The soluble substances are
removed by washing
Ideal Washing Solution
1. No solvent action upon the precipitate but
dissolve foreign substance easily
2. No dispersive action on precipitate
3. Form no volatile or insoluble substance
with the precipitate
4. Easily volatile at the temperature of drying
of the precipitate
5. Contain no substance which is interfere the
subsequent operation to the filtrate
Caution!
• Use minimum volume of washing solution
since no precipitate is insoluble
• Do qualitative test of removal the
impurities
• Wash with a number of small portion of
washing solution with well drained
between each washing than large portion
of washing solution or adding a new
portion while the solution still remain
Choosing the washing
solution
• Pure water should not be used unless it
certain will not dissolve appreciable
amount or peptise the precipitate
• Colloidal/gelatinous precipitate is
washed with electrolyte solution
• Crystalline precipitate is washed with a
solution contain common ion
Washing by decantation