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hkl
= Dtan2u
hkl
Geometry
Lattice strain
c
hkl
=
d
hkl
d
hkl
0
d
hkl
0
Experimental Setup
Circumferential integration (caking) generates spectra
for azimuthal angles, q
An {hkl} peak location from spectrum at q and recorded
at N is compared to the same {hkl}s peak location from
spectrum at the same q recorded at virgin state to
calculate lattice strain
Repeat for all {hkl}s for all q at N
Data Reduction
Data Reduction
Actual Al 7075 T6 Data
Strain Pole Figures
Stress-Strain Curve for 7075 T6
In-situ X-ray diffraction provides a
snap shot of the aggregate lattice
strain
Can invert lattice strain to find full
strain tensor
Validates micromechanical models
What In-situ X-ray Diffraction gives us
References
Aluminum: Properties and Physical Metallurgy by John Hatch
Experimental measurement of lattice strain pole figures using synchrotron
x rays by M. P. Miller
Measuring crystal lattice strains and their evolution in cyclic loading by J-
S. Park
On the mechanical behaviour of AA 7075-T6 during cyclic loading by
Turkmen
Influence of modelling variables on the distribution of lattice strains in a
deformed polycrystal, with reference to neutron diffraction experiments by
Loge
Elements of X-ray Diffraction by Cullity
http://www.sintef.no/static/mt/norlight/ProjectPortfolio/HeatTreatmentFun
damentals/dispersoids.htm
http://www.alcoa.com
http://www.msm.cam.ac.uk/phasetrans/2002/robson/img4.htm
Electrochemical Characterization of 7075 Aluminum Alloys Using The
Microcell by Barbara N. Padgett