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Introduction

STRUCTURAL EVOLUTION AND MAGNETIC PROPERTIES OF

NANOCRYSTALLINE MAGNESIUMZINC SOFT FERRITES SYNTHESIZED
BY GLYCINENITRATE COMBUSTION PROCESS
S. Hajarpour a, A. Honarbakhsh Raouf a,n, Kh. Gheisari b

Materials
and methods

Results and
discussion

Conclution
Rachmad Almi Putra

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INTRODUCTION
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Introduction

Recent studies reveal that nanoparticle ferrites show an unu- sual magnetic behavior. This
unusual behavior is caused by redistribution from inverse to mixed spinel type, which
occurs at nanolevel, resulting in an enhancement of magnetization as compared to the
bulk.

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Conclution

MG1-XZNXFE2O4(DENGAN X===0, 0,1, 0,2, 0,3, 0,4, 0,5DAN 0,6) DENGAN METODE
GLYCINE NITRATE COMBUTISION PROCESS

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Materials and Method

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2.1. Materials and Chemical Reaction

(1-x)Mg(NO3)2.6H2O+xZn(NO3)2.6H2O+2Fe(NO3)3.9H2O+6NH2CH2COOH+3,5O2
Mg1-xZnxFe2O4+7N2+12CO2+15H2O

2.2. Preparation Techniques

Structural studies on the as-prepared powders are conducted using X-ray
diffraction(XRD,BrukerD8) with Cuk radiation.
The microstructure evaluation and morphological features of the product powders
are determined by field emission scanning electron microscopy(FESEM;HitachiS4160)ofthegold-coated samples.

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Result and Discussion

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3.1. Nature of Combustion Synthesis

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3.1. Nature of Combustion Synthesis

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3.2. Stucture Evolution

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3.2. Stucture Evolution

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3.3. Magnetic Properties

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3.3. Magnetic Properties

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3.3. Magnetic Properties

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3.3. Magnetic Properties

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CONCLUSION
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Nanocrystalline Mg1-xZnxFe2O4 ferrite powders are produced

throught he glycinenitrate process. Analys is of the X-ray diffraction
spectrum shows that the prepared samples have single-phase spinel
structures. Crystallitesizes, calculated from XRD data, are in the
range3647nm. Magnetic measurements show that anti parallel spin
couplingexists when Zn content is less than 0.4. For higher Zn
contents,spincanting occurs and saturation magnetization decreases.
It is concluded from the conducted work that MgZn ferrite can be
successfully produced by glycinenitrate process with higher values
of saturation magnetization, inless time and with easier steps, when
compared toot her techniques.

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REFERENCE
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and methods

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