Electron Probe

Characterization
Techniques
Electron Probe Characterization
Techniques
Welcome to our presentation!
Electron Probe Characterization
Techniques SEARCH
 SCANNING
HIGH-
ELECTRON
RESOLUTION TEM
1 MICROSCOPY 4
(HRTEM)
(SEM)
SCANNING
ELECTRON PROBE TRANSMISSION
Contents 2 MICRO-ANALYZER
(EPMA)
5 ELECTRON
MICROSCOPY
TRANSMISSION (STEM)
3 ELECTRON 6 LOW-ENERGY
MICROSCOPY ELECTRON
(TEM) DIFFRACTION:
 7 ELECTRON ENERGY-LOSS
SPECTROSCOPY

AUGER ELECTRON
8 SPECTROSCOPY

Contents 9

Conclusionsd
4
 SCANNING
ELECTRON
MICROSCOPY
(SEM)
DEFINITION
HOW IT WORKS?
APPLICATION
 ELECTRON
PROBE MICRO-
ANALYZER
(EPMA)
DEFINITION
HOW IT WORKS?
APPLICATION
 ELECTRON
PROBE MICRO-
ANALYZER
(EPMA)
DEFINITION
HOW IT WORKS?
APPLICATION
TRANSMISSIO
N ELECTRON
MICROSCOPY
(TEM)
DEFINITION
HOW IT WORKS?
APPLICATION
 High-
Resolution TE
M (HRTEM)
DEFINITION
HOW IT WORKS?
APPLICATION
 SCANNING
TRANSMISSION
ELECTRON
MICROSCOPY
(STEM)
DEFINITION
HOW IT WORKS?
APPLICATION
LOW-ENERGY
ELECTRON
DIFFRACTION:
 DEFINITION

• Low-energy electron diffraction (LEED) is one of the principal

techniques for the determination of surface structures. This
technique can be used in one of the following two ways:
 DEFINITION

Qualitatively: The diffraction pattern is recorded and analysis of the

spot positions yields information on the size, symmetry and
rotational alignment of the adsorbate unit cell with respect to the
substrate unit cell.
Quantitatively: The intensities of the various diffracted beams are
recorded as a function of the incident electron beam energy to
generate so-called I-V curves which by comparison with theoretical
curves may provide accurate information on atomic positions.
 HOW IT WORKS?
A beam of electrons of a well-defined low energy
(typically in the range 20-400 eV) is incident normally on
the sample as shown in Figure 7.01. The diffracted
electrons can be observed on a fluorescent screen after
energy-filtering grids, which selects only the electrons
with the same kinetic energy as the primary electrons.
HOW IT WORKS?
APPLICATION

Low energy electron diffraction (LEED) is one of the most powerful

techniques available for surface analysis. It is widely used in
materials science research to study surface structure, bonding and
the effects of structure on surface processes

• It measure the intensity profiles of diffraction beams

with respect to the surface component of the
electron momentum transfer.
• Compositional ordering of alloy surfaces.
• Disordering surface.
• surface analysis
 ELECTRON
ENERGY-LOSS
SPECTROSCO
PY
DEFINITION
HOW IT WORKS?
APPLICATION
 ELECTRON
PROBE MICRO-
ANALYZER
(EPMA)
DEFINITION
HOW IT WORKS?
APPLICATION
 AUGER
ELECTRON
SPECTROSCOPY
DEFINITION
HOW IT WORKS?
APPLICATION
 Thank you!

Batangas State University

College of Engineering, Architecture and Fine Arts
Chemical and Food Engineering Department
 Anorico, Joselle Techie Cuiat, Matthew Dalisay, Arvin Dave
Members

Del mundo, Zoren Generoso, John Llyod Untalan, Paola